HomeMy WebLinkAbout20160870.tiff INVENTORY OF ITEMS FOR CONSIDERATION
Applicant Miller HFI, Inc. Case Number USR15-0073
Submitted or Prepared
Prior to At
Hearing Hearing
PC Exhibits
1 Letter from Lisa and Brad Olson dated 11/12/2015 X
2 E-mail from Lisa and Brad Olson dated 11 /16/2015 X
3 E-mail and attachments from Lisa Olson dated 1/28/2016 X
4 Letter and Report from Olsson Associates dated 11/30/15 X
I hereby certify that the 4 items identified herein was submitted to the Department of Planning Services at or prior to the scheduled
Planning Commissioners hearing.
Chris Gathman — Planner
11/12/2015
To whom it may concern,
We are extremely opposed to the Miller NFl LLC project. First thing this area is zoned Agricultural. We
have already had issues here from Miller. The rain came and washed Frac material onto our neighbor's
property. We do not want the traffic or noise either.
If this was in town next to someone's house this would never come up. We have lived out here before all
the oil activity began. The county does not keep up the roads even with increased traffic. These bad roads
are extremely hard on our vehicles. These tanks would also encourage rattlesnakes.
Again we are saying no to this Miller Project case # USR15-0073. Ask yourself would you want this
right next to your home and your children? Would you let us put up a trailer park out here? If this project
is approved we will have no choice but to file a lawsuit against Miller HFl LI.C and Weld County. This
would devalue our property tremendously. We have worked for many years to have a place like this. We
will not sit back and let a company finically devastate us. All for their personal financial gain with no
regard to us or our family.
We have a young child in our home. This is unsafe for everyone involved. Again we do not want the
ground water and air polluted. We live clear out here because it used to be peaceful. The oil companies
have stolen that peace from us.
Sincerely,
Lisa and Brad Olson
EXHIBIT
I Usg/S - WM
1
From: olsonbrgq@aol.com [mailto:olsonbrgy@aol.com]
Sent: Monday, November 16, 2015 5:44 PM
To: Tim Naylor
Subject: Case # USR 15-0073
To Mr Naylor,
I see your are the authorized agent for this project. We are going to fight this. I
understand this is your job . We live here. Would you want a chemical factory next to
your home?
We are extremely opposed to the Miller HFI LLC project. First thing this area is zoned
Agricultural. We have already had issues here from Miller. The rain came and washed
Frac material onto our neighbor's property. We do not want the traffic or noise either.
If this was in town next to someone's house this would never come up. We have lived
out here before all the oil activity began . The county does not keep up the roads even
with increased traffic. These bad roads are extremely hard on our vehicles. These
tanks would also encourage rattlesnakes.
Again we are saying no to this Miller Project case # USR15-0073. Ask yourself would
you want this right next to your home and your children? If this project is approved we
will have no choice but to file a lawsuit against Miller HFI LLC . This would devalue our
property tremendously. We will not sit back and let a company finically devastate
us. All for their personal financial gain with no regard to us or our family.
We have a young child in our home. This is unsafe for everyone involved . Again we do
not want the ground water and air polluted . We live clear out here because it used to be
peaceful. The oil companies have stolen that peace from us.
Sincerely,
Lisa and Brad Olson
EXHIBIT
tic C.iS ,Ub'73
From: olsonbrgg@aol.com [mailto:olsonbrgg@aoLcom]
Sent: Thursday, January 28, 2016 7:33 PM
To: Ben Frissell <bfrissell-durley@co.weld.co.us>; Chris Gathman <cgathman@co.weld.co.us>
Subject: USR15-0073
Hello,
Please see attached. . Chris I had mailed our complaint to you by certified mail here is a copy. I have
included the report from the mud farm results. Please note the high levals of diesal fuel, aresnic and
Napthalene. I have also included the MSDS for Napthalene that shows can cause organ failure. We are
real people with real children. Our six your old Grandson lives here we want to do everything we can to
protect him and the rest of our family. Our lives and our home should matter. You would never put these
toxins next to someone in town. I had asked since April for this report and just recieved it this
Monday. What about our well water? This could one day hit the aquafir.
Beside all the health concerns what about our property values. . The noise and traffic will be bad. We
have moved here for peace the oil companies have stolen that from us . The road are already bad. What
will happen on County rd 83? No one will be able to come out here without 4 wheel drive. You are saying
that they could deliver all times day and night. Again would you want this next to you?
If Miller can not follow the rules for the mud farm , why would he now follow them. Here is a picture of two
tanks they just moved in . with out a permit. You can not guarantee the tanks will be empty.
We can not put up a second home here but for some reason you are wanting to zone our Ag community
into Industrial. If we wanted to live next to an industrial park we would live in town. Again this would not
happen to anyone living in town. With all the tanks it would encourage more rattlesnakes.
Whats next a trailer park out here for the oil workers? When we moved here it was peaceful) and a great
place to raise our family . We paid the price to live in an area zoned Ag . Not Industrial . Please consider
our familys health, the value or our home and our right to live in a peaceful place. That is what we
bought.
Thanks,
Lisa Olson
EXHIBIT
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1S
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSOI Lab ID: 1511253- 1
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 : 16 Percent Moisture: 14.5
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SOW
Diesel Range Organics 170 DMH 5.7 MG/KG 1 11/19/2015 10:25
Surr: O-TERPHENYL 91 49-114 %REC 1 11/19/2015 10:25
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 16:00
Sum 2,3,4-TRIFLUOROTOLUENE 90 76-126 %REC 1 11/16/2015 16:00
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 40 16 UG/KG 4 11/17/2015 14:01
Surr: NITROBENZENE-O5 73 28-113 %REC 4 11/17/2015 14:01
Surr: 2-FLUOROBIPHENYL 67 41-106 %REC 4 11/17/2015 14:01
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 15:43
TOLUENE ND 5.8 UG/KG 1 11/17/2015 15:43
ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 15:43
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 15:43
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 15:43
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 15:43
Sum DIBROMOFLUOROMETNANE 107 61-134 %REC 1 11/17/2015 15:43
Surr: TOLUENE-D8 98 57-135 %REC 1 11/17/2015 15:43
Sum 4-BROMOFLUOROBENZENE 93 52-151 %REC 1 11/17/2015 15:43
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 1 of 4710 of 63
ALS Environmental — FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Sprcadfield Work Order: 1511253
Sample ID: Miller 1 SS02 Lab ID: 1511253-2
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :51 Percent Moisture: 10.8
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics ND 5.5 MG/KG 1 11/19/2015 10:56
Surr: O-TERPHENYL 88 49-114 %REC 1 11/19/2015 10:56
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 16:22
Sum 2,3,4-TRIFLUOROTOLUENE 95 76-126 %REC 1 11/16/2015 16:22
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.7 UG/KG 1 11/17/2015 11 :02
Sum NITROBENZENE-D5 57 28-113 %REC 1 11/17/2015 11 :02
Sum 2-FLUOROBIPHENYL 56 41-106 %REC 1 11/17/2015 11 :02
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 16:10
TOLUENE ND 5.6 UG/KG 1 11/17/2015 16:10
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 16:10
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 16:10
O-XYLENE ND 5.6 UG/KG 1 11/17/2015 16:10
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 16:10
Sum DIBROMOFLUOROMETHANE 102 61-134 %REC 1 11/17/2015 16:10
Sum TOLUENE-D8 98 57-135 %REC 1 11/17/2015 16:10
Sum 4-BROMOFLUOROBENZENE 97 52-151 %REC 1 11/17/2015 16:10
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 2 of 4711 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec- 15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS03 Lab ID: 1511253-3
Legal Location: Matrix: SOIL
Collection Date: 11 /12/2015 11 :05 Percent Moisture: 9.2
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics ND 5.2 MG/KG 1 11/19/2015 11 :27
Surr: O-TERPHENYL 86 49-114 %REC 1 11/19/2015 11 :27
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.47 MG/KG 1 11/16/2015 16:44
Sur : 2,3,4-TRIFLUOROTOLUENE 101 76-126 %REC 1 11/16/2015 16:44
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.6 UG/KG 1 11/17/2015 09:44
Surr: NITROBENZENE-D5 59 28-113 %REC 1 11/17/2015 09:44
Sum 2-FLUOROBIPHENYL 58 41-106 %REC 1 11/17/2015 09:44
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.5 UG/KG 1 11/17/2015 16:32
TOLUENE ND 5.5 UG/KG 1 11/17/2015 16:32
ETHYLBENZENE ND 5.5 UG/KG 1 11/17/2015 16:32
M+P-XYLENE ND 5.5 UG/KG 1 11/17/2015 16:32
O-XYLENE ND 5.5 UG/KG 1 11/17/2015 16:32
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 16:32
Sum DIBROMOFLUOROMETHANE 104 61-134 %REC 1 11/17/2015 16:32
Surr: TOLUENE-D8 97 57-135 %REC 1 11/17/2015 16:32
Sum 4-BROMOFLUOROBENZENE 96 52-151 %REC 1 11/17/2015 16:32
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 3 of 4712 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller l SSO4 Lab ID: 1511253-4
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :05 Percent Moisture: 19.9
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 340 DMH 6.1 MG/KG 1 11/19/2015 11 :58
Surr: O-TERPHENYL 99 49-114 %REC 1 11/19/2015 11 :58
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.52 MG/KG 1 11/16/2015 17:07
Sum 2,3,4-TRIFLUOROTOLUENE 86 76-126 %REC 1 11/16/2015 17:07
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 150 16 UG/KG 4 11/17/2015 14:28
Surr: NITROBENZENE-D5 59 28-113 %REC 4 11/17/2015 14:28
Surr: 2-FLUOROBIPHENYL 64 41-106 %REC 4 11/17/2015 14:28
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 Prepay: JXK
BENZENE ND 6.2 UG/KG 1 11/17/2015 16:54
TOLUENE ND 6.2 UG/KG 1 11/17/2015 16:54
ETHYLBENZENE ND 6.2 UG/KG 1 11/17/2015 16:54
M+P-XYLENE ND 6.2 UG/KG 1 11/17/2015 16:54
O-XYLENE ND 6.2 UG/KG 1 11/17/2015 16:54
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 16:54
Surr: DIBROMOFLUOROMETHANE 103 61-134 %REC 1 11/17/2015 16:54
Surr: TOLUENE-O8 110 57-135 %REC 1 11/17/2015 16:54
Sum 4-BROMOFLUOROBENZENE 80 52-151 %REC 1 11/17/2015 16:54
Sodium Adsorption Ratio USDA60 Prep Date: 11 /18/2015 PrepBy: TLB
PASTE PH 7.9 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 4 of 4713 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS05 Lab ID: 1511253-5
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :45 Percent Moisture: 12.4
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics ND 5.6 MG/KG 1 11/19/2015 12:29
Surr.• O-TERPHENYL 83 49-114 %REC 1 11/19/2015 12:29
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.51 MG/KG 1 11/16/2015 17:29
Surr.• 2,3,4-TRIFLUOROTOLUENE 97 76-126 %REC 1 11/16/2015 17:29
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.8 UG/KG 1 11/17/2015 11 :28
Sum NITROBENZENE-D5 56 28-113 %REC 1 11/17/2015 11 :28
Surr: 2-FLUOROBIPHENYL 54 41-106 %REC 1 11/17/2015 11 :28
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.7 UG/KG 1 11/17/2015 17:15
TOLUENE ND 5.7 UG/KG 1 11/17/2015 17:15
ETHYLBENZENE ND 5.7 UG/KG 1 11/17/2015 17:15
M+P-XYLENE ND 5.7 UG/KG 1 11/17/2015 17:15
O-XYLENE ND 5.7 UG/KG 1 11/17/2015 17:15
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 17:15
Sum DIBROMOFLUOROMETHANE 102 61-134 %REC 1 11/17/2015 17:15
Surr: TOLUENE-D8 97 57-135 %REC 1 11/17/2015 17:15
Sum 4-BROMOFLUOROBENZENE 94 52-151 %REC 1 11/17/2015 17:15
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8.3 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 5 of 4714 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1 5
Project: Noble Miller Sprcadfield Work Order: 151 1253
Sample ID: Miller 1 SSO6 Lab ID: 1511253-6
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :33 Percent Moisture: 7.4
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics ND 5.3 MG/KG 1 11/19/2015 13:29
Sum O-TERPHENYL 87 49-114 %REC 1 11/19/2015 13:29
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.49 MG/KG 1 11/16/2015 17:51
Surr: 2,3,4-TRIFLUOROTOLUENE 99 76-126 %REC 1 11/16/2015 17:51
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.6 UG/KG 1 11/17/2015 12:44
Sum NITROBENZENE-O5 52 28-113 %REC 1 11/17/2015 12:44
Sum 2-FLUOROBIPHENYL 52 41-106 %REC 1 11/17/2015 12:44
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.4 UG/KG 1 11/17/2015 17:36
TOLUENE ND 5.4 UG/KG 1 11/17/2015 17:36
ETHYLBENZENE ND 5.4 UG/KG 1 11/17/2015 17:36
M+P-XYLENE ND 5.4 UG/KG 1 11/17/2015 17:36
O-XYLENE ND 5.4 UG/KG 1 11/17/2015 17:36
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 17:36
Sum DIBROMOFLUOROMETHANE 101 61-134 %REC 1 11/17/2015 17:36
Sum TOLUENE-D8 98 57-135 %REC 1 11/17/2015 17:36
Sum 4-BROMOFLUOROBENZENE 97 52-151 %REC 1 11/17/2015 17:36
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 6.8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 6 of 4715 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS07 Lab ID: 1511253-7
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :39 Percent Moisture: 16.6
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 65 DMH 5.6 MG/KG 1 11/19/2015 14:00
Surr: O-TERPHENYL 83 49-114 %REC 1 11/19/2015 14:00
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.53 MG/KG 1 11/16/2015 18:36
Surr: 2,3,4-TRIFLUOROTOLUENE 90 76-126 %REC 1 11/16/2015 18:36
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 22 16 UG/KG 4 11/17/2015 14:48
Surr: NITROBENZENE-D5 58 28-113 %REC 4 11/17/2015 14:48
Sum 2-FLUOROBIPHENYL 61 41-106 %REC 4 11/17/2015 14:48
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 17:58
TOLUENE ND 5.8 UG/KG 1 11/17/2015 17:58
ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 17:58
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 17:58
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 17:58
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 17:58
Sum DIBROMOFLUOROMETHANE 107 61-134 %REC 1 11/17/2015 17:58
Sum TOLUENE-D8 109 57-135 %REC 1 11/17/2015 17:58
Surr: 4-BROMOFLUOROBENZENE 81 52-151 %REC 1 11/17/2015 17:58
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 7 of 4716 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spread-field Work Order: 1511253
Sample ID: Miller 1 SSO8 Lab ID: 1511253-8
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :24 Percent Moisture: 13.9
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 210 DMH 5.7 MG/KG 1 11/19/2015 14:31
Surr.• O-TERPHENYL 100 49-114 %REC 1 11/19/2015 14:31
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.52 MG/KG 1 11/16/2015 18:58
Sun':: 2,3,4-TRIFLUOROTOLUENE 87 76-126 %REC 1 11/16/2015 18:58
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 41 15 UG/KG 4 11/17/2015 15:23
Sum NITROBENZENE-D5 48 28-113 %REC 4 11/17/2015 15:23
Sum 2-FLUOROBIPHENYL 58 41-106 %REC 4 11/17/2015 15:23
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 18:19
TOLUENE ND 5.8 UG/KG 1 11/17/2015 18:19
ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 18:19
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 18:19
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 18:19
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 18:19
Sum DIBROMOFLUOROMETHANE 106 61-134 %REC 1 11/17/2015 18:19
Sum TOLUENE-O8 113 57-135 %REC 1 11/17/2015 18:19
Sumo-BROMOFLUOROBENZENE 79 52-151 %REC 1 11/17/2015 18:19
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.5 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 8 of 4717 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample TD: Miller 1 SS09 Lab ID: 1511253-9
legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :39 Percent Moisture: 10.3
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 21 DMH 5.5 MG/KG 1 11/19/2015 15:02
Surr O-TERPHENYL 84 49-114 %REC 1 11/19/2015 15:02
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.47 MG/KG 1 11/16/2015 19:20
Surr: 2,3,4-TRIFLUOROTOLUENE 95 76-126 %REC 1 11/16/2015 19:20
GC/MS Semi-volatiles SW8270SIM Prep Date: 11 /13/2015 PrepBy: ACK
NAPHTHALENE 9.7 3.7 UG/KG 1 11/17/2015 15:24
Sum NITROBENZENE-D5 61 28-113 %REC 1 11/17/2015 15:24
Sum 2-FL UOROBIPHENYL 62 41-106 %REC 1 11/17/2015 15:24
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 18:40
TOLUENE ND 5.6 UG/KG 1 11/17/2015 18:40
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 18:40
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 18:40
O-XYLENE ND 5.6 UG/KG 1 11/17/2015 18:40
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 18:40
Sum D/BROMOFLUOROMETHANE 103 61-134 %REC 1 11/17/2015 18:40
Surr: TOLUENE-D8 97 57-135 %REC 1 11/17/2015 18:40
Surr: 4-BROMOFLUOROBENZENE 96 52-151 %REC 1 11/17/2015 18:40
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 Prepay: TLB
PASTE PH 8.1 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 9 of 4718 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS l 0 Lab ID: 1511253- 10
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 : 10 Percent Moisture: 11 .0
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/1812015 PrepBy: SDW
Diesel Range Organics 170 DMH 5.6 MG/KG 1 11/19/2015 16:04
Sum O-TERPHENYL 88 49-114 %REC 1 11/19/2015 16:04
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.48 MG/KG 1 11/16/2015 19:42
Sum 2,3,4-TRIFLUOROTOLUENE 94 76-126 %REC 1 11/16/2015 19:42
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 26 15 UG/KG 4 11/17/2015 15:41
Sum NITROBENZENE-D5 63 28-113 %REC 4 11/17/2015 15:41
Sum 2-FLUOROBIPHENYL 63 41-106 %REC 4 11/17/2015 15:41
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 19:02
TOLUENE ND 5.6 UG/KG 1 11/17/2015 19:02
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 19:02
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:02
O-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:02
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 19:02
Sum DIBROMOFLUOROMETHANE 101 61-134 %REC 1 11/17/2015 19:02
Sum TOLUENE-D8 102 57-135 %REC 1 11/17/2015 19:02
Sum 4-BROMOFLUOROBENZENE 88 52-151 %REC 1 11/17/2015 19:02
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.7 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 10 of 4719 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS11 Lab ID: 1511253-11
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:45 Percent Moisture: 14.2
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 220 DMH 5.3 MG/KG 1 11/19/2015 16:35
Surr: O-TERPHENYL 97 49-114 %REC 1 11/19/2015 16:35
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 20:04
Sum 2,3,4-TRIFLUOROTOLUENE 81 76-126 %REC 1 11/16/2015 20:04
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 48 15 UG/KG 4 11/17/2015 15:59
Sum NITROBENZENE-O5 84 28-113 %REC 4 11/17/2015 15:59
Sum 2-FLUOROBIPHENYL 69 41-106 %REC 4 11/17/2015 15:59
GC/MS Volatiles SW8260 Prep Date: 11117/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 19:24
TOLUENE ND 5.8 UG/KG 1 11/17/2015 19:24
- ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 19:24
