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Home My WebLink About20151060.tiff October 31 , 2014 FedEx: Colorado Department of Public Health and Environment Air Pollution Control Division 4300 Cherry Creek Drive South, APCD-SS-B 1 Denver, CO 80246- 1530 Subject: C-10 Salt Water Disposal Facility General Permit Applications and Construction Permit Application NGL Water Solutions Di, LLC Weld County, Colorado To Whom It May Concern: NGL Water Solutions DJ, LLC is submitting this application for the C- 10 Salt Water Disposal Facility (Facility), a new facility, located at Section 35, T7N, R65W, Weld County, CO to request coverage under a GP01 for the oil heating tank, oil tanks, slop oil tank and sale oil tank; coverage under a GP05 for the desand tanks, sand and oil removal tanks and the produced water unloading sump; and coverage under a construction permit for the condensate loadout and fugitive emissions. The facility will have a maximum facility throughput of 20,000 hbl/day of tricked in water. Facility wide emission units will include: Desanding Tanks (2 x 700 bbl) Sale Oil Tank ( 1 x 400 bbl) Sand and Oil Removal Tanks (2 x 1000 bbl) Produced Water Unloading Sump Oil Heating Tank ( 1 x 400 bbl) Electric Tank Heater Water Equalization Tanks (8 x 840 bbl) Loadout Post-Filter Tanks (2 x 1000 bbl) Fugitives Oil Tanks (3 x 400 bbl) Diesel Tank ( 1 x 500 gal) Slop Oil Tank ( 1 x 400 bbl) The facility emission calculations, application forms, APENs, and supporting documentation are included in the attachments. A check for $3, 126. 10 in full payment of the APEN tiling and general permit registration fees as broken down below is attached. Fee Breakdown $ 152.90 x 9 APEN Filing Fee = $ 1 ,376. 10 $250 x 3 Produced Water Tank Battery GP05 Registration Fee = $750 $250 x 4 Midstream Condensate Tank Battery GP01 Registration Fee = $1 ,000 If you have any questions or need additional information, please contact me at 970-356-5560 (jpatterson @highsierraenergy.com). Sincerely, NGL Water Solutions DJ, LLC Josh Patterson VP of Operations Enclosures Appendix A — Construction Permit Application Appendix B — APCD- 102 and APEN Forms Appendix C — Regulatory Review Appendix D — Facility Emission Calculations and Supporting Documentation Appendix E — Process Description, Process Flow, Facility Location, and Plot Plan Appendix A Construction Permit Application Air Pollution Control Division (APCD) - Construction Permit Application PLEASE READ INSTRUCTIONS ON REVERSE SIDE. I . Permit to be issued to: NGL Water Solutions DJ, LLC 2. Mailing Address: 8207 West 20th Street, Suite B Greeley, CO 80634 3. General Nature of Business: Oil and Gas Produced Water Storage SIC code (if known) 4. Air Pollution Source Description: CIO Salt Water Disposal Facility ( List permit numbers if existing source, Permit Pending, GPO! Pending, GP05 Pending attach additional pages if needed) Is this a Portable Unit? No 5. Source Location Address (Include Location Map) If portable, include the initial location and home base location SECTION 35, T7N, R65W 6. Reason for Application: (Check all that apply) New or Previously Unreported Source Administrative Permit Amendments ❑ Modification of Existing Source ❑ Transfer of Ownership (Complete Section 9 & 10 below) ❑ Request for Synthetic Minor Permit ❑ Company Name Change (Complete Section 9 below) ❑ Other: ❑ Other: 7. Projected Startup Date: 2014 Signature of Legally Authorized Person of Company listed in Section 1 Date Signed Josh Patterson, VP of Operations Phone: 970-356-5560 Type or Print Name and Official Title of Person Signing Above Fax: 970-356-5563 M. Check appropriate box if you want: ® Copy of preliminary analysis conducted I )i \ ( ion ® To review a draft of the hermit Ipri ( H' to i � ucnRTC "These sections are to be completed only i/'a company name change or transfer of ownership has occurred. k 9. Permit previously issued to: 10. Transfer of Ownership Information Effective Date of Permit Transfer: As responsible party for the emission source(s) listed above, I certify that the business associated with this source has been sold, and agree to transfer the permit to said party. Signature of Legally Authorized Person of Company listed in Section 9 Date Signed Phone: Type or Print Name and Official Title of Person Signing Above Fax: Mail completed application, APENs, and filing fee to: Colorado Department of Public Health and Environment http://www.cdphe.state.co.us/ap/stationary.html Air Pollution Control Division Phone: (303) 692-3150 4300 Cherry Creek Drive South, APCD-SS-B1 Denver, Colorado 80246-1530 Revised August 2004 Appendix B APCD- 102 and APEN Forms Department of Public Health and Environment �� ` Form APCD- 100 Colorado De Air Pollution Control Division 41a76 F Oil Colorado Deparunent & Gas Industry of Public l Iealth Construction Permit Application Completeness Checklist and Environment Ver. September 28, 2009 Company Name: NGL Water Solutions DJ, LLC Source Name: C10 Salt Water Disposal Facility Date: October 2014 Yes No Are you requesting a facility wide permit for multiple emissions points? /1 ■ In order to have a complete application, the following attachments must be provided, unless stated otherwise. If application is incomplete, it will be returned to sender and filing fees will not be refunded. Attachment Application Element Applicant AP('l) A APEN Filing Fees /1 B Air Pollutant Emission Notice(s) (APENs) & Application(s) for Construction Permit(s) — APCD Form Series 200 C Emissions Calculations and Supporting Documentation /1 • D Company Contact Information - Form APCD-101 ►1 • E Ambient Air Impact Analysis / Check here if source emits only VOC (Attachment E not required) F Facility Emissions Inventory — Form APCD-102 • Check here if single emissions point source (Attachment F not required) G Process description, flow diagram and plot plan of emissions unit and/or facility • Check here if single emissions point source (Attachment Ci not required) H Operating & Maintenance (O&M) Plan — APCD Form Series 300 ■ Check here if true minor emissions source or application is for a general permit (Attachment H not required) I Regulatory Analysis ►1 • Check here to request APCD to complete regulatory analysis (Attachment I not required) Colorado Oil and Gas Conservation Commission (COGCC) 805 Series Rule • Requirements— Form APCD-105 Check here if source is not subject to COGCC 805 Series requirements (Attachment J not required) Send Complete, Application to: Colorado Department of Public Health & Environment APCD-SS-B1 4300 Cherry Creek Drive South Denver, Colorado 80246- 1530 Check box if facility is an existing Title V source: Send an additional application copy Check box if refined modeling analysis included: Send an additional application copy Page 1 of ICI 0 Form APCD- 100 Construction Permit Application Completeness Checklist.doc Form APCD- 101 s �tc Colorado Department of Public Health and Environment t. Air Pollution Control Division r; * 1876 .E Colorado Department of Public I Iealth Company Contact Information Form dlaivironntent Ver. September 10, 2008 Company Name: NGL Water Solutions DJ, LLC Source Name: C10 0 Salt Water Disposal Facility Permit Lori Marquez, Marquez Compliance Contact': Environmental Services, Inc. Contact2: Josh Patterson 13860 Braun Rd. 8207 West 20th Street, Suite B Address: Street _ Address: Street Golden CO 80401 Greeley CO 80634 City State Zip City State Zip Phone Phone 303-503-4735 970-356-5560 Number: Number: Fax Fax Number: 970-356-5563 Number: h:-mail: lorikm@aol.com E-mail : jpLttterson@highsierraenergy.com Billing Billing Contact: Naomi Lauer Contact: Naomi Lauer Permit Annual 4 Fees Fees) 8207 West 20th Street, Suite B 8207 West 20th Street, Suite B .address: Street Address: Street Greeley CO 80634 Greeley CO N0634 City State Zip City State lip Phone 970-356-5560 Phone 970-356-5560 Number: Number: Fax Number: 970-356-5563 Fax 970-356-5563 Number: E-mail: naomi.lauer@nglep.com E-mail: naomi.lauer@nglep.com Check how would you like to receive your permit fee invoice? Mail: VI E-mail: i1 Fax: ■ Footnotes: I The permit contact should be the point of contact for technical information contained in the permit application. This may be a company representative or a consultant. 2 The compliance contact should be the point of contact for discussing inspection and compliance at the permitted facility. 3 The billing contact (Permit fees) should be the point of contact that should receive the invoice for fees associated with processing the permit application & issuing the permit. (Reg. 3, Part A, Section VI.B) ° The billing contact (Annual fees) should be the point of contact that should receive the invoices issued on an annual basis for fees associated with actual emissions reported on APENs for the facility. 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Z U N W a w 'o O Q N D O )T Tr) CsC Q .) a) Q O Cr) C W >' W .0 O O O CD In 1.0O -D C) F— z in `/) J LC) Q N CO C O 0 Cr) += o Z > O) O I C) Z �_ ` O Q 0- O Q ^ L L U ° O C w °; o a) Cn o o E E o 8 o — y Z Z cn0 W F o �i co w Ha r Q Z E o Q U O 3� In 11- D p U O J -2 ° o _ Z � . .� D E c Cr) 4-0 `� L o id w o Q. .� Z w Q O C W a� 0 E E � cz CD 0 w J a'> U CO o �- o C Co m w J >, >, CD a) J w ° a o `n a al C ° 0 a >, re Cu- O C .C) U) a O Co O ,0 Q a o a O o a z I a oCD a �- v) Q rt N o W O D C 0) 4) (� •L 13 O L Cn O� 2 N_ < L L z }' •L _ O Ct -rd ° co Q W J U ) _C a E a) Q Q I— 4-1 CU D Ce (� a) -c C) >, Z U O D I . . O a) Q C O) U Z o co ti o L C ai O .l E C C cn Cll C ° 76 CD O O a 0 Q L- -0 O CL O L Z Z U UA >- o _ Z o o Q a_ �' _ ~ O •>ac a3 CL 0 CC LE c co Cv C E E CI) o a cobc� ._ w co a U a. w O o a cn o Z u_ Appendix C Regulatory Review CDPHE Air Quality Control Regulations Regulation 1 - Emission Control for Particulate Matter, Smoke, Carbon Monoxide and Sulfur Oxides The Facility is not subject to Regulation 1 . (5 CCR 1001 -3). There are no combustion sources at the facility. Regulation 2 - Odor Regulation 2 (5 CCR 10014 Part A. 1) States 'No person, wherever located, shall cause or allow the emission of odorous air contaminants from any single source such as to result in detectable odors which are measured in excess of the following limits. . . ' . The Facility is subject to this regulation and NGL Water Solutions DJ, LLC will comply with the requirements of this regulation. Regulation 3 — Stationary Source Permitting The Facility is subject to Regulation 3 (5 CCR 1001 -5) because it meets the definition as a source of air pollutants. Per Regulation 3, a new source located within a nonattainment area must comply with Section II.B . An Air Pollutant Emission Notice (APEN) is required for each individual emissions point in a nonattainment area with uncontrolled actual emissions of one ton per year or more of any individual criteria pollutant for which the area is nonattainment. Because the Facility is located within an 8-hour ozone control area, an APEN is required for each emission point with VOC emissions greater than 1 ton per year, and 2 tons per year for all other criteria pollutants. This application is being submitted in compliance with the applicable sections of Regulation 3. Regulation 6 - Standards of Performance for New Stationary Sources The Facility is subject to Regulation 6 (5 CCR 1001-8) Part A, `Federal regulations adopted by reference' . See below for Federal NSPS for applicability review. Regulation 7 — Emissions of Volatile Organic Compounds The Facility is subject to Regulation 7 (5 CCR 1001 -9) under Sections III and VI. Section III outlines general requirements for storage and transfer of volatile organic liquids. Section VI specifies requirements for the storage and transfer of petroleum liquid. The tanks storing oil at the Facility are subject to the