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HomeMy WebLinkAbout20252981.tiffINVENTORY OF ITEMS FOR CONSIDERATION Applicant NGL Water Solutions DJ LLC Case Number USR24-0019 Submitted or Prepared Prior to Hearing At Hearing 1 Jeri Yarbrough letter received September 4, 2024 X — 2 Gina Michel, Dave and Joe Sack — letter received September 23, 2024 X 3 Reininger — letter received September 15, 2024 X Travis 4 Colleen O'Neil letter received September 17, 2024 X — 5 Sharon O'Neil — letter received September 25, 2024 X 6 Rachel Brown email received September 17, 2024 X — 7 Tony Hale email via Jeri Yarbrough received December 12, 2023 X 8 James Stewardson — letter received October 21, 2024 X 9 Hale letter dated September 17, 2024 X Tony — 10 Environmental 9, 2024 and Animal Defense (eaDefense) — letter received October X 11 Dr. Chelsea Luedke, DVM — letter received October 16, 2024 X 12 Response from applicant February 26, 2025 Letter addressing concerns X — 13 Response created p equal from Application and ppX how to tell February 26, 2025 — All Biochars are not them apart 14 Response Laboratories from (PAH applicant and PCB February test 26, results) 2025 Northern California Accutest X — 15 Response from applicant February 26, 2025 Emissions summary X — 16 letter Response from applicant February 26, 2025 — Response to eaDefense X 17 Response site from applicant February 26, 2025 CDPHE requirements for the X — 18 Biochar Community Meeting notice and summary October 12, 2024 X 19 Colleen O'Neil — letter received October 7, 2025 X 20 Alexa 2025 McKay — CDPHE enforcement reports email received October 7, X 21 Jeremy October McKay 7, 2025 Environmental and Animal Defense, email received X — I hereby certify that the twenty one items identified herein were submitted to the Department of Planning Services at or prior to the scheduled Planning Commissioners' hearing. OvcQ9,_, Diana Aungst, Planner Diana Aungst From: Sent: To: Subject: Jeri Yarbrough <yarbroughacres@icloud.com> Wednesday, September 4, 2024 12:27 PM Diana Aungst Bio char Caution: This email originated from outside of Weld County Government. Do not click links or open attachments unless you recognize the sender and know the content is safe. Hi Diana I got your post card in the mail. Does all the objections need to be written up by sept 23rd? Of course I oppose the special use permit for the Bio Char facility, it will affect my right to farm my alfalfa field located next to property . With the run off of water and the historic flood irrigation. The concerns for my health and my animals from the dust and smoke. The dust from the charcoal can cause cancer. Also from burning can cause contamination to the ground. I will loose income from my horse boarding facility my boarders plan on leaving if this is approved they have concerns about the welfare of their horses health, being that they will be 100 feet from Bio Char. Also the wildlife will be impacted from the bald eagles to the pelicans, water fowl and hawks. I have hired an environment and animal welfare lawyers. They will be contacting you also , I will be sending the articles I have found about the health concerns living next to bio char. Also Bio char was on an episode dirtiest jobs. This is not the place for such a facility located so close to all of our homes. Jeri Yarbrough 303-210-8974 Sent from my iPhone 1 Diana Aungst From: Sent: To: Subject: Jeri Yarbrough <yarbroughacres@icloud.com> Wednesday, September 4, 2024 12:33 PM Diana Aungst Bio char Caution: This email originated from outside of Weld County Government. Do not click links or open attachments unless you recognize the sender and know the content is safe. Articles about bio char 1 Environ Sci Pollut Res (2014) 21:3646-3652 DOI 10.1007/s11356-013-2334-1 RESEARCH ARTICLE Biochar production increases the polycyclic aromatic hydrocarbon content in surrounding soils and potential cancer risk Marcin Kusmierz • Patryk Oleszczuk Received: 28 August 2013 /Accepted: 4 November 2013 /Published online: 26 November 2013 CO The Author(s) 2013. This article is published with open access at Springerlink.com Abstract The objectives of the study were the identification of the source of contamination of soils and estimation of the potential cancer risk that may be caused by contact with soils situated in the vicinity of biochar production sites. Samples of soils collected in the immediate vicinity of traditional biochar- producing plants, located within the area of the Bieszczady National Park (Poland), were analysed for the content of polycyclic aromatic hydrocarbons (PAHs). The sum of the content of 16 PAHs varied within the range of 1.80-101.3 µg/ g, exceeding the norms permitted in many European coun- tries. The calculated coefficients on the basis of which one can determine the origin of PAHs (molecular diagnostic ratios) demonstrated that the potential source of PAHs in the soils may be processes related with the production of biochar. Estimation on the basis of the results of incremental lifetime cancer risks (ILCRs) within the range of 2.33.1O 4-1.05.1O indicated that the soils studied may constitute a significant cancer risk for persons who have contact with them. The values of ILCRS should be considered as at least high, which permits the conclusion that sites of that type may create a hazard to human