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 19:24
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 19:24
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 19:24
Sum DIBROMOFLUOROMETHANE 108 61-134 %REC 1 11/17/201519:24
Sum TOLUENE-D8 108 57-135 %REC 1 11/17/2015 19:24
Sum 4-BROMOFLUOROBENZENE 80 52-151 %REC 1 11/17/2015 19:24
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.9 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 11 of 4720 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec- 15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS12 Lab ID: 1511253- 12
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:40 Percent. Moisture: 11 .5
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 110 DMH 5.4 MG/KG 1 11/19/2015 17:07
Sum O-TERPHENYL 85 49-114 %REC 1 11/19/2015 17:07
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.38 MG/KG 1 11/16/2015 20:26
Surr: 2,3,4-TRIFLUOROTOLUENE 86 76-126 %REC 1 11/16/2015 20:26
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 42 15 UG/KG 4 11/17/2015 16:17
Surr: NITROBENZENE-D5 74 28-113 %REC 4 11/17/2015 16:17
Sum 2-FLUOROBIPHENYL 68 41-106 %REC 4 11/17/2015 16:17
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 19:50
TOLUENE ND 5.6 UG/KG 1 11/17/2015 19:50
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 19:50
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:50
O-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:50
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 19:50
Sum DIBROMOFLUOROMETHANE 102 61-134 %REC 1 11/17/2015 19:50
Sum TOLUENE-O8 112 57-135 %REC 1 11/17/2015 19:50
Sum 4-BROMOFLUOROBENZENE 80 52-151 %REC 1 11/17/2015 19:50
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
AIMS Version: 6.795 AR Page 12 of 4'121 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec- 15
Project: Noble Miller Spreadficld Work Order: 1511253
Sample ID: Miller 1 SS13 Lab ID: 1511253- 13
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:35 Percent Moisture: 10.2
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 6.3 DMH 5.5 MG/KG 1 11/19/2015 17:38
Surr: O-TERPHENYL 91 49-114 %REC 1 11/19/2015 17:38
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.47 MG/KG 1 11/16/2015 20:48
Surr: 2,3,4-TRIFLUOROTOLUENE 96 76-126 %REC 1 11/16/2015 20:48
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.7 UG/KG 1 11/17/2015 15:44
Sum NITROBENZENE-O5 47 28-113 %REC 1 11/17/2015 15:44
Surr: 2-FLUOROBIPHENYL 48 41-106 %REC 1 11/17/2015 15:44
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.5 UG/KG 1 11/17/2015 20:12
TOLUENE ND 5.5 UG/KG 1 11/17/2015 20:12
ETHYLBENZENE ND 5.5 UG/KG 1 11/17/2015 20:12
M+P-XYLENE ND 5.5 UG/KG 1 11/17/2015 20:12
O-XYLENE ND 5.5 UG/KG 1 11/17/2015 20:12
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 20:12
Surr: DIBROMOFLUOROMETHANE 105 61-134 %REC 1 11/17/2015 20:12
Surr: TOLUENE-D8 98 57-135 %REC 1 11/17/2015 20:12
Surr: 4-BROMOFLUOROBENZENE 92 52-151 %REC 1 11/17/2015 20:12
Sodium Adsorption Ratio USDA60 Prep Date: 11 /18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 13 of 4722 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS14 Lab ID: 1511253- 14
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:28 Percent Moisture: 14. 1
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 190 LDMHZ 5.6 MG/KG 1 11/19/2015 18:09
Sum O-TERPHENYL 89 49-114 %REC 1 11/19/2015 18:09
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.49 MG/KG 1 11/16/2015 21 :10
Surr: Z3,4-TRIFLUOROTOLUENE 89 76-126 %REC 1 11/16/2015 21 :10
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 45 15 UG/KG 4 11/17/2015 16:11
Surr: NITROBENZENE-D5 62 28-113 %REC 4 11/17/2015 16:11
Sum 2-FLUOROBIPHENYL 66 41-106 %REC 4 11/17/2015 16:11
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.7 UG/KG 1 11/17/2015 20:37
TOLUENE ND 5.7 UG/KG 1 11/17/2015 20:37
ETHYLBENZENE ND 5.7 UG/KG 1 11/17/2015 20:37
M+P-XYLENE ND 5.7 UG/KG 1 11/17/2015 20:37
O-XYLENE ND 5.7 UG/KG 1 11/17/2015 20:37
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 20:37
Sum DIBROMOFL UOROMETHANE 100 61-134 %REC 1 11/17/2015 20:37
Surr: TOLUENE-D8 104 57-135 %REC 1 11/17/2015 20:37
Surr: 4-BROMOFLUOROBENZENE 84 52-151 %REC 1 11/17/2015 20:37
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.9 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6 795 AR Page 14 of 4723 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Sprcadfield Work Order: 1511253
Sample ID: Miller 1 SS 15 Lab ID: 1511253-15
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:20 Percent Moisture: 8.5
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 130 DMH 5.4 MG/KG 1 11/19/2015 18:40
Surr. O-TERPHENYL 91 49-114 %REC 1 11/19/2015 18:40
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 21 :32
Sum 2314-TRIFLUOROTOLUENE 100 76-126 %REC 1 11/16/2015 21 :32
GC/MS Semi-volatiles SW8270SIM Prep Date: 11113/2015 PrepBy: ACK
NAPHTHALENE 52 14 UG/KG 4 11/17/2015 16:38
Sum NITROBENZENE-D5 58 28-113 %REC 4 11/17/2015 16:38
Sum 2-FLUOROBIPHENYL 68 41-106 %REC 4 11/17/2015 16:38
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.5 UG/KG 1 11/17/2015 21 :02
TOLUENE ND 5.5 UG/KG 1 11/17/2015 21 :02
ETHYLBENZENE ND 5.5 UG/KG 1 11/17/2015 21 :02
M+P-XYLENE ND 5.5 UG/KG 1 11/17/2015 21 :02
O-XYLENE ND 5.5 UG/KG 1 11/17/2015 21 :02
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 21 :02
Sum DIBROMOFLUOROMETHANE 105 61-134 %REC 1 11/17/2015 21 :02
Sum TOLUENE-D8 102 57-135 %REC 1 11/17/2015 21 :02
Sum 4-BROMOFLUOROBENZENE 88 52-151 %REC 1 11/17/2015 21 :02
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.6 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 15 of 4-24 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spread-field Work Order: 1511253
Sample ID: Miller 1 Composite Lab ID: 1511253-16
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 12:05 Percent Moisture: 12.0
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 25 3.7 UG/KG 1 11/17/2015 12:16
ACENAPHTHENE 4.5 3.7 UG/KG 1 11/17/2015 12:16
FLUORENE 9.1 3.7 UG/KG 1 11/17/2015 12:16
ANTHRACENE ND 3.7 UG/KG 1 11/17/2015 12:16
FLUORANTHENE ND 3.7 UG/KG 1 11/17/2015 12:16
PYRENE 15 3.7 UG/KG 1 11/17/2015 12:16
BENZO(A)ANTHRACENE ND 3.7 UG/KG 1 11/17/2015 12:16
CHRYSENE 41 3.7 UG/KG 1 11/17/2015 12:16
BENZO(B)FLUORANTHENE 9.7 3.7 UG/KG 1 11/17/2015 12:16
BENZO(K)FLUORANTHENE ND 3.7 UG/KG 1 11/17/2015 12:16
BENZO(A)PYRENE ND 3.7 UG/KG 1 11/17/2015 12:16
INDENO(1 ,2,3-CD)PYRENE ND 3.7 UG/KG 1 11/17/2015 12:16
DIBENZO(A,H)ANTHRACENE ND 3.7 UG/KG 1 11/17/2015 12:16
Surr: NITROBENZENE-D5 56 28-113 %REC 1 11/17/2015 12:16
Sum 2-FLUOROBIPHENYL 56 41-106 %REC 1 11/17/2015 12:16
Burr: TERPHENYL-D14 60 25-147 %REC 1 11/17/2015 12:16
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 16 of 4'15 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO1 Lab ID: 1511253-17
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11: 16 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.3 0.19 MG/KG 10 11/20/2015 12:59
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 17 of 4'16 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1 S
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS02 Lab ID: 1511253-18
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :51 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.7 0.19 MG/KG 10 11/20/2015 13:20
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 18 of 417 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS03 Lab ID: 1511253-19
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :05 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 2.8 0.19 MG/KG 10 11/2012015 13:24
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 19 of 418 of 63
ALS Environmental — FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO4 Lab ID: 1511253-20
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :05 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 7.1 0.19 MG/KG 10 11/20/2015 13:40
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 20 of 419 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS05 Lab ID: 1511253-21
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 3.7 0.19 MG/KG 10 11/20/2015 13:44
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 21 of 4730 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1S
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS06 Lab ID: 1511253-22
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :33 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 2 0.19 MG/KG 10 11/20/2015 13:47
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 22 of 4731 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS07 Lab ID: 1511253-23
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 6.6 0.19 MG/KG 10 11/20/2015 13:51
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 23 of 4$2 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO8 Lab ID: 1511253-24
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :24 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 6.6 0.19 MG/KG 10 11/20/2015 13:54
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 24 of 4733 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO9 Lab ID: 1511253-25
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.8 0.19 MG/KG 10 11/20/2015 13:58
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 25 of 4$4 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: OLsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample lD: Miller 1 SS10 Lab ID: 1511253-26
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 : 10 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.9 0.19 MG/KG 10 11/20/2015 14:01
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 26 of 4735 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS1 l Lab ID: 1511253-27
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 7.8 0.19 MG/KG 10 11/20/2015 14:05
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 27 of 4736 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS12 Lab ID: 1511253-28
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:40 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.4 0.2 MG/KG 10 11/20/2015 14:08
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 28 of 4'x37 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS13 Lab ID: 1511253-29
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:35 Percent Moisture:
Report Dilution
Analyses Result Qua! Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 2.5 0.19 MG/KG 10 11/20/2015 14:12
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 29 of 4738 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-IS
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS14 Lab ID: 1511253-30
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:28 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 6 0.19 MG/KG 10 11/20/2015 14:28
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 30 of 4'x39 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1S
Project: Noble Miller Sprcadficld Work Order: 1511253
Sample ID: Miller 1 SS15 Lab ID: 1511253-31
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:20 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 5 0.19 MG/KG 10 11/20/2015 14:31
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 31 of 4740 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS01 Lab ID: 1511253-32
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 : 16 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 350 10 MG/L 10 11/18/2015 12:00
MAGNESIUM 71 10 MG/L 10 11/18/2015 12:00
SODIUM 670 10 MG/L 10 11/18/2015 12:00
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 5800 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 8.6 0.54 NU 10 11/18/2015 12:00
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 32 of 4711 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS02 Lab ID: 1511253-33
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :51 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
1CP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 53 10 MGIL 10 11/181201512:01
MAGNESIUM ND 10 MGIL 10 11/18/2015 12:01
SODIUM ND 10 MG/L 10 11/18/2015 12:01
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 340 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.33 S 0.54 NU 10 11/18/2015 12:01
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 33 of 47i2 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS03 Lab ID: 1511253-34
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :05 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 37 10 MG/L 10 11/18/2015 12:02
MAGNESIUM 13 10 MG/L 10 11/18/2015 12:02
SODIUM 27 10 MGR_ 10 11/18/2015 12:02
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 460 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.97 0.54 NU 10 11/18/2015 12:02
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 34 of 4713 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO4 Lab ID: 1511253-35
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :05 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 450 10 MG/L 10 11/18/2015 12:03
MAGNESIUM 60 10 MG/L 10 11/18/2015 12:03
SODIUM 420 10 MG/L 10 11/18/2015 12:03
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 5000 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 4.9 0.54 NU 10 11/18/2015 12:03
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 35 of 4714 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO5 Lab ID: 1511253-36
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 69 10 MG/L 10 11/18/201512:04
MAGNESIUM 10 10 MG/L 10 11/18/2015 12:04
SODIUM ND 10 MG/L 10 11/18/2015 12:04
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 400 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.3 s 0.54 NU 10 11/18/2015 12:04
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ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS06 Lab ID: 1511253-37
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :33 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 35 10 MG/L 10 11/18/2015 12:05
MAGNESIUM 12 10 MG/L 10 11/18/2015 12:05
SODIUM ND 10 MG/L 10 11/1812015 12:05
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 310 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.37 S 0.54 NU 10 11/18/2015 12:05
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ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1 S
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS07 Lab ID: 1511253-38
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 85 10 MG/L 10 11/18/2015 12:06
MAGNESIUM 19 10 MG/L 10 11/18/2015 12:06
SODIUM 97 10 MG/L 10 11/18/2015 12:06
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 1200 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 2.5 0.54 NU 10 11/18/2015 12:06
ALS Environmental -- FC
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ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spread-field Work Order: 1511253
Sample ID: Miller 1 SSO8 Lab ID: 1511253-39
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :24 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 510 10 MGIL 10 11/18/2015 12:08
MAGNESIUM 80 10 MG/L 10 11/18/2015 12:08
SODIUM 890 10 MG/L 10 11/18/2015 12:08
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 7700 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 9.6 0.54 NU 10 11/18/2015 12:08
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 39 of 4748 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS09 Lab ID: 1511253-40
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 93 10 MG/L 10 11/18/2015 12:09
MAGNESIUM 13 10 MG/L 10 11/18/2015 12:09
SODIUM 57 10 MG/L 10 11/18/2015 12:09
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 1200 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 1.5 0.54 NU 10 11/18/2015 12:09
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 40 of 4749 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller I SS10 Lab ID: 1511253-41
Legal Location: Matrix: SATIXTRACT
Collection Date: 11/12/2015 11 : 10 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 370 10 MG/L 10 11/18/2015 12:10
MAGNESIUM 46 10 MGIL 10 11/18/2015 12:10
SODIUM 450 10 MG/L 10 11/18/2015 12:10
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 4600 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 5.9 0.54 NU 10 11/18/2015 12:10
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 41 of 4'$0 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS 11 Lab ID: 1511253-42
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 500 10 MG/L 10 11/18/2015 12:14
MAGNESIUM 68 10 MG/L 10 11/18/2015 12:14
SODIUM 530 10 MG/L 10 11/18/2015 12:14
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY@ 5600 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 5.9 0.54 NU 10 11/18/2015 12:14
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 42 of 4'51 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS12 Lab ID: 1511253-43
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:40 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 260 10 MGIL 10 11/18/2015 12:15
MAGNESIUM 33 10 MG/L 10 11/18/2015 12:15
SODIUM 190 10 MG/L 10 11/18/2015 12:15
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 2800 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 2.9 0.54 NU 10 11/18/2015 12:15
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 43 of 4'$2 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample lD: Miller 1 SS 13 Lab ID: 1511253-44
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:35 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/1312015 PrepBy: SMW
CALCIUM 44 10 MG/L 10 11/18/2015 12:16
MAGNESIUM 12 10 MG/L 10 11/18/2015 12:16
SODIUM 18 10 MG/L 10 11/18/2015 12:16
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 400 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.61 0.54 NU 10 11/18/2015 12:16
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ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS 14 Lab ID: 1511253-45
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:28 Percent Moisture:
Report Dilution
Analyses Result Quad Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 430 10 MG/L 10 11/18/2015 12:17
MAGNESIUM 60 10 MG/L 10 11/18/2015 12:17
SODIUM 270 10 MG/L 10 11/18/2015 12:17
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 4300 1 umhos/cm 1 11/19/2015
SATU RATION
SODIUM ADSORPTION RATIO 3.2 0.54 NU 10 11/18/2015 12:17
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 45 of 4't4 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS15 Lab ID: 1511253-46
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:20 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 490 10 MG/L 10 11/18/201512:18
MAGNESIUM 84 10 MG/L 10 11/18/2015 12:18
SODIUM 900 10 MG/L 10 11/18/2015 12:18
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 7500 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 9.9 0.54 NU 10 11/18/2015 12:18
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 46 of 4145 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS15 Lab ID: 1511253-46
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:20 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Explanation of Qualifiers
Radiochemistry:
U or ND - Result is less than the sample specific MDC. M3 - The requested MDC was not met, but the reported
Y1 - Chemical Yield is in control at 100-110%. Quantitative yield is assumed. activity is greater than the reported MDC.