requirements under Sections III, and VI. NGL Water Solutions DJ, LLC will comply with applicable requirements of this regulation. The facility is located in an Ozone nonattainment area and is therefore, potentially subject to Section XII. However, the facility does not meet the definition of affected operations with respect to Section XII of Regulation 7; therefore, it is not subject to Section XII. Regulation 8 — Control of Hazardous Air Pollutants The Facility is subject to Regulation 8 (5 CCR 1001- 10) Part E, `Federal regulations adopted by reference' . See Section 5 below for Federal applicability review. Dispersion modeling — Potential NOx and CO emissions are below the significant emissions rate (SER); therefore modeling is not required in accordance with CDPHE PS Memo 10-01 . Potentially Applicable Federal Air Quality Regulations Prevention of Significant Deterioration (PSD) Total potential emissions of any criteria pollutant from the Facility are less than 250 ton/year. Potential greenhouse gas (GHG) emissions at the Facility are below PSD major source threshold levels. Therefore, it is not subject to the PSD or the non-attainment NSR permitting programs. New Source Performance Standards (NSPS): The Facility includes sources which may potentially be subject to NSPS requirements included in Title 40 of the Code of Federal Regulations (CFR) Part 60. A review of each potentially applicable subpart is included below. Subpart A Subpart A, General Provisions, applies to any stationary source that contains an affected facility to which an NSPS standard is applicable. Subpart Dc There are only electric heaters operating at the Facility, therefore, this subpart does not apply. Subpart Kb Subpart Kb applies to volatile organic liquid storage vessels constructed, reconstructed, or modified after July 23, 1984, with a capacity greater than or equal to 75 m3 (471 bbl). This subpart does not apply to storage vessels with a capacity greater than 151 m3 (949 bbl) storing liquid with a max true vapor pressure less than 3.5 kPa, or storage vessels with a capacity greater than 75 m3 but less than 151 m3, storing liquid with a max true vapor pressure less than 15.0 kPa. The oil tanks are less than the 75 m3 applicability threshold, therefore, this subpart does not apply to the oil tanks. There are several water tanks at the facility with storage capacities between 75 m3 (471bb1) and 151 m3 (949.7 bbl) or greater than 151 m3 (949.7 bbl). The maximum true vapor pressure is less than the 15.0 kPa applicability threshold for tanks between 75 m3 and 151 mi and less than the 3.5 kPa applicability threshold for tanks greater than 151 m3. Therefore, this subpart does not apply to any of the water tanks. Subpart GG There are no turbines at this facility. Therefore, this facility is not subject to 40 CFR §60.330 Subpart KKK The facility does not meet the definition of an "onshore natural gas processing plant" as defined by this subpart. Therefore, the facility is not subject to 40 CFR §60.630 Subpart LLL There are no sweetening units at this facility. Therefore, this subpart is not applicable. Subpart 1111, JJJJ There are no SI or CI internal combustion engines at the facility. Therefore, this subpart is not applicable. Subpart KKKK There are no turbines at this facility. Therefore, this subpart is not applicable. Subpart OOOO The storage tanks at this facility were constructed, modified or reconstructed after August 23, 2011 . However, the potential to emit, as defined by this subpart, is less than 6 tons per year per tank. In addition, the oil loadout limitation for the facility that will be contained in the construction permit will establish a practically enforceable limit on the tank throughputs to demonstrate that emissions from the tanks cannot exceed the OOOO threshold. Therefore, the tanks are not affected facilities under this regulation. There are no continuous high-bleed pneumatics at the facility. Therefore, the pneumatics are not affected facilities under this regulation. Maximum Achievable Control Technology (MACT): The Facility will be a true minor source of HAPs. Thus, there are no sources at the Facility which are subject to MACT major requirements. Because there are no dehydrators or engines at the facility, area source requirements for MACT HH and MACT ZZZZ do not apply. Greenhouse Gases (GHG): Because this is a water storage facility and there are no combustion sources, GHG are expected to be negligible. Calculation Methods The facility receives post flash produced water from oil and gas operations. Emissions were estimated as follows: 1 . Hydrocarbon Liquid Storage Tanks — Emissions were calculated using E&P TANKS with a sample analysis from a similar facility. The sample is considered representative because the facility receives similar trucked in liquids. Margin was added to the throughput to allow for operational flexibility and to provide a conservative estimate. 2. Produced Water Storage Tanks — Emissions were calculated using EPA TANKS using a mixed composition of water and condensate. The liquid sample from a similar facility showed that the condensate portion of the liquid has a Reid Vapor Pressure of 3.2 psig at 100°F, corrected API Gravity of 47.0 at 60°F, and a molecular weight of 147. 12 lb/lb- mol. The sample is representative of the oil coming into the facility. While the composition is similar to crude oil, gasoline RVP 10 was conservatively used for the hydrocarbon portion of the liquid because any light end hydrocarbons present in the initial offload of the liquids would be present at the produced water system tanks. 3. Loadout — Working loss emissions from truck loading were estimated using the USEPA loadout equation from AP-42 Section 5.2, and the annual maximum volume of condensate loaded. 4. Fugitive Emissions — Process piping fugitive emissions were estimated using USEPA emission factors and estimated component counts. 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C O ....0H o O Cat ON H ct O ,Q C es o O O V O n m o CO -) CU ti L U 4Di � Z o ° °' Doi e— (.) O f° y Q 0 " � 6 a r rC 0 v N to CNI czs 0 0 ..i CO to to atnN- CO r N 'Cr i-1 N O N - E 4 r N E N W To O LL O RS C u it • v/ W ( on`r 1CNI Z COO a HO ~ m cID 03 COo -- N Z J v) C 13 Y T3 0 •> c L. N C w E •E - O co N co (0 N O O W in N o cn Q) .L-- M , N ON X O O LL t 73 0 C E cri N J 00 C a 0 Q o C ON is ca en O I w C O 1 0 ', Q. L 5 O C) N @ E cu ce pu) 0 O c 0 C E o co O 0. O -O O a to o �. ` Cl) V) o cts O a) co V 0 11) N- L- 0 O E '- O O O Q < W a 0 0 O .. InNzi- O N N a) N al 0 CL .. 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Ot c :ea � > . •p) • CO a`> >, a) E o a) E '= Q) E ca t a) a� o o .c ,o) a a) c) m O U) = ;S o >,>, a) G t 4, Q' > O O a) ~ V t _coo C) >, a) O t ca N V 2 � DU (nUHt7 C (n0JQ > F- Z ccncn � � C ~ = fn > d a? to (5 O H a M m 2 In NT O N N v N to N e3 v, O a co .— N II 0 tri I I co aN O a co n N II V m N < an 4) , c0 a o 0 8 II a a co O p I V N N U C C O O N 0 0 0 0 Co) v o O O C4 T::. Iv cooi � w Ln v) O U a CO m Cal 07 a Li- M ( O co to co = v in N V O O O CO ocal CO CO LL I- O a O as co - (O O O / 75 Z TT CD a � i >. m o 00 VI E o �1 N t0 O 3 Cn ch co N //� WOx I- Q) N w/ to r07 - M o O Y m a co a Cl) ta O C D Z _ _ a^�. 0 C 00oN en La OD - Q W = 0 2 o at o Ce tit O X a in [ ' (6 ci) CD M 60) C �/ X > Q NO N .� O O O6 O •— •— 3 LL O MI N .a' as E E J V v .c a. LL in . > > E � `t E t p•co 1 4) C N W0 J CA -v X N CS C0O1 Li 2 O O CL t O1 D CD CA Y vv o ``' C CMI cr P, C N �y J@ � v �V ?" & CU 4E) 00 0 F to O _- O X E � o G) L N O O C CO CNI 6. ON oO. CO > cts o co_ c O B o w 4) 3...• 00 n m > 0...01 O CO .c • j r L U 4Di .� z O ° °' Doi leC r O v f° y a r rC N0 v N CNI czs 0 0 ..t cn co v o a O co o co • - co) co 4-. N O� N CO m E v Ni E N w i o O r3 46 ....• LL O cZ C Ca E N 0• c •it E u) O N W a) N co Z O C H O ~ 0 CC ° 00 c� Cl) 03 0 Z J X "C'3 .N •� IL 1. Cl)_ v - E •E t N O ( M O W > -' r v .L-- V .- N O O a cn x Y = c ct cz Ct j 00 0 X E 0 C a) N C Q 0 en 0O 5 N 0 a)C as CC wca as C C n 0 O 4 0 o o -El o a� 0. Cl) � p ct c ai co (C) 0 CP L- c) 0C� V _ O o . H W U U O a .. E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 ****************************************************************************************** * Project Setup Information * * ************************************************************** *** *********************** Project File : G : \NGL Permits and Cert Checklists\C10\C10 400 bbl Oil Heating Tank (P4 ) . ept Model : Stable Oil Tank Calculation Method : AP42 Control Efficiency : 100 . 0% Filed Name : C10 Oil Heat Tank ( 1 x 400 bbl ) . Modeled for one tank Well Name : C10 Date : 2014 . 10 . 03 ************ ********* * ** **** ************************************************************** * Data Input ** *** ************* ******* *** ************************************************************** Separator Pressure : 23 . 00 [psig] Separator Temperature : 85 . 00 [F] Ambient Pressure : 14 . 70 [psia] Ambient Temperature : 70 . 00 [F] C10+ SG : 0 . 9240 C10+ MW : 194 . 40 -- Stable Oil No . Component mol % 1 H2S 0 . 0000 2 O2 0 . 0000 3 CO2 0 . 0000 4 N2 0 . 0000 5 Cl 0 . 0000 6 C2 0 . 0000 7 C3 0 . 0000 8 i-C4 0 . 0000 9 n-C4 0 . 0000 10 i-05 0 . 8300 11 n-05 0 . 8300 12 C6 4 . 8800 13 C7 14 . 4100 14 C8 9 . 9600 15 C9 14 . 9200 16 C10+ 39 . 7800 17 Benzene 0 . 8100 18 Toluene 4 . 2100 19 E-Benzene 0 . 2700 20 Xylenes 4 . 7700 21 n-C6 4 . 3300 22 224Trimethylp 0 . 0000 -- Sales Oil Production Rate : 600 [bbl/day] Days of Annual Operation : 365 [days/year ] API Gravity . 47 . 0 Reid Vapor Pressure : 3 . 20 [psia] Bulk Temperature : 100 . 00 [F] -- Tank and Shell Data Diameter : 12 . 00 [ ft ] Shell Height : 20 . 00 [ ft ] Cone Roof Slope : 0 . 30 Average Liquid Height . 10 . 00 [ ft ] Vent Pressure Range : 0 . 03 [psi ] Solar Absorbance : 0 . 54 -- Meteorological Data City : Denver, CO page 1 E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 Ambient Pressure : 14 . 70 [psia] Ambient Temperature : 70 . 00 [F ] Min Ambient Temperature : 36 . 20 [F ] Max Ambient Temperature : 64 . 30 [F] Total Solar Insolation : 1568 . 00 [Btu/ft^2*day] ******************************************************* *********************************** * Calculation Results * ************ ****************************************************************************** -- Emission Summary Item Uncontrolled Uncontrolled [ton/yr] [ lb/hr] Total HAPs 0 . 410 0 . 094 Total HC 1 . 819 0 . 415 VOCs , C2+ 1 . 819 0 . 415 VOCs , C3+ 1 . 819 0 . 415 Uncontrolled Recovery Info . Vapor 42 . 5400 x1E-3 [MSCFD ] HC Vapor 42 . 5400 x1E-3 [MSCFD] GOR 0 . 07 [SCF/bbl ] -- Emission Composition No Component Uncontrolled Uncontrolled [ton/yr] [ lb/hr] 1 H2S 0 . 000 0 . 000 2 O2 0 . 000 0 . 000 3 CO2 0 . 000 0 . 000 4 N2 0 . 000 0 . 000 5 Cl 0 . 000 0 . 000 6 C2 0 . 000 0 . 000 7 C3 0 . 000 0 . 000 8 i-C4 0 . 000 0 . 000 9 n-C4 0 . 000 0 . 000 10 i-05 0 . 165 0 . 038 11 n-05 0 . 134 0 . 031 12 C6 0 . 374 0 . 085 13 C7 0 . 500 0 . 114 14 C8 0 . 142 0 . 032 15 C9 0 . 090 0 . 021 16 C10+ 0 . 001 0 . 000 17 Benzene 0 . 035 0 . 008 18 Toluene 0 . 070 0 . 016 19 E-Benzene 0 . 002 0 . 000 20 Xylenes 0 . 029 0 . 007 21 n-C6 0 . 276 0 . 063 22 224Trimethylp 0 . 000 0 . 000 Total 1 . 818 0 . 415 -- Stream Data No . Component MW Stable Oil Sales Oil Total Emissions mol % mol % mol 1 H2S 34 . 80 0 . 0508 0 . 0000 0 . 0000 2 O2 32 . 00 0 . 0000 0 . 0000 0 . 0000 3 CO2 44 . 01 0 . 2437 0 . 0000 0 . 0000 4 N2 28 . 01 0 . 0102 0 . 0000 0 . 0000 5 Cl 16 . 04 0 . 9543 0 . 0000 0 . 0000 6 C2 30 . 07 0 . 6701 0 . 0000 0 . 0000 7 C3 44 . 10 2 . 1827 0 . 0000 0 . 0000 8 i-C4 58 . 12 1 . 1269 0 . 0000 0 . 0000 9 n-C4 58 . 12 4 . 6091 0 . 0000 0 . 0000 10 i-05 72 . 15 3 . 1066 0 . 8290 11 . 1943 11 n-05 72 . 15 5 . 0558 0 . 