health. Keywords PAHs • Biochar • Soil • Risk assessment • Molecular diagnostic ratios • Incremental lifetime cancer risks Responsible editor: Philippe Garrigues Electronic supplementary material The online version of this article (doi:10.1007/s 11356-013-2334-1) contains supplementary material, which is available to authorized users. M. Kusmierz • P. Oleszczuk (�) Department of Environmental Chemistry, Faculty of Chemistry, 3 Maria Curie-Sklodowska Square, Lublin 20-031, Poland e-mail: patryk.oleszczuk@poczta.umcs.lublin.pl Introduction The method of sequestration (capture and long-term storage) of atmospheric CO2 proposed by Lehmann (2007), consisting in the transformation of biomass into biochar and its deposi- tion in soils, gained notable interest in the world of science. Research in this area is conducted in many places in the world, e.g. in Zambia, Tanzania, Malaysia and Nepal. Biochars used in such studies are usually produced locally, with traditional methods. Also, the unloading of kilns, reloading, transport and dosage of biochars to soils are most frequently done by hand. Unfortunately, due to their properties, biochars may be dan- gerous to ecosystems and to human health. Polycylic aromatic hydrocarbons (PAHs) contained in biochars create a risk to living organisms and to humans when they come in contact with those materials as well as with the soils amended with them (Oleszczuk et al. 2013; Sims and Overcash 1983). Workers employed in the production and transport of biochars are particularly exposed. The area of that risk increases fol- lowing the growing popularity of biochar use. The methods of biochar production are simple, known for a very long time, and can be applied in countries that do not have advanced technologies. The results of numerous studies indicate a positive effect of biochars on the physical, chemical and biological properties of soils. Biochars are becoming a material that is more and more often used for the improvement of soil properties, with simultaneous beneficial effect consisting in mitigating climate change. With relation to the growing popularity of the utilisation of biochar, an increasing number of people will have contact with biochars and with soils remediated with their use, which may cause a notable expansion of the risk group. This results from the fact that in the course of biochar production, highly dangerous PAHs are formed (Freddo et al. 2012; Oleszczuk et al. 2013). They are formed through the degradation of lignins and cellulose, on the pathway of unimolecular reactions, such as dealkylation, Springer Environ Sci Pollut Res (2014) 21:3646-3652 3647 dehydrogenation, cyclisation, aromatisation and/or radical re- actions. Sixteen of them, due to their potentially mutagenic and carcinogenic properties, have been given the status of priority substances in the USA and in the European Union (Sims and Overcash 1983). Biochar produced with the traditional method is characterised by very low mechanical strength and high brit- tleness; therefore, during the emptying of kilns, shifting, reloading and transport, it undergoes considerable fragmenta- tion. As a consequence, in the vicinity of kilns, fine coal gets into the soil, and the silt fractions of biochar are carried with the wind over longer distances. In the immediate vicinity of the kilns, soil may also be contaminated with the liquid products of pyrolysis. PAHs migrating into the soil together with biochar are very hard -biodegradable (Koelmans et al. 2006), which contributes to their increased stability in the soils and extends the time over which they may pose a threat to organisms and to the environment. Workers employed in the production and transport of bio- char are particularly exposed to contact with contaminated soil. Soil particles cannot only settle on the skin but they can also be accidentally ingested and inhaled. As mentioned ear- lier, the numbers of people involved in the production of biochar, and thus exposed to contact with contaminated soil, will grow following the scale of application of those materials. In this context, the assessment of risk related with environ- mental pollution resulting from biochar production is important. The objectives of the study were to determine the level of polycyclic aromatic hydrocarbons in soils in the vicinity of traditional biochar kilns, to identify by means of the molec- ular diagnostic ratios (MDRs) the sources of the PAHs and to assess the risk of cancer related with the presence of those compounds in soils. This will permit to determine how sites related with the production of biochar affect the quality of soils and indirectly human health. Methods and materials Soil sampling and preparation Soil samples for analyses were taken from five localities where biochars are produced with the traditional methods on a seasonal basis: Smerek (Wla, a, Wlb, b, W 1 c), Habkowice (W2a, W2b), Smolnik (W2a, W3b), Maniow (W4a, W4b) and Muczne (W5a, W5b). All of those localities are situated in the area on the Bieszczady National Park in the south- eastern part of Poland (Fig. S1). The portable ring kilns with a capacity of 15 m3 are used to obtain biochars in this area. Mixture of grey alder, silver birch and aspen poplar is used for biochar production. During the burning process, the tempera- ture inside the kiln is about 400-500 °C. The primary products of the process are solids (charcoal, coke breeze), liquids (tar, methanol, water), gases and atmospheric particles bound with organic and inorganic contaminants. All the biochar- producing facilities from which soil samples were taken were situated in forest areas. Soil samples were collected in the spring of 2012 from a 0 - to 20 -cm horizon close to the kilns (5-10 m) using a stainless steel corer (5 x 60 cm i.d.). The cores were placed into ziplock bags and transported to the laboratory. Samples for the deter- mination of physico-chemical properties and PAH contents were air-dried in an air-conditioned storage room for 2 days (20 °C, in darkness), mechanically crushed and passed through a 2 -mm sieve. Then, samples were kept in glass jars (previously cleaned by rinsing with acetonitrile) and stored in a laboratory freezer (-4 °C). Physico-chemical properties of the soil studied are presented in Table S1 (Supplemental Material, page 3). PAH analysis Dry soil samples were extracted using an accelerated solvent extractor (ASE 100) from Dionex GmbH (Idstein, Germany). The extraction program was based on the ASE Dionex appli- cation note 313 for PAHs in soil and sediment. Next, the extracts were evaporated and purified by solid -phase extrac- tion according to the procedure described elsewhere (Oleszczuk and Baran 2004). A qualitative and quantitative analysis of PAHs was carried out on a high-performance liquid chromatograph (Waters, e2695) with photodiode array (Waters 2998) and fluorescence (Waters 2475) detectors. A Waters PAH Cl8RP 8RP (5 pm, 4.6 x 250 mm) column was used for the separation of 16 PAHs. Detection was carried out at 254 nm. Elution of all PAH was carried out for 32 min. Recoveries for the total procedures (sample preparation, ex- traction and SPE) ranged between 81 and 90 % for individual PAHs. Precision expressed as relative standard deviation was below 12 %. The concentrations reported here have, therefore, not been corrected for losses. The procedural blank was de- termined by going through the same extraction and clean-up procedures for each series of samples. None of the analytical blanks were found to have detectable contamination of the monitoring PAHs, and thus, the results were not blank - corrected. A diagnostic tool that is frequently used for the identifica- tion of the sources of PAHs is the MDRs (Oleszczuk and Pranagal 2007; Tobiszewski and Namiesnik 2012). Their application is based on the assumption that certain PAHs are emitted at relatively constant source -related proportions and that those proportions are retained after reaching the receiver (Katsoyiannis et al. 2011). Individual MDRs do not uniquely identify the source of PAHs: some of them, like, e.g. BaA/(BaA+CHR), are characterised by considerable variability within a source type; Springer 3648 Environ Sci Pollut Res (2014) 21:3646-3652 others, like FLA/(FLA+PYR), may have similar values for various sources (Tobiszewski and Namiesnik 2012). For a more accurate determination of the origin of PAHs, two or more MDRs can be used. In this study, three MDRs were used: FLA/(FLA+PYR), IcdP/(IcdP+BghiP) and ANT/ (ANT+PHE). However, some authors question the applicabil- ity of the latter ratio (Brandli et al. 2008); their use is widely adopted in the literature for the identification of the origin of PAHs in soils (Bucheli et al. 2004; De La Tone -Roche et al. 2009; Liu et al. 2010; Maliszewska-Kordybach et al. 2008; Marusenko et al. 2011; Placha et al. 2009; Wang et al. 2007, 2010). Incremental lifetime cancer risk Assessing the threat to human health, the incremental lifetime cancer risks (ILCRs) were estimated. It was assumed that PAHs penetrate into the human organism in three ways: through accidental ingestion of soil particles, inhalation of soil particles and dermal contact. The calculations were performed on the basis of the following equations (Peng et al. 2011; US EPA, OSWER 1991, 2009): CS = CNAP•TEFNAP + • • • + CIcdP•TEFIcdP (1) ILCRsingestion = (CSCFCSFinw(BW/70)113•IRsoirEF•ED /(BW•AT) ILCRSdernal = (2) (CSCFCSFder'(BW/70)'/3 •SA•EV•AF•ABS•EF•ED /(BW•AT) ILCRsinhalation (CS.CSF.nh•IRair• (BW/70)1 /3 •EF•ED /BW•AT•PEF ILCRs = ILCRsingestion + ILCRsdernal + ILCRsinhalation (3) (5) For calculations of benzo(a)pyrene (BaP) equivalent con- centrations (CS), the scheme developed by Nisbet and LaGoy (1992) was used, due to the current knowledge about toxic potency of individual PAHs relative to their BaP concentration (Petry et al. 1996), reliability and consistency across many studies (Masiol et al. 2013). It was assumed that exposed persons are working in biochar manufacturing for 25 years, 250 days per year, their average body weight is 70 kg and their life expectancy is 70 years. Conservative values of inhalation rate (15 m3/day) (US EPA National Center for Environmental Assessment and Washington 2011) and ingestion cancer slope factor CSFi„g= 1.2 (mg kg -1 day -ill were used (Gaylor et al. 2000). All the parameters used in the calculations are present- ed in the Supplementary material (Table S2, page 4). Results and discussion It is accepted that combustion processes and release of petro- leum products are the two main sources of anthropogenic PAHs in the environment (Sims and Overcash 1983). Most of those compounds accumulate in the soil (Desaules et al. 