Y2 Chemical Yield outside default limits. L - LCS Recovery below lower control limit.
H - LCS Recovery above upper control limit.
W - DER is greater than Warning Limit of 1.42
" P - LCS, Matrix Spike Recovery within control limits.
- Aliquot Basis is 'As Received' while the Report Basis is 'Dry Weight'.
# - Aliquot Basis is 'Dry Weight' while the Report Basis is 'As Received'. N - Matrix Spike Recovery outside control limits
G - Sample density differs by more than 15% of LCS density. NC - Not Calculated for duplicate results less than 5 times MDC
D - DER is greater than Control Limit B - Analyte concentration greater than MDC.
M - Requested MDC not met. B3 - Analyte concentration greater than MDC but less than Requested
LT - Result is less than requested MDC but greater than achieved MDC. MDC.
Inorganics:
B - Result is less than the requested reporting limit but greater than the instrument method detection limit (MDL).
U or ND - Indicates that the compound was analyzed for but not detected.
E - The reported value is estimated because of the presence of interference. An explanatory note may be included in the narrative.
M - Duplicate injection precision was not met.
N - Spiked sample recovery not within control limits. A post spike is analyzed for all ICP analyses when the matrix spike and or spike
duplicate fail and the native sample concentration is less than four times the spike added concentration.
Z - Spiked recovery not within control limits. An explanatory note may be included in the narrative.
• - Duplicate analysis (relative percent difference) not within control limits.
S - SAR value is estimated as one or more analytes used in the calculation were not detected above the detection limit.
Organics:
U or ND - Indicates that the compound was analyzed for but not detected.
B - Analyte is detected in the associated method blank as well as in the sample. It indicates probable blank contamination and warns the data user.
E - Analyte concentration exceeds the upper level of the calibration range.
J - Estimated value. The result is less than the reporting limit but greater than the instrument method detection limit (MDL).
A - A tentatively identified compound is a suspected aldol-condensation product.
X - The analyte was diluted below an accurate quantitation level.
* - The spike recovery is equal to or outside the control criteria used.
+ - The relative percent difference (RPD) equals or exceeds the control criteria.
G - A pattern resembling gasoline was detected in this sample.
D - A pattern resembling diesel was detected in this sample.
M - A pattern resembling motor oil was detected in this sample.
C - A pattern resembling crude oil was detected in this sample.
4 - A pattern resembling JP-4 was detected in this sample.
5 - A pattern resembling JP-5 was detected in this sample.
H - Indicates that the fuel pattern was in the heavier end d the retention time window for the analyte of interest.
L - Indicates that the fuel pattern was in the lighter end of the retention time window for the analyte of interest.
Z - This flag indicates that a significant fraction of the reported result did not resemble the patterns of any of the following petroleum hydrocarbon products:
- gasoline
- JP-8
- diesel
- mineral spirits
- motor oil
- Stoddard solvent
- bunker C
ALS Environmental -- FC
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ALS Environmental -- FC Date: 12/4/2015 1:54:
Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadficld
Batch ID: HC151116-6-1 Instrument ID: FUELS-1 Method: SW8015
LCS Sample ID: HC151116.6 Units: MG/KG Analysis Date: 11/16/2015 10:22
Client ID: Run ID: HC151116-6A Prep Date: 11/1612015 DE: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
GASOLINE RANGE ORGANICS 2.58 0.5 2.5 103 79-118 20
Sum 2,3,4-TRIFLUOROTOLUENE 0.578 0.5 116 76-126
MB Sample ID: HC151116-6 Units: MG/KG Analysis Date: 11/16/2015 11 :39
Client ID: Run ID: HC151116-6A Prep Date: 11/16/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
GASOLINE RANGE ORGANICS ND 0.5
Sum 2,3,4-TRIFLUOROTOLUENE 0 508 0.5 102 76-126
The following samples were analyzed in this batch: 1511253-1 1511253-2 1511253-3
1511253-4 1511253-5 1511253-6
1511253-7 1511253-8 1511253-9
1511253-10 1511253-11 1511253-12
1511253-13 1511253-14 1511253-15
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: HC151118-100-1 Instrument ID: FUELS-1 Method: SW8015M
LCS Sample ID: HC151118-100 Units: MG/KG Analysis Date: 11/19/2015 20:13
Client ID: Run ID: HC151119-7A Prep Date: 11/18/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
Diesel Range Organics 127 5 125 102 76-124 20
Sum O-TERPHENYL 4-42 6.25 71 49-114
MB Sample ID: HC151118-100 Units: MG/KG Analysis Date: 11/19/2015 09:54
Client ID: Run ID: HC151119-7A Prep Date: 11/18/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
Diesel Range Organics ND 5
Sum O-TERPHENYL 4.7 6.25 75 49-114
MS Sample ID: 1511253-15 Units: MG/KG Analysis Date: 111191201519:11
Client ID: Miller 1 SS15 Run ID: HC151119-7A Prep Date: 11/18/2015 DF: 1
SPK Ref Control Decision RPO RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
Diesel Range Organics 291 5.21 130 130 124 76-124 20
Sur. O-TERPHENYL 6 32 6.51 97 49-114
MSD Sample ID: 1511253-15 Units: MG/KG Analysis Date: 1111912015 19:42
Client ID: Miller 1 SS15 Run ID: HC151119-7A Prep Date: 11/18/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
Diesel Range Organics 283 5.3 133 130 116 76-124 291 3 20
Sum O-TERPHENYL 647 6.63 98 49-114 2
The following samples were analyzed in this batch: 1511253-1 1511253-2 1511253-3
1511253-4 1511253-5 1511253-6
1511253-7 1511253-8 1511253-9
1511253-10 1511253-11 1511253-12
1511253-13 1511253-14 1511253-15
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: IP151119-2-1 Instrument ID: ICPMS2 Method: SW6020
LCS Sample ID: IP151119-2 Units: MG/KG Analysis Date: 1112012015 12:56
Client ID: Run ID: IM1 51 1 20-1 0A1 Prep Date: 11/19/2015 DF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
ARSENIC 8 83 0.2 10 88 80-120 20
MB Sample ID: IP151119.2 Units: MG/KG Analysis Date: 11/20/2015 12:52
Client ID: Run ID: IM151120-10A1 Prep Date: 11/19/2015 DF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
ARSENIC NO 0.2
MS Sample ID: 1511253.17 Units: MG/KG Analysis Date: 11/20/2015 13:10
Client ID: Miller 1 SS01 Run ID: IM151120-10A1 Prep Date: 11/19/2015 DF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
ARSENIC 12 8 0.188 9.38 4.3 91 75-125 20
MSD Sample ID: 1511253.17 Units: MG/KG Analysis Date: 11/20/2015 13:13
Client ID: Miller 1 SS01 Run ID: IM1 51 1 20-1 0A1 Prep Date: 11/19/2015 DF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
ARSENIC 12 2 0.188 9.4 4.3 84.1 75-125 12.8 5 20
The following samples were analyzed in this batch: 1511253-17 1511253-18 1511253-19
1511253-20 1511253-21 1511253-22
1511253-23 1511253-24 1511253-25
1511253-26 1511253-27 1511253-28
1511253-29 1511253-30 1511253-31
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: EX151113-1-1 Instrument ID: HPSV1 Method: SW8270SIM
MS Sample ID: 15112533 Units: UG/KG Analysis Date: 11/17/2015 10:21
Client ID: Miller 1 SSO3 Run ID: SV151117-2 Prep Date: 11/13/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
NAPHTHALENE 39 3 3.63 72.5 3.6 54 40-107 30
Surr. NITROBENZENE-05 42 72.5 58 28-113
Sum 2-FLUOROBIPHENYL 409 72.5 56 41-106
MSD Sample ID: 1511253-3 Units: UG/KG Analysis Date: 11/17/2015 10:41
Client ID: Miller 1 SSO3 Run ID: SV151117-2 Prep Date: 11/13/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
NAPHTHALENE 39.7 3.61 72.2 3.6 55 40-107 39.3 1 30
Surr. NITROBENZENE-DS 41.9 72.2 58 28-113 0
Sum 2-FLUOROBIPHENYL 39.5 72.2 55 41-106 4
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: EX151113.1-2 Instrument ID: HPSV1 Method: SW8270SIM
LCS Sample ID: EX151113-1 Units: UG/KG Analysis Date: 11/17/2015 09:23
Client ID: Run ID: SV151117-2 Prep Date: 11/13/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
NAPHTHALENE 424 3.33 66.7 64 40-107 30
ACENAPHTHENE 40.9 3.33 66.7 61 46-108 30
FLUORENE 41 3.33 66.7 61 49-108 30
ANTHRACENE 40 3.33 66.7 60 53-107 30
FLUORANTHENE 41-7 3.33 66.7 62 54-114 30
PYRENE 44.9 3.33 66.7 67 46-123 30
BENZO(A)ANTHRACENE 43.6 3.33 66.7 65 52-111 30
CHRYSENE 42.3 3.33 66.7 63 53-112 30
BENZO(B)FLUORANTHENE 409 3.33 66.7 61 45-114 30
BENZO(K)FLUORANTHENE 47.3 3.33 66.7 71 45-123 30
BENZO(A)PYRENE 415 3.33 66.7 62 50-111 30
INDENO(1,2,3-CD)PYRENE 371 3.33 66.7 56 38-121 30
DIBENZO(A,H)ANTHRACENE 389 3.33 66.7 58 41-125 30
Sum NITROBENZENE-O5 44 2 66.7 66 28-113
Surr•. 2-FLUOROBIPHENYL 42 7 66.7 64 41-106
Sum TERPHENYL-D14 438 66.7 66 25-147
MB Sample ID: EX151113-1 Units: UG/KG Analysis Date: 11/17/2015 09:03
Client ID: Run ID: SV151117-2 Prep Date: 11/13/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
NAPHTHALENE ND 3.3
ACENAPHTHENE ND 3.3
FLUORENE ND 3.3
ANTHRACENE ND 3.3
FLUORANTHENE ND 3.3
PYRENE ND 3.3
BENZO(A)ANTHRACENE ND 3.3
CHRYSENE ND 3.3
BENZO(B)FLUORANTHENE ND 3.3
BENZO(K)FLUORANTHENE ND 3.3
BENZO(A)PYRENE ND 3.3
INDEN0(1,2,3-CD)PYRENE ND 3.3
DIBENZO(A,H)ANTHRACENE ND 3.3
Surr: NITROBENZENE-D5 43.6 66.7 65 28-113
Sum 2-FLUOROBIPHENYL 42 66.7 63 41-106
Surr. TERPHENYL-014 46.3 66.7 69 25-147
The following samples were analyzed in this batch: 11511253-2 1511253-3 1511253-5 I
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: VL151117-2.1 Instrument ID: HPV1 Method: SW8260
LCS Sample ID: VL151117-2 Units: UG/KG Analysis Date: 11/17/2015 14:38
Client ID: Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
BENZENE 39 4 5 40 98 73-126 30
TOLUENE 4D6 5 40 102 71-127 30
ETHYLBENZENE 412 5 40 103 74-127 30
M+P-XYLENE 86 6 5 80 108 79-126 30
O-XYLENE 42 7 5 40 107 77-125 30
Sum 52 50 104 61-134
DIBROMOFLUOROMETHANE
Sum TOLUENE-D8 47.9 50 96 57-135
Surr 4- 48.7 50 97 52-151
BROMOFLUOROBENZENE
LCSD Sample ID: VL151117-2 Units: UG/KG Analysis Date: 11/17/2015 14:59
Client ID: Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
BENZENE 40 5 40 100 73-126 39.4 2 30
TOLUENE 41.8 5 40 104 71-127 40.6 3 30
ETHYLBENZENE 424 5 40 106 74-127 41.2 3 30
M+P-XYLENE B75 5 80 109 79-126 86.6 1 30
O-XYLENE 42 9 5 40 107 77-125 42.7 0 30
Sum 50 7 50 101 61-134 3
DIBROMOFLUOROMETHANE
Surr. TOLUENE-DS 48,6 50 97 57-135 1
Surr 4- 49 50 98 52-151 1
BROMOFLUOROBENZENE
MB Sample ID: VL151117-2 Units: UG/KG Analysis Date: 11/17/2015 15:21
Client ID: Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
BENZENE ND 5
TOLUENE ND 5
ETHYLBENZENE ND 5
M+P-XYLENE ND 5
O-XYLENE ND 5
TOTAL XYLENES ND 5
Surr. 49.8 50 100 61-134
DIBROMOFLUOROMETHANE
Sum TOLUENE-D8 48 50 96 57-135
Surr. 4- 47 7 50 95 52-151
BROMOFLUOROBENZENE
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: VL151117-2-1 Instrument ID: HPV1 Method: SW8260
MS Sample ID: 1511253.15 Units: UGIKG Analysis Date: 11/17/2015 21 :26
Client ID: Miller 1 SS15 Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
BENZENE 26,2 5.45 43.6 5.5 60 73-126 30 `
TOLUENE 221 5.45 43.6 5.5 51 71-127 30
ETHYLBENZENE 17.4 5.45 43.6 5.5 40 74-127 30 '
M+P-XYLENE 34 8 5.45 87.3 5.5 40 79-126 30 '
O-XYLENE 18 6 5.45 43.6 5.5 43 77-125 30 '
Sum 58 3 54.5 107 61-134
DIBROMOFLUOROMETHANE
Sum TOLUENE-O8 54 3 54.5 100 57-135
Surr. 4- 47 5 54.5 87 52-151
BROMOFLUOROBENZENE
MSD Sample ID: 1511253.15 Units: UG/KG Analysis Date: 11/17/2015 21 :50
Client ID: Miller 1 SS15 Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
BENZENE 241 5.44 43.5 5.5 55 73-126 26.2 8 30 '
TOLUENE 186 5.44 43.5 5.5 45 71-127 22.1 12 30 *
ETHYLBENZENE 14 5.44 43.5 5.5 32 74-127 17.4 22 30 *
M+P-XYLENE 272 5.44 87.1 5.5 31 79-126 34.8 25 30 *
O-XYLENE 15 2 5.44 43.5 5.5 35 77-125 18.6 20 30 '
Surr. 56.7 54.4 104 61-134 3
DIBROMOFLUOROMETHANE
Surr TOLUENE-D8 54.4 54.4 100 57-135 0
Surr 4- 47 7 54.4 88 52-151 0
BROMOFLUOROBENZENE
The following samples were analyzed in this batch: 1511253-1 1511253-2 1511253-3
1511253-4 1511253-5 1511253-6
1511253-7 1511253-8 1511253-9
1511253-10 1511253-11 1511253-12
1511253-13 1511253-14 1511253-15
ALS Environmental -- FC QC Page: 7 of 7
LIMS Version: 6.795
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� Health 2
/1\ Science
_�all " - u " " " Fire 2
Chemicals & Laborato Equipment 2 , 0
ryReactivity 0
Personal E
Protection
Material Safety Data Sheet
Naphthalene MSDS
Section 1 : Chemical Product and Company Identification
Product Name: Naphthalene Contact Information:
Catalog Codes: SLN1789, SLN2401 Sciencelab.com, Inc.
14025 Smith Rd.
CAS#: 91 -20-3 Houston, Texas 77396
RTECS: QJ0525000 US Sales: 1 -800-901 -7247
International Sales: 1 -281 -441 -4400
TSCA: TSCA 8(b) inventory: Naphthalene
Order Online: ScienceLab.com
CI#: Not available.