8292 9 . 0929 12 C6 86 . 16 4 . 1726 4 . 8784 21 . 7249 13 C7 100 . 20 10 . 3655 14 . 4090 25 . 1387 14 C8 114 . 23 10 . 8426 9 . 9604 6 . 2461 page 2 E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 15 C9 128 . 28 5 . 5127 14 . 9211 3 . 5889 16 C10+ 194 . 40 45 . 9695 39 . 7838 0 . 0347 17 Benzene 78 . 11 0 . 5685 0 . 8099 2 . 2011 18 Toluene 92 . 13 0 . 2132 4 . 2101 3 . 6874 19 E-Benzene 106 . 17 0 . 0711 0 . 2700 0 . 0860 20 Xylenes 106 . 17 0 . 6802 4 . 7703 1 . 3452 21 n-C6 86 . 18 3 . 5939 4 . 3289 15 . 6599 22 224Trimethylp 114 . 24 0 . 0000 0 . 0000 0 . 0000 MW 139 . 45 139 . 45 88 . 82 Stream Mole Ratio 1 . 0000 0 . 9999 0 . 0001 Heating Value [BTU/SCF] 4817 . 75 Gas Gravity [Gas/Air] 3 . 07 Bubble Pt . @ 100F [psia] 1 . 48 1 . 48 RVP @ 100F [psia] 10 . 09 10 . 09 SG @ 100F 0 . 807 0 . 807 page 3 In NT O N N b N A ct 0 CL .-- CO V 1 'i CC i o co u_ c % o tv 03 CZ c an o a L N_ a• co >. II v/ a po 2 t _ U) Z Q E a .2 d = > r ct O >, -- .— N Cl) V o cn C .N •- I— Q s... C O O O O O O co O O co M M 7 CCI N O O O N O COO O a E ▪_ w Co J C antn � Nt� rO OO O O E N J Cu NrNrMMCL) ' 0 WC A Y H N O N V Z ,02 cn D O CCD > M N.ari o Y W C ~ O U n- CS L" O O O M L 0 CU To w O - > � Q C` O O a) = 2 5 X a E. L O cc: O a N T6 ii- a) cm eri C H g N S J J O O O CJfCO 5,-8 -5-N. 18 C Co r O 0 0 o X Toffs. O O = 00 0002 > ao Z CCU' 00 0 a f° O N N O � cn Q) E .... .-. . . �. W LT" t0 o v)•2 S N O C Lis O >, ca) a) a) to a) gin U) Cn CO O Q. O . . .� CJ a V C CT E C_pp 2) Cn .. CT U c ^ .... O O O. �? U) L O t Cp N U d .C • `� I-. �.. t = t CCn = V) = ` v co a) ca I. O N C , vi ww ~ a c CP a) I Q v a) O = c o O p o ( c d E U L 1... 2 aO .`= d = O OJ ? O .C C :us a- > = •p) • CO a`) >, a) E Op 0() N - '= CT_O ` ~ - t N N O O .c 5.,O) a d a mu' O c to z o >, a) G .c .� Q• > O O a) ~ V L _coo U >. a) O . a) N V 2 � � U (nUH O C (n � JQ > F- Z c (n (nM � C ~ = fn > d a? O is co 0 O y F¢-' -a H a m In NT O N N N v N 00 N e3 v) O G. co •— N II II co aN o a co n N II c m N < an 4) . CO a o N. 8 II r- a a o 0 p I V N N U o o O O N m U 0 0 0 0 0 T:0 a, 5 o rDJ oca ) to N N U a m � *Cr*Crgo,rot is o a) 0 0 gla co^ I. C v N U O Q) O CO re ro �2 � o UL I- O a O as L Cl m co •- o N O > erg O O �1 tD O 3 U) �•i N V N M (O)0 M i CoO N O fD O it en Fa_ E Z Q 0.) C o)le inc w DI o w .� Q 4) 03 a o v O OY.- @ t- N CO in U O > �, QM Q. CT; th CO < N O N .rat O "O A/ O � O v •tow LL N .a' a' E 'E -I K 5 E LL�1 Q 0-CO 4) N N E W J a C.) vi t x N Os CD LIT 2 Q1 O > `° NI.rn (/) r o N �y Q 3 L co •E N; cv nr F- C 2 w CCI i—• a) - 0O I- Q C O C t N st c COtip - Q O �C 3 L a O W N L O o . L E N C ct 2 O .Q O c o O 4) S... OO O w eL n m CA I' CO g C' U CO L U 4D) .c z o ° °' � � � r O f° y Q OO ` (9 • - a r ,0 N v N czs to CNI a ..i CO N- LI) Ni C c) o c9 • co N v 4-1 CO r r- 0 N CO CO E N W 3 o r3 -cfs LL o CZ C C it W • J c0• o t Y tr) in o Z Q ets _o c �_ CO- - m` cz r CO Cl) Z O J v) C 13 O -10 CD •> 1. cx 'N _ C X N o LL NO •CD N E W Ri in , cn C N- O >O O J ? Cl) i x f- as _ Y ct cts 00 = I-- X C O 0 Q ClO o cz oN N en o 76 O N O Q O W. L o ce `ci - > as �, '- Cr: u 0 o c a O C o -0 O o a# -, V) CI) co O a) co a V 0 can co L- E o ° Q < W O O 0 a .. WI NT O N N A N b Ct O CL .-- CO V 1 'i 03 i o co LL .c c � v (.5 a) U, 03 mmm oa u)a 03-O E v L N ,_ o a• coz N I C O 3 Z a ea E n- .2 Hd C O a cc ' sa a cct N 'm — O - C ° E .0 O •- •_ — N r Q 3.. N H 6 CD 0 0 0 0 0 0 O CO M CO > LO N_ C U N 00000 (00 00 00 Q E '� en H J C-IC co .— M t— M00 00 00 OE W = J N .4- v = 0C V' CD 0 C 0Cs O O N 0 .. L Ha. oa o > a c ...4.73 co 100 ii f9WOp a) a) C H ye a) Cii J J O O > -J N 5.18 C cep O� o 0 O (D X i.. 0 L O O 00 O O O Z > N Z U' U' U' U' O a fU O N N O � vn a) E .... W O . . O �.+ o v)•� .E N i.. C o CC U) co a a n 'O O a • • .C . . a) >. CO a) a) U) O C to CO O Q. O . . .� V a t) C CT _pp N e. p O1 co U c ^ . . O O aC D � U) t O t CO U) U a) 4—.. `• I-. O• N C ,~ T-1 C N I Q v a) `O = eO9 0 0 0 0 •ico c d E U CL 3.. 47, 2 a0 .`= N = O OJ ? Ot C ling � > > = •p) 0a`> >, a) Eo a) E '= a) 2E - ta) a) o0 .c 3...t2 ,.‘a dam O U) = ;S o >,>, a) G t 4, Q• > O O a) ~ V t _coo C) >. a) O t co mu' iO V 2 � DU (nUHO C (n0JQ > F- Z c (n (n � � wr C ~ = fn > a a? O RIcp 0 O O F-H¢ -a H a m In71- O N N v N ti) N e3 In0 Cl.* co •— N II 0 II co aN o O cn n N II c m N < an 4) . (o a o N. 8 II a a co 0 p 1 V N N U o o O O N cum ca 8. m 0 0 0 T::. Co) 0 0 0 • 5 0 0 a U to N N a m *Cr 0) LL O 0) 0 0 via co bc i C a N U0 00 0 O CO re CO �2 � o ch LL I- o a O as L eZ O •- O N 1� o O > 4) N O O c • �1 tD t CO O 3 Al 0) N 4 0 44 - i 2 111 `� M Co 1 O N a co a v E Z O COoC < d/ = a 0v0 1.e O O tt in V `a° 0 M CO C C > < N O N .a O L O in a O 1_ fr (r a' W.O [T3 •— O , AC a LL in N p•co 4) 2) N E J w V F- V) • N CS LL _ co. 0 Cr j d o cn Cl, ra v O 4 a � C4 ` J co .c 7 F- 1 >. a ^ o y 6 to a) - 00 0 X N O Y L N C 0 H Q 0 LCD 1-1-. O LL"-' N o a c° ' E B o o .O s w 4) 3-) 00 n m > 0....0....0 - CA CD CO D c j r L U 4D i .� z 0 O d 3 e- 0 O f° y Q U ` " ' -- a r rC 0 v N to CNI czs O O .—i COCoCOLO C CO r N- o • T \I- \I" +, N co v C N N E N N E N w To O r3 t LL O C O c �E cn V COcr, CO it • W J CO O LO CCD Z O a Hi-Ce ~ CO m 03 w o N Z _i v) O 96 E •� C IX O N. T• Y! E• • W W o) cn X - N N -a it ON _ O O cn a x (1) (id > (N 00 =I_x c v O Qes ca en O I ra O ii N t o. N L ooN O C) O > E ce aQ > a. Cc CO CD O o O c o 0. C/) � o ct c a) co c`a o O oCO V 0 in E _ o 0 H W O O 0 a .. E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 ****************************************************************************************** * Project Setup Information * * ************************************************************** *** *********************** Project File : G : \NGL Permits and Cert Checklists\C10\C10 400 bbl Oil Tank (T3) . ept Model : Stable Oil Tank Calculation Method : AP42 Control Efficiency : 100 . 0% Filed Name : C10 Oil Tank (3 x 400 bbl ) . Modeled for one tank . Well Name : C10 Date : 2014 . 10 . 22 ************ ********* * ** **** ************************************************************** * Data Input ** *** ************* ******* *** ************************************************************** Separator Pressure : 23 . 00 [psig] Separator Temperature : 85 . 00 [F] Ambient Pressure : 14 . 70 [psia] Ambient Temperature : 70 . 00 [F] C10+ SG : 0 . 9240 C10+ MW : 194 . 40 -- Stable Oil No . Component mol % 1 H2S 0 . 0000 2 O2 0 . 0000 3 CO2 0 . 0000 4 N2 0 . 0000 5 Cl 0 . 0000 6 C2 0 . 0000 7 C3 0 . 0000 8 i-C4 0 . 0000 9 n-C4 0 . 0000 10 i-05 0 . 8300 11 n-05 0 . 8300 12 C6 4 . 8800 13 C7 14 . 4100 14 C8 9 . 9600 15 C9 14 . 9200 16 C10+ 39 . 7800 17 Benzene 0 . 8100 18 Toluene 4 . 2100 19 E-Benzene 0 . 2700 20 Xylenes 4 . 7700 21 n-C6 4 . 3300 22 224Trimethylp 0 . 0000 -- Sales Oil Production Rate : 200 [bbl/day] Days of Annual Operation : 365 [days/year ] API Gravity . 47 . 0 Reid Vapor Pressure : 3 . 20 [psia] Bulk Temperature : 70 . 00 [F] -- Tank and Shell Data Diameter : 12 . 00 [ ft ] Shell Height : 20 . 00 [ ft ] Cone Roof Slope : 0 . 30 Average Liquid Height . 10 . 00 [ ft ] Vent Pressure Range : 0 . 03 [psi ] Solar Absorbance : 0 . 54 -- Meteorological Data City : Denver, CO page 1 E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 Ambient Pressure : 14 . 70 [psia] Ambient Temperature : 70 . 00 [F ] Min Ambient Temperature : 36 . 20 [F ] Max Ambient Temperature : 64 . 30 [F] Total Solar Insolation : 1568 . 00 [Btu/ft^2*day] ******************************************************* *********************************** * Calculation Results * ************ ****************************************************************************** -- Emission Summary Item Uncontrolled Uncontrolled [ton/yr] [ lb/hr] Total HAPs 0 . 160 0 . 037 Total HC 0 . 702 0 . 160 VOCs , C2+ 0 . 702 0 . 160 VOCs , C3+ 0 . 702 0 . 160 Uncontrolled Recovery Info . Vapor 16 . 6500 x1E-3 [MSCFD ] HC Vapor 16 . 6500 x1E-3 [MSCFD] GOR 0 . 08 [SCF/bbl ] -- Emission Composition No Component Uncontrolled Uncontrolled [ton/yr] [ lb/hr] 1 H2S 0 . 000 0 . 000 2 O2 0 . 000 0 . 000 3 CO2 0 . 000 0 . 000 4 N2 0 . 000 0 . 000 5 Cl 0 . 000 0 . 000 6 C2 0 . 000 0 . 000 7 C3 0 . 000 0 . 000 8 i-C4 0 . 000 0 . 000 9 n-C4 0 . 000 0 . 000 10 i-05 0 . 076 0 . 017 11 n-05 0 . 060 0 . 014 12 C6 0 . 152 0 . 035 13 C7 0 . 183 0 . 042 14 C8 0 . 047 0 . 011 15 C9 0 . 027 0 . 006 16 C10+ 0 . 000 0 . 000 17 Benzene 0 . 014 0 . 003 18 Toluene 0 . 024 0 . 005 19 E-Benzene 0 . 001 0 . 000 20 Xylenes 0 . 009 0 . 002 21 n-C6 0 . 109 0 . 025 22 224Trimethylp 0 . 000 0 . 000 Total 0 . 702 0 . 160 -- Stream Data No . Component MW Stable Oil Sales Oil Total Emissions mol % mol % mol 1 H2S 34 . 80 0 . 0508 0 . 0000 0 . 0000 2 O2 32 . 00 0 . 0000 0 . 0000 0 . 0000 3 CO2 44 . 01 0 . 2437 0 . 0000 0 . 0000 4 N2 28 . 01 0 . 0102 0 . 0000 0 . 0000 5 Cl 16 . 04 0 . 9543 0 . 0000 0 . 0000 6 C2 30 . 07 0 . 6701 0 . 0000 0 . 0000 7 C3 44 . 10 2 . 1827 0 . 0000 0 . 0000 8 i-C4 58 . 12 1 . 1269 0 . 0000 0 . 0000 9 n-C4 58 . 12 4 . 6091 0 . 0000 0 . 0000 10 i-05 72 . 15 3 . 1066 0 . 8286 13 . 2102 11 n-05 72 . 15 5 . 0558 0 . 8289 10 . 3988 12 C6 86 . 16 4 . 1726 4 . 8780 22 . 5161 13 C7 100 . 20 10 . 3655 14 . 4090 23 . 5142 14 C8 114 . 23 10 . 8426 9 . 9605 5 . 2671 page 2 E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 15 C9 128 . 28 5 . 5127 14 . 9213 2 . 7479 16 C10+ 194 . 40 45 . 9695 39 . 7844 0 . 0162 17 Benzene 78 . 11 0 . 5685 0 . 8098 2 . 1879 18 Toluene 92 . 13 0 . 2132 4 . 2101 3 . 2715 19 E-Benzene 106 . 17 0 . 0711 0 . 2700 0 . 0694 20 Xylenes 106 . 17 0 . 6802 4 . 7704 1 . 0686 21 n-C6 86 . 18 3 . 5939 4 . 3287 15 . 7320 22 224Trimethylp 114 . 24 0 . 0000 0 . 0000 0 . 0000 MW 139 . 45 139 . 45 87 . 50 Stream Mole Ratio 1 . 0000 0 . 9999 0 . 0001 Heating Value [BTU/SCF] 4752 . 21 Gas Gravity [Gas/Air] 3 . 02 Bubble Pt . @ 100F [psia] 1 . 48 1 . 48 RVP @ 100F [psia] 10 . 09 10 . 09 SG @ 100F 0 . 807 0 . 807 page 3 E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 ****************************************************************************************** * Project Setup Information * * ************************************************************** *** *********************** Project File : G : \NGL Permits and Cert Checklists\C10\C10 400 bbl Slop-Sale Oil Tank (T4 , T5) . ept Model : Stable Oil Tank Calculation Method : AP42 Control Efficiency : 100 . 0% Filed Name : C10 Slop/Sale Oil Tanks ( 1 x 400 bbl) . Modeled for one tank Well Name : C10 Date : 2014 . 10 . 03 ************ ********* * ** **** ************************************************************** * Data Input ** *** ************* ******* *** ************************************************************** Separator Pressure : 23 . 00 [psig] Separator Temperature : 85 . 00 [F] Ambient Pressure : 14 . 70 [psia] Ambient Temperature : 70 . 00 [F] C10+ SG : 0 . 9240 C10+ MW : 194 . 40 -- Stable Oil No . Component mol % 1 H2S 0 . 0000 2 O2 0 . 0000 3 CO2 0 . 0000 4 N2 0 . 0000 5 Cl 0 . 0000 6 C2 0 . 0000 7 C3 0 . 0000 8 i-C4 0 . 0000 9 n-C4 0 . 0000 10 i-05 0 . 8300 11 n-05 0 . 8300 12 C6 4 . 8800 13 C7 14 . 4100 14 C8 9 . 9600 15 C9 14 . 9200 16 C10+ 39 . 7800 17 Benzene 0 . 8100 18 Toluene 4 . 2100 19 E-Benzene 0 . 2700 20 Xylenes 4 . 7700 21 n-C6 4 . 3300 22 224Trimethylp 0 . 0000 -- Sales Oil Production Rate : 600 [bbl/day] Days of Annual Operation : 365 [days/year ] API Gravity . 47 . 0 Reid Vapor Pressure : 3 . 20 [psia] Bulk Temperature : 70 . 00 [F] -- Tank and Shell Data Diameter : 12 . 00 [ ft ] Shell Height : 20 . 00 [ ft ] Cone Roof Slope : 0 . 30 Average Liquid Height . 10 . 00 [ ft ] Vent Pressure Range : 0 . 03 [psi ] Solar Absorbance : 0 . 54 -- Meteorological Data City : Denver, CO page 1 E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 Ambient Pressure : 14 . 70 [psia] Ambient Temperature : 70 . 00 [F ] Min Ambient Temperature : 36 . 