2008; Maliszewska-Kordybach et al. 2009), but precise deter- mination of the source of their origin is not an easy task (Tobiszewski and Namiesnik 2012). PAH content in soils Table 1 presents the total content of 16 PAHs in the soil samples analysed. The values of the total content fall within the range of 1.8-101.3 µg/g (median 16.5 µg/g, mean value 29.7 µg/g). The lowest levels of PAHs were observed in samples W2a (1.80 µg/g), W 1 c (4.20 µg/g) and W3a (6.83 µg/g). A particularly high level of those compounds was noted in sample W3b (101.28 µg/g). The level of PAHs at as many as four out of the five localities (W 1 a—W5b) was higher than 10 µg/g, and at two (W3b and W5b) sites, it exceeded 50 µg/g. Compared to the average levels of PAHs in the soils of Switzerland (0.145-0.593 µg/g), Germany (0.100-0.775 µg/g) (Desaules et al. 2008) and Poland (0.028-2.445 µg/g) (Maliszewska-Kordybach 1996; Oleszczuk and Pranagal 2007), those values are very high. The difference is smaller compared to the soils in the big cities of Asia. The levels of PAHs in the soils in Hong Kong fall within the range of 0.147-8.04 µg/g (average) (Man et al. 2013), while in Beijing, they vary from 0.178 to 12.14 µgig Table 1 The concentration of PAHs in examined samples, BaPeq benzo(a )pyrene equivalent concentrations and incremental lifetime can- cer risks (ILCRs) Sample name PAHl6 (µg/g) BaPeci (µg/g) ILCRs (—) Wla Wlb Wlc W2a W2b W3a W3b W4a W4b W5a W5b 9.89 8.23 4.29 1.80 45.42 68.34 101.28 16.54 16.58 28.15 87.41 0.99 0.76 0.32 0.17 1.92 2.12 77.89 0.27 0.74 2.88 7.08 , 1.34.10 1.03.10 4.33.10-4 2.3310-4 , 2.60.10 2.8T 10-3 1.0510-1 3.5910-4 1.0010-3 , 3.8910 , 9.58.10 Springer Environ Sci Pollut Res (2014) 21:3646-3652 3649 (average), attaining a maximum level of 28.50 µg/g (Peng et al. 2011). The contents of the individual PAHs were varied and clearly depended on the sampling site. Detailed analysis of the contribution of the individual PAHs indicated the dom- inance of four -ring compounds in most of the samples studied (Table S3). In accordance with the current regulations in Poland (Dz 2002), the content of the individual PAHs: naphthalene, phen- anthrene, anthracene, fluoranthene, chrysene, benzo(a)anthracene, benzo(a)fluoranthene and benzo(g,h , i )perylene, in protected areas should be lower than 0.10 µg/ g. At the same time, the highest permissible concentration of the 16 most important PAHs in soils of protected areas cannot exceed 1.00 µg/g. Similarly, strict norms are in force in the Czech Republic, Italy, Slovakia and Denmark (Carlon 2007). The warning level values in force in Germany amount to 3 µg/ g at organic carbon content lower than 8 %, and 10 µg/g at organic carbon above 10 % (Desaules et al. 2008). The total concentrations in all of the samples studied considerably exceed the values permissible in Poland. The soils analysed should be considered as strongly contaminated and potentially dangerous for human health. The high level of PAHs in the soils studied is all the more notable in view of the fact that they were sampled in an area with highly limited anthropopressure. In the vicinity of the sampling sites, there were no active industrial facilities, and there were no intensively used transport routes. At present, that area is a national park and a UNESCO biosphere reserve. We speculate that the only potential source of contamination of soils with such high PAH levels in the area is the activity related with biochar production that has been conducted here for a number of years. Molecular diagnostic ratios The literature provides descriptions of more than ten different molecular diagnostic ratios (Katsoyiannis et al. 2011; Tobiszewski and Namiesnik 2012). As it was mentioned earlier, for the purpose of this study, the following MDRs were chosen: ANT/(ANT+PHE), FLA/(FLA+PYR) and IcdP/(IcdP+BghiP). The pyrogenic origin of PAHs is indicat- ed by the values of the ratio ANT/(ANT+PHE) above 0.1 and FLA/(FLA+PYR) and IcdP/(IcdP+BghiP) higher than 0.4, with the values of the latter two exceeding the level of 0.5 being indicators of the processes of combustion of coal or biomass (grass, wood). As mentioned before, the sole potential source of PAHs in the area under study is processes related with biochar produc- tion. To confirm that, MDRs were calculated for particular samples (Table 2). The values of the ratio ANT/(ANT+PHE) for the samples studied fall within the range of 0.172-0.807, exceeding the threshold of 0.1, characteristic for contaminants of pyrogenic origin, and thus related with biochar production. Six samples (Wlb, b, W2a, W2b, W4a, W5a, W5b) were characterised with the ratio FLA/(FLA+PYR) above 0.5, in- dicating that the source of the PAHs contained in them can be grass, wood or coal combustion, and for three of the samples (Wla, a, W 1 c, W4a) that ratio is very close to 0.5 (0.495, 0.492 and 0.495, respectively). All of those values indicate clearly that the source of PAHs in the area can be processes related with biochar production. In the eight samples, the ratio of the content of indeno(c, d)pyrene and the sum of the contents of indeno(c ,d)pyrene and benzo(g,h ,i)perylene is higher than 0.5 (Table 2), which indicates that the PAHs contained in them were formed in the processes of combustion of biomass and, possibly, coal, while for sample W4a, it exceeds the value