CHEMTREC (24HR Emergency Telephone), call:
Synonym: 1 -800-424-9300
Chemical Name: Not available. International CHEMTREC, call: 1 -703-527-3887
Chemical Formula: C10H8 For non-emergency assistance, call: 1 -281 -441 -4400
Section 2 : Composition and Information on Ingredients
Composition:
Name CAS # % by Weight
Naphthalene 91 -20-3 100
Toxicological Data on Ingredients: Naphthalene: ORAL (LD50): Acute: 490 mg/kg [Rat]. 533 mg/kg [Mouse]. 1200 mg/kg
[Guinea pig]. DERMAL (LD50): Acute: 20001 mg/kg [Rabbit]. VAPOR (LC50): Acute: 170 ppm 4 hour(s) [Rat].
Section 3: Hazards Identification
Potential Acute Health Effects:
Very hazardous in case of ingestion. Hazardous in case of eye contact (irritant), of inhalation. Slightly hazardous in case of
skin contact (irritant, permeator). Severe over-exposure can result in death.
Potential Chronic Health Effects:
CARCINOGENIC EFFECTS: A4 (Not classifiable for human or animal.) by ACGIH. MUTAGENIC EFFECTS: Not available.
TERATOGENIC EFFECTS: Not available. DEVELOPMENTAL TOXICITY: Classified Development toxin [POSSIBLE]. The
substance is toxic to blood, kidneys, the nervous system, the reproductive system, liver, mucous membranes, gastrointestinal
tract, upper respiratory tract, central nervous system (CNS). Repeated or prolonged exposure to the substance can produce
target organs damage. Repeated exposure to an highly toxic material may produce general deterioration of health by an
accumulation in one or many human organs.
Section 4: First Aid Measures
p. 1
Eye Contact:
Check for and remove any contact lenses. Immediately flush eyes with running water for at least 15 minutes, keeping eyelids
open. Cold water may be used. Do not use an eye ointment. Seek medical attention.
Skin Contact:
After contact with skin, wash immediately with plenty of water. Gently and thoroughly wash the contaminated skin with running
water and non-abrasive soap. Be particularly careful to clean folds, crevices, creases and groin. Cover the irritated skin with an
emollient. If irritation persists, seek medical attention. Wash contaminated clothing before reusing.
Serious Skin Contact: Not available.
Inhalation: Allow the victim to rest in a well ventilated area. Seek immediate medical attention.
Serious Inhalation:
Evacuate the victim to a safe area as soon as possible. Loosen tight clothing such as a collar, tie, belt or waistband. If
breathing is difficult, administer oxygen. If the victim is not breathing, perform mouth-to-mouth resuscitation. WARNING: It may
be hazardous to the person providing aid to give mouth-to-mouth resuscitation when the inhaled material is toxic, infectious or
corrosive. Seek immediate medical attention.
Ingestion:
Do not induce vomiting. Examine the lips and mouth to ascertain whether the tissues are damaged, a possible indication that
the toxic material was ingested; the absence of such signs, however, is not conclusive. Loosen tight clothing such as a collar,
tie, belt or waistband. If the victim is not breathing, perform mouth-to-mouth resuscitation. Seek immediate medical attention.
Serious Ingestion: Not available.
Section 5: Fire and Explosion Data
Flammability of the Product: Flammable.
Auto-Ignition Temperature: 567°C (1052.6°F)
Flash Points: CLOSED CUP: 88°C (190.4°F). OPEN CUP: 79°C (174.2°F).
Flammable Limits: LOWER: 0.9% UPPER: 5.9%
Products of Combustion: These products are carbon oxides (CO, 0O2).
Fire Hazards in Presence of Various Substances: Not available.
Explosion Hazards in Presence of Various Substances:
Risks of explosion of the product in presence of mechanical impact: Not available. Risks of explosion of the product in
presence of static discharge: Not available.
Fire Fighting Media and Instructions:
Flammable solid. SMALL FIRE: Use DRY chemical powder. LARGE FIRE: Use water spray or fog. Cool containing vessels
with water jet in order to prevent pressure build-up, autoignition or explosion.
Special Remarks on Fire Hazards: Not available.
Special Remarks on Explosion Hazards: Not available.
Section 6: Accidental Release Measures
Small Spill: Use appropriate tools to put the spilled solid in a convenient waste disposal container.
Large Spill:
Flammable solid. Stop leak if without risk. Do not touch spilled material. Use water spray curtain to divert vapor drift. Prevent
entry into sewers, basements or confined areas; dike if needed. Eliminate all ignition sources. Call for assistance on disposal.
Be careful that the product is not present at a concentration level above TLV. Check TLV on the MSDS and with local
authorities.
p. 2
Section 7: Handling and Storage
Precautions:
Keep locked up Keep away from heat. Keep away from sources of ignition. Ground all equipment containing material. Do not
ingest. Do not breathe dust. Avoid contact with eyes Wear suitable protective clothing In case of insufficient ventilation, wear
suitable respiratory equipment If ingested, seek medical advice immediately and show the container or the label. Keep away
from incompatibles such as oxidizing agents.
Storage:
Flammable materials should be stored in a separate safety storage cabinet or room. Keep away from heat. Keep away from
sources of ignition. Keep container tightly closed. Keep in a cool, well-ventilated place. Ground all equipment containing
material. Keep container dry. Keep in a cool place.
Section 8: Exposure Controls/Personal Protection
Engineering Controls:
Use process enclosures, local exhaust ventilation, or other engineering controls to keep airborne levels below recommended
exposure limits. If user operations generate dust, fume or mist, use ventilation to keep exposure to airborne contaminants
below the exposure limit.
Personal Protection :
Splash goggles. Lab coat. Dust respirator. Be sure to use an approved/certified respirator or equivalent. Gloves.
Personal Protection in Case of a Large Spill:
Splash goggles. Full suit. Dust respirator. Boots. Gloves. A self contained breathing apparatus should be used to avoid
inhalation of the product. Suggested protective clothing might not be sufficient; consult a specialist BEFORE handling this
product.
Exposure Limits:
Israel: TWA: 10 (ppm) TWA: 10 STEL: 15 (ppm) from ACGIH (TLV) [1995] TWA: 52 STEL: 79 (mg/m3) from ACGIH [1995]
Australia: STEL: 15 (ppm) Consult local authorities for acceptable exposure limits.
Section 9: Physical and Chemical Properties
Physical state and appearance: Solid. (Crystalline solid.)
Odor: Aromatic.
Taste: Not available.
Molecular Weight: 128. 19 g/mole
Color: White.
pH (1 % soln/water): Not available.
Boiling Point: 218°C (424.4°F)
Melting Point: 80.2°C (176.4°F)
Critical Temperature: Not available.
Specific Gravity: 1 . 162 (Water = 1 )
Vapor Pressure: Not applicable.
Vapor Density: 4.4 (Air = 1 )
Volatility: Not available.
Odor Threshold : 0.038 ppm
Water/Oil Dist. Coeff. : Not available.
P. 3
lonicity (in Water): Not available.
Dispersion Properties:
Partially dispersed in hot water, methanol, n-octanol. Very slightly dispersed in cold water. See solubility in methanol , n-
octanol .
Solubility:
Partially soluble in methanol, n-octanol. Very slightly soluble in cold water, hot water.
Section 10 : Stability and Reactivity Data
Stability: The product is stable.
Instability Temperature: Not available.
Conditions of Instability: Not available.
Incompatibility with various substances: Highly reactive with oxidizing agents.
Corrosivity: Non-corrosive in presence of glass.
Special Remarks on Reactivity: Not available.
Special Remarks on Corrosivity: May attack some forms of rubber and plastic
Polymerization : No.
Section 11 : Toxicological Information
Routes of Entry: Absorbed through skin. Dermal contact. Eye contact. Inhalation. Ingestion.
Toxicity to Animals:
WARNING: THE LC50 VALUES HEREUNDER ARE ESTIMATED ON THE BASIS OF A 4-HOUR EXPOSURE. Acute oral
toxicity (LD50): 490 mg/kg [Rat]. Acute dermal toxicity (LD50): 20001 mg/kg [Rabbit]. Acute toxicity of the vapor (LC50): 170
ppm 4 hour(s) [Rat].
Chronic Effects on Humans:
CARCINOGENIC EFFECTS: A4 (Not classifiable for human or animal.) by ACGIH . DEVELOPMENTAL TOXICITY: Classified
Development toxin [POSSIBLE]. The substance is toxic to blood, kidneys, the nervous system , the reproductive system, liver,
mucous membranes, gastrointestinal tract, upper respiratory tract, central nervous system (CNS).
Other Toxic Effects on Humans:
Very hazardous in case of ingestion. Hazardous in case of inhalation. Slightly hazardous in case of skin contact (irritant,
permeator).
Special Remarks on Toxicity to Animals: Not available.
Special Remarks on Chronic Effects on Humans: Not available.
Special Remarks on other Toxic Effects on Humans: Not available.
Section 12: Ecological Information
Ecotoxicity: Ecotoxicity in water (LC50): 305.2 ppm 96 hour(s) [Trout].
BOD5 and COD: Not available.
Products of Biodegradation:
Possibly hazardous short term degradation products are not likely. However, long term degradation products may arise.
Toxicity of the Products of Biodegradation: The products of degradation are more toxic.
p. 4
Special Remarks on the Products of Biodegradation: Not available.
Section 13: Disposal Considerations
Waste Disposal:
Section 14: Transport Information •
DOT Classification: CLASS 4. 1 : Flammable solid.
Identification : : Naphthalene, refined : UN1334 PG: Ill
Special Provisions for Transport: Marine Pollutant
Section 15: Other Regulatory Information
Federal and State Regulations:
Rhode Island RTK hazardous substances: Naphthalene Pennsylvania RTK: Naphthalene Florida: Naphthalene Minnesota:
Naphthalene Massachusetts RTK: Naphthalene TSCA 8(b) inventory: Naphthalene TSCA 8(a) PAIR: Naphthalene TSCA 8(d)
H and S data reporting: Naphthalene: 06/01 /87 SARA 313 toxic chemical notification and release reporting: Naphthalene: 1 %
CERCLA: Hazardous substances. : Naphthalene: 100 lbs. (45.36 kg)
Other Regulations:
OSHA: Hazardous by definition of Hazard Communication Standard (29 CFR 1910. 1200). EINECS: This product is on the
European Inventory of Existing Commercial Chemical Substances.
Other Classifications:
WHMIS (Canada):
CLASS B-4: Flammable solid. CLASS D-1 B: Material causing immediate and serious toxic effects (TOXIC). CLASS D-2B:
Material causing other toxic effects (TOXIC) .
DSCL (EEC):
R36- Irritating to eyes. R40- Possible risks of irreversible effects. R48/22- Harmful: danger of serious damage to health
by prolonged exposure if swallowed. R48/23- Toxic: danger of serious damage to health by prolonged exposure through
inhalation. R63- Possible risk of harm to the unborn child.
HMIS (U.S.A.):
Health Hazard : 2
Fire Hazard: 2
Reactivity: 0
Personal Protection: E
National Fire Protection Association (U.S.A.) :
Health : 2
Flammability: 2
Reactivity: 0
Specific hazard :
Protective Equipment:
Gloves. Lab coat. Dust respirator. Be sure to use an approved/certified respirator or equivalent. Wear appropriate respirator
when ventilation is inadequate. Splash goggles.
P. 5
Section 16: Other Information
References: Not available.
Other Special Considerations: Not available.
Created : 10/11/2005 01 :30 PM
Last Updated: 05/21 /2013 12:00 PM
The information above is believed to be accurate and represents the best information currently available to us. However, we
make no warranty of merchantability or any other warranty, express or implied, with respect to such information, and we assume
no liability resulting from its use. Users should make their own investigations to determine the suitability of the information for
their particular purposes. In no event shall ScienceLab.corn be liable for any claims, losses, or damages of any third party or for
lost profits or any special, indirect, incidental, consequential or exemplary damages, howsoever arising, even if ScienceLab.corn
has been advised of the possibility of such damages.
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EXHIBIT
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Ott\
OLSSON t'6
ASSOCIATES \,
November 30, 2015
Mr. Jacob Evans
Senior Environmental Specialist
Noble Energy, Inc.
2115 117th Ave
Greeley, CO 80631
RE : Spreadfield Monitoring Report
Miller 1 Spreadfield
Weld County, CO
Dear Mr. Evans:
Olsson Associates (Olsson), under the direction of Noble Energy, Inc. (Noble) conducted
confirmation soil sampling on November 12 , 2015 at the Miller North #1 Spreadfield (Site) to
assess the post-incorporation arsenic levels.
Location Description
The Site is located in Weld County at the northwest corner of the intersection of County Road
83 and County Road 70. The legal site description is Section 11 , Township 6 North, Range 62
West, 6th Principal Meridian . The historical application area is currently being utilized as an
active agricultural field by the landowner.
Sampling Procedures
On November 12, 2015, Olsson collected fifteen samples from the site as depicted on the
attached Soil Sample Location Map as well as one composite sample. The samples were
collected using clean sampling equipment and placed into laboratory prepared glassware.
Equipment was cleaned with Alconox and deionized water between samples. Each sample
represents six to eight inches below the surface of the windrow. Samples were delivered by
hand on the same day to ALS Environmental laboratory (ALS) in Fort Collins, Colorado
following chain of custody procedures.
A subset of the samples were corn posited and ground by ALS using the following procedures.
After the samples were delivered to the lab they were transferred to an aluminum pan and
spread out across the bottom of the pan and allowed to air dry. When dry, the sample was
sieved through a 1/4-inch sieve to remove large rocks, grass, twigs. The sample was then
sectioned into several approximate 2-inch sections. A small aliquot from each section was taken
to create an approximately 20 gram subsample. This aliquot was ground and used for metals
analysis or arsenic by EPA Method 6020A.
Analytical Results
A copy of the laboratory analytical report is included as Attachment 2 and is summarized in
attached Table 1 as well as attached Soil Sample Location Map. Total Petroleum Hydrocarbons
300 E 16th Street, Unit 309 TEL 303.237.2072
Greeley, CO 80631 FAX 303.237.2659 www.olssonassociates.com
Miller 1 Spreadfield
Page 2
November 2015
(TPH) was below the Table 910-1 concentration levels of 500 miligrams/kilogram (mg/kg) for all
samples. Benzene, toluene, ethylbenzene, and total xylenes (BTEXZ) were non-detect (ND) for
all soil samples. Naphthalene was below the Table 910-1 concentration levels of 23 mg/kg for
all samples. All pH samples were within the Table 910-1 standards of 6-9. . All soil samples
were below Table 910-1 standards for sodium adsorption radio (SAR) of less than 12. Arsenic
ranged between 2.5 mg/kg for SS13 and 7.8 for SS 11 ; all samples were above the Table 910-1
concentration levels of 0.039 mg/kgElectrical conductivity (EC) ranged between 0.31 millimhos
per centimeter (mmhos/cm) and 7.7 mmhos/cm; six samples were above the table 910-1
standard of 4 mmhos/cm.
A composite sample was run for PAH's (polycyclic aromatic hydrocarbons). All results were
below Table 910-1 standards, results are summarized in attached Table 1 .
Summary and Conclusions
Olsson collected fifteen samples and on composite sample from the Miller 1 Spreadfield which
were submitted for laboratory analysis at ALS. TPH , BTEX, naphthalene, pH, SAH , and PAH's
were all below Table 910-1 standards. EC ranged between 0.31 millimhos per centimeter
(mmhos/cm) and 7.7 mmhos/cm with six samples above Table 910-1 standards; however, these
were similar to previous samples collected by LT Environmental on behalf of Noble. Arsenic
concentrations ranged from 2.0 to 7.8 mg/kg ; all above Table 910-1 standards of 0.039 mg/kg.
Soils in Weld County are characteristically high in Arsenic and these samples are within 1 .25
normal background ranges for the area.
Olsson recommends Noble request closure status for the Miller North #1 Spreadfield.
Please call me if you have any questions.