20 [F ] Max Ambient Temperature : 64 . 30 [F] Total Solar Insolation : 1568 . 00 [Btu/ft^2*day] ******************************************************* *********************************** * Calculation Results * ************ ****************************************************************************** -- Emission Summary Item Uncontrolled Uncontrolled [ton/yr] [ lb/hr] Total HAPs 0 . 270 0 . 062 Total HC 1 . 220 0 . 279 VOCs , C2+ 1 . 220 0 . 279 VOCs , C3+ 1 . 220 0 . 279 Uncontrolled Recovery Info . Vapor 28 . 9600 x1E-3 [MSCFD ] HC Vapor 28 . 9600 x1E-3 [MSCFD] GOR 0 . 05 [SCF/bbl ] -- Emission Composition No Component Uncontrolled Uncontrolled [ton/yr] [ lb/hr] 1 H2S 0 . 000 0 . 000 2 O2 0 . 000 0 . 000 3 CO2 0 . 000 0 . 000 4 N2 0 . 000 0 . 000 5 Cl 0 . 000 0 . 000 6 C2 0 . 000 0 . 000 7 C3 0 . 000 0 . 000 8 i-C4 0 . 000 0 . 000 9 n-C4 0 . 000 0 . 000 10 i-05 0 . 133 0 . 030 11 n-05 0 . 105 0 . 024 12 C6 0 . 264 0 . 060 13 C7 0 . 318 0 . 073 14 C8 0 . 082 0 . 019 15 C9 0 . 047 0 . 011 16 C10+ 0 . 000 0 . 000 17 Benzene 0 . 024 0 . 005 18 Toluene 0 . 042 0 . 010 19 E-Benzene 0 . 001 0 . 000 20 Xylenes 0 . 016 0 . 004 21 n-C6 0 . 189 0 . 043 22 224Trimethylp 0 . 000 0 . 000 Total 1 . 221 0 . 279 -- Stream Data No . Component MW Stable Oil Sales Oil Total Emissions mol % mol % mol 1 H2S 34 . 80 0 . 0508 0 . 0000 0 . 0000 2 O2 32 . 00 0 . 0000 0 . 0000 0 . 0000 3 CO2 44 . 01 0 . 2437 0 . 0000 0 . 0000 4 N2 28 . 01 0 . 0102 0 . 0000 0 . 0000 5 Cl 16 . 04 0 . 9543 0 . 0000 0 . 0000 6 C2 30 . 07 0 . 6701 0 . 0000 0 . 0000 7 C3 44 . 10 2 . 1827 0 . 0000 0 . 0000 8 i-C4 58 . 12 1 . 1269 0 . 0000 0 . 0000 9 n-C4 58 . 12 4 . 6091 0 . 0000 0 . 0000 10 i-05 72 . 15 3 . 1066 0 . 8292 13 . 2102 11 n-05 72 . 15 5 . 0558 0 . 8294 10 . 3988 12 C6 86 . 16 4 . 1726 4 . 8789 22 . 5161 13 C7 100 . 20 10 . 3655 14 . 4094 23 . 5142 14 C8 114 . 23 10 . 8426 9 . 9603 5 . 2671 page 2 E&P TANK V2 . 0 Calculation Report--- Developed by DB Robinson & Associates Ltd . 2014 . 10 . 22 15 C9 128 . 28 5 . 5127 14 . 9208 2 . 7479 16 C10+ 194 . 40 45 . 9695 39 . 7826 0 . 0162 17 Benzene 78 . 11 0 . 5685 0 . 8099 2 . 1879 18 Toluene 92 . 13 0 . 2132 4 . 2101 3 . 2715 19 E-Benzene 106 . 17 0 . 0711 0 . 2700 0 . 0694 20 Xylenes 106 . 17 0 . 6802 4 . 7702 1 . 0686 21 n-C6 86 . 18 3 . 5939 4 . 3293 15 . 7320 22 224Trimethylp 114 . 24 0 . 0000 0 . 0000 0 . 0000 MW 139 . 45 139 . 45 87 . 50 Stream Mole Ratio 1 . 0000 0 . 9999 0 . 0001 Heating Value [BTU/SCF] 4752 . 21 Gas Gravity [Gas/Air] 3 . 02 Bubble Pt . @ 100F [psia] 1 . 48 1 . 48 RVP @ 100F [psia] 10 . 09 10 . 09 SG @ 100F 0 . 807 0 . 807 page 3 NGL Water Solutions DJ , LLC Facility: C10 Salt Water Disposal Facility Permit #: TBD AIRS ID : TBD Emission Unit ID : SUMP Description : Produced Water Unloading Sump Dimensions Width 10 ft Length 10 ft Depth 11 ft Volume 1100 (ft 3) Capacity 196 bbl (ft 3 X 0. 1781 bbl/ft3) Capacity 8228 gal Effective diameter 11 .28 ft Throughput (gal/yr) 306,600,000 Emissions* Pollutant Ib/yr TPY VOC 2437.69 1 .22 Benzene 46.78 0.02 Toluene 82.50 0.04 Ethylbenzene 2.02 0.00 Xylenes 31 .05 0.02 n- Hexane 371 . 11 0. 19 Methanol 0.00 0.00 * Emissions were calculated using EPA TANKS 4.0.9d. HAPS Speciation * Analyte Mass Benzene 1 .92% Toluene 3.38% Ethylbenzene 0.08% Xylenes 1 .27% n-Hexane 15.22% Methanol 0.00% ' Speciation from E&P Tank Results kr) NT O N N A N b al O CL .. 00 N r r O r) w a) E a, to a) > 0 t 0 C Cu C.) t. ._ 3 .— CO L In as 4-• a) L L O U.In E U co to — Q to 03 a �a aa) N a CNI C• co r A r n I 1.L x 2 Y t o iin n E C �. x cnco 2 Z O ea oo P- a G) _ > - Q r < •v) O 0 m a _CCD CCt N ' Q -C C) c a = 0 -a V E Cl) .47. C) a) E oco0or� cno oca 0 Cl) N Il O (Ni O O M O O O O O a E •r V L C e- rr6ei6Ci 00 00 E E -0 co J � '� rrire NG0O V N N OZ W C D o c " E M et) O 0 Y s u) H O N Co 0 C og > � M 0 0 CU DCf 8r 0 r > .� 8 D }BxM ..... .. .. O CCS 0 t .C L a2a`> > 33r 0 - O O C J O (� Cd CO C a 00 N— O O U� O O C � O .. O O 000Z > W ca Z 0000 0 o f)0 O ca N 0 .0 Cn co in Q) E .... W O i.. _ — C re 0 a Q0 O co Q o . . .•.• L ^0) co �v „ .0 V C C O ("(np' CM 'O C 7 p :►+ N C CO C ?a 0 t g,C C� U C � � � = O L rfjj in � co •O Cl) O w .."., co0 L. 0 C C ca c >.�- O .N 'P a) = U 2 a .13. c 0 .� C O - 3.. d- ..Ci) CO a ui a0 CD ti a) � � t 0> .....c zc 6- UU ,U'-O . co ` N O. v • 0i o ,a, a`�i as = ,'a- >o r m ~ V .c .c 00 00 V >a. a) o r a t o V � D0W0E- O ,cv) bJQ > HZ � cocnwcc wF- m .5., ant m O '° a Ce m 2 4. In NT O N N v N to N e3 �, O a co .— N II 0 CI tri II co a. N o a co n N II j I- CD N < an 4) . CO a o 0 8 II a a co 0 p 1 V N N U o o O O N m 0 0 0 0 C4 o Co) v o o Iv CO NJ LO v) N U Cal a m m m > 2 l i M CD O O 11.0 co = a in N V O O O CO • ro co �2 � tn N- ol LL I- O O O CU co - CO O O /� O >. m X 0 0 VI E ..1 N CO O 3 Y elU, N Ili (n Ws C ct, CON- 0 Ch M Co Qiii O CD O it N I— E C O 2. el cCt. C0oQD O Ima Q _ a o v o r Ce v..# V o tit d a to CJ x > 0) � M V) C LL Q N O N O LO O O — RI .N 3 a s...s...MI in Cr.. W i - C/) v 3 CD . N CS 03 W CO J 't• cn O v' -v0) - U o C cryNJ 2, k t Q L @ c vH E owE 6 CO o) 0O X CD C O .o N O Q `n 0 C M O L N Ott. > ct N 'd a 1...O O v o o O O 5 a a � U ° D o z O r O Cl.) Q U U ` (9 -- a r ,O O 71-v N to CNI czs 0 a .—i cn Lc) cn co C f•-• CO O O • • , N N- L() 4-. NO co co N N N N E N w To O 4-• U-LL O F— RS C Ca E N a = .� C o to rn TT i' W H J 1- (C) 't c N Z OC o 1-o- - _o c Q E— ;-Fic m ~ to cG o -> ca s.. Cl) - O o rn CO W co CO o -D - N U) O O C) O C U cri a t as = \O = cn OO x c o-) O Q t cv en L.: o a) O .� D w 0 ge a ccz L 5 O @ O E CI, CC c > �. 0N v � a) O 0 0 cn a. L_ O CO V E O o H W U O O a cu .. NGL Water Solutions DJ , LLC Facility: C10 Salt Water Disposal Facility Permit #: TBD AIRS ID : TBD Emission Unit ID : Loadout Description : Oil Loadout Throughput (gal/yr) 9, 198,000 Saturation Factor, S* 0.6 Vapor Pressure. P (psia) ** 2.8 Vapor Molecular Weight, M (Ib/Ib-mol) ** 50 Liquid Temperature, T (°F) 60 Liquid Temperature, T (°R) 520 * From AP-42 Table 5.2- 1 . for tank trucks in submerged loading : dedicated normal service ** From AP42 Table 7. 1 -2. Crude Oil (RVP 5) , 60 deg Loading Loss (lb VOC/1000 gal) = (12.46*S*P*M)/T AP42 Section 5.2 ( 1 /95) Loading Loss (lb VOC/1000 gal) = 2.01 Loading Loss Throughput Emissions Pollutant lb/1000 gal gal/yr lb/yr TPY VOC 2.01 9. 198. 000 18513.45 9.26 Benzene 0.039 9. 198.000 355.27 0. 18 Toluene 0.068 9, 198.000 626.57 0.31 Ethylbenzene 0.002 9. 198.000 15.32 0.01 n-Hexane 0.306 9, 198.000 2818.44 1 .41 Xylenes 0.026 9. 198.000 235.85 0. 12 Methanol 0.00 9, 198.000 0.00 0.00 NGL Water Solutions Di, LLC Facility: C10 Salt Water Disposal Facility Permit #: TBD AIRS ID: TBD Process Piping Fugitives Calculation Hours of Total HC Total VOC Component Type Emission Factors' Source Count Percent VOC Total VOC Emissions Operation Emissions Emissions (lb/hr/source) hrs (lb/hr) (lb/hr) TPY i Valve-gas (oil tanks) 0.009921 6 100.00% 8760 0.06 0.06 0.26 Flanges -gas (oil tanks) 0.000860 18 100.00% 8760 0.02 0.02 0.07 Connectors -gas (oil tanks) 0.000441 75 100.00% 8760 0.03 0.03 0.14 Others -gas (oil tanks) 0.019401 12 100.00% 8760 0.23 0.23 1.02 Open-Ended Lines-gas (oil tanks) 0.004409 15 100.00% 8760 0.07 0.07 0.29 Pump Seals-gas (oil tanks) 0.005291 0 100.00% 8760 0.00 0.00 0.00 Valve-gas (PW tanks) 0.009921 0 3.00% 8760 0.00 0.00 0.00 Flanges -gas (PW tanks) 0.000860 56 3.00% 8760 0.05 0.00 0.01 Connectors -gas (PW tanks) 0.000441 112 3.00% 8760 0.05 0.00 0.01 Others -gas (PW tanks) 0.019401 8 3.00% 8760 0.16 0.00 0.02 Open-Ended Lines-gas (PW tanks) 0.004409 0 3.00% 8760 0.00 0.00 0.00 Pump Seals-gas (PW tanks) 0.005291 0 3.00% 8760 0.00 0.00 0.00 Valve-Light Oil 0.005512 32 100.00% 8760 0.18 0.18 0.77 Flanges -Light Oil 0.000243 0 100.00% 8760 0.00 0.00 0.00 Connectors -Light Oil 0.000463 191 100.00% 8760 0.09 0.09 0.39 Others -Light Oil 0.016535 6 100.00% 8760 0.10 0.10 0.43 Open-Ended Lines-Light Oil 0.000309 2 100.00% 8760 0.00 0.00 0.00 Pump Seals-Light Oil 0.028660 1 100.00% 8760 0.03 0.03 0.13 Valve -Water/Oil 0.000216 92 100.00% 8760 0.02 0.02 0.09 Flanges-Water/Oil 0.000006 234 100.00% 8760 0.00 0.00 0.01 Connectors -Water/Oil 0.000243 364 100.00% 8760 0.09 0.09 0.39 Others -Water/Oil 0.030865 4 100.00% 8760 0.12 0.12 0.54 Open-Ended Lines-Water/Oil 0.000551 20 100.00% 8760 0.01 0.01 0.05 Pump Seals-Water/Oil 0.000053 4 100.00% 8760 0.00 0.00 0.00 Valve-Heavy Oil 0.000019 3 100.00% 8760 0.00 0.00 0.00 Flanges -Heavy Oil 0.000001 0 100.00% 8760 0.00 0.00 0.00 Connectors -Heavy Oil 0.000017 17 100.00% 8760 0.00 0.00 0.00 Others -Heavy Oil 0.000071 0 100.00% 8760 0.00 0.00 0.00 Open-Ended Lines-Heavy Oil 0.003086 3 100.00% 8760 0.01 0.01 0.04 Pump Seals-Heavy Oil 0.028660 0 100.00% 8760 0.00 0.00 0.00 'EPA-453/R-95.017, Table 2-4 1275 I TOTALS: 1.31 1.06 4.65 HAPs Component Wt% lb/hr ton/yr lb/yr BZ 0.53% 0.01 0.03 61 Not Reportable Tol 3.27% 0.04 0.19 375 Reportable EB 0.25% 0.00 0.01 28 Not Reportable Xyl 4.27% 0.06 0.24 488 Reportable n-Hex 3.14% 0.04 0.18 360 Reportable Tank Description 1$ of Tanks VOC wt% Oil Vessels 6 100.00% Produced Water Vessels 4 3.00% for vapor factors only -Offload and Sump 1 100.00% Diesel Tank 1 100.00% Emulsion Breaker Drum 1 100.00% Fugitive component counts based on hard counts from similar facilities Emissions presented take no credit for the AVO program NGL Water Solutions D1, LLC C10 Salt Water Disposal Facility Specific Gravity Calc Composition used in E&P TANK modeling analysis (Wt% ` SG) C10+ C10+ MW MW Specific C10+ Component Mole % Mole% Wt % Wt% MW Calc C10+ Gravity Average normalized C 1 0.00% 0.00% 16.04 0.00 0.300 0 C 2 0.00% 0.00% 30.07 0.00 0.356 0 C 3 0.00% 0.00% 44.10 0.00 0.507 0 C 4 0.00% 0.00% 58.12 0.00 0.563 0 C 4 0.00% 0.00% 58.12 0.00 0.584 0 C 5 0.00% 0.00% 72.15 0.00 0.624 0 C 5 1 .66% 0.79% 72.15 1.20 0.631 0.0050 C 6 10.02% 5.70% 86.18 8.64 0.664 0.0378 C 7 18.62% 12.31% 95.88 17.85 0.709 0.0873 C 8 15.00% 11 .30% 107.35 16.10 0.740 0.0836 C 9 14.92% 12.62% 116.95 17.45 0.785 0.0991 C 10 6.81% 17.12% 6.39% 11.16% 134.00 9.13 22.95 0.779 0.0498 0.0869 C 11 5.33% 13.40% 5.49% 9.59% 147.00 7.84 19.70 0.790 0.0434 0.0758 C 12 4.23% 10.64% 4.75% 8.30% 161.00 6.81 17.12 0.801 0.0380 0.0665 C 13 3. 17% 7.97% 3.86% 6.74% 175.00 5.55 13.95 0.812 0.0313 0.0547 C 14 3. 19% 8.02% 4. 17% 7.28% 190.00 6.06 15.24 0.823 0.0343 0.0599 C 15 2. 19% 5.51% 3.06% 5.34% 206.00 4.51 11.34 0.833 0.0255 0.0445 C 16 1 .95% 4.90% 2.91% 5.08% 222.00 4.33 10.89 0.840 0.0244 0.0427 C 17 1 .47% 3.70% 2.32% 4.05% 237.00 3.48 8.76 0.848 0.0197 0.0344 C 18 1 .07% 2.69% 1 .80% 3.14% 251.00 2.69 6.75 0.853 0.0154 0.0268 C 19 1 .31% 3.29% 2.32% 4.05% 263.00 3.45 8.66 0.858 0.0199 0.0348 C 20 0.99% 2.49% 1 .85% 3.23% 275.00 2.72 6.85 0.863 0.0160 0.0279 C 21 1 .24% 3.12% 2.43% 4.24% 291.00 3.61 9.07 0.868 0.0211 0.0368 C 22 0.90% 2.26% 1 .85% 3.23% 305.00 2.75 6.90 0.873 0.0162 0.0282 C 23 0.86% 2.16% 1 .85% 3.23% 318.00 2.73 6.88 0.878 0.0162 0.0284 C 24 0.71% 1 .79% 1 .58% 2.76% 331.00 2.35 5.91 0.882 0.0139 0.0243 C 25 0.68% 1 .71% 1 .58% 2.76% 345.00 2.35 5.90 0.886 0.0140 0.0245 C 26 0.66% 1 .66% 1 .58% 2.76% 359.00 2.37 5.96 0.890 0.0141 0.0246 C 27 0.63% 1 .58% 1 .58% 2.76% 374.00 2.36 5.92 0.894 0.0141 0.0247 C 28 0.34% 0.85% 0.90% 1.57% 388.00 1.32 3.32 0.897 0.0081 0.0141 C 29 0.33% 0.83% 0.90% 1.57% 402.00 1.33 3.34 0.900 0.0081 0.0141 C 30 plus 1 .71% 4.30% 4.08% 7.13% 478.00 8.17 20.55 0.917 0.0374 0.0654 Total 100.0% 100.0% 147.12 0.794 C10+ 39.77% 100.0% 57.25% 100.0% 85.89 216.0 0.840 C10+ with margin of: 10% 56.57 194.4 0.924 Parameters (MW and SG) from above calculations correlate with sample results shown below: Specific Average MW Gravity 147.16 0.794 mol% Composition less HAP Benzene C6 0.81% C6 = 4.88% Toluene C7 4.21% C7 = 14.41% Ethylbenzene C8 0.27% C8 = 9.96% Xylenes C8 4.77% C10+ = 39.77% n-hexane C6 4.33% Representative Liquid Analysis Normalized to 63.23% % of Hydrocarbons Mass % Vol % Mol% Mass % Vol % Mol% 1 .954 300 propane P3 0.035 0.053 0.095 0.06% 0.08% 0. 