of 0.2 (0.3978) which is the threshold value for those contaminants that are the pyro- genic origin. The results obtained for those indicators also confirm that the primary source of contamination of the soils studied can be processes related with biochar production. Samples W3a and W3b are characterised by notably lower FLA/(FLA+PYR) (0.272 and 0.160) and IcdP/(IcdP+BghiP) (0.223 and 0.086) ratios than those for the remaining samples in the series, which suggests a different origin of the PAHs. It is possible that the soil at the sampling sites was contaminated with liquid products of pyrolysis, such as creosotes. However, a simple, direct comparison with the ratio FLA/(FLA+PYR) for various creosotes, calculated on the basis of literature data (Melber et al. 2004), yielded negative results. The results of the calculations of MDR for various creosotes, presented in Table S4, fall within the range of 0.52-0.80, and thus, they are considerably higher that the values for samples W3a and W3b (Table 2). Also, the values of the ratio ANT/(ANT+PHE) for those samples (0.8017 and 0.7758) are outside of the range of values of that parameter calculated for creosotes (0.039- 0.327) (Table S4). It appears, therefore, that the site from which samples W3a and W3b were collected could have been accidentally contaminated with fuel or oils from vehicles used for serving the kilns and for the transport of wood and biochar. The results of calculations of MDRs for the soil samples studied are presented in Fig. 1 in the form of the so-called crossplots. That analysis indicates that the source of contam- ination of soils at the sites described is the processes of biomass combustion. Only samples W3a and W3b appear to be contaminated with hydrocarbons of petrogenic origin. Those results were additionally juxtaposed with MDRs calcu- lated for various biochars on the basis of literature data (Fig. 2, Table 2). Out of 13 values of the ratio ANT/(ANT+PHE), nine fall within the range of 0.10-0.28, while six values of the ratio FLA/(FLA+PYR) fall in the range of 0.42-0.59, indicating considerable similarity to the soils studied, which strongly supports our thesis concerning the source of the contaminants. Taking even several MDRs as the basis for the classifica- tion (identification) of a source may lead to misleading con- clusions. Katsoyiannis et al. (2011) demonstrated than in Springer 3650 Environ Sci Pollut Res (2014) 21:3646-3652 Table 2 Calculated FLA/(FLA+ PYR) and ANT/(ANT+PHE) ra- tios in examined soil samples and various biochars — no pyrene content Sample name ANT/(ANT+PHE) FLA(FLA+PYR) Literature Wla Wlb Wlc W2a W2b W3a W3b W4a W4b W5a W5b grass 300 °C grass 400 °C grass 500 °C grass 600 °C wood 300 °C wood 400 °C wood 500 °C wood 600 °C biochar (median) biochar 1 biochar 2 biochar 3 biochar 4 BC -2 BC -W BC -O MC -M 0.2396 0.1969 0.2139 0.2373 0.2361 0.8072 0.7758 0.2096 0.1820 0.1974 0.1719 0.0943 0.2803 0.1964 0.0773 0.1006 0.1238 0.0683 0.1923 0.1571 0.1668 0.1705 0.1533 0.1625 0.2198 0.2105 0.4951 0.5303 0.4916 0.5568 0.5478 0.2724 0.1596 0.4959 0.5564 0.5255 0.5468 0.2293 0.4263 0.4918 0.3038 0.3889 0.3715 0.3302 0.3667 0.1875 0.4627 0.5304 0.5840 0.5495 0.3230 0.1781 Present work Keiluweit et al. (2012) Freddo et al. (2012) Hilber et al. (2012) Oleszczuk et al. (2013) many cases, the application of MDRs does not yield coherent results, as between the emitter and the receiver PAHs may undergo chemical transformations (interfering with the MDRs described above), and also PAHs may reach the receiver arriving from various sources. Biochar production processes as the source of PAHs found in the samples studied are indicated, however, not only by the MDRs discussed above but also by the lack of any reports of forest fires in the area of soil sampling, by the considerable distance from intensively used transport routes and other Fig. 1 Molecular diagnostic ratios for identification of PAH pollution sources ANT f (ANT + PHE) 1.0 0.8 0.6 0.4 0.2 0.0 sources of PAHs, the immediate vicinity of kilns and the very high level of those compounds in the samples. Incremental lifetime cancer risks High levels of carcinogenic substances in soils may create a considerable threat to ecosystems and to human health, espe- cially with relation to people involved in the traditional pro- duction of biochar. The most exposed individuals are the "biochar men", working in the production of biochar 0 k- ` pyrogenic source peifogenic source _ 1 .1.-1 L 1 2 a2 LI' 1 4-1 1 L 1 Y 1 1 J. 0.0 0.2 0.4 0.6 FLA/ (FLA + PYR) FLA / (FLA + PYP) 1.0 0.8 0.6 0.4 0.2 0M , 0.8 1.0 0.0 0,2 !x,4. 0, IcdP / (MP + BOP) to Springer Environ Sci Pollut Res (2014) 21:3646-3652 3651 1.0 0.8 ri z i~ 0.4 z 4 0.6 01 0.0 _• O pyrogenic source # -f- ii :g this work (KeKu veil -2012) (Oieszczuk-2'013) (Hiiber-2012) 0 + - • J r petrogeoic source + + .,_1 1 I L, 1 i . . 1 1 1 - L e . • I , . . 