Sincerely,
Olsson Associates, Inc.
qv/e Or--
Nikki Graber Mike Storey
Associate Scientist Associate Scientist
Attachments: Table 1 - Soil Analytical Results
Attachment 1 - Soil Sample Location Map
Attachment 2 - ALS Laboratory Analytical Reports
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
Benzene mg/kg 0. 17
COGCC 910-1 Concentration Toluene mg/kg 85
Levels Ethylbenzene mg/kg 100
Xylenes (total) mg/kg 175
Sample Number BTEX (mg/kg) 11/12/15
Miller 1 SS01 Benzene ND
Toluene ND,
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS02 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS03 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SSO4 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS05 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS06 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS07 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS08 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS09 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS10 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS11 Benzene ND
I
Toluene ND
Ethylbenzene ND,
Xylenes (total) ND
Miller 1 SS12 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS13 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS14 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
Miller 1 SS15 Benzene ND
Toluene ND
Ethylbenzene ND
Xylenes (total) ND
mg/kg - Milligrams per Kilogram
ND - Non Detect
BOLD- Over Table 910-1 Concentration Level
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
COGCC 910-1 TPH (GRO+DRO) mg/kg 500
Concentration Level
Sample Number TPH (mg/kg) 11/12/15
DRO 170
Miller 1 SS01 GRO ND
TPH (GRO+DRO) 170
DRO ND
Miller 1 SS02 GRO ND
TPH (GRO+DRO) ND
DRO ND
Miller 1 SS03 GRO ND
TPH (GRO+DRO) ND
DRO 340
Miller 1 SSO4 GRO ND
TPH (GRO+DRO) 340
DRO ND
Miller 1 SS05 GRO ND
TPH (GRO+DRO) ND
DRO ND
Miller 1 SS06 GRO ND
TPH (GRO+DRO) ND
DRO 65
Miller 1 SS07 GRO ND
TPH (GRO+DRO) 65
DRO 210
Miller 1 SS08 GRO ND
TPH (GRO+DRO) 210
DRO 21
Miller 1 SS09 GRO ND
TPH (GRO+DRO) 21
DRO 170
Miller 1 SS10 GRO ND
TPH (GRO+DRO) 170
DRO 220
Miller 1 SS11 GRO ND
TPH (GRO+DRO) 220
DRO 110
Miller 1 SS12 GRO ND
TPH (GRO+DRO) 110
DRO 6.3
Miller 1 SS13 GRO ND
TPH (GRO+DRO) 6.3
DRO 190
Miller 1 SS14 GRO ND
TPH (GRO+DRO) 190
DRO 130
Miller 1 SS15 GRO ND
TPH (GRO+DRO) 130
mg/kg - Milligrams per Kilogram
ND - Non Detect
TPH - Total Petroleum Hydrocarbons
BOLD- Over Table 910-1 Concentration Level
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
COGCC 910-1 Napthalene mg/kg 23
Concentration Level
Sample Number Naphthalene (mg/kg) 11/12/15
Miller 1 SS01 0.040
Miller 1 SS02 ND
Miller 1 SS03 ND
Miller 1 SSO4 0.150
Miller 1 SS05 ND
Miller 1 SS06 ND
Miller 1 SS07 0.022
Miller 1 SS08 0.041
Miller 1 SS09 0.0097
Miller 1 SS10 0.026
Miller 1 SS11 0.048
Miller 1 SS12 0.042
Miller 1 SS13 ND
Miller 1 SS14 0.045
Miller 1 SS15 0.052
mg/kg - Milligrams per Kilogram
ND - Non Detect
BOLD- Over Table 910-1 Concentration Level
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
COGCC 910-1 Arsenic mg/kg 0.039
Concentration Level
Sample Number Arsenic (mg/kg) 11/12/15
Miller 1SS01 4.3
Miller 1 SS02 4.7
Miller 1 SS03 2.8
Miller 1 SSO4 7.1
Miller 1 5505 3.7
Miller 1 SS06 2
Miller 1 SS07 6.6
Miller 1 SSO8 6.6
Miller 1 SS09 4.8
Miller 1 SS10 4.9
Miller 1 SS11 7.8
Miller 1 SS12 4.4
Miller 1 SS13 2.5
Miller 1 SS14 6
Miller 1 SS15 5
mg/kg - Milligrams per Kilogram
ND - Non Detect
BOLD- Over Table 910-1 Concentration Level
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
COGCC 910-1 Sodium Adsorption 12
Concentration Level Ratio (SAR ) (unitless)
Sample Number SAR 11/12/15
Miller 1 SS01 8.60
Miller 1 SS02 0.33
Miller 1 SS03 0.97
Miller 1 SSO4 4.90
Miller 15505 0.30
Miller 1 SS06 0.37
Miller 1 SS07 2.50
Miller 1 SS08 9.60
Miller 1 SS09 1.50
Miller 1 SS10 5.90
Miller 1 SS11 5.90
Miller 1 SS12 2.90
Miller 1 SS13 0.61
Miller 1 SS14 3.20
Miller 1 SS15 9.90
BOLD- Over Table 910-1 Concentration Level
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
COGCC 910-1 Electrical Condicutivity <4 or 2x
Concentration Level (EC) mmhos/cm background
Sample Number EC mmhos/cm 11/12/15
Miller 1 SS01 5.80
Miller 1 SS02 0.34
Miller 1 SS03 0.46
Miller 1 SSO4 5.00
Miller 1 SS05 0.40
Miller 1 SS06 0.31
Miller 1 SS07 1.20
Miller 1 SS08 7.70
Miller 1 SS09 1.20
Miller 1 SS10 4.60
Miller 1 SS11 5.60
Miller 1 SS12 2.80
Miller 15513 0.40
Miller 1 SS14 4.30
Miller 1 SS15 7.50
mmhos/cm - millimho per centimeter
ND - Non Detect
BOLD- Over Table 910-1 Concentration Level
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
COGCC 910-1
pH 6 to 9
Concentration Level
Sample Number pH11/12/15
Miller 1 SS01 7.8
Miller 1 SS02 8.0
Miller 1 SS03 8.0
Miller 1 SSO4 7.9
Miller 1 SS05 8.3
Miller 1 SS06 6.8
Miller 1 SS07 8.0
Miller 1 SS08 7.5
Miller 1 SS09 8.1
Miller 1 SS10 7.7
Miller 1 SS11 7.9
Miller 1 SS12 8.0
Miller 15S13 8.0
Miller 15514 7.9
Miller 1 SS15 7.6
mg/kg - Milligrams per Kilogram
ND - Non Detect
TPH - Total Petroleum Hydrocarbons
WB - Water Based Mud
OBM - Oil Based Mud
BOLD- Over Table 910-1 Concentration Level
Laboratory Analytical Summary
COGCC ID #'s Spreadfield
425661 Miller 1 Spreadfield
Table 910-1
Analyte Result mg/kg
Concentration mg/kg
Napthalene 0.025 23.0
Acenpathaene 0.0045 1000
Flourene 0.0091 1000
Anthracene ND 1000
Fluoranthene ND 1000
Pyrene 0.015 1000
Benzo(a)anthracene ND 0.22
Chrysene 0.014 22
Benzo(b)fluoranthene 0.0097 0.22
Benzo(k)fluoranthene ND 2.2
Benzo(a)pyrene ND 0.022
Indeno(1,2,3,c,d)pyrene ND 0.22
Dibenzo(a,h)anthracene ND 0.022
mg/kg - Milligrams per Kilogram
ND - Non Detect
BOLD- Over Table 910-1 Concentration Level
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ALS Er i r 0rirnerltat
Ft. Collins, Colorado LIMS Version: 6.795 Page 1 of 1
Friday, December 04, 2015
Nikki Graber
Olsson Associates
5285 McWhinney Blvd, Suite 160
Loveland, CO 80538
Re: ALS Workorder: 1511253
Project Name: Noble Miller Spreadfield
Project Number:
Dear Ms. Graber:
Thirty one soil samples were received from Olsson Associates, on 11 /12/2015. The samples were scheduled for the
following analyses:
GC/MS Semivolatiles
GC/MS Volatiles
Inorganics
Metals
Total Extractable Petroleum Hydrocarbons (Diesel)
Total Volatile Petroleum Hydrocarbons (Gasoline)
The results for these analyses are contained in the enclosed reports.
The data contained in the following report have been reviewed and approved by the personnel listed below. In
addition, ALS certifies that the analyses reported herein are true, complete and correct within the limits of the
methods employed.
Thank you for your confidence in ALS Environmental. Should you have any questions, please call.
S c- rely,
i �
A S n 'ron e tal
Amy R. Wolf
Project Manager
ADDRESS 225 Commerce Drive, Fort Collins, Colorado, USA 80524 I PHONE +1 970 490 1511 I FAX +1 970 490 1522
ALS GROUP USA, CORP. Part of the ALS Laboratory Group An ALS Limited Company
Environmental Jik www.atsglobal.com
FIGHT SOLUTIOTIS RICH ? PARTn[_n 1 of63
ALS Environmental — Fort Collins is accredited by the following accreditation bodies for
various testing scopes in accordance with requirements of each accreditation body. All
testing is performed under the laboratory management system , which is maintained to
meet these requirement and regulations. Please contact the laboratory or accreditation
body for the current scope testing parameters.
_ ALS Environmental — Fort Collins
Accreditation Body License or Certification Number
Alaska (AK) UST-086
Alaska (AK) CO01099
Arizona (AZ: AZ0742
California (CA) 06251 CA
Colorado (CO) CO01099
Connecticut (CT) PH-0232
Florida (FL: E87914
Idaho ;ID) CO01099
Kansas (KS) E-10381
Kentucky (KY) 90137
L-A-B (DoD ELAP/ISO 170250 L2257
Louisiana (LA) 05057
Maryland (MD) 285
Missouri (MO; 175
Nebraska(NE) _ NE-OS-24-13
Nevada (NV) 00000782008A
New York (NY) 12036
North Dakota (ND) R-057
Oklahoma (OK) 1301
Pennsylvania (PA) 68-03116
Tennessee (TN) 2976
Texas (TX) T104704241
Utah (UT) CO01099
Washington (WA) C1280
2 of 63
ALS Fnuironmental
1511253
GC/MS Volatiles:
The samples were analyzed using GC/MS following the current revision of SOP 525 based on SW-
846 Method 8260C.
• All matrix spike and matrix spike duplicate recoveries and RPDs were within acceptance criteria
with the following exceptions:
Spiked Compound QC Sample Direction
All Comt'ounds MS & MSD Low
The recoveries of these compounds in the laboratory control sample and laboratory control
sample duplicate were within control limits, which suggest the outliers in the matrix spikes may
have been due to matrix effects. No further action was taken.
• All internal standard recoveries were within acceptance criteria with the following exception:
Internal Standard Sample Direction
1 ,4-Dichlorobenzene-d4 -4, -7, -8, -11 & -12 Low
The samples were re-analyzed to evaluate whether the original outlier was due to matrix effects
or laboratory performance. The re-analysis also had internal standards outside the control limits,
which suggests the presence of matrix effects.
All remaining acceptance criteria were met.
GC/MS Semivolatiles:
The samples were analyzed using GC/MS following the current revision of SOP 506 based on SW-
846 Method 8270D. The samples were analyzed using selective ion monitoring (SIM), in order to
achieve lower reporting limits.
• All internal standard recoveries were within acceptance criteria with the following exception:
Internal Standard Sample Direction
Chrysene-d12 -16 High
The sample was re-analyzed to evaluate whether the original outlier was due to matrix effects or
laboratory performance. The re-analysis also had internal standards outside the control limits,
which suggests the presence of matrix effects.
All remaining acceptance criteria were met.
ADDRESS 225 Commerce Drive, Fort Collins Colorado 80524 USA I PHONE i- 1 970 490 1 51 1 FAX + 1 970 490 1 522 3 of 63
ALS GROUP USA, CORP. Pan of the ALS Group An ALS Limited Company
ALS
GRO:
The samples were analyzed following the current revision of SOP 425 generally based on SW-846
Methods 8000C and 8015D. TVPH is a multicomponent mixture and is quantitated by summing the
entire carbon range, rather than individual peaks. The carbon range integrated in this test extends
from C6 to C10
All acceptance criteria were met.
DRO:
The samples were analyzed following the current revision of SOP 406 generally based on SW-846
Methods 8000C and 8015D. TEPH is a multicomponent mixture and is quantitated by summing the
entire carbon range, rather than individual peaks. The carbon range integrated in this test extends
from C10 to C28.
All acceptance criteria were met.
Metals:
The samples were analyzed following SW-846, 3ifi Edition procedures. Analysis by ICPMS followed
method 6020A and the current revision of SOP 827.
Samples 17 through 31 were prepared utilizing the following procedures:
The sample was transferred to an aluminum pan and spread out across the bottom of the pan and
allowed to air dry. When dry, the sample was sieved through a 1 /4 inch sieve to remove large rocks,
grass, twigs. The sample was then sectioned into several —2 inch sections. A small aliquot from
each section was taken to create an -20 g subsample. This aliquot was ground and used for metals
analysis or arsenic by ICP-MS method 6020k The digestate was treated through a cation column
to remove potential interferences.
All acceptance criteria were met.
Inorganics:
The samples were analyzed following USDA Handbook 60 Chapter 6 procedures for the current
revision of the following SOP and method:
Analyte Method SOP #
Electrical conductivity USDA60 810 Draft
Sodium Adsorption Ratio USDA60 810 Draft
Paste pH USDA60 810 Draft
All acceptance criteria were met.
ADDRESS 225 Commerce Drive, Fort Collins Colorado 80524 USA . PHONE + 1 970 490 1 51 1 I FAX 4 1 970 490 1 522 4 of 63
ALS GROUP USA, CORP. Part of the ALS Group An ALS Limited Company
ALS Environmental -- FC
Sample Number(s) Cross-Reference Table
OrderNum : 1511253
Client Name: Olsson Associates
Client Project Name: Noble Miller Spreadfield
Client Project Number:
Client PO Number:
Client Sample Lab Sample COC Number Matrix Date Time
Number Number Collected Collected
Miller 1 SS01 1511253-1 SOIL 12-Nov-15 11 : 16
Miller 1 SS02 1511253-2 SOIL 12-Nov-15 11 :51
Miller 1 SS03 1511253-3 SOIL 12-Nov-15 11 :05
Miller 1 SSO4 1511253-4 SOIL 12-Nov-15 11 :05
Miller 1 SSO5 1511253-5 SOIL 12-Nov-15 11 :45
Miller 1 SS06 1511253-6 SOIL 12-Nov-15 11 :33
Miller 1 SS07 1511253-7 SOIL 12-Nov-15 11 :39
Miller 1 SS08 1511253-8 SOIL 12-Nov-15 11 :24
Miller 1 SS09 1511253-9 SOIL 12-Nov-15 11 :39
Miller 1 SS10 1511253-10 SOIL 12-Nov-15 11 :10
Miller 1 SS11 1511253-11 SOIL 12-Nov-15 10:45
Miller 1 SS12 1511253-12 SOIL 12-Nov-15 10:40
Miller 1 SS13 1511253-13 SOIL 12-Nov-15 10:35
Miller 1 SS14 1511253-14 SOIL 12-Nov-15 10:28
Miller 1 SS15 1511253-15 SOIL 12-Nov-15 10:20
Miller 1 Composite 1511253-16 SOIL 12-Nov-15 12:05
Miller 1 SS01 1511253-17 SOIL 12-Nov-15 11 :16
Miller 1 SS02 1511253-18 SOIL 12-Nov-15 11 :51
Miller 1 SS03 1511253-19 SOIL 12-Nov-15 11 :05
Miller 1 SSO4 1511253-20 SOIL 12-Nov-15 11 :05
Miller 1 SS05 1511253-21 SOIL 12-Nov-15 11 :45
Miller 1 SS06 1511253-22 SOIL 12-Nov-15 11 :33
Miller 1 SS07 1511253-23 SOIL 12-Nov-15 11 :39
Miller 1 SS08 1511253-24 SOIL 12-Nov-15 11 :24
Miller 1 SS09 1511253-25 SOIL 12-Nov-15 11 :39
Miller 1 SS10 1511253-26 SOIL 12-Nov-15 11 : 10
Miller 1 SS11 1511253-27 SOIL 12-Nov-15 10:45
Miller 1 SS12 1511253-28 SOIL 12-Nov-15 10:40
Miller 1 SS13 1511253-29 SOIL 12-Nov-15 10:35
Miller 1 SS14 1511253-30 SOIL 12-Nov-15 10:28
Page 1 of 2 ALS Environmental -- FC Date Printed: Friday, December 04, 2015
LIMS Version: 6.795
5of63
ALS Environmental -- FC
Sample Number(s) Cross-Reference Table
OrderNum : 1511253
Client Name: Olsson Associates
Client Project Name: Noble Miller Spreadfield
Client Project Number:
Client PO Number:
Client Sample Lab Sample COC Number Matrix Date Time
Number Number Collected Collected
Miller 1 SS15 1511253-31 SOIL 12-Nov-15 10:20
Miller 1 SS01 1511253-32 SatExtract 12-Nov-15 11 : 16
Miller 1 SS02 1511253-33 SatExtract 12-Nov-15 11 :51
Miller 1 SS03 1511253-34 SatExtract 12-Nov-15 11 :05
Miller 1 SSO4 1511253-35 SatExtract 12-Nov-15 11 :05
Miller 1 SSO5 1511253-36 SatExtract 12-Nov-15 11 :45
Miller 1 SSO6 1511253-37 SatExtract 12-Nov-15 11 :33
Miller 1 SS07 1511253-38 SatExtract 12-Nov-15 11 :39
Miller 1 SS08 1511253-39 SatExtract 12-Nov-15 11 :24
Miller 1 SS09 1511253-40 SatExtract 12-Nov-15 11 :39
Miller 1 SS10 1511253-41 SatExtract 12-Nov-15 11 : 10
Miller 1 SS11 1511253-42 SatExtract 12-Nov-15 10:45
Miller 1 SS12 1511253-43 SatExtract 12-Nov-15 10:40
Miller 1 SS13 1511253-44 SatExtract 12-Nov-15 10:35
Miller 1 SS14 1511253-45 SatExtract 12-Nov-15 10:28
Miller 1 SS15 1511253-46 SatExtract 12-Nov-15 10:20
Page 2 of 2 ALS Environmental -- FC Date Printed: Friday, December 04, 2015
LIMS Version: 6.795
6 of 63
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ALS Environmental - Fort Coffins
CONDITION OF SAMPLE UPON RECEIPT FORM
A
Client: 61-500r) Workorder No: 1 c i/a 5-3
Project Manager: 4 Initials: Date: !/fia/
I. Does this project require any special handling in addition to standard ALS procedures? YES Elan
2. Are custody seals on shipping containers intact? O)) YES NO
3. Are Custody seals on sample containers intact? O YES NO
4. Is there a COC (Chain-of-Custody) present or other representative documents? YE NO
5. Are the COC and bottle labels complete and legible? YES NO
6. Is the COC in agreement with samples received? (IDs, dates, times, no. of samples, no. ofCO NO
containers, matrix, requested analyses, etc.)