15% 2.072 361 .4 14 i-butane 0.066 0.088 0. 135 0. 10% 0. 14% 0.21 % 2. 173 402.94 P4 n-butane 0.346 0.443 0.706 0.55% 0.70% 1 . 12% 2.543 470.415 i-pentane 0.654 0.784 1 .076 1 .03% 1 .24% 1 .70% 2.744 497.74 P5 n-pentane 1 .079 1 .28 1 .776 1 .71 % 2.02% 2.81 % 3.54 564.38 16 2.3-dimethylbutane 0.27 0.303 0.372 0.43% 0.48% 0.59% 3.609 568.916 2-methylpentane 0.977 1 . 11 1 .345 1 .55% 1 .76% 2. 13% 3.848 583.32 16 3-methylpentane 0.629 0.703 0.867 0.99% 1 . 11 % 1 .37% 4. 157 600 P6 n-hexane 1 .988 2.239 2.739 3. 14% 3.54% 4.33% 4.645 622.73 17 2.2-dimethylpentane 0.064 0.071 0.076 0. 10% 0. 11 % 0. 12% 4.729 626.29 N6 methylcyclopentane 0.849 0.842 1 . 198 1 .34% 1 .33% 1 .89% 4.787 628.72 17 2,4-dimethylpentane 0. 152 0. 167 0. 18 0.24% 0.26% 0.28% 5.364 650.54 A6 benzene 0.335 0.283 0.509 0.53% 0.45% 0.81 % 5.453 653.6 O7 2-methyl-c-hexene-3 0.036 0.039 0.044 0.06% 0.06% 0.07% 5.599 658.5 N6 cyclohexane 0.958 0.914 1 .352 1 .52% 1 .45% 2. 14% 5.841 666.26 17 2-methylhexane 0.937 1 .025 1 . 11 1 .48% 1 .62% 1 .76% 5.893 667.89 17 2.3-dimethylpentane 0.254 0.272 0.301 0.40% 0.43% 0.48% 5.993 670.92 X6 t-amylmethylether 0.25 0.247 0.291 0.40% 0.39% 0.46% 6. 13 674.99 17 3-methylhexane 0.953 1 .03 1 . 129 1 .51 % 1 .63% 1 .79% 6.348 681 .21 N7 1 c.3-dimethylcyclopentane 0.261 0.26 0.316 0.41 % 0.41 % 0.50% 6.449 684 N7 1t.3-dimethylcyclopentane 0.307 0.305 0.372 0.49% 0.48% 0.59% 6.551 686.76 N7 1t.2-dimethylcyclopentane 0.381 0.377 0.461 0.60% 0.60% 0.73% 7.069 700 P7 n-heptane 2.582 2.804 3.059 4.08% 4.43% 4.84% 7.971 722.71 N7 methylcyclohexane 2.789 2.691 3.372 4.41 % 4.26% 5.33% 8.002 723.44 -- unknown 0.041 0.043 0.049 0.06% 0.07% 0.08% 8.048 724.49 18 2.2-dimethylhexane 0. 162 0. 173 0. 169 0.26% 0.27% 0.27% 8.487 734.34 N7 ethylcyclopentane 0.231 0.224 0.279 0.37% 0.35% 0.44% 8.59 736.56 18 2,4-dimethyihexane 0.2 0.213 0.208 0.32% 0.34% 0.33% 8.881 742.65 -- unknown 0. 17 0. 18 0. 177 0.27% 0.28% 0.28% 8.935 743.75 N8 1 c.2t.4-trimethylcyclopentane 0.046 0.045 0.049 0.07% 0.07% 0.08% 9.254 750. 11 O7 O37 0. 132 0. 134 0. 159 0.21 % 0.21 % 0.25% 9.754 759.58 A7 toluene 2.068 1 .771 2.665 3.27% 2.80% 4.21 % 9.973 763.56 18 2.3-dimethylhexane 0. 129 0. 134 0. 134 0.20% 0.21 % 0.21 % 10.017 764.34 18 2-methyl-3-ethylpentane 0.075 0.078 0.078 0. 12% 0. 12% 0. 12% 10.338 769.96 18 2-methylheptane 1 .089 1 . 158 1 . 132 1 .72% 1 .83% 1 .79% 10.403 771 .05 18 4-methylheptane 0.325 0.343 0.338 0.51 % 0.54% 0.53% 10.476 772.318 3,4-dimethylhexane 0.056 0.058 0.059 0.09% 0.09% 0.09% 10.762 777.05 N8 1 c,2c,4-trimethylcyclopentane 0.796 0.776 0.843 1 .26% 1 .23% 1 .33% 10.813 777.88 3-methylhE I8 0.05 0.052 0.052 0.08% 0.08% 0.08% 10.842 778.36 18 3-ethylhexane 0.83 0.864 0.863 1 .31 % 1 .37% 1 .36% 10.928 779.75 N8 1t,4-dimethylcyclohexane 0.359 0.349 0.379 0.57% 0.55% 0.60% 11 . 197 784.02 N8 1 . 1 -dimethylcyclohexane 0. 142 0. 135 0. 151 0.22% 0.21 % 0.24% 11 .385 786.93 19 2.2.5-trimethylhexane 0.035 0.036 0.032 0.06% 0.06% 0.05% 11 .576 789.83 N8 3t-ethylmethylcyclopentane 0.052 0.05 0.055 0.08% 0.08% 0.09% 11 .859 794.03 N8 1t,2-dimethylcyclohexane 0.325 0.311 0.343 0.51 % 0.49% 0.54% 12.274 800 P8 n-octane 2.581 2.728 2.682 4.08% 4.31 % 4.24% 13.339 819.05 19 2.3,4-trimethylhexane 0.086 0.086 0.079 0. 14% 0.14% 0. 12% 13.617 823.75 O9 O52 0.25 0.258 0.235 0.40% 0.41 % 0.37% 14.025 830.45 -- unknown 0.798 0.846 0.75 1 .26% 1 .34% 1 . 19% 14.06 831 .02 19 2.2.3-trimethylhexane 0.177 0. 184 0. 164 0.28% 0.29% 0.26% 14.35 835.63 N8 N4 0.236 0.225 0.25 0.37% 0.36% 0.40% 14.505 838.05 19 3,3-&3.5-dimethylheptane 0.337 0.345 0.312 0.53% 0.55% 0.49% 14.604 839.59 19 2,6-dimethylheptane 0.069 0.073 0.064 0. 11 % 0. 12% 0. 10% 15.36 850.94 N8 N7 0.291 0.277 0.308 0.46% 0.44% 0.49% 15.439 852.09 A8 ethylbenzene 0. 155 0. 133 0. 173 0.25% 0.21 % 0.27% 16.147 862.11 A8 1 ,3-dimethylbenzene 2.181 1 .874 2.439 3.45% 2.96% 3.86% 16.212 863.01 A8 1 ,4-dimethylbenzene 0.516 0.445 0.577 0.82% 0.70% 0.91 % 16.276 863.88 19 2.3-dimethylheptane 0.036 0.037 0.034 0.06% 0.06% 0.05% 16.425 865.92 19 3,4-dimethylheptane 0. 101 0. 103 0.094 0. 16% 0. 16% 0. 15% 16.714 869.79 19 3.4-dimethylheptane 0.387 0.393 0.358 0.61 % 0.62% 0.57% 16.809 871 .06 19 15 0.468 0.476 0.433 0.74% 0.75% 0.68% 17. 171 875.79 -- unknown 0. 111 0. 118 0. 103 0. 18% 0. 19% 0. 16% 17.295 877.39 19 3-ethylheptane 0.518 0.53 0.48 0.82% 0.84% 0.76% 17.623 881 .54 N9 1 c.2t.4c-trimethylcyclohexane 0.037 0.036 0.035 0.06% 0.06% 0.06% 17.738 882.98 N9 1 c.2t.3c-trimethylcyclohexane 0.58 0.568 0.545 0.92% 0.90% 0.86% 17.976 885.93 N9 N18 0.04 0.038 0.037 0.06% 0.06% 0.06% 18.093 887.36 N9 N19 0.344 0.328 0.324 0.54% 0.52% 0.51 % 18.222 888.93 N9 N20 0.211 0.201 0. 199 0.33% 0.32% 0.31 % 18.812 895.95 N9 N22 0.044 0.042 0.041 0.07% 0.07% 0.06% 19. 162 900 P9 n-nonane 2. 104 2. 177 1 .948 3.33% 3.44% 3.08% 19.231 901 .69 N9 1 .1 -methylethylcyclohexane 0. 18 0. 166 0. 17 0.28% 0.26% 0.27% 19.408 906.01 N9 N25 0.07 0.066 0.066 0. 11 % 0. 10% 0. 10% 19.705 913. 17 A9 i-propylbenzene 0.05 0.043 0.049 0.08% 0.07% 0.08% 19.806 915.58 110 I 1 1 0. 134 0. 136 0. 111 0.21 % 0.22% 0. 18% 19.911 918.06 -- unknown 0.065 0.069 0.054 0. 10% 0. 11 % 0.09% 19.986 919.83 110 112 0.036 0.037 0.03 0.06% 0.06% 0.05% 20. 114 922.84 2,4-dimeth 110 0. 194 0. 198 0. 162 0.31 % 0.31 % 0.26% 20.208 925.02 110 2.2-dimethyloctane 0.039 0.039 0.032 0.06% 0.06% 0.05% 20.489 931 .51 110 2,5-dimethyloctane 0.524 0.533 0.437 0.83% 0.84% 0.69% 20.68 935.87 -- unknown 0. 1 0. 106 0.083 0. 16% 0. 17% 0. 13% 20.733 937.07 N9 n-butylcyclopentane 0.054 0.051 0.05 0.09% 0.08% 0.08% 20.927 941 .44 110 3.3-dimethyloctane 0.333 0.335 0.278 0.53% 0.53% 0.44% 21 . 193 947.34 110 3.6-dimethyloctane 0. 117 0. 118 0.098 0. 19% 0. 19% 0. 15% 21 .25 948.6 -- unknown 0.083 0.088 0.07 0. 13% 0. 14% 0. 11 % 21 .571 955.61 A9 1 .4-methylethylbenzene 0.384 0.331 0.379 0.61 % 0.52% 0.60% 21 .649 957.31 -- unknown 0. 145 0. 154 0. 144 0.23% 0.24% 0.23% 21 .747 959.41 N10 N33 0.049 0.045 0.041 0.08% 0.07% 0.06% 21 .819 960.95 -- unknown 0.035 0.037 0.029 0.06% 0.06% 0.05% 21 .854 961 .7 A9 1 ,3.5-trimethyibenzene 0. 148 0. 127 0. 146 0.23% 0.20% 0.23% 21 .926 963.24 110 115 0.46 0.462 0.384 0.73% 0.73% 0.61 % 22.031 965.48 110 116 0.037 0.037 0.031 0.06% 0.06% 0.05% 22.092 966.77 110 5-methylnonane 0. 127 0. 129 0. 106 0.20% 0.20% 0. 17% 22. 178 968.59 110 4-methylnonane 0.316 0.317 0.264 0.50% 0.50% 0.42% 22.291 970.94 A9 1 ,2-methylethylbenzene 0.384 0.323 0.379 0.61 % 0.51 % 0.60% 22.409 973.41 110 3-ethyioctane 0.051 0.051 0.043 0.08% 0.08% 0.07% 22.509 975.48 N10 N35 0.049 0.046 0.042 0.08% 0.07% 0.07% 22.559 976.52 110 3-methylnonane 0.275 0.278 0.229 0.43% 0.44% 0.36% 22.634 978.07 N10 N36 0.037 0.034 0.031 0.06% 0.05% 0.05% 22.848 982.45 A9 1 .2,4-trimethyibenzene 0.034 0.029 0.034 0.05% 0.05% 0.05% 22.974 985.01 110 120 0.893 0.896 0.745 1 .41 % 1 .42% 1 . 18% 23.06 986.75 110 121 0.185 0. 186 0. 154 0.29% 0.29% 0.24% 23.393 993.42 O10 2.3-dimethyloctene-2 0.048 0.048 0.04 0.08% 0.08% 0.06% 23.461 994.76 N10 1 t-methyl-2-n-propylcyclohexane 0.075 0.069 0.063 0. 12% 0. 11 % 0. 10% 23.726 1000 P10 n decant 1 .803 1 .834 1 .505 2.85% 2.90% 2.38% 23.994 1008.73 A9 1 ,2,3-trimethylbenzene 0. 102 0.085 0. 101 0. 16% 0. 13% 0. 16% 24.053 1010.63 A10 1 ,3-methyl-i-propylbenzene 0.079 0.068 0.07 0. 12% 0. 11 % 0. 11 % 24. 162 1014. 14 I11 127 0.043 0.043 0.032 0.07% 0.07% 0.05% 24.213 1015.8 111 128 0.039 0.04 0.03 0.06% 0.06% 0.05% 24.242 1016.72 -- unknown 0.046 0.049 0.035 0.07% 0.08% 0.06% 24.434 1022.86 N10 sec-butylcyclohexane 0.077 0.07 0.065 0. 12% 0. 11 % 0. 10% 24.487 1024.54 Ill 130 0.095 0.095 0.072 0. 15% 0. 15% 0. 11 % 24.548 1026.47 A10 1 .2-methyl-i-propylbenzene 0.307 0.26 0.271 0.49% 0.41 % 0.43% 24.71 1031 .59 -- unknown 0.067 0.071 0.06 0. 11 % 0. 1 1 % 0.09% 24.748 1032.79 Ni 1 N40 0.252 0.234 0. 194 0.40% 0.37% 0.31 % 24.877 1036.83 111 132 0.067 0.062 0.052 0. 11 % 0. 10% 0.08% 24.932 1038.53 -- unknown 0.079 0.084 0.061 0. 12% 0. 13% 0. 10% 24.997 1040.55 A10 1 .3-diethylbenzene 0.049 0.042 0.044 0.08% 0.07% 0.07% 25.087 1043.34 A10 1 ,3-methyl-n-propylbenzene 0.271 0.234 0.24 0.43% 0.37% 0.38% 25.213 1047.23 Al 0 1 .4-diethylbenzene 0.079 0.068 0.07 0. 12% 0. 11 % 0. 11 % 25.247 1048.29 A10 1 .3-dimethyl-5-ethylbenzene 0.032 0.027 0.028 0.05% 0.04% 0.04% 25.316 1050.38 A10 n-butylbenzene 0. 138 0. 119 0. 122 0.22% 0. 19% 0. 19% 25.395 1052.81 111 134 0.038 0.039 0.029 0.06% 0.06°/0 0.05% 25.485 1055.55 N11 N41 0. 14 0. 129 0. 107 0.22% 0.20% 0. 17% 25.592 1058.82 I11 135 0.034 0.035 0.026 0.05% 0.06% 0.04% 25.669 1061 . 14 111 136 0. 169 0. 17 0. 129 0.27% 0.27% 0.20% 25.769 1064. 13 111 138 0. 161 0. 161 0. 122 0.25% 0.25% 0. 19% 25.885 1067.61 Al 0 1 ,4.dimethyl-2-ethylbenzene 0.241 0.204 0.213 0.38% 0.32% 0.34% 25.926 1068.85 A10 A3 0.042 0.036 0.037 0.07% 0.06% 0.06% 25.981 1070.5 111 139 0.074 0.074 0.056 0. 12% 0. 12% 0.09% 26.082 1073.51 111 140 0. 171 0. 171 0. 13 0.27% 0.27% 0.21 % 26. 173 1076. 18 A10 1 .2-dimethyl-4-ethylbenzene 0.081 0.069 0.072 0. 13% 0. 11 % 0. 11 % 26.483 1085.29 111 143 0.092 0.093 0.07 0. 15% 0. 15% 0. 11 % 26.603 1088.79 -- unknown 0.062 0.066 0.047 0. 10% 0. 10% 0.07% 26.663 1090.53 O11 undecene-1 0.055 0.055 0.042 0.09% 0.09% 0.07% 26.72 1092.2 Al 0 1 ,2-dimethyl-3-ethylbenzene 0.058 0.048 0.051 0.09% 0.08% 0.08% 26.788 1094. 17 Al 1 1 ,4-methyl-t-butylbenzene 0.07 0.061 0.056 0. 11 % 0. 10% 0.09% 26.863 1096.31 All 1 ,2-ethyl-i-propylbenzene 0.069 0.058 0.055 0. 11 % 0.09% 0.09% 26.991 1100 P11 n-undecane 1 .628 1 .625 1 .236 2.58% 2.57% 1 .95% 27.097 1104. 16 A10 1 ,2,4,5-tetramethylbenzene 0.039 0.033 0.035 0.06% 0.05% 0.06% 27. 155 1106.44 Al 1 1 ,2-methyl-n-butylbenzene 0.053 0.044 0.043 0.08% 0.07% 0.07% 27.258 1110.47 A10 1 ,2.3,5-tetramethylbenzene 0.037 0.031 0.033 0.06% 0.05% 0.05% 27.287 1111 .6 -- unknown 0.06 0.063 0.053 0.09% 0. 10% 0.08% 27.458 1118.22 -- unknown 0.068 0.072 0.06 0. 11 % 0. 11 % 0.09% 27.491 1119.51 A11 1 ,2-methyl-t-butylbenzene 0.065 0.054 0.052 0. 10% 0.09% 0.08% 27.647 1125.51 -- unknown 0.04 0.043 0.032 0.06% 0.07% 0.05% 27.763 1129.97 Al0 5-methylindan 0. 149 0. 125 0. 134 0.24% 0.20% 0.21 % 27.948 1137.04 Al 1 1 .2-ethyl-n-propylbenzene 0.237 0. 197 0. 19 0.37% 0.31 % 0.30% 28.039 1140.46 Al 1 1 .3-methyl-n-butylbenzene 0.032 0.026 0.025 0.05% 0.04% 0.04% 28. 155 1144.84 All s-pentylbenzene 0.05 0.042 0.04 0.08% 0.07% 0.06% 28.348 1152. 11 N12 1 t-M-2-(4-MP)cyclopentane 0.086 0.08 0.061 0. 14% 0. 13% 0. 10% 28.401 1154. 1 Al2 1 .2-di-i-propylbenzene 0.042 0.035 0.031 0.07% 0.06% 0.05% 28.468 1156.59 -- unknown 0. 107 0. 114 0.078 0. 17% 0. 18% 0. 12% 28.503 1157.88 1 ,4-di-i-prc Al2 0. 119 0.099 0.087 0. 19% 0. 16% 0. 14% 28.605 1161 .69 A10 tetrahydronaphthalene 0. 119 0.091 0. 107 0. 19% 0. 14`)/0 0. 17% 28.719 1165.91 112 145 0. 175 0. 173 0. 122 0.28% 0.27% 0. 19% 28.756 1167.28 A10 naphthalene 0.04 0.029 0.037 0.06% 0.05% 0.06% 28.893 1172.31 Al2 1 ,4-ethyl-t-butylbenzene 0. 174 0. 145 0. 127 0.28% 0.23% 0.20% 29. 137 1181 .23 112 147 0.04 0.04 0.028 0.06% 0.06% 0.04% 29.231 1184.64 112 148 0.062 0.061 0.043 0. 10% 0. 10% 0.07% 29.337 1188.45 Al2 1 ,3-di-n-propylbenzene 0. 117 0.098 0.086 0. 19% 0. 15% 0. 14% 29.46 1192.88 O12 dodecene-1 0.065 0.064 0.046 0. 10% 0. 10% 0.07% 29.658 1200 P12 n-dodecane 1 .414 1 .394 0.985 2.24% 2.20% 1 .56% 29.721 1202.79 -- unknown 0.037 0.04 0.026 0.06% 0.06% 0.04% 29.777 1205.28 -- unknown 0.036 0.038 0.025 0.06% 0.06% 0.04% 29.923 1211 .78 Al2 1 ,3.5-triethylbenzene 0.044 0.037 0.032 0.07% 0.06% 0.05% 30.01 1215.61 -- unknown 0.298 0.316 0.218 0.47% 0.50% 0.34% 30.085 1218.92 unknown 0.052 0.055 0.038 0.08% 0.09% 0.06% 30. 