1 . , . I j_y__ 0.0 0.1 0.2 0.3 0.4 0.5 FLA / (FLA + PYR) Fig. 2 Crossplot for MDRs presented in Table 2 0.6 0,7 0.8 throughout the season. A parameter frequently used for the description of hazard to human health is the so-called ILCRs. This unitless factor represents the increased probability of occurrence of cancer due to prolonged exposure to a toxic agent, usually taking into consideration three exposure path- ways: ingestion, inhalation and dermal contact. Following the literature data (Man et al. 2013; New York State Department of Health 2007), the ILCRs applied for the estimation of cancer risk are here classified as low (<10-6), medium (10-6-10-4), moderate (10-4-10-3), high (10-3-10-1) and very high (>10-1). The sums of the calculated ILCRs are presented in Table 1, and the full compilation (ILCRsingestion, ILCRSinhalation, ILCRSde a1) is shown in Table S5 (supple- mental material, page 6). The estimated ILCRs fall within the range of 2.33 10-4 (sampleW2a)-1.05.10 1 (sample W3b). Only in the case of three samples (Wlc, c, W2a, W4a) cancer risk can be considered to be moderate. As many as seven of the soils studied posed a high cancer risk: W 1 a, Wlb, b, W2b, W3a, W4b, W5a and W5b (ILCRs from 1.00.1 0-3 to 9.58.10-3), and soil W3b presented a very high risk (ILCR=1.05.10-1). Occupational cancer risk resulting from contact with soils contaminated with PAHs was estimated by Man et. (2013). Those authors analysed soils from 55 locations in Hong Kong, under various uses (e.g. car dismantling workshops, open burning sites, e -waste open burning sites, etc.). The ILCRs values estimated by those authors fell within the range of 1.90.10-7-4.53 while the risk level was estimated as very low, low and moderate.. The potential risk created by PAHs in soils within the area of Beijing was estimated by Peng et. al. (2011). The ILCRs calculated by those authors did not exceed the limit of 1.24.10-4, and one of the highest values (1.24.10-3) was measured in the vicinity of a coking plant in that city. The results obtained in this study are higher by 1 to 3 orders of magnitude, which is due primarily to the higher concentrations of PAHs. Therefore, the risk formally attributable to the calculated values of ILCRs should be con- sidered as high and very high. Similar to the results obtained in references Man et al. (2013), Peng et al. (2011), we also observed a relation be- tween the dermal and ingestion and the inhalation risks, which were lower by 4 orders of magnitude (ILCRsingestion and ILCRsdernial»ILCRsinhalation) (Table S5). It should be emphasised that in reality, workers working with kilns have contact not only with contaminated soil but also with the biochar itself and with the fme particles formed during its production. As mentioned earlier, due to its me- chanical properties, it is a much more dangerous source of dusts than the soil itself As our analysis also does not take into account the dusts formed from biochars, the risk described should be considered as underestimated, and thus, the risk of disease among the workers may be considerably higher. Conclusions The study demonstrated that soils in the immediate vicinity of kilns are strongly contaminated with PAHs. The concentra- tions of PAHs are considerably higher than the permissible limits laid down in the regulations in force in many countries. Both the analysed MDRs and the features of the situation of the sampling sites indicate potentially that the source of those contaminants is the production of biochar in that area. In accordance with the estimated values of ILCRs, the cancer risk resulting from contact with the contaminated soils should be considered at least high. It should be strongly emphasised that the level of the risk may be underestimated. It should also be noted that apart from the cancer risk to humans, there is a great hazard to animals in that region. The fauna of the region includes many protected species that should be granted special protection. Those sites may, therefore, create serious hazard to the ecosystems and to human health. Acknowledgments This work was supported by a grant from Switzer- land through the Swiss Contribution to the enlarged European Union. Open Access This article is distributed under the terms of the Creative Commons Attribution License which permits any use, distribution, and reproduction in any medium, provided the original author(s) and the source are credited. References Brandli RC, Bucheli TD, Ammann S, Desaules A, Keller A, Blum F, Stahel WA (2008) Critical evaluation of PAH source apportionment tools using data from the Swiss soil monitoring network. J Environ Monit 10:1278-1286 Bucheli TD, Blum F, Desaules A, Gustafsson 0 (2004) Polycyclic aromatic hydrocarbons, black carbon, and molecular markers in soils of Switzerland. Chemosphere 56:1061-1076 Carlon C (ed) (2007) Derivation methods of soil screening values in Europe. A review and evaluation of national procedures towards Springer 3652 Environ Sci Pollut Res (2014) 21:3646-3652 harmonization. European Commission, Joint Research Centre, Ispra [WWW Document]. URL http://eusoils.jrc.ec.europa.eu/esdb_ archive/eusoils docs/other/EUR22805.pdf. Accessed 9 Oct 2013 De La Tone -Roche RJ, Lee W -Y, Campos -Diaz SI (2009) Soil -borne polycyclic aromatic hydrocarbons in El Paso, Texas: analysis of a potential problem in the United States/Mexico border region. J Hazard Mater 163:946-958 Desaules A, Ammann S, Blum F, Brandli RC, Bucheli TD, Keller A (2008) PAH and PCB in soils of Switzerland status and critical review. 