7. Were airbills / shipping documents present and/or removable? ROP OFF) YES NO
s. Are all aqueous samples requiring preservation preserved correctly? (excluding volatiles) /A YES NO
9. Are all aqueous non-preserved samples pH 4-9? /A YES NO
to. Is there sufficient sample for the requested analyses? NO
1 i• Were all samples placed in the proper containers for the requested analyses? NO
12. Are all samples within holding times for the requested analyses? NO
13. Were all sample containers received intact? (not broken or leaking, etc.) S NO
14- Are all samples requiring no headspace (VOC, GRO, RSK/MEE, Rx CN/S, radon) N/A YES NO
headspace free? Size of bubble: < green pea > green pea
15. Do any water samples contain sediment? Amount
N/A YES NO
Amount of sediment: dusting moderate heavy
16. Were the samples shipped on ice? // ids.
17. Were cooler temperatures measured at 0. 1-6.0°C? IR gun used*: #2 #4 ONLY W NO
Cooler #: /
Temperature (°C): b,0
No. of custody seals on cooler:
DOT Survey)
Acceptance External µR/hr reading:
Information
Background µR/hr reading: ,
Were external NR/hr readings s two times background and within DOT acceptance criteria? YES / NO N (If no, see Form 008.)
Additional Information: PROVIDE DETAILS BELOW FOR A NO RESPONSE TO ANY QUESTION ABOVE, EXCEPT #1 AND #16.
If applicable, was the client contacted? YES / N 6 , : o tact: Date/Time:
Project Manager Signature / Date: (1.àtIA) It ) 1-115
"IR Gun #2: Oakton, SN 9922500201-0066
Form 201r24.xls (06/04/2012) "IR Gun #4: Oakton, SN 2372220101-0002
Page 1 ofo f 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS01 Lab ID: 1511253-1
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 : 16 Percent Moisture: 14.5
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 170 DMH 5.7 MG/KG 1 11/19/2015 10:25
SUM O-TERPHENYL 91 49-114 %REC 1 11/19/2015 10:25
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 16:00
Sum 2,3,4-TRIFLUOROTOLUENE 90 76-126 %REC 1 11/16/2015 16:00
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 40 16 UG/KG 4 11/17/2015 14:01
Sum NITROBENZENE-D5 73 28-113 %REC 4 11/17/2015 14:01
Sum 2-FLUOROBIPHENYL 67 41-106 %REC 4 11/17/2015 14:01
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 15:43
TOLUENE ND 5.8 UG/KG 1 11/17/2015 15:43
ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 15:43
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 15:43
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 15:43
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 15:43
Sum DIBROMOFLUOROMETHANE 107 61-134 %REC 1 11/17/2015 15:43
Surr: TOLUENE-D8 98 57-135 %REC 1 11/17/2015 15:43
Sum 4-BROMOFLUOROBENZENE 93 52-151 %REC 1 11/17/2015 15:43
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 1 of 4710 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS02 Lab ID: 1511253-2
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:51 Percent Moisture: 10.8
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics ND 5.5 MG/KG 1 11/19/2015 10:56
Surr: O-TERPHENYL 88 49-114 %REC 1 11/19/2015 10:56
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 16:22
Sum 2,3,4-TRIFLUOROTOLUENE 95 76-126 %REC 1 11/16/2015 16:22
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.7 UG/KG 1 11/17/2015 11 :02
Sum NITROBENZENE-D5 57 28-113 %REC 1 11/17/2015 11 :02
Sum 2-FLUOROBIPHENYL 56 41-106 %REC 1 11/17/2015 11 :02
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 16:10
TOLUENE ND 5.6 UG/KG 1 11/17/2015 16:10
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 16:10
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 16:10
O-XYLENE ND 5M UG/KG 1 11/17/2015 16:10
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 16:10
Sum D/BROMOFLUOROMETHANE 102 61-134 %REC 1 11/17/2015 16:10
Sum TOLUENE-D8 98 57-135 %REC 1 11/17/2015 16:10
Sum 4BROMOFLUOROBENZENE 97 52-151 %REC 1 11/17/2015 16:10
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 2 of 4711 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS03 Lab ID: 1511253-3
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :05 Percent Moisture: 9.2
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 Prepay: SDW
Diesel Range Organics ND 5.2 MG/KG 1 11/19/2015 11:27
Surr: O-TERPHENYL 86 49-114 %REC 1 11/19/2015 11:27
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.47 MG/KG 1 11/16/2015 16:44
Sum Z3,4-TRIFLUOROTOLUENE 101 76-126 %REC 1 11/16/2015 16:44
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.6 UG/KG 1 11/17/2015 09:44
Sum NITROBENZENE-D5 59 28-113 %REC 1 11/17/2015 09:44
Sum 2-FLUOROBIPHENYL 58 41-106 %REC 1 11/17/2015 09:44
GC/MS Volatiles SW6260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.5 UG/KG 1 11/17/2015 16:32
TOLUENE ND 5.5 UG/KG 1 11/17/2015 16:32
ETHYLBENZENE ND 5.5 UG/KG 1 11/17/2015 16:32
M+P-XYLENE ND 5.5 UG/KG 1 11/17/2015 16:32
O-XYLENE ND 5.5 UG/KG 1 11/17/2015 16:32
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 16:32
Surr: DIBROMOFLUOROMETHANE 104 61-134 %REC 1 11/17/2015 16:32
Sum TOLUENE-D8 97 57-135 %REC 1 11/17/2015 16:32
Sum 4-BROMOFLUOROBENZENE 96 52-151 %REC 1 11/17/2015 16:32
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 3 of 4712 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO4 Lab ID: 1511253-4
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:05 Percent Moisture: 19.9
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 340 DMH 6.1 MG/KG 1 11/19/2015 11 :58
Sum O-TERPHENYL 99 49-114 %REC 1 11/19/2015 11 :58
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.52 MG/KG 1 11/16/2015 17:07
Sum 2,3,4-TRIFLUOROTOLUENE 86 76-126 %REC 1 11/16/2015 17:07
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 150 16 UG/KG 4 11/17/2015 14:28
Surr: NITROBENZENE-D5 59 28-113 %REC 4 11/17/2015 14:28
Sum 2-FLUOROBIPHENYL 64 41-106 %REC 4 11/17/2015 14:28
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 6.2 UG/KG 1 11/17/2015 16:54
TOLUENE ND 6.2 UG/KG 1 11/17/2015 16:54
ETHYLBENZENE ND 6.2 UG/KG 1 11/17/2015 16:54
M+P-XYLENE ND 6.2 UG/KG 1 11/17/2015 16:54
O-XYLENE ND 6.2 UG/KG 1 11/17/2015 16:54
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 16:54
Sum DIBROMOFLUOROMETHANE 103 61-134 %REC 1 11/17/2015 16:54
Sum TOLUENE-D8 110 57-135 %REC 1 11/17/2015 16:54
Sum 4-BROMOFLUOROBENZENE 80 52-151 %REC 1 11/17/2015 16:54
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.9 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 4 of 4713 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS05 Lab ID: 1511253-5
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :45 Percent Moisture: 12.4
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics ND 5.6 MG/KG 1 11/19/2015 12:29
Sum O-TERPHENYL 83 49-114 %REC 1 11/19/2015 12:29
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.51 MG/KG 1 11/16/2015 17:29
Sum Z3,4-TRIFLUOROTOLUENE 97 76-126 %REC 1 11/16/2015 17:29
GC/MS Seml-volatiles SW82T0SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.8 UG/KG 1 11/17/2015 11 :28
Sum. NITROBENZENE-D5 56 28-113 %REC 1 11/17/2015 11 :28
Sum 2-FLUOROBIPHENYL 54 41-106 %REC 1 11/17/2015 11 :28
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.7 UG/KG 1 11/17/2015 17:15
TOLUENE ND 5.7 UG/KG 1 11/17/2015 17:15
ETHYLBENZENE ND 5.7 UG/KG 1 11/17/2015 17:15
M+P-XYLENE ND 5.7 UG/KG 1 11/17/2015 17:15
O-XYLENE ND 5.7 UG/KG 1 11/17/2015 17:15
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 17:15
Sum DIBROMOFLUOROMETHANE 102 61-134 %REC 1 11/17/2015 17:15
Surr.• TOLUENE-D8 97 57-135 %REC 1 11/17/2015 17:15
Sum 4-BROMOFLUOROBENZENE 94 52-151 %REC 1 11/17/2015 17:15
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8.3 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 5 of 4714 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS06 Lab ID: 1511253-6
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :33 Percent Moisture: 7.4
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics ND 5.3 MG/KG 1 11/19/2015 13:29
Surr: O-TERPHENYL 87 49-114 %REC 1 11/19/2015 13:29
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.49 MG/KG 1 11/16/2015 17:51
Sum 2,3,4-TR/FLUOROTOLUENE 99 76-126 %REC 1 11/16/2015 17:51
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.6 UG/KG 1 11/17/2015 12:44
Sum NITROBENZENE-D5 52 28-113 %REC 1 11/17/2015 12:44
Sum 2-FLUOROBIPHENYL 52 41-106 %REC 1 11/17/2015 12:44
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.4 UG/KG 1 11/17/2015 17:36
TOLUENE ND 5.4 UG/KG 1 11/17/2015 17:36
ETHYLBENZENE ND 5.4 UG/KG 1 11/17/2015 17:36
M+P-XYLENE ND 5.4 UG/KG 1 11/17/2015 17:36
O-XYLENE ND 5.4 UG/KG 1 11/17/2015 17:36
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 17:36
Sum DIBROMOFLUOROMETHANE 101 61-134 %REC 1 11/17/2015 17:36
Sum TOLUENE-D8 98 57-135 %REC 1 11/17/2015 17:36
Sum 4-BROMOFLUOROBENZENE 97 52-151 %REC 1 11/17/2015 17:36
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 6.8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 6 of 4715 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1S
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS07 Lab ID: 1511253-7
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :39 Percent Moisture: 16.6
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 65 DMH 5.6 MG/KG 1 11/19/2015 14:00
Sum O-TERPHENYL 83 49-114 %REC 1 11/19/2015 14:00
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.53 MG/KG 1 11/16/2015 18:36
Sum 2,3,4-TRIFLUOROTOLUENE 90 76426 %REC 1 11/16/2015 18:36
GC/MS Semi-volatiles SW8274SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 22 16 UG/KG 4 11/17/2015 14:48
Sum NITROBENZENE-D5 58 28-113 %REC 4 11/17/2015 14:48
Surf: 2-FLUOROBIPHENYL 61 41-106 %REC 4 11/17/2015 14:48
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 17:58
TOLUENE ND 5.8 UG/KG 1 11/17/2015 17:58
ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 17:58
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 17:58
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 17:58
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 17:58
Sum DIBROMOFLUOROMETHANE 107 61-134 %REC 1 11/17/2015 17:58
Sum TOLUENE-D8 109 57-135 %REC 1 11/17/2015 17:58
Sum 4-BROMOFLUOROBENZENE 81 52-151 %REC 1 11/17/2015 17:58
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 7 of 4716 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1 5
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS08 Lab ID: 1511253-8
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :24 Percent Moisture: 13.9
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 210 DMH 5.7 MG/KG 1 11/19/2015 14:31
Surr O-TERPHENYL 100 49-114 %REC 1 11/19/2015 14:31
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.52 MG/KG 1 11/16/2015 18:58
Sum 2,3,4-TRIFLUOROTOLUENE 87 76-126 %REC 1 11/16/2015 18:58
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 41 15 UG/KG 4 11/17/2015 15:23
Surr: NITROBENZENE-O5 48 28-113 %REC 4 11/17/2015 15:23
Sum2-FLUOROBIPHENYL 58 41-106 %REC 4 11/17/2015 15:23
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 18:19
TOLUENE ND 5.8 UG/KG 1 11/17/2015 18:19
ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 18:19
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 18:19
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 18:19
TOTAL XYLENES ND 5 UG/KG 1 11/17/201518:19
Sun-: D/BROMOFLUOROMETHANE 106 61-134 %REC 1 11/17/2015 18:19
Surr TOLUENE-D8 113 57-135 %REC 1 11/17/2015 18:19
Sum 4-BROMOFLUOROBENZENE 79 52-151 %REC 1 11/17/2015 18:19
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.5 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 8 of 4717 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO9 Lab ID: 1511253-9
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :39 Percent Moisture: 10.3
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 21 DMH 5.5 MG/KG 1 11/19/2015 15:02
Sum O-TERPHENYL 84 49-114 %REC 1 11/19/2015 15:02
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.47 MG/KG 1 11/16/2015 19:20
Sum 213,4-TRIFLUOROTOLUENE 95 76-126 %REC 1 11/161201519:20
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 9.7 3.7 UG/KG 1 11/17/2015 15:24
Sur-: NITROBENZENE-D5 61 28-113 %REC 1 11/17/2015 15:24
Surr: 2-FLUOROBIPHENYL 62 41-106 %REC 1 11/17/2015 15:24
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 Prepay: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 18:40
TOLUENE ND 5.6 UG/KG 1 11/1712015 18:40
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 18:40
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 18:40
0-XYLENE ND 5.6 UG/KG 1 11/17/2015 18:40
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 18:40
Sum DIBROMOFLUOROMETHANE 103 61-134 %REC 1 11/17/2015 18:40
Sum TOLUENE-D8 97 57-135 %REC 1 11/17/2015 18:40
Sum 4-BROMOFLUOROBENZENE 96 52-151 %REC 1 11/17/2015 18:40
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8.1 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 9 of 4718 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS10 Lab ID: 1511253-10
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 : 10 Percent Moisture: 11 .0
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 170 DMH 5.6 MG/KG 1 11/19/2015 16:04
Sum O-TERPHENYL 88 49-114 %REC 1 11/19/2015 16:04
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.48 MG/KG 1 11/16/2015 19:42
Sum 2,3,4-TRIFLUOROTOLUENE 94 76-126 %REC 1 11/16/2015 19:42
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 26 15 UG/KG 4 11/17/2015 15:41
Sum NITROBENZENE-D5 63 28-113 %REC 4 11/17/2015 15:41
Sum 2-FLUOROBIPHENYL 63 41-106 %REC 4 11/17/2015 15:41
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 19:02
TOLUENE ND 5.6 UG/KG 1 11/17/2015 19:02
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 19:02
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:02
O-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:02
TOTAL XYLENES ND 5 UG/KG 1 11/17/201519:02
Sum DIBROMOFLUOROMETHANE 101 61-134 %REC 1 11/17/2015 19:02
Sum TOLUENE-D8 102 57-135 %REC 1 11/17/2015 19:02
Sumo-BROMOFLUOROBENZENE 88 52-151 %REC 1 11/17/201519:02
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.7 0.1 pH 1 11/18/2015
ALS Environmental -• FC
LIMS Version: 6.795 AR Page 10 of 4719 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS11 Lah TD: 1511253-11
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:45 Percent Moisture: 14.2
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 220 DMH 5.3 MG/KG 1 11/19/2015 16:35
Surr: O-TERPHENYL 97 49-114 %REC 1 11/19/2015 16:35
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 20:04
Surr: Z3,4-TRIFLUOROTOLUENE 81 76-126 %REC 1 11/16/2015 20:04
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 48 15 UG/KG 4 11/17/2015 15:59
Surr: NITROBENZENE-D5 84 28-113 %REC 4 11/17/2015 15:59
Surr 2-FLUOROBIPHENYL 69 41-106 %REC 4 11/17/2015 15:59
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.8 UG/KG 1 11/17/2015 19:24
TOLUENE ND 5.8 UG/KG 1 11/17/2015 19:24
ETHYLBENZENE ND 5.8 UG/KG 1 11/17/2015 19:24
M+P-XYLENE ND 5.8 UG/KG 1 11/17/2015 19:24
O-XYLENE ND 5.8 UG/KG 1 11/17/2015 19:24
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 19:24
Sum DIBROMOFLUOROMETHANE 108 61-134 %REC 1 11/17/2015 19:24
Surr: TOLUENE-D8 108 57-135 %REC 1 11/17/2015 19:24
Sum 4-BROMOFLUOROBENZENE 80 52-151 %REC 1 11/17/2015 19:24
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.9 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 11 of 4'10 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS12 Lab ID: 1511253-12
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:40 Percent Moisture: 11.5
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 110 DMH 5.4 MG/KG 1 11/19/2015 17:07
SUM O-TERPHENYL 85 49-114 %REC 1 11/19/2015 17:07
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.38 MG/KG 1 11/16/2015 20:26
Sum 2,3,4-TRIFLUOROTOLUENE 86 76-126 %REC 1 11/16/2015 20:26
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 42 15 UG/KG 4 11/17/2015 16:17
Sum NITROBENZENE-D5 74 28-113 %REC 4 11/17/2015 16:17
Sum 2-FLUOROBIPHENYL 68 41-106 %REC 4 11/17/2015 16:17
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.6 UG/KG 1 11/17/2015 19:50
TOLUENE ND 5.6 UG/KG 1 11/17/2015 19:50
ETHYLBENZENE ND 5.6 UG/KG 1 11/17/2015 19:50
M+P-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:50
O-XYLENE ND 5.6 UG/KG 1 11/17/2015 19:50
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 19:50
Surr. DIBROMOFLUOROMETHANE 102 61-134 %REC 1 11/17/2015 19:50
Surr: TOLUENE-O8 112 57-135 %REC 1 11/17/2015 19:50
Sum 4-BROMOFLUOROBENZENE 80 52-151 %REC 1 11/17/2015 19:50
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 Prepay: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 12 of 411 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS 13 Lab ID: 1511253-13
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:35 Percent Moisture: 10.2
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/16/2015 PrepBy: SDW
Diesel Range Organics 6.3 DMH 5.5 MGIKG 1 11/19/2015 17:38
Surr: O-TERPHENYL 91 49-114 %REC 1 11/19/2015 17:38
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.47 MG/KG 1 11/16/2015 20:48
Sum 2,3,4-TRIFLUOROTOLUENE 96 76-126 %REC 1 11/16/2015 20:48
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE ND 3.7 UG/KG 1 11/17/2015 15:44
Sum NITROBENZENE-D5 47 28-113 %REC 1 11/17/2015 15:44
Sum 2-FLUOROBIPHENYL 48 41-106 %REC 1 11/17/2015 15:44
GC/MS Volatiles SW8260 Prep Date: 11/1712015 PrepBy: JXK
BENZENE ND 5.5 UG/KG 1 11/17/2015 20:12
TOLUENE ND 5.5 UG/KG 1 11/17/2015 20:12
ETHYLBENZENE ND 5.5 UG/KG 1 11/17/2015 20:12
M+P-XYLENE ND 5.5 UG/KG 1 11/17/2015 20:12
O-XYLENE ND 5.5 UG/KG 1 11/17/2015 20:12
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 20:12