193 1223.65 -- unknown 0.051 0.054 0.038 0.08% 0.09% 0.06% 30.313 1228.91 -- unknown 0.034 0.036 0.025 0.05% 0.06% 0.04% 30.352 1230.59 Al2 1 .2.4-triethylbenzene 0.047 0.039 0.034 0.07% 0.06% 0.05% 30.634 1242.83 Al2 1 .4-methyl-n-pentylbenzene 0. 128 0. 107 0.094 0.20% 0. 17% 0. 15% 30.674 1244.55 -- unknown 0.049 0.052 0.036 0.08% 0.08% 0.06% 30.887 1253.69 Al2 n-hexylbenzene 0.095 0.079 0.07 0. 15% 0. 12% 0. 11 % 30.934 1255.72 -- unknown 0.095 0. 1 0.069 0. 15% 0. 16% 0. 11 % 31 .042 1260.33 -- unknown 0. 187 0. 198 0. 137 0.30% 0.31 % 0.22% 31 . 151 1264.97 -- unknown 0. 154 0. 163 0. 112 0.24% 0.26% 0. 18% 31 .201 1267.07 -- unknown 0.035 0.037 0.025 0.06% 0.06`)/0 0.04% 31 .309 1271 .64 113 150 0. 128 0. 125 0.082 0.20% 0.20% 0. 13% 31 .406 1275.74 All 1 .2.3,4,5-pentamethylbenzene 0.216 0. 16 0. 173 0.34% 0.25% 0.27% 31 .696 1287.89 -- unknown 0.207 0.22 0. 166 0.33% 0.35% 0.26% 31 .788 1291 .68 O13 tridecene-1 0.034 0.033 0.022 0.05% 0.05% 0.03% 31 .81 1292.61 -- unknown 0.043 0.045 0.028 0.07% 0.07% 0.04% 31 .896 1296. 16 Al 1 1 -methylnaphthalene 0.036 0.027 0.03 0.06% 0.04°/0 0.05% 31 .988 1300 P13 n-tridecane 1 . 189 1 . 167 0.765 1 .88% 1 .85% 1 .21 % 32.064 1303.68 + O14+ 0. 106 0. 103 0.064 0. 17% 0. 16% 0. 10% 32.292 1314.8 + O14+ 0.039 0.038 0.024 0.06% 0.06% 0.04% 32.348 1317.52 + O14+ 0.041 0.04 0.025 0.06% 0.06% 0.04% 32.387 1319.41 + C14+ 0.085 0.083 0.051 0. 13% 0. 13% 0.08% 32.745 1336.63 + C14+ 0.06 0.058 0.036 0.09% 0.09% 0.06% 32.827 1340.54 + C14+ 0.055 0.054 0.033 0.09% 0.09% 0.05% 32.987 1348. 17 + C14+ 0. 158 0. 154 0.094 0.25% 0.24% 0. 15% 33.058 1351 .5 + C14+ 0.091 0.088 0.054 0. 14% 0. 14% 0.09% 33. 119 1354.4 + C14+ 0.063 0.061 0.038 0. 10% 0. 10% 0.06% 33.225 1359.41 + C14+ 0.099 0.096 0.059 0. 16% 0. 15% 0.09% 33.331 1364.41 + C14+ 0. 121 0. 118 0.072 0. 19% 0. 19% 0. 11 % 33.479 1371 .34 + C14+ 0. 118 0. 115 0.071 0. 19% 0. 18% 0. 11 % 33.542 1374.25 + C14+ 0.036 0.035 0.021 0.06% 0.06% 0.03% 33.655 1379.51 + C14+ 0.22 0.214 0. 132 0.35% 0.34% 0.21 % 34.098 1400 + C14+ 0.954 0.929 0.571 1 .51 % 1 .47% 0.90% 34. 166 1400 + C14+ 0.041 0.04 0.024 0.06% 0.06% 0.04% 34. 184 1400 + C14+ 0.053 0.051 0.032 0.08% 0.08% 0.05% 34.286 1400 + C14+ 0.062 0.061 0.037 0. 10% 0. 10% 0.06% 34.437 1400 + C14+ 0.099 0.097 0.059 0. 16% 0. 15% 0.09% 34.517 1400 + C14+ 0.073 0.071 0.044 0. 12% 0. 11 % 0.07% 34.844 1400 + C14+ 0.047 0.045 0.028 0.07% 0.07% 0.04% 35. 125 1400 + C14+ 0. 137 0. 133 0.082 0.22% 0.21 % 0. 13% 35.234 1400 + C14+ 0.057 0.055 0.034 0.09% 0.09% 0.05% 35.357 1400 + C14+ 0.319 0.311 0. 191 0.50% 0.49% 0.30% 35.48 1400 + C14+ 0.071 0.069 0.042 0. 11 % 0. 11 % 0.07% 35.624 1400 + C14+ 0.049 0.048 0.03 0.08% 0.08% 0.05% 35.718 1400 + C14+ 0.044 0.043 0.026 0.07% 0.07% 0.04% 36.05 1400 + C14+ 0.906 0.881 0.542 1 .43% 1 .39% 0.86% 36. 13 1400 + C14+ 0.038 0.037 0.023 0.06% 0.06% 0.04% 36.223 1400 + C14+ 0.044 0.043 0.026 0.07% 0.07% 0.04% 36.314 1400 + C14+ 0.052 0.051 0.031 0.08% 0.08% 0.05% 36.559 1400 + C14+ 0.034 0.034 0.021 0.05% 0.05% 0.03% 36.669 1400 + C14+ 0.047 0.045 0.028 0.07% 0.07% 0.04% 36.896 1400 + C14+ 0.044 0.043 0.027 0.07% 0.07% 0.04% 37.076 1400 + C14+ 0.048 0.047 0.029 0.08% 0.07% 0.05% 37. 109 1400 + C14+ 0.094 0.092 0.056 0. 15% 0. 15% 0.09% 37.203 1400 + C14+ 0.091 0.089 0.055 0. 14% 0. 14% 0.09% 37.296 1400 + C14+ 0.062 0.061 0.037 0. 10% 0. 10% 0.06% 37.344 1400 + C14+ 0.063 0.061 0.038 0. 10% 0. 10% 0.06% 37.59 1400 + C14+ 0.039 0.038 0.023 0.06% 0.06% 0.04% 37.734 1400 + C14+ 0.041 0.04 0.025 0.06% 0.06% 0.04% 37.876 1400 + C14+ 0.756 0.736 0.453 1 .20% 1 .16% 0.72% 38.657 1400 + C14+ 0.067 0.065 0.04 0. 11 % 0. 10% 0.06% 38.77 1400 + C14+ 0.209 0.204 0. 125 0.33% 0.32% 0.20% 38.88 1400 + C14+ 0.046 0.045 0.028 0.07% 0.07% 0.04% 38.975 1400 + C14+ 0.084 0.082 0.05 0. 13% 0. 13% 0.08% 39. 121 1400 + C14+ 0.051 0.049 0.03 0.08% 0.08% 0.05% 39.671 1400 + C14+ 0.645 0.628 0.386 1 .02% 0.99% 0.61 % 39.851 1400 + C14+ 0.232 0.226 0. 139 0.37% 0.36% 0.22% 63.22 63.23 63.23 100.00% 100.00% 100.00% TECHNOLOGY LABORATORY, INC. ENTRE PROFESSIONAL OFFICE PARK 1012 Centre Avenue Fort Collins, Colorado 80526 (970) 490-1414 CERTIFICATE OF ANALYSIS CGRS Sampled : 06/15/09 PO Box 1489 Received: 06/ 15/09 Fort Collins, CO 80522 Analyzed: 06/ 18/09 Sample ID: Separation Tank Project # : 1-8019- 10695aa Laboratory ID : 8528-03 Matrix: Water HAZARDOUS AIR POLLUTANTS CAS Concentration Concentration Number Compound Analyzed (mg/L) (°/0 Wt/ Wt) 71-43-2 Benzene 1070 0. 1070 108-88-3 Toluene 6246 0.6246 100-41-4 Ethylbenzene 931 0.0931 1330-20-7 Total Xylenes 10161 1.0161 1634-04-4 MTBE Non Detected 0.0000 91-20-3 Naphthalene 177 0.0177 540-84- 1 Iso-Octane Non Detected 0.0000 110-54-3 n-Hexane 11909 1. 1909 98-82-8 Isopropylbenzene 247 0.0247 QA/ QC SURROGATE RECOVERIES Compound 0/0 Recovery % Rec. Limits Dibromofluoromethane 89 68-120 1,2 Dichloroethane-d4 86 70-119 Toluene-d8 96 80-114 Page 2 of 20 TECHNOLOGY LABORATORY, INC. , // CENTRE PROFESSIONAL OFFICE PARK /,, 7>it1 1012 Centre Avenue Fort Collins, Colorado 80526 (970) 490-1414 CERTIFICATE OF ANALYSIS CGRS . INC. Sampled : 06/15/09 PO Box 1489 Received : 06/15/09 Fort Collins, CO 80522 Sample ID: Separation Tank-001 Project No. : 1-8019- 10695aa Laboratory ID : 8528-03 Matrix: Water Date Parameter Result Units % Wt/Wt Method Analyzed DRO (TEPH ) 7942 mg/L 0 .7942 EPA-8015B 06/17/09 Methanol < 10.0 mg/L 0 .0000 EPA-8015B 06/ 16/09 Modified GRO (TVPH) 438342 mg/L 43.8342 EPA-8260B 06/ 18/09 Page 4 of 20 Detailed Hydrocarbon Analysis Summary Report - Report Date: 6/18/2009 11 :38:08 AM RawFile: C:\Chem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% SUMMARY REPORT Group Type Total(Mass%) Total(Vor/o) Total(Mol%) Paraffins: 16.7489 17.7420 17.4960 I-Paraffins: 15.1992 16.0238 15.8027 Olefins: 0.6206 0.6299 0.5896 Napthenes: 10.3480 9.9832 11 .7975 Aromatics: 9.7136 8.2373 10.2396 Total C144-: 6.9938 6.8074 4.1851 Total Unknowns: 3.3556 3.5592 2.8287 Oxygenates: Total: 0.2503(Mass%) 0.2473(Vol%) Total Oxygen Content: 0.0392(Mass%) Multisubstituted Aromatics: 6.4361 (Mass%) 5.4603(Vol%) Average Molecular Weight: 118.2459 Relative Density: 0.7395 Vapor Pressure: 1 .9843 Calculated Octane Number: 62.2351 IBP T10 T50 T90 FBP Boiling Point (Deg F) 82.11 195.80 391 .50 T90 488.66 Percent Carbon: 85.8715 Percent Hydrogen: 14.0893 Bromine Number (Calc): 0.4324 Page 5 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:\Chem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% Molecular Weight and Relative Density Data Group Avq Mw. Avq Rel . Density Cl 0.000 0.000 C2 0.000 0.000 C3 44.097 0.501 C4 58. 124 0.575 C5 72. 151 0.624 C6 85.075 0.697 C7 97 .871 0.741 C8 111 .527 0.755 C9 126.460 0.753 010 140. 135 0.766 C11 154.203 0.781 C12 167. 767 0.790 C13 184.318 0.757 Total Sample: 118.00 0.74 Octane Number Research Octane Number: 62.20 (Calculated from individual Component Values) Contribution to Total by: Paraffins: 12 .90 'so-Paraffins: 18.20 Aromatics: 17.50 Napthenes: 12. 50 Olefins: 0.82 Oxygenates: 0.40 Page 6 of 20 Created with novaPDF Printer (www.novaPDF.com). 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Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:\Chem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% Totals by Group Type & Carbon Number (in Mass Percent) Paraffins I-Paraffins Olefins Napthenes Aromatics Total 01 0.00000 0.00000 0.00000 0.00000 0.00000 0.00000 C2 0.00000 0.00000 0.00000 0.00000 0.00000 0.00000 C3 0.03541 0.00000 0.00000 0.00000 0.00000 0.03541 C4 0.34550 0.06608 0.00000 0.00000 0.00000 0.41158 C5 1 .07932 0.65402 0.00000 0.00000 0.00000 1 .73334 C6 1 .98812 1 .87623 0.00000 1 .80740 0.33487 6.00662 C7 2.58211 2.36062 0.16795 3.97004 2.06811 11 .14883 C8 2.58079 2.91737 0.00000 2.24663 2.85199 10.59679 C9 2.10419 2.21533 0.25022 1 .56046 1 .10238 7.23258 010 1 .80340 3.72118 0.04782 0.28619 1 .76131 7.61991 011 1 .62794 0.98366 0.05522 0.39113 0.82801 3.88597 C12 1 .41356 0.27707 0.06493 0.08611 0.76687 2.60855 C13 1 .18855 0.12768 0.03447 0.00000 0.00000 1 .35069 Total: 16.74889 15.19925 0.62061 10.34797 9.71355 52.63026 Oxygenates 0.25034 Total 014+: 6.99378 Total Unknowns: 3.35562 Grand Total. 63.23000 Totals by Group Type & Carbon Number (in Volume Percent) Paraffins 1-Paraffins Olefins Napthenes Aromatics Total C 1 0.00000 0.00000 0.00000 0.00000 0.00000 0.00000 C2 0.00000 0.00000 0.00000 0.00000 0.00000 0.00000 C3 0.05253 0.00000 0.00000 0.00000 0.00000 0.05253 C4 0.44320 0.08805 0.00000 0.00000 0.00000 0.53125 C5 1 .27972 0.78372 0.00000 0.00000 0.00000 2.06343 C6 2.23857 2.11695 0.00000 1 .75609 0.28289 6.39451 C7 2.80406 2.56525 0.17211 3.85725 1 .77106 11 . 16972 C8 2.72763 3.07417 0.00000 2. 16750 2.45148 10.42077 C9 2.17711 2.26289 0.25817 1 .49502 0.93868 7.13187 010 1 .83420 3.75228 0.04798 0.26438 1 .48350 7.38235 011 1 .62459 0.98188 0.05464 0.36300 0.66984 3.69395 C12 1 .39379 0.27320 0.06357 0.07992 0.63984 2.45031 C13 1 .16666 0.12539 0.03342 0.00000 0.00000 1 .32547 Total: 17.74205 16.02378 0.62989 9.98316 8.23728 52.61617 Oxygenates 0.24726 Total C14+: 6.80737 Total Unknowns: 3.55920 Grand Total. 63.23000 Page 7 of 20 Created with novaPDF Printer (www.novaPDF.com). 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Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:\Chem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% Totals by Group Type & Carbon Number (in Mol Percent) Paraffins I-Paraffins Olefins Napthenes Aromatics Total 01 0.00000 0.00000 0.00000 0.00000 0.00000 0.00000 C2 0.00000 0.00000 0.00000 0.00000 0.00000 0.00000 C3 0.09532 0.00000 0.00000 0.00000 0.00000 0.09532 C4 0.70567 0.13497 0.00000 0.00000 0.00000 0.84064 C5 1 .77589 1 .07612 0.00000 0.00000 0.00000 2.85200 C6 2.73877 2.58463 0.00000 2.54946 0.50893 8.38179 C7 3.05910 2.79670 0.20306 4.80000 2.66453 13.52339 C8 2.68210 3.03189 0.00000 2.37677 3.18907 11 .27982 C9 1 .94762 2.05050 0.23531 1 .46742 1 .08882 6.78967 010 1 .50466 3.10476 0.04047 0.24221 1 .56313 6.45524 011 1 .23638 0.74774 0.04249 0.30095 0.66414 2.99169 C12 0.98516 0. 19315 0.04580 0.06074 0.56103 1 .84587 C13 0.76531 0.08221 0.02244 0.00000 0.00000 0.86996 Total: 17.49599 15.80265 0.58956 11 .79754 10.23964 55.92538 Oxygenates 0.29085 Total 014+: 4.18505 Total Unknowns: 2.82871 Grand Total 63.23000 Page 8 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:lChem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% NOTE: Components with a Weight % of Less Than 0.01 Not Reported. Components Listed in Chromatographic Order Page: 5 Minutes Index Group Component Mass % Volume % Mol % 1 .954 300.000 P3 propane 0.035 0.053 0.095 2.072 361 .400 14 i-butane 0.066 0.088 0. 135 2. 173 402.940 P4 n-butane 0.346 0.443 0.706 2.543 470.400 I5 i-pentane 0.654 0.784 1 .076 2.744 497.740 P5 n-pentane 1 .079 1 .280 1 .776 3.540 564.380 16 2,3-dimethylbutane 0.270 0.303 0.372 3.609 568.900 16 2-methylpentane 0.977 1 . 110 1 .345 3.848 583.320 16 3-methylpentane 0.629 0.703 0.867 4. 157 600.000 P6 n-hexane 1 .988 2.239 2.739 4.645 622.730 17 2.2-dimethylpentane 0.064 0.071 0.076 4.729 626.290 N6 methylcyclopentane 0.849 0.842 1 . 198 4.787 628.720 17 2,4-dimethylpentane 0. 152 0. 167 0. 180 5.364 650.540 A6 benzene 0.335 0.283 0.509 5.453 653.600 O7 2-methyl-c-hexene-3 0.036 0.039 0.044 5.599 658.500 N6 cyclohexane 0.958 0.914 1 .352 5.841 666.260 17 2-methylhexane 0.937 1 .025 1 . 110 5.893 667.890 17 2,3-dimethylpentane 0.254 0.272 0.301 5.993 670.920 X6 t-amylmethylether 0.250 0.247 0.291 6. 130 674.990 17 3-methylhexane 0.953 1 .030 1 . 129 6.348 681 .210 N7 1 c.3-dimethylcyclopentane 0.261 0.260 0.316 6.449 684.000 N7 1 t,3-dimethylcyclopentane 0.307 0.305 0.372 6.551 686.760 N7 1t,2-dimethylcyclopentane 0.381 0.377 0.461 7.069 700.000 P7 n-heptane 2.582 2.804 3.059 7.971 722.710 N7 methylcyclohexane 2.789 2.691 3.372 8.002 723.440 -- unknown 0.041 0.043 0.049 8.048 724.490 18 2,2-dimethylhexane 0. 