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Accessed 9 Oct 2013 Wang Z, Chen J, Yang P, Qiao X, Tian F (2007) Polycyclic aromatic hydrocarbons in Dalian soils: distribution and toxicity assessment. J Environ Monit 9:199-204 Wang W, Massey Simonich SL, Xue M, Zhao J, Zhang N, Wang R, Cao J, Tao S (2010) Concentrations, sources and spatial distribution of polycyclic aromatic hydrocarbons in soils from Beijing, Tianjin and surrounding areas, North China. Environ Pollut 158:1245-1251 Springer Diana Aungst From: Jeri Yarbrough <yarbroughacres@icloud.com> Sent: Wednesday, September 4, 2024 12:30 PM To: Diana Aungst Subject: Bio char Caution: This email originated from outside of Weld County Government. Do not click links or open attachments unless you recognize the sender and know the content is safe. Here are some pictures of the wildlife located on my property. Also some photos of how close this will be to my home and horses. Thank you . Jeri Yarbrough 1 n r_ r_ • 1 5 e b 2023 By Ellie Mulder Leonard Jordan Gaspard knew that working at Biochar Now, the Berthoud -based company where she serves as managing director, could be a "dirty job" — but she never expected to aopear on the Discovery Channel show "Dirty Job ", alongside host Mike Rowe. :When Mike was here, he said, 'This is probab'y one of the dirUest jobs I've ever done,"' said Gaspard, who received both her bachelor's degree and VBA from the OSU College of Business. Diana Aungst From: Sent: To: Subject: Follow Up Flag: Flag Status: Gina Michel <gmichel9013@gmail.com> Monday, September 23, 2024 11:59 AM Diana Aungst Opposing Biochar project case #USR24-0019. Flag for follow up Flagged Caution: This email originated from outside of Weld County Government. Do not click links or open attachments unless you recognize the sender and know the content is safe. Dear Weld County Commissioner and Weld County Planner, I am writing this letter to express our strong opposition to the proposed development of the NGL owned facility to include Biochar project case #USR24-0019. Our family farming business has been established for over 30 years now. Here we raise crops and cattle. With the proposed 24/7 kiln -based operation that emits air pollution, noise pollution, light pollution, tractor trailer traffic, and potential fire risks, will severely impact our farm operations. - Air pollution can harm wildlife in two main ways. • It affects the quality of the environment or habitat in which they live • It affects the availability and quality of the food supply - Noise pollution, or sound pollution, is the propagation of noise or sound with ranging impacts on the activity of human or animal life, most of which are harmful to a degree. The source of outdoor noise worldwide is mainly caused by machines, transport and propagation systems. - Light pollution, or artificial light at night, is the excessive or poor use of artificial outdoor light, and it disrupts the natural patterns of wildlife, contributes to the increase in carbon dioxide (CO2) in the atmosphere, disrupts human sleep, and obscures the stars in the night sky. - Tractor -trailers damage ecosystems, disturbing wildlife and natural habitats. Road and traffic pollution affects the ecosystem, making healthy living difficult. When a commercial vehicle accident dumps toxic materials into the environment, the harmful effects of the spill can be almost immediate. Many hazardous chemicals impact air, soil, and water quality and can cause long-lasting damage, depending on the type of chemical. I feel it is important to note since road 6 curves around part of our lake, also where the proposed site is, there are at least 3 wrecks per year where drivers tend to not notice the road curves and go straight through our fence. Furthermore, we have two takes that are less than 500 feet from this facility and are the only water source for our several head of cattle, horses, as well as alfalfa and corn crops. Any runoff from the 1 Biochar kiln site has the high potential to contaminate our water sources. We have some of our cattle herd that graze on the west side of this facility and use the lake water that runs under road 6 as their water source. Any run off with contaminants from the Biochar kiln site will impact the health of our animals and our livelihood. The small red buildings are located on the proposed Biochar kiln site In addition, we have two lakes that are next to this proposed facility which house bald eagle's nests in our cottonwood trees for over 30 years now. Bald eagles are recognized as the country's national symbol, a distinction it has held since 1782 and are on the endangered species list. Air pollution, noise pollution, light pollution, water contamination, and high fire risk, will jeopardize the Bald Eagles livelihood. 2 Two Bald eagles that just left their nests in our cottonwood trees along the lake. We are wanting our voices heard in this matter and to document our strong opposition and our request for the committee to deny the special use permit Case Number USR24-0019 in our community with many homes and animals that require a healthy environment to survive. Thank you for all that you do and for your time to read my letter! Warmly, Gina Michel, Dave Sack and Joe Sack 3 .r . is Re n ing&r • 464 I I u r i l er C i * Bri. hton., CO t n01: lib 303-6594665 66 September 15 2024 a fi US- 24-0[119 N .rri —NCI_ Water Solutions 1 a.rr, ri Oniz this letter to voice my concern with ibis pwjccl. We have been operating across the siTedt from the proposed site for over 30 Saar&.. My biggest concern Rh h this project is the inim id (ne; ativc) impact on the wi ldi i I e in areas in I.