Sum DIBROMOFLUOROMETHANE 105 61-134 %REC 1 11/17/2015 20:12
Sum TOLUENE-DA 98 57-135 %REC 1 11/17/2015 20:12
Sum 4-BROMOFLUOROBENZENE 92 52-151 %REC 1 11/17/2015 20:12
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 8 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 13 of 4'12 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS14 Lab ID: 1511253-14
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:28 Percent Moisture: 14.1
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 190 LDMHZ 5.6 MG/KG 1 11/19/2015 18:09
Sum O-TERPHENYL 89 49-114 %REC 1 11/19/2015 18:09
Gasoline Range Organics SW8015 Prep Date: 11/16/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.49 MG/KG 1 11/16/2015 21 :10
Sum 2,3,4-TRIFLUOROTOLUENE 89 76-126 %REC 1 11/16/2015 21 :10
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 45 15 UG/KG 4 11/17/2015 16:11
Sun-: NITROBENZENE-D5 62 28-113 %REC 4 11/17/2015 16:11
Surr: 2-FLUOROBIPHENYL 66 41-106 %REC 4 11/17/2015 16:11
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 PrepBy: JXK
BENZENE ND 5.7 UG/KG 1 11/17/2015 20:37
TOLUENE ND 5.7 UG/KG 1 11/17/2015 20:37
ETHYLBENZENE ND 5.7 UG/KG 1 11/17/2015 20:37
M+P-XYLENE ND 5.7 UG/KG 1 11/17/2015 20:37
O-XYLENE ND 5.7 UG/KG 1 11/17/2015 20:37
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 20:37
Sum DIBROMOFLUOROMETHANE 100 61-134 %REC 1 11/17/2015 20:37
Sum TOLUENE-D8 104 57-135 %REC 1 11/17/2015 20:37
Sum 4-BROMOFLUOROBENZENE 84 52-151 %REC 1 11/17/2015 20:37
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 Prepay: TLB
PASTE PH 7.9 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 14 of 413 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS15 Lab ID: 1511253-15
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:20 Percent Moisture: 8.5
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Diesel Range Organics SW8015M Prep Date: 11/18/2015 PrepBy: SDW
Diesel Range Organics 130 DMH 5.4 MG/KG 1 11/19/2015 18:40
Surr: O-TERPHENYL 91 49-114 %REC 1 11/19/2015 18:40
Gasoline Range Organics SW8015 Prep Date: 11116/2015 PrepBy: TWK
GASOLINE RANGE ORGANICS ND 0.5 MG/KG 1 11/16/2015 21 :32
Sum 2,3,4-TRIFLUOROTOLUENE 100 76-126 %REC 1 11/16/2015 21 :32
GC/MS Semi-volatiles SW8270SIM Prep Date: 11/1312015 PrepBy: ACK
NAPHTHALENE 52 14 UG/KG 4 11/17/2015 16:38
Sum NITROBENZENE-D5 58 28-113 %REC 4 11/17/2015 16:38
Sum 2-FLUOROBIPHENYL 68 41-106 %REC 4 11/17/2015 16:38
GC/MS Volatiles SW8260 Prep Date: 11/17/2015 Prepay: JXK
BENZENE ND 5.5 UG/KG 1 11/17/2015 21:02
TOLUENE ND 5.5 UG/KG 1 11/17/2015 21:02
ETHYLBENZENE ND 5.5 UG/KG 1 11/17/2015 21:02
M+P-XYLENE ND 5.5 UG/KG 1 11/17/2015 21:02
O-XYLENE ND 5.5 UG/KG 1 11/17/2015 21:02
TOTAL XYLENES ND 5 UG/KG 1 11/17/2015 21 :02
Sum DIBROMOFLUOROMETHANE 105 61-134 %REC 1 11/17/2015 21 :02
Sum TOLUENE-D8 102 57-135 %REC 1 11/17/2015 21 :02
Sum 4-BROMOFLUOROBENZENE 88 52-151 %REC 1 11/17/2015 21 :02
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
PASTE PH 7.6 0.1 pH 1 11/18/2015
ALS Environmental -- FC
LiMS Version: 6/95 AR Page 15 of 414 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 Composite Lab ID: 1511253- 16
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 12:05 Percent Moisture: 12.0
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
GC/MS Semi-volatiles SW8270S1M Prep Date: 11/13/2015 PrepBy: ACK
NAPHTHALENE 25 3.7 UG/KG 1 11/17/2015 12:16
ACENAPHTHENE 4.5 3.7 UGIKG 1 11/17/2015 12:16
FLUORENE 9.1 3.7 UG/KG 1 11/17/2015 12:16
ANTHRACENE ND 3.7 UG/KG 1 11/17/2015 12:16
FLUORANTHENE ND 3.7 UG/KG 1 11/17/2015 12:16
PYRENE 15 3.7 UG/KG 1 11/17/2015 12:16
BENZO(A)ANTHRACENE ND 3.7 UG/KG 1 11/17/2015 12:16
CHRYSENE 41 3.7 UG/KG 1 11/17/2015 12:16
BENZO(B)FLUORANTHENE 9.7 3.7 UG/KG 1 11/17/2015 12:16
BENZO(K)FLUORANTHENE ND 3.7 UG/KG 1 11/17/2015 12:16
BENZO(A)PYRENE ND 3.7 UG/KG 1 11/17/2015 12:16
INDENO(1 ,2,3-CD)PYRENE ND 3.7 UG/KG 1 11/17/2015 12:16
DIBENZO(A,H)ANTHRACENE ND 3.7 UG/KG 1 11/17/2015 12:16
Sum NITROBENZENE-D5 56 28-113 %REC 1 11/17/2015 12:16
Sum 2-FLUOROBIPHENYL 56 41-106 %REC 1 11/17/2015 12:16
Sum TERPHENYL-D14 60 25-147 %REC 1 11/17/2015 12:16
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 16 of 415 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample lD: Miller 1 SS01 Lab ID: 1511253-17
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:16 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy. CDR
ARSENIC 4.3 0.19 MG/KG 10 11/20/2015 12:59
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 17 of 416 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS02 Lab ID: 1511253-18
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:51 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.7 0.19 MG/KG 10 11/20/2015 13:20
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 18 of 4'27 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS03 Lab ID: 1511253-19
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:05 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 2.8 0.19 MG/KG 10 11/20/2015 13:24
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 19 of 4'JZS of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-I 5
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO4 Lab ID: 1511253-20
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :05 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 7.1 0.19 MG/KG 10 11/20/2015 13:40
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 20 of 4129 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS05 Lab ID: 1511253-21
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 3.7 0.19 MGIKG 10 11/20/2015 13:44
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 21 of 4230 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-IS
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS06 Lab ID: 1511253-22
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:33 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 2 0.19 MG/KG 10 11/20/2015 13:47
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 22 of 4'01 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-i5
Project: Noble Miller Spreadfield Work Order: 1511253
Sample lD: Miller 1 SS07 Lab ID: 1511253-23
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11:39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 6.6 0.19 MG/KG 10 11/20/2015 13:51
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 23 of 4732 of 63
ALS Environmental r- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO8 Lab ID: 1511253-24
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :24 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 6.6 0.19 MG/KG 10 11/20/2015 13:54
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 24 of CO of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS09 Lab ID: 1511253-25
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.8 0.19 MG/KG 10 11/20/2015 13:58
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 25 of 4734 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample lD: Miller 1 SS10 Lab ID: 1511253-26
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 11 :10 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.9 0.19 MG/KG 10 11/20/201514:01
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 26 of 4$5 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS11 Lab ID: 1511253-27
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 7.8 0.19 MG/KG 10 11/20/2015 14:05
ALS Environmental -- FC
L{MS Version: 6.795 AR Page 27 of 4736 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1.5
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS12 Lab ID: 1511253-28
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:40 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 4.4 0.2 MG/KG 10 11/20/2015 14:08
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 28 of 4'$7 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS13 Lab ID: 1511253-29
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:35 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 2.5 0.19 MG/KG 10 11/20/2015 14:12
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 29 of 4138 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-I5
Project: Noble Miller Spreadfield Work Order: 1511253
Sample 1D: Miller 1 SS14 Lab ID: 1511253-30
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:28 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 6 0.19 MG/KG 10 11/20/2015 14:28
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 30 of 4139 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS15 Lab ID: 1511253-31
Legal Location: Matrix: SOIL
Collection Date: 11/12/2015 10:20 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICPMS Metals SW6020 Prep Date: 11/19/2015 PrepBy: CDR
ARSENIC 5 0.19 MG/KG 10 11/20/2015 14:31
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 31 of 4710 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSOI Lab ED: 1511253-32
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 : 16 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
1CP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 350 10 MG/L 10 11/18/2015 12:00
MAGNESIUM 71 10 MG/L 10 11/18/2015 12:00
SODIUM 670 10 MG/L 10 11/18/2015 12:00
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 5800 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 8.6 0.54 NU 10 11/18/2015 12:00
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 32 of 4741 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS02 Lab ID: 1511253-33
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11:51 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 53 10 MG/L 10 11/18/2015 12:01
MAGNESIUM ND 10 MG/L 10 11/18/2015 12:01
SODIUM ND 10 MG/L 10 11/18/2015 12:01
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 340 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.33 s 0.54 NU 10 11/18/2015 12:01
ALS Environmental -- FC
LIMS Version: 6.795 AR. Page 33 of 4712 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS03 Lab ID: 1511253-34
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :05 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 37 10 MG/L 10 11/18/2015 12:02
MAGNESIUM 13 10 MG/L 10 11/18/2015 12:02
SODIUM 27 10 MGIL 10 11/18/2015 12:02
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 460 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.97 0.54 NU 10 11/18/2015 12:02
ALS Environmental -- FC
LIMS Verson: 6.795 AR Page 34 of 4743 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Sprcadfield Work Order: 1511253
Sample ID: Miller 1 SSO4 Lab ID: 1511253-35
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :05 Percent Moisture:
Report Dilution
Analyses Result Quad Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 450 10 MG/L 10 11/18/2015 12:03
MAGNESIUM 60 10 MG/L 10 11/18/2015 12:03
SODIUM 420 10 MGIL 10 11/18/2015 12:03
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 5000 1 umhos/cm 1 11/19/2015
SATU RATION
SODIUM ADSORPTION RATIO 4S 0.54 NU 10 11/18/2015 12:03
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 35 of 4744 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO5 Lab ID: 1511253-36
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 69 10 MG/L 10 11118/201512:04
MAGNESIUM 10 10 MG/L 10 11/18/2015 12:04
SODIUM ND 10 MG/L 10 11/18/2015 12:04
Sodium Adsorption Ratio USDA60 Prep Date: 11/1812015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 400 1 umhoslcm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.3 s 0.54 NU 10 11/18/2015 12:04
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 36 of 4745 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-1.5
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO6 Lab ID: 1511253-37
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :33 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 35 10 MGIL 10 11/18/2015 12:05
MAGNESIUM 12 10 MG/L 10 11/18/2015 12:05
SODIUM ND 10 MG/L 10 11/18/2015 12:05
Sodium Adsorption Ratio USDA60 Prep Date: 11/1812015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 310 1 umhoslcrn 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.37 S 0.54 NU 10 11/18/2015 12:05
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 37 of 4116 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS07 Lab ID: 1511253-38
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 85 10 MG/L 10 11/18/2015 12:06
MAGNESIUM 19 10 MG/L 10 11/18/2015 12:06
SODIUM 97 10 MG/L 10 11/18/2015 12:06
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 1200 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 2.5 0.54 NU 10 11/18/2015 12:06
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 38 of 4717 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SSO8 Lab ID: 1511253-39
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :24 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 510 10 MG/L 10 11/18/2015 12:08
MAGNESIUM 80 10 MG/L 10 11/18/2015 12:08
SODIUM 890 10 MG/L 10 11/18/2015 12:08
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 7700 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 9.6 0.54 NU 10 11/18/2015 12:08
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 39 of 4718 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS09 Lab ID: 1511253-40
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11 :39 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 93 10 MG/L 10 11/18/2015 12:09
MAGNESIUM 13 10 MG/L 10 11/18/2015 12:09
SODIUM 57 10 MG/L 10 11118/2015 12:09
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 1200 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 1.5 0.54 NU 10 11/18/2015 12:09
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 40 of 4749 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS10 Lab ID: 1511253-41
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 11: 10 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 370 10 MG/L 10 11/18/2015 12:10
MAGNESIUM 46 10 MG/L 10 11/18/2015 12:10
SODIUM 450 10 MG/L 10 11/18/2015 12:10
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 4600 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 5S 0.54 NU 10 11/18/2015 12:10
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 41 of 4-$0 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS11 Lab ID: 1511253-42
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:45 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 Prepay: SMW
CALCIUM 500 10 MG/L 10 11118/201512:14
MAGNESIUM 68 10 MGIL 10 11118/2015 12:14
SODIUM 530 10 MG/L 10 11/18/2015 12:14
Sodium Adsorption Ratio USDA60 Prep Date: 11/1812015 PrepBy TLB
ELECTRICAL CONDUCTIVITY @ 5600 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 5.9 0.54 NU 10 11/18/2015 12:14
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 42 of 4.51 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS12 Lab ID: 1511253-43
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:40 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 260 10 MG/L 10 11/18/2015 12:15
MAGNESIUM 33 10 MG/L 10 11/18/2015 12:15
SODIUM 190 10 MG/L 10 11/18/2015 12:15
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 2800 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 2.9 0.54 NU 10 11/18/2015 12:15
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 43 of 4'$2 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sampler!): Miller 1 SS13 Lab ID: 1511253-44
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:35 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA80 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 44 10 MG/L 10 11/18/2015 12:16
MAGNESIUM 12 10 MG/L 10 11/18/2015 12:16
SODIUM 18 10 MG/L 10 11/18/2015 12:16
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 400 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 0.61 0.54 NU 10 11/18/2015 12:16
ALS Environmental -• FC
LIMS Version: 6.795 AR Page 44 of 4'{3 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS14 Lab ID: 1511253-45
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:28 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 430 10 MG/L 10 11/18/201512:17
MAGNESIUM 60 10 MG/L 10 11/18/2015 12:17
SODIUM 270 10 MG/L 10 11/18/2015 12:17
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 4300 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 3.2 0.54 NU 10 11/18/2015 12:17
ALS Environmental -- FC
LIMS Version: 6.795 AR Page 45 of 4-$4 of 63
ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS15 Lab ID: 1511253-46
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:20 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
ICP Metals USDA60 Prep Date: 11/13/2015 PrepBy: SMW
CALCIUM 490 10 MG/L 10 11/18/2015 12:18
MAGNESIUM 84 10 MG/L 10 11118/201512:18
SODIUM 900 10 MG/L 10 11118/201512:18
Sodium Adsorption Ratio USDA60 Prep Date: 11/18/2015 PrepBy: TLB
ELECTRICAL CONDUCTIVITY @ 7500 1 umhos/cm 1 11/19/2015
SATURATION
SODIUM ADSORPTION RATIO 9S 0.54 NU 10 11/18/2015 12:18
ALS Environmental -- FC
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ALS Environmental -- FC SAMPLE SUMMARY REPORT
Client: Olsson Associates Date: 04-Dec-15
Project: Noble Miller Spreadfield Work Order: 1511253
Sample ID: Miller 1 SS 15 Lab ID: 1511253-46
Legal Location: Matrix: SATEXTRACT
Collection Date: 11/12/2015 10:20 Percent Moisture:
Report Dilution
Analyses Result Qual Limit Units Factor Date Analyzed
Explanation of Qualifiers
Radiochemistry:
U or ND - Result is less than the sample specific MDC. M3 - The requested MDC was not met, but the reported
Y1 - Chemical Yield is in control at 100-110%. Quantitative yield is assumed, activity is greater than the reported MDC.
Y2 - Chemical Yield outside default limits.
L - LCS Recovery below lower control limit.
W - DER is greater than Warning Limit of 1.42 H LCS Recovery above upper contra limit.
' - Aliquot Basis is 'As Reeived while the Report Basis is 'Dry Weight'. P LCS, Matrix Spike Recovery within control limits.
c
# - Aliquot Basis is 'Dry Weight' while the Report Basis is 'As Received'. N - Matrix Spike Recovery outside control limits
G - Sample density differs by more than 15% of LCS density. NC - Not Calculated for duplicate results less than 5 times MDC
D - DER is greater than Control Limit B - Analyte concentration greater than MDC.
M - Requested MDC not met. B3 - Analyte concentration greater than MDC but less than Requested
LT - Result is less than requested MDC but greater than achieved MDC. MDC.
Inorganics:
B - Result is less than the requested reporting limit but greater than the Instrument method detection limit (MDL).
U or ND - Indicates that the compound was analyzed for but not detected.
E - The reported value is estimated because of the presence of interference. An explanatory note may be included in the narrative.
M - Duplicate injection precision was not met.
N - Spiked sample recovery not within control limits. A post spike is analyzed for all ICP analyses when the matrix spike and or spike
duplicate fall and the native sample concentration is less than four times the spike added concentration.
Z - Spiked recovery not within control limits. An explanatory note may be included in the narrative.
' - Duplicate analysis (relative percent difference) not within control limits.
S - SAR value is estimated as one or more analytes used in the calculation were not detected above the detection limit.
Organics:
U or ND - Indicates that the compound was analyzed for but not detected.
B - Analyte is detected in the associated method blank as well as in the sample. It indicates probable blank contamination and warns the data user.
E - Analyte concentration exceeds the upper level of the calibration range.
J - Estimated value. The result is less than the reporting limit but greater than the instrument method detection limit (MDL).
A - A tentatively identified compound is a suspected aldol-condensation product.
X - The analyte was diluted below an accurate quantitation level.
• - The spike recovery is equal to or outside the control criteria used.
+ - The relative percent difference (RPD) equals or exceeds the control criteria.
G - A pattern resembling gasoline was detected in this sample.
D - A pattern resembling diesel was detected in this sample.
M - A pattern resembling motor oil was detected in this sample.
C - A pattern resembling crude oil was detected in this sample.
4 - A pattern resembling JP-4 was detected in this sample.
5 - A pattern resembling JP-5 was detected in this sample.
H - Indicates that the fuel pattern was in the heavier end of the retention time window for the analyte of interest.
L - Indicates that the fuel pattern was In the lighter end of the retention time window for the analyte of interest.
Z - This flag indicates that a significant fraction of the reported result did not resemble the patterns of any of the following petroleum hydrocarbon products:
- gasoline
- JP-8
- diesel
- mineral spirits
- motor al
- Stoddard solvent
- bunker C
ALS Environmental -- FC
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ALS Environmental -- FC Date: 12/4/2015 1:54:
Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: HC151116-6-1 Instrument ID: FUELS-1 Method: SW8015
LCS Sample ID: HC151116-6 Units: MG/KG Analysis Date: 11/161201510:22
Client ID: Run ID: HC151116.6A Prep Date: 11/16/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
GASOLINE RANGE ORGANICS 2.58 0.5 2.5 103 79-118 20
Sum 2,3,4-TRIFLUOROTOLUENE 0.578 0.5 116 76-126
MB Sample ID: HC151116-6 Units: MG/KG Analysis Date: 11/16/2015 11:39
Client ID: Run ID: HC151116-6A Prep Date: 11/16/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
GASOLINE RANGE ORGANICS NO 0.5
Sum 2,3,4-TRIFLUOROTOLUENE 0.508 0.5 102 76-126
The following samples were analyzed In this batch: 1511253-1 1511253-2 1511253-3
1511253-4 1511253-5 1511253-6
1511253-7 1511253-8 1511253-9
1511253-10 1511253-11 1511253-12
1511253-13 1511253-14 1511253-15
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: HC151118-100.1 Instrument ID: FUELS-1 Method: SW8015M
LCS Sample ID: HC151118.100 Units: MG/KG Analysis Date: 11/19/2015 20:13
Client ID: Run ID: HC151119-7A Prep Date: 11/18/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua'
Diesel Range Organics 127 5 125 102 76-124 20
Sum 0-TERPHENYL 4.42 8.25 71 49-114
MB Sample ID: HC151118-100 Units: MG/KG Analysis Date: 11/19/2015 09:54
Client ID: Run ID: HC151119-7A Prep Date: 11/1812015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Dual
Diesel Range Organics ND 5
Sum 0-TERPHENYL 4.7 625 75 49-114
MS Sample ID: 1511253-15 Units: MG/KG Analysis Date: 11/19/2015 19:11
Client ID: Miller 1 SS15 Run ID: HC151119-7A Prep Date: 11/18/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua'
Diesel Range Organics 291 5.21 130 130 124 76-124 20
Sum 0-TERPHENYL 6 32 6.51 97 49-114
MSD Sample ID: 1511253-15 Units: MG/KG Analysis Date: 11/19/2015 19:42
Client ID: Miller 1 SS15 Run ID: HC151119-7A Prep Date: 11/18/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua!
Diesel Range Organics 283 5.3 133 130 116 76.124 291 3 20
Sum 0-TERPHENYL 6.47 6.63 98 49-114 2
The following samples were analyzed in this batch: 1511253-1 1511253-2 1511253-3
1511253-4 1511253-5 1511253-6
1511253-7 1511253-8 1511253-9
1511253-10 1511253-11 1511253-12
1511253-13 1511253-14 1511253-15
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: IP151119.2.1 Instrument ID: ICPMS2 Method: SW6020
LCS Sample ID: IP151119-2 Units: MG/KG Analysis Date: 11120/2015 12:56
Client ID: Run ID: 1M151120-10A1 Prep Date: 11/1912015 DF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Quai
ARSENIC 8.83 0.2 10 88 80-120 20
MB Sample ID: IP151119-2 Units: MG/KG Analysis Date: 11/20/2015 12:52
Client ID: Run ID: IM151120-10A1 Prep Date: 11119/2015 DF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua'
ARSENIC ND 0.2
MS Sample ID: 1511253-17 Units: MG/KG Analysis Date: 11/20/2015 13:10
Client ID: Miller 1 SS01 Run ID: IM151120-10A1 Prep Date: 11/19/2015 OF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
ARSENIC t2 8 0.188 9.38 4.3 91 75-125 20
MSD Sample ID: 1511253-17 Units: MG/KG Analysis Date: 11/20/2015 13:13
Client ID: Miller 1 SS01 Run ID: IM151120.10A1 Prep Date: 11/19/2015 DF: 10
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua'
ARSENIC 12.2 0.188 9.4 4.3 84.1 75-125 12.8 5 20
The following samples were analyzed in this batch: 1511253-17 1511253-18 1511253-19
1511253-20 1511253-21 1511253-22
1511253-23 1511253-24 1511253-25
1511253-26 1511253-27 1511253-28
1511253-29 1511253-30 1511253-31
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: EX151113-1-1 Instrument ID: HPSV1 Method: SW8270SIM
MS Sample ID: 1511253-3 Units: UGIKG Analysis Date: 11/17/2015 10:21
Client ID: Miller 1 SSO3 Run ID: SV151117-2 Prep Date: 11/13/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qual
NAPHTHALENE 39.3 3.63 72.5 3.6 54 40-107 30
Sun: NITROBENZENE-D5 42 72.5 58 28-113
Sum 2-FLUOROBIPHENYL 40.9 72.5 56 41-106
MSD Sample ID: 15112534 Units: UG/KG Analysis Date: 11/17/2015 10:41
Client ID: Miller 1 SSO3 Run ID: SV151117-2 Prep Date: 11/13/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua,
NAPHTHALENE 39.7 3.61 72.2 3.6 55 40-107 39.3 1 30
Surr: NITROBENZENE-D5 41.9 72.2 58 28-113 0
Sum 2-FLUOROBIPHENYL 39.5 72.2 55 41-106 4
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: EX151113.1-2 Instrument ID: HPSV1 Method: SW8270SIM
LCS Sample ID: EX151113-1 Units: UG/KG Analysis Date: 11/17/2015 09:23
Client ID: Run ID: SV151117-2 Prep Date: 11/13/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua/
NAPHTHALENE 42.4 3.33 66.7 64 40-107 30
ACENAPHTHENE 40.9 3.33 66.7 61 46-108 30
FLUORENE 41 3.33 66.7 61 49-108 30
ANTHRACENE 40 3.33 66.7 6O 53-107 30
FLUORANTHENE 41.7 3.33 66.7 62 54-114 30
PYRENE 44.9 3.33 66.7 67 46-123 30
BENZO(A)ANTHRACENE 43.6 3.33 66.7 65 52-111 30
CHRYSENE 42.3 3.33 66.7 63 53-112 30
BENZO(B)FLUORANTHENE 40.9 3.33 66.7 61 45-114 30
BENZO(K)FLUORANTHENE 47.3 3.33 66.7 71 45-123 30
BENZO(A)PYRENE 41.5 3.33 66.7 62 50-111 30
INDENO(1,2,3-CD)PYRENE 37.1 3.33 66.7 56 38-121 30
DIBENZO(A,H)ANTHRACENE 38.9 3.33 66.7 58 41-125 30
Sum NITROBENZENE-D5 44.2 66.7 66 28-113
Surr: 2-FLUOROBIPHENYL 42.7 66.7 64 41-106
Sum TERPHENYL-O14 43.8 66.7 66 25-147
MB Sample ID: EX151113-1 Units: UG/KG Analysis Date: 11/17/2015 09:03
Client ID: Run ID: SV151117-2 Prep Date: 11/13/2015 OF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua'
NAPHTHALENE ND 5,3
ACENAPHTHENE ND 3.3
FLUORENE ND 3.3
ANTHRACENE ND 3.3
FLUORANTHENE ND 33
PYRENE ND 33
BENZO(A)ANTHRACENE ND 3.3
CHRYSENE ND 3.3
BENZO(B)FLUORANTHENE ND 33
BENZO(K)FLUORANTHENE ND 3.3
BENZO(A)PYRENE ND 3.3 -
INDENO(1,2,3-CD)PYRENE ND 3.3
DIBENZO(A,H)ANTHRACENE ND 3.3
Sum NITROBENZENE--05 43.6 66.7 65 28-113
Sum 2-FLUOROBIPHENYL 42 66.7 63 41-106
Sum TERPHENYL-D14 46.3 66.7 69 25-147
The following samples were analyzed In this batch: 1511253-2 1511253-3 1511253-5 1
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: VL151117-2-1 Instrument ID: HPV1 Method: SW8260
LCS Sample ID: VL151117-2 Units: UG/KG Analysis Date: 11/17/2015 14:38
Client ID: Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua!
BENZENE 39.4 5 40 98 73-126 30
TOLUENE 40.6 5 40 102 71-127 30
ETHYLBENZENE 41.2 5 40 103 74-127 30
M+P-XYLENE 86.6 5 80 108 79-126 30
O-XYLENE 42/ 5 40 107 77-125 30
Sum 52 50 104 61-134
DIBROMOFLUOROMETHANE
Sum TOLUENE-D8 47.9 50 96 57-135
Surr. 4- 48/ 50 97 52-151
BROMOFLUOROBENZENE
LCSD Sample ID: VL151117-2 Units: UGIKG Analysis Date: 11117/2015 14:59
Client ID: Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua'
BENZENE 40 5 40 100 73-126 39.4 2 30
TOLUENE 41.8 5 40 104 71-127 40.6 3 30
ETHYLBENZENE 42.4 5 40 106 74127 41.2 3 30
M+P-XYLENE B7.5 5 80 109 79-126 86.6 1 30
O-XYLENE 42.9 5 40 107 77-125 42.7 0 30
Sum 50.7 50 101 61-134 3
DIBROMOFLUOROMETHANE
Sum TOLUENE-D8 48.6 50 97 57-135 1
SUIT: 4- 49 50 98 52-151 1
BROMOFLUOROBENZENE
MB Sample ID: VL151117-2 Units: UG/KG Analysis Date: 11/1712015 15:21
Client ID: Run ID: VL151117.2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLlmit SPK Val Value %REC Limit Level Ref RPD Limit Qum
BENZENE ND 5
TOLUENE ND 5
ETHYLBENZENE ND 5
M+P-XYLENE ND 5
O-XYLENE ND 5 - - - -
TOTAL XYLENES ND 5
Sum 49.8 50 100 61-134
DIBROMOFLUOROMETHANE
Suit TOLUENE-D8 48 50 96 57-135
Sum 4- 47/ 50 95 52-151
BROMOFLUOROBENZENE
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Client: Olsson Associates QC BATCH REPORT
Work Order: 1511253
Project: Noble Miller Spreadfield
Batch ID: V1151117-2-1 Instrument ID: HPV1 Method: SW8280
MS Sample ID: 1511253-15 Units: UG1KG Analysis Date: 11/17/2015 21:26
Client ID: Miller 1 SS15 Run ID: VL151117-2A Prep Date: 11/17/2015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value voREC Limit Level Ref RPD Limit Qua'
BENZENE 26.2 5A5 43.6 5.5 60 73-126 30 •
TOLUENE 22.1 5.45 43.6 5.5 51 71-127 30 •
ETHYLBENZENE 17A 5.45 43.6 5.5 40 74-127 30 *
M+P-XYLENE 34.8 5.45 87.3 5.5 40 79-126 30 •
O-XYLENE 18.6 5.45 43.6 5.5 43 77-125 30 •
Sun: 58.3 54.5 107 61-134
DIBROMOFLUOROMETHANE
Sum TOLUENE-D8 54.3 54.5 100 57-135
Sumo 47.5 54.5 87 52-151
BROMOFLUOROBENZENE
MSD Sample ID: 1511253-15 Units: UG/KG Analysis Date: 11/17/2015 21:50
Client ID: Miller 1 SS15 Run ID: 111151117-2A Prep Date: 11/1712015 DF: 1
SPK Ref Control Decision RPD RPD
Analyte Result ReportLimit SPK Val Value %REC Limit Level Ref RPD Limit Qua'
BENZENE 24.1 5.44 43.5 5.5 55 73-126 26.2 8 30 •
TOLUENE 19.6 5.44 43.5 5.5 45 71-127 22.1 12 30
ETHYLBENZENE 14 5.44 43.5 5.5 32 74-127 17.4 22 30 •
M+P-XYLENE 27.2 5.44 87.1 5.5 31 79-126 34.8 25 30 •
O-XYLENE 15.2 5.44 43.5 5.5 35 77-125 18.6 20 30 '
Sum 56.7 54.4 104 61-134 3
DIBROMOFLUOROMETHANE
Sum TOLUENE-D8 54.4 54.4 100 57-135 0
Surr: 4- 47.7 54.4 88 52-151 0
BROMOFLUOROBENZENE
The following samples were analyzed In this batch: 1511253-1 1511253-2 1511253-3
1511253-4 1511253-5 1511253-6
1511253-7 1511253.8 1511253-9
1511253-10 1511253-11 1511253-12
1511253-13 1511253-14 1511253-15
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