162 0. 173 0. 169 8.487 734.340 N7 ethylcyclopentane 0.231 0.224 0.279 8.590 736.560 18 2,4-dimethylhexane 0.200 0.213 0.208 8.881 742.650 __ unknown 0. 170 0. 180 0. 177 8.935 743.750 N8 1 c,2t,4-trimethylcyclopentane 0.046 0.045 0.049 9.254 750. 110 O7 O37 0. 132 0. 134 0. 159 9.754 759.580 A7 toluene 2.068 1 .771 2.665 9.973 763.560 18 2,3-dimethylhexane 0. 129 0. 134 0. 134 10.017 764.340 18 2-methyl-3-ethylpentane 0.075 0.078 0.078 10.338 769.960 18 2-methylheptane 1 .089 1 . 158 1 . 132 10.403 771 .050 18 4-methylheptane 0.325 0.343 0.338 10.476 772.300 18 3,4-dimethylhexane 0.056 0.058 0.059 10.762 777.050 N8 1 c,2c,4-trimethylcyclopentane 0.796 0.776 0.843 Page 9 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:lChem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% NOTE: Components with a Weight % of Less Than 0.01 Not Reported. Components Listed in Chromatographic Order Page: 6 Minutes Index Group Component Mass % Volume % Mol % 10.813 777.880 18 3-methylheptane 0.050 0.052 0.052 10.842 778.360 18 3-ethylhexane 0.830 0.864 0.863 10.928 779.750 N8 1t,4-dimethylcyclohexane 0.359 0.349 0.379 11 . 197 784.020 N8 1 , 1 -dimethylcyclohexane 0. 142 0. 135 0. 151 11 .385 786.930 19 2,2,5-trimethylhexane 0.035 0.036 0.032 11 .576 789.830 N8 3t-ethylmethylcyclopentane 0.052 0.050 0.055 11 .859 794.030 Ng 1t,2-dimethylcyclohexane 0.325 0.311 0.343 12.274 800.000 P8 n-octane 2.581 2.728 2.682 13.339 819.050 19 2,3.4-trimethylhexane 0.086 0.086 0.079 13.617 823.750 O9 O52 0.250 0.258 0.235 14.025 830.450 __ unknown 0.798 0.846 0.750 14.060 831 .020 19 2,2,3-trimethylhexane 0. 177 0. 184 0. 164 14.350 835.630 N8 N4 0.236 0.225 0.250 14.505 838.050 19 3,3-&3,5-dimethylheptane 0.337 0.345 0.312 14.604 839.590 19 2,6-dimethylheptane 0.069 0.073 0.064 15.360 850.940 N8 N7 0.291 0.277 0.308 15.439 852.090 A8 ethylbenzene 0. 155 0. 133 0. 173 16. 147 862.110 A8 1 ,3-dimethylbenzene 2. 181 1 .874 2.439 16.212 863.010 A8 1 ,4-dimethylbenzene 0.516 0.445 0.577 16.276 863.880 19 2,3-dimethylheptane 0.036 0.037 0.034 16.425 865.920 19 3,4-dimethylheptane 0. 101 0. 103 0.094 16.714 869.790 19 3,4 -dimethylheptane 0.387 0.393 0.358 16.809 871 .060 19 15 0.468 0.476 0.433 17. 171 875.790 -- unknown 0. 111 0. 118 0. 103 17.295 877.390 19 3-ethylheptane 0.518 0.530 0.480 17.623 881 .540 N9 1c,2t.4c-trimethylcyclohexane 0.037 0.036 0.035 17.738 882.980 N9 1 c,2t.3c-trimethylcyclohexane 0.580 0.568 0.545 17.976 885.930 N9 N18 0.040 0.038 0.037 18.093 887.360 N9 N19 0.344 0.328 0.324 18.222 888.930 N9 N20 0.211 0.201 0. 199 18.812 895.950 N9 N22 0.044 0.042 0.041 19. 162 900.000 pg n-nonane 2. 104 2. 177 1 .948 19.231 901 .690 N9 1 , 1 -methylethylcyclohexane 0. 180 0. 166 0. 170 19.408 906.010 N9 N25 0.070 0.066 0.066 19.705 913. 170 A9 i-propylbenzene 0.050 0.043 0.049 19.806 915.580 110 I11 0. 134 0. 136 0. 111 19.911 918.060 __ unknown 0.065 0.069 0.054 19.986 919.830 110 112 0.036 0.037 0.030 Page 10 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:lChem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% NOTE: Components with a Weight % of Less Than 0.01 Not Reported. Components Listed in Chromatographic Order Page: 7 Minutes Index Group Component Mass % Volume % Mol % 20. 114 922.840 110 2,4-dimethyloctane 0. 194 0. 198 0. 162 20.208 925.020 110 2,2-dimethyloctane 0.039 0.039 0.032 20.489 931 .510 110 2,5-dimethyloctane 0.524 0.533 0.437 20.680 935.870 __ unknown 0. 100 0. 106 0.083 20.733 937.070 N9 n-butylcyclopentane 0.054 0.051 0.050 20.927 941 .440 110 3,3-dimethyloctane 0.333 0.335 0.278 21 . 193 947.340 110 3,6-dimethyloctane 0. 117 0. 118 0.098 21 .250 948.600 __ unknown 0.083 0.088 0.070 21 .571 955.610 A9 1 ,4-methylethylbenzene 0.384 0.331 0.379 21 .649 957.310 -- unknown 0. 145 0. 154 0. 144 21 .747 959.410 N10 N33 0.049 0.045 0.041 21 .819 960.950 __ unknown 0.035 0.037 0.029 21 .854 961 .700 A9 1 ,3.5-trimethylbenzene 0. 148 0. 127 0. 146 21 .926 963.240 110 115 0.460 0.462 0.384 22.031 965.480 110 116 0.037 0.037 0.031 22.092 966.770 110 5-methylnonane 0. 127 0. 129 0. 106 22. 178 968.590 110 4-methylnonane 0.316 0.317 0.264 22.291 970.940 A9 1 ,2-methylethylbenzene 0.384 0.323 0.379 22.409 973.410 110 3-ethyloctane 0.051 0.051 0.043 22.509 975.480 N10 N35 0.049 0.046 0.042 22.559 976.520 110 3-methylnonane 0.275 0.278 0.229 22.634 978.070 N10 N36 0.037 0.034 0.031 22.848 982.450 A9 1 ,2,4-trimethylbenzene 0.034 0.029 0.034 22.974 985.010 110 120 0.893 0.896 0.745 23.060 986.750 110 121 0. 185 0. 186 0. 154 23.393 993.420 O10 2,3-dimethyloctene-2 0.048 0.048 0.040 23.461 994.760 N10 1t-methyl-2-n-propylcyclohexane0.075 0.069 0.063 23.726 1000.000 P10 n-decane 1 .803 1 .834 1 .505 23.994 1008.730 A9 1 ,2.3-trimethylbenzene 0. 102 0.085 0. 101 24.053 1010.630 A10 1 ,3-methyl-i-propylbenzene 0.079 0.068 0.070 24. 162 1014. 140 111 127 0.043 0.043 0.032 24.213 1015.800 111 128 0.039 0.040 0.030 24.242 1016.720 __ unknown 0.046 0.049 0.035 24.434 1022.860 N10 sec-butylcyclohexane 0.077 0.070 0.065 24.487 1024.540 111 130 0.095 0.095 0.072 24.548 1026.470 A10 1 ,2-methyl-i-propylbenzene 0.307 0.260 0.271 24.710 1031 .590 __ unknown 0.067 0.071 0.060 24.748 1032.790 N11 N40 0.252 0.234 0. 194 Page 11 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:\Chem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% NOTE: Components with a Weight % of Less Than 0.01 Not Reported. Components Listed in Chromatographic Order Page: 8 Minutes Index Group Component Mass % Volume % Mol % 24.877 1036.830 111 132 0.067 0.062 0.052 24.932 1038.530 __ unknown 0.079 0.084 0.061 24.997 1040.550 A10 1 ,3-diethylbenzene 0.049 0.042 0.044 25.087 1043.340 A10 1 ,3-methyl-n-propylbenzene 0.271 0.234 0.240 25.213 1047.230 A10 1 ,4-diethylbenzene 0.079 0.068 0.070 25.247 1048.290 A10 1 ,3-dimethyl-5-ethylbenzene 0.032 0.027 0.028 25.316 1050.380 A10 n-butylbenzene 0. 138 0. 119 0. 122 25.395 1052.810 111 134 0.038 0.039 0.029 25.485 1055.550 N11 N41 0. 140 0. 129 0. 107 25.592 1058.820 111 135 0.034 0.035 0.026 25.669 1061 . 140 111 136 0. 169 0. 170 0. 129 25.769 1064. 130 111 138 0. 161 0. 161 0. 122 25.885 1067.610 A10 1 ,4,dimethyl-2-ethylbenzene 0.241 0.204 0.213 25.926 1068.850 A10 A3 0.042 0.036 0.037 25.981 1070.500 111 139 0.074 0.074 0.056 26.082 1073.510 111 140 0. 171 0. 171 0. 130 26. 173 1076. 180 A10 1 ,2-dimethyl-4-ethylbenzene 0.081 0.069 0.072 26.483 1085.290 111 143 0.092 0.093 0.070 26.603 1088.790 __ unknown 0.062 0.066 0.047 26.663 1090.530 O11 undecene-1 0.055 0.055 0.042 26.720 1092.200 A10 1 ,2-dimethyl-3-ethylbenzene 0.058 0.048 0.051 26.788 1094. 170 A11 1 ,4-methyl-t-butylbenzene 0.070 0.061 0.056 26.863 1096.310 A11 1 ,2-ethyl-i-propylbenzene 0.069 0.058 0.055 26.991 1100.000 P11 n-undecane 1 .628 1 .625 1 .236 27.097 1104. 160 A10 1 ,2.4, 5-tetramethylbenzene 0.039 0.033 0.035 27. 155 1106.440 All 1 ,2-methyl-n-butylbenzene 0.053 0.044 0.043 27.258 1110.470 A10 1 ,2.3,5-tetramethylbenzene 0.037 0.031 0.033 27.287 1111 .600 __ unknown 0.060 0.063 0.053 27.458 1118.220 __ unknown 0.068 0.072 0.060 27.491 1119.510 All 1 ,2-methyl-t-butylbenzene 0.065 0.054 0.052 27.647 1125.510 __ unknown 0.040 0.043 0.032 27.763 1129.970 A10 5-methylindan 0. 149 0. 125 0. 134 27.948 1137.040 All 1 ,2-ethyl-n-propylbenzene 0.237 0. 197 0. 190 28.039 1140.460 All 1 ,3-methyl-n-butylbenzene 0.032 0.026 0.025 28. 155 1144.840 All s-pentylbenzene 0.050 0.042 0.040 28.348 1152. 110 N12 lt-M-2-(4-MP)cyclopentane 0.086 0.080 0.061 28.401 1154. 100 Al2 1 ,2-di-i-propylbenzene 0.042 0.035 0.031 28.468 1156.590 __ unknown 0. 107 0. 114 0.078 Page 12 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:lChem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% NOTE: Components with a Weight % of Less Than 0.01 Not Reported. Components Listed in Chromatographic Order Page: 9 Minutes Index Group Component Mass % Volume % Mol % 28.503 1157.880 A12 1 ,4-di-i-propylbenzene 0. 119 0.099 0.087 28.605 1161 .690 A10 tetrahydronaphthalene 0. 119 0.091 0. 107 28.719 1165.910 112 145 0. 175 0. 173 0. 122 28.756 1167.280 A10 naphthalene 0.040 0.029 0.037 28.893 1172.310 Al2 1 ,4-ethyl-t-butylbenzene 0. 174 0. 145 0. 127 29. 137 1181 .230 112 147 0.040 0.040 0.028 29.231 1184.640 112 148 0.062 0.061 0.043 29.337 1188.450 Al2 1 ,3-di-n-propylbenzene 0. 117 0.098 0.086 29.460 1192.880 O12 dodecene-1 0.065 0.064 0.046 29.658 1200.000 P12 n-dodecane 1 .414 1 .394 0.985 29.721 1202.790 __ unknown 0.037 0.040 0.026 29.777 1205.280 __ unknown 0.036 0.038 0.025 29.923 1211 .780 Al2 1 ,3.5-triethylbenzene 0.044 0.037 0.032 30.010 1215.610 -- unknown 0.298 0.316 0.218 30.085 1218.920 -- unknown 0.052 0.055 0.038 30. 193 1223.650 __ unknown 0.051 0.054 0.038 30.313 1228.910 __ unknown 0.034 0.036 0.025 30.352 1230.590 Al2 1 ,2,4-triethylbenzene 0.047 0.039 0.034 30.634 1242.830 A12 1 ,4-methyl-n-pentylbenzene 0. 128 0. 107 0.094 30.674 1244.550 __ unknown 0.049 0.052 0.036 30.887 1253.690 A12 n-hexylbenzene 0.095 0.079 0.070 30.934 1255.720 __ unknown 0.095 0. 100 0.069 31 .042 1260.330 -- unknown 0. 187 0. 198 0. 137 31 . 151 1264.970 __ unknown 0. 154 0. 163 0. 112 31 .201 1267.070 __ unknown 0.035 0.037 0.025 31 .309 1271 .640 113 150 0. 128 0. 125 0.082 31 .406 1275.740 A11 1 ,2.3,4,5-pentamethylbenzene 0.216 0. 160 0. 173 31 .696 1287.890 -- unknown 0.207 0.220 0. 166 31 .788 1291 .680 O13 tridecene-1 0.034 0.033 0.022 31 .810 1292.610 __ unknown 0.043 0.045 0.028 31 .896 1296. 160 All 1 -methylnaphthalene 0.036 0.027 0.030 31 .988 1300.000 P13 n-tridecane 1 . 189 1 . 167 0.765 32.064 1303.680 + C14+ 0. 106 0. 103 0.064 32.292 1314.800 + C14+ 0.039 0.038 0.024 32.348 1317.520 + C14+ 0.041 0.040 0.025 32.387 1319.410 + C14+ 0.085 0.083 0.051 32.745 1336.630 + C14+ 0.060 0.058 0.036 32.827 1340.540 + C14+ 0.055 0.054 0.033 Page 13 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:\Chem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% NOTE: Components with a Weight % of Less Than 0.01 Not Reported. Components Listed in Chromatographic Order Page: 10 Minutes Index Group Component Mass % Volume % Mol % 32.987 1348. 170 + C14+ 0. 158 0. 154 0.094 33.058 1351 .500 + C14+ 0.091 0.088 0.054 33. 119 1354.400 + C14+ 0.063 0.061 0.038 33.225 1359.410 + C14+ 0.099 0.096 0.059 33.331 1364.410 + O14+ 0. 121 0. 118 0.072 33.479 1371 .340 + C14+ 0. 118 0. 115 0.071 33.542 1374.250 + C14+ 0.036 0.035 0.021 33.655 1379.510 + C14+ 0.220 0.214 0. 132 34.098 1400.000 + C14+ 0.954 0.929 0.571 34. 166 1400.000 + C14+ 0.041 0.040 0.024 34. 184 1400.000 + C14+ 0.053 0.051 0.032 34.286 1400.000 + C14+ 0.062 0.061 0.037 34.437 1400.000 + C14+ 0.099 0.097 0.059 34.517 1400.000 + C14+ 0.073 0.071 0.044 34.844 1400.000 + O14+ 0.047 0.045 0.028 35. 125 1400.000 + C14+ 0. 137 0. 133 0.082 35.234 1400.000 + C14+ 0.057 0.055 0.034 35.357 1400.000 + C14+ 0.319 0.311 0. 191 35.480 1400.000 + C14+ 0.071 0.069 0.042 35.624 1400.000 + C14+ 0.049 0.048 0.030 35.718 1400.000 + C14+ 0.044 0.043 0.026 36.050 1400.000 + C14+ 0.906 0.881 0.542 36. 130 1400.000 + C14+ 0.038 0.037 0.023 36.223 1400.000 + C14+ 0.044 0.043 0.026 36.314 1400.000 + C14+ 0.052 0.051 0.031 36.559 1400.000 + C14+ 0.034 0.034 0.021 36.669 1400.000 + O14+ 0.047 0.045 0.028 36.896 1400.000 + C14+ 0.044 0.043 0.027 37.076 1400.000 + C14+ 0.048 0.047 0.029 37. 109 1400.000 + C14+ 0.094 0.092 0.056 37.203 1400.000 + C14+ 0.091 0.089 0.055 37.296 1400.000 + C14+ 0.062 0.061 0.037 37.344 1400.000 + C14+ 0.063 0.061 0.038 37.590 1400.000 + C14+ 0.039 0.038 0.023 37.734 1400.000 + C14+ 0.041 0.040 0.025 37.876 1400.000 + C14+ 0.756 0.736 0.453 38.657 1400.000 + C14+ 0.067 0.065 0.040 38.770 1400.000 + C14+ 0.209 0.204 0. 125 Page 14 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Detailed Hydrocarbon Analysis Detail Report - Report Date: 6/18/2009 11 :38:35 AM RawFile: C:lChem32111DATA\TLIIDHA-061709-8528-02.DIDHA-061709-8528-02.CDF Acquired: 06/17/09 11 :15:44 Sample: Condensate-001 Analyzed: 6/18/2009 11 :31 :41 AM Processed 233 Peaks Reference File: C:1Chem32111DHARef1PONA-VI.DHA Comments: Normalized to 63.2300% NOTE: Components with a Weight % of Less Than 0.01 Not Reported. Components Listed in Chromatographic Order Page: 11 Minutes Index Group Component Mass % Volume % Mol 38.880 1400.000 + C14+ 0.046 0.045 0.028 38.975 1400.000 + C14+ 0.084 0.082 0.050 39. 121 1400.000 + C14+ 0.051 0.049 0.030 39.671 1400.000 + C14+ 0.645 0.628 0.386 39.851 1400.000 + C14+ 0.232 0.226 0. 139 Page 15 of 20 Created with novaPDF Printer (www.novaPDF.com). Please register to remove this message. Signal 0 0 g o g o g $ gP o g a g o o < ti, a CD O 6 O O O � • a T 6 n � Les � co f 6 o D o -a O r• ny538 : propane g < u ;3fle o —42 . 1732 : n -butane de N cp =2 .5430 : i-pentane =2 .7436 n -pentane: 6 x Ca V O to caD 3 .6094 : 2 -methylpentane b pentane o n4 . 1565 : n -hexane jUla=l t4 7288 : methylcyclopentane d . 2 .y -u .methylpentane aa5 .3g41 : benzene_ F5 4526 : 2 -methyl-c-nexene -3 X5 .5985 cyclohexane r_1 8931 2�imetfii,@ § ta inethylhexane � 9 28 • t-am methylether L =6 . 1299 . 3-methylhexane 3479 . 1c 3 -dim thylcvflo entane er- a^ Qi8g6 : it 1 -dime h tc C1 pentane 6 .5505 : 1t.2 - it eihylcycropentane 7 .0692 : n -heptane �"'s' g4f'&k� simethylhexane 7 ,9107 : methylcyclohexane 4g13 : ethylc clo entane r $ 5904 : 2 .4 -dimethylhexane F2536§ 1edtgAethylcyclopentape: O37 ay69 .7539 : toluene �� 0 35733 . 2.3 -dimctjj9ic +ai' C Page 16 of 20 e� �a pp�� ppop e� p p� po p� Qo WpSignal Q� p� pp�ap p� �v n O O O O S O O O O S O O O O O O O O O O O g O § O O O S O O 3 n CDr . . . . . . . . r . . . . . . r . . , r . . . r . . . i Li v' 3 a . (fl N X9 .7539 : toluene cn b Ewoe ` �•r�'0t t 0@l� tane a 8 /��j 0 39M341lifillaentplhePtane CO J Y CD N ' l -� ' �d �, t ch,ylcyclopentone O 6 rH 9 7 8im�e hyicycioehexane o > 3 1 . 191 - . 1 .1 -dimethylcyclohexane 6 _: .3852 : 2 ,2 ,5 -trimethylhexane g 11 .5762 : 3t-ethylmethylcyclopentane a' v O 11 .8591 11,2 -dimelhylcyclohexane nJ '---... . b ~^ —^an12 .2743 : n -octane b ,..- 6 `1, g ) <D 6O N CO _ ni . .3386 : 2 ..3 .4-trimethylhexane b J' n ' 3 .6172 : O52 C -n . bad:- ? ,' INRIVRPtrRexane 1 .1 .3501 : N4 n ' 4 .5Q48 : 3 .33 5 -dimelhylheptane -g ' 4 .6041 e .6 -1 .6 N U, U, 11 .94 :•eth7ylbenzene U, 0 a • 8 .2757 : '2d'��tthty, �` OpOigiimtpyldenzene 6 .4251 : 3 ,4 -dim ethylheptane Cr ? 16 7091 .4tm ethylheptane 47 171 r: unknown —_ ' 7 .2954 : 3 -ethylheptane CJI 1 c,2t.4c-trimethylcyclohexane n17 .7376 . 1 c,2t,3c-trimethylcyclohexane - 7. 761 : N18 18 .0931 N19 18 .2223 . N20 V, 18 .8123 : N22 19 .2307 : 1 ,1 -m ethyle�jityicidne'ange nave 9 .4078 : N25 ' 47c88h i�ep�lrkopylbenzene o *9%iJb . • ItT "`nt o n Page 17 of 20 Signal o 8 8 $ 8 s 8 8 S 8 s rg o g ig g `g o g g O g g g ` g E § o . . l . . . 1 . . . 1 . i. 1 . u S . . 1 . . t . , '-1 lal c„ a tyg882jw1py'benzene Za 61o. l4 4-di a hyloctane .. : 0 0 } 9 : ,2?dime y�octane m 6 r ry cp X20 .4888 : 2 ,5 -dimethyloctane 3 N g.5 § 94 n feflilopentane o 5 N 20 .9214 : 3 .3 -dimethyloctane o n O fr:. 1.2b0%%8. U4.0n$Virpthyloctane 6 "1 ��6�h1 5.uOt oaw�methylethylbenzene o Nerifirethylbenzene a, 3. ' ti hn NJ Z '1 e�4ymet a/inonane b 22 .2905 : 1 ,2 -m ethylethylbenzene o N 1089 Ainhyloctane 6 "' ' 2 634" ,' ier : 3 -methylnonane = g 4 7 : 1 ,2 ,4-trimethylbenzene `a qc"a23 .0599 • 12 t =22 9739 H20 ril b 23334 �6 :21.t-iggli l'ACIt$Sjr?cyclohexane ^' C" 6 cp 23 .7265 : n -decane NJi. 1 : 11 52-A difl3F it0ti.1&9t Vile n e t& (tCiknown $ is . 1 .�4 c•butylcyyclohexane �' 278 : 1 .7•methyl-i•pre pylbenzene en � ' 48 itiltig,q - Ib�n �ene 08 et y -n -propylbenzene f 1 t4 PMItbenzene rc); - 4849 : N41 UN hil ; 138 F.) V 6 . 1 ,4 .dimethyl-2 -ethylbenzene g I1o .4826 .2-dimethyl-4 -ethylbenzene ' 143 % ... 1 N. -r-p �Or lyrlen ~' 26.9911 : n -undecane 1,49{4 j 112 -rrt8e9 tb q�,ee9M91% � j.. :. %, ,$etf�'%rameth +I benzene v �. 71�t :.uln,t4Rliti‘ yl-t-butylbenzene 466 : unknown 27 .7630 : 5 -methylindan co , 8 .03 714 4 : 1 2 -eth I- ro lbenzene -methyyl-n -outyi% erizyene X8 . 1546 . s-pentylbenzene ' ugf } b� - plane N, 7' . 0i opYIbbenze ne .607 3 : tetrahy ronaphthalene 4 . r44)0h:tl ene 8 .8933 : 1 ,4 -ethyl-t-butylbenzene 371 I 114478 .3361 : 1 ,3 -di-n -propylbenzene 8 :_ 0 4599 : dodecene - 1 :f0a . iiiikil8WRCP 9 .6585 : n -dodecane 0?3_5 1 3 5 -trie_thyIhJ+ n_7Qnc - Page 18 of 20 Signal w co •0 O o S 8 O P3 8 "(Si _g 8 r8 8 O 0 t S `a' 0 8 8 8 O 0 0 o o Q 9cn 9 .6585 : n -dodecane g : >r3a : tiRkA8* fl 0 085 Du0n . I�ienhlcnow'n er, e o b ,��, 0 . 1931 : un nown m c; .lMl % 4 .aQP119thylbenzene a CD 63RkA ,rHethyl-n -pentylbenzene 95. C : {�i t � 6 nzene > O - 1 .0420 : unknown d1019 rlkll own 1 06 : 1 .2 .3 ,4 ,5 -pentamethylbenzene a 65• unknown o JU.�e� l w 2 .0638 : C14 + x1 .9885 : n -tridecane b N 3 97:26: 4 + 9, • 0 ': C1 ++4 + N 23 � 13 �C14 + b N ei9e 1 +14+ 0 3 .6545 : C14 + (� .0983 : C14 + "4 .2861; : C14 + 31T.1? .' ' 4 .8444 : C14 + .1253 : C14 + .2 39 : C14 + 3'5 .35 u, ! 69 : I4 + 7176 •: � id + 0.a a' + .0499 : C14 + 111 al � + .5586 : C14 + 6 .6687 : C14 + " .8956 : C14 + 71� 9x114+ ji$ Cr' n3 .5904 : C14 + n3 344 : C14 + "37 .8761 : C14 + C,, n3 66 ' C14 + 6.72696 : C14 + 889754 : 1C4 4 + n .1207 : C14 + C.) u, '39 .6707 : C14 + 508 . C 14 * - - Page 19 of 20 Technology Laboratory Inc. Centre Professional Office Park 1012 Centre Avenue Fort Collins, CO 80526 970-490-1414 info(Wtechlabusa.com Compositional Analysis of Liquid (Atmospheric Pressure) CGRS Date Sampled: 06/15/09 PO Box 1489 Date Received: 06/15/09 Fort Collins. CO Date Analyzed: 06/16/09 Sample ID: Condensate-001 1 -8019-10695aa Lab ID: 8528-02 Molecular Specific Component Mole °/U Volume `)/0 Weight % Weight Gravity C 1 0.00 0.00 0.00 16.04 0.300 C 2 0.00 0.00 0.00 30.07 0.356 C 3 0.00 0.00 0.00 44. 10 0.507 C 4 0.00 0.00 0.00 58. 12 0.563 C 4 0.00 0.00 0.00 58.12 0.584 C 5 0.00 0.00 0.00 72. 15 0.624 C 5 1 .66 0.99 0.79 72. 15 0.631 C 6 10.02 6.77 5.70 86.18 0.664 C 7 18.62 13.68 12.31 95.88 0.709 C 8 15.00 12.04 11 .30 107.35 0.740 C 9 14.92 12.67 12.62 116.95 0.785 C 10 6.81 6.46 6.39 134.00 0.779 C 11 5.33 5.48 5.49 147.00 0.790 C 12 4.23 4.68 4.75 161 .00 0.801 C 13 3. 17 3.74 3.86 175.00 0.812 C 14 3.19 4.00 4. 17 190.00 0.823 C 15 2.19 2.90 3.06 206.00 0.833 C 16 1 .95 2.73 2.91 222.00 0.840 C 17 1 .47 2. 16 2.32 237.00 0.848 C 18 1 .07 1 .66 1 .80 251 .00 0.853 C 19 1 .31 2. 13 2.32 263.00 0.858 C 20 0.99 1 .69 1 .85 275.00 0.863 C 21 1 .24 2.21 2.43 291 .00 0.868 C 22 0.90 1 .67 1 .85 305.00 0.873 C 23 0.86 1 .66 1 .85 318.00 0.878 C 24 0.71 1 .42 1 .58 331 .00 0.882 C 25 0.68 1 .41 1 .58 345.00 0.886 C 26 0.66 1 .40 1 .58 359.00 0.890 C 27 0.63 1 .40 1 .58 374.00 0.894 C 28 0.34 0.79 0.90 388.00 0.897 C 29 0.33 0.79 0.90 402.00 0.900 C 30 plus 1 .71 3.50 4.08 478.00 0.917 Total 100.00 100.00 100.00 147.16 0.794 Average Specific Gravity Page 20 of 20 3ZA1VNV 1A00 `OIOH 43. r SISAIVNV a31dV OIOH Y tY O I —j CC ❑ H. i a �� 00 c a 04 z Ts cr w Alstirv`A Et/ X _ 00 >. Q se0d ■■■ ■■ . ■ ■■ _ Z el-13 ` .O3 `z0 QN) S3SVD (mad O v p ■■■ ■■ ■ ■■ } LI . . I f..."" w OOO / 008 m � ' m I- ■■ ■ ■ ■ - zwz W VINOWWV /311d1IN / 31W:111N a w.■. a D D cCu n w Uo w oU HdAl/ SL-OIIVL-OZ/ l-Ol . . Uw ! I as�1d ,u;e d / ..uo0 / *auu61 / weals __ ■ (03A1OSSIG /e,3l /1%9101) S7dl3ih 8 Vasa ■ ■ ■ . C" O } SSl / Hd z U Q — ■ ■ ■ __ ■■■■ 9 _-__ Z HVd / 0LZB / SZ93OAS dial. lbtol O9Z8 / tiZ9 OOA ■ ■■ ■ ■■ O Cii di iii di Q Q Q tr99 t / l'£ 117 aseai0 I' PO a f= o ,= I V8lti Hdal l U OR' O to (080) Hd31 tiq Ild-VH eac .Cse Sa3NIV1N00 JO 1:1381111Nti ■■■ ■ ■■ (O) tnHl0 (1 ) snoanov• (v) uiv (s) -IoS :Xtti1V1't< 3ldMVS a ■■ ■■ -._. C D W )--{ E2 -- 0 N 3 • :3 W `�d N z _ °;) 1$.- LO ' ` Qi Q w JO � N OU o CD m W Cg. It J Us 0 O E—� ...� O z Lu I til I ,+ W `� d 0 w 5 Z. "' r r h� U t� • 2 o a 00 a (�� E'" a � ! �` — 0 w o w 0 G � � n �, w ► U U Q U as 76 iLD 42) = iti 3 ~ z (I) - 2 2 ii, cc oc 0 3 • C C EE n-a ^ r . Is Ca 8 E �v w a --^� O t- _ .� 3 Z `o 0 w n a u o �x z z `'' u Q O I Q it cr 'n 0 `!l N , Z 2 Cr U t cc ¢ iti O- w F- E (if ? ? 2 O a ti 2CL 00 C'3 0 m o a a ate. CO Q " — N a ,•, n ❑ ❑ / TECHNOLOGY LABORATORY, INC. CENTRE PROFESSIONAL OFFICE PARK 1012 Centre Avenue Fort Collins, Colorado 80526 (970) 490-1414 CGRS Sampled : 06/ 15/09 PO Box 1489 Received: 06/ 15/09 Fort Collins, CO 80522 Analyzed: 06/24/09 Sample ID: Condensate-001 Project # : 1-8019- 10695aa Laboratory ID : 8528-02 Matrix: Oil This oil sample was received in good condition and was sent to Questar Energy Services on June 23, 2009 for Reid Vapor Pressure Analysis. The results contained in this report relate only to those items tested . TECHNOLOGY LABORAT RY, INC. Page 1 of 2 1210 D Street Rock Springs, Wy. 82901 Ph: 307-352-7292 Fax: 307-352-7326 Questar Energy Services Applied TechnologyServices API Gravity Reid Vapor Pressure Producer: Tech Lab Inc. Well Name: Project # 8528-2 Field: N/A County and State: N/A Corrected API Gravity: 47.0 @ 60*F RVP: 3.2 # @100 *F Date Sampled: 6/15/09 DafAnalyled: 6/24/09 Sampled By: N/A Analyzed By: Putnam Page 2 of 2 NGL Water Solutions DJ, LLC C10 Salt Water Disposal Facility Slop Oil Tank and Sale Oil Tank Emission Composition from E&P Tanks Molecular Weight VOC Weight Liquid Constituent Weight Mole % (Ib/Ibmole Corrected % ;Ib/Ib-mol) Liquid) Weight * Methane 16.04 0.00% 0.00 0.00% NA Ethane 30.07 0.00% 0.00 0.00% NA Total HC (Non- VOC) 0.00% 0.00 0.00% NA Propane 44. 10 0.00% 0.00 0.00% 0.00% Iso-Butane 58. 12 0.00% 0.00 0.00% 0.00% N-Butane 58. 12 0.00% 0.00 0.00% 0.00% Iso-Pentane 72. 15 13.21 % 9.53 10.70% 10.70%. N-Pentane 72. 15 10.40% 7.50 8.42% 8.42% i-Hexanes 86. 16 22.52% 19.40 21 .78% 21 .78% n-Hexane 86. 18 15.73% 13.56 15.22% 15.22% Heptanes 100.20 23.51 % 23.56 26.46% 26.46% Octanes 114.23 5.27% 6.02 6.76% 6.76% Nonanes 128.28 2.75% 3.53 3.96% 3.96% Decanes+ 194.40 0.02% 0.03 0.04% 0.04% Benzene 78. 11 2. 19% 1 .71 1 .92% 1 .92% Toluene 92. 13 3.27% 3.01 3.38% 3.38% Ethylbenzene 106. 17 0.07% 0.07 0.08% 0.08% Xylenes 106. 17 1 .07% 1 . 13 1 .27% 1 .27% 2-2-4 TM P 114.24 0.00% 0.00 0.00% 0.00% Total NMNE VOC 100.00% 89.06 100.00% 100.00% Hydrogen Sulfide 34.80 0.00% 0.00 0.00% NA Carbon Dioxide 44.01 0.00% 0.00 0.00% NA Nitrogen 28.01 0.00% 0.00 0.00% NA Totals 100.00% 89.06 100.00% 100.00% Weight Percent corrected to remove Non-VOC Hydrocarbons. Carbon Dioxide,Nitrogen, and H2S content. Appendix E Process Description, Process Flow, Facility Location, and Plot Plan Process description The Facility accepts production water from oil and gas exploration and production sites in Colorado and separates residual condensate and oil from the production water through a closed system of manifolded aboveground storage tanks. The refined production water is injected into one of two on-site class II injection wells for disposal. The oil recovered at the facility is transported offsite for further refinement. A simplified process flow diagram is attached. l A7 t ! 1 ,- ot. 7--O _ R ul 1 r 1O fil 11 i ; Ch o ce . a a ; o a 634 - 3 1 _ 2 a l O Q O - -"--- --- - - -I I 0 . J I I L.L. I n w Q ms - n U 0 t CD 1131. Ct aili a. ! I - § S i I I I w ~ I 8 a 1 _ 3A a � I x � � ` i £ `' < can ' i I cQ o a 6)I 1 ) Q 9M J - J IPA o Pell 9 r O I Z a L I Id D - M 6 . O i- - i— H-r , r 3 _ IS ! u1 eq I Oi 0 a B U tinfint I c. i a o Ci g a ino • d god ;a i R :6.:o .i.ti 2% A F 322 6 - Y2 t o O I Z Z w II ; i _ k NUco "iii ›- i! a Q Q o a V ° Iii 1 a i I , # 1 b a 1 W j z c i a i C4 Q 3 o W ₹ g iZ I— I O p 0 0 . -J ' Q{ .; Z u I Q • t le p a 2 1 1.4 2 =Ara 1VOTKL9A911 VA'91 Sill 115,O5M;WW, Jragaa tWIV* pem,. `M1, Hello