%.0 courseof i� e year we will see Canada Geese, . Mallard, MI iaeen. CiarividrelL American Shoveler, Green and Blue v.inid, * I e* Pintail, Mourning Doves, Coot, Snow Geese as well as other migratory brr l h,. My biggest concern is these art all r_mgr toffy birds that stop to rest and Teruel in. (ab rya&& on their migration South_ These birds look to this farm in getmunch needed relaxation and rest before they continue their 1j Rmiey_ Habitat t.at is getting men away from the w i 1:.I i to at an alarming rate in this arm. Not only art i he mip-atory species directly ikcted by the loss of habitat but also the birds and animals th t cal I, this area honks (White -tall deer. Mule Dieer, Bald I '.4.-dit). There is a Bald Tale nest right across the street from this proposed site. These a bird's art very w rel ve during their nesting seasons and they will be directly affected by the, primed construction and operation of this site. Habitat is disappearing ut y rapid rate and I feelthat :hero is a m uch Nu tri h1,t and safe spot for this Procx)sue projcet that isn't right next 10 a lifCbilg w ld lih sanctuary. Slit [water 0 ul raters LLC N talent i �rav i s Ihunger Colleen Kay O'Neil, Ed.D. 1865 County Road 31, Fort Lupton, CO 80621 cell 970.302.9517 email colleenkoneil@gmail.com Subject: Concerns Regarding Biochar's Special Use Permit, Case Number USR24-0019 Dear Weld County Commissioners and Weld County Planner, I am writing to express my strong opposition to the proposed NGL biochar project case number USR24- 0019, located near 14512 Co Rd 6, Fort Lupton, CO 80621. I live about 2500 feet from this location and own competitive rodeo horses and animals. As you may recall, this land was previously purchased by NGL for the purpose of establishing injection well sites. That as an underground operation that was approved by the Weld County Commissioners at the time. Biochar is not that. It is a 24/7 kiln -based operation that emits air pollution, noise, traffic and poses fire risks in an already too dry area of Weld County. This type of business in our agricultural neighborhood is deeply concerning due to the potential for light pollution, environmental contamination, and negative impacts on our livestock. The proposed biochar facility could pose significant risks to our us and to our animals, including: • Air pollution: Particulate matter and harmful gases emitted by the kiln could irritate human and animals' respiratory systems and cause health problems. Biochar is known to produce black soot in the atmosphere which can cause harm to those who are near it. • Noise pollution: The noise from the kiln operation could disturb animals, causing stress, reduced productivity, and difficulty in sleeping or resting. • Light pollution: Excessive light pollution could disrupt animals' natural sleep -wake cycles, leading to stress and health problems. • Water contamination: Runoff from the kiln site could contaminate nearby water sources used by animals for drinking or grazing. • Fire risk: The kiln operation could pose a fire risk that could directly harm animals if it spreads to nearby pastures or habitats. The image of the proposed kiln factory speaks for itself. Such an industrial facility is incompatible with our residential and agricultural zoned areas, particularly in close proximity to heavily traveled roads and homes with livestock. Biochar has a place in the ecoclimate and is a sustainable resource. However, having a 24 -hour kiln operation in a neighborhood with many homes and animals is not acceptable. I am requesting that you deny the special use permit Case Number USR24-0019. I urge you to carefully consider the negative impacts of this project on both human health and the well- being of our animals. Thank you for your time and attention to this matter. I appreciate the work you do as Commissioners representing the best interests of your constituents. Sincerely, Colleen O'Neil, Ed.D. Sharon A. O'Neil 14952 County Road 6, Fort Lupton, CO 80621 cell 303.710.0560 email sherrieoneil@gmail.com S ubject: Concerns Regarding Biochar's Special Use Permit, Case Number USR24-0019 Dear Weld County Commissioners and Weld County Planner, I am writing to express my strong opposition to the proposed NGL biochar project case number USR24- 0019, located near 14512 Co Rd 6, Fort Lupton, CO 80621. I live about 2500 feet from this location at the corner of roads 6 and 31. What and where is the feedstock coming from and how will it be delivered to the facility? Roads 6 and 31 are already overloaded with traffic so this is a critical situation to the health, safety and wellbeing of the people of this community. As you may recall, this land was previously purchased by NGL for the purpose of establishing injection well sites. That as an underground operation that was approved by the Weld County Commissioners at the time. Biochar is not that. It is a 24/7 kiln -based operation that emits air pollution, noise, traffic and poses fire risks in an already too dry area of Weld County. This type of business in our agricultural neighborhood is deeply concerning due to the potential for light pollution, environmental contamination, and negative impacts on our livestock. The proposed biochar facility could pose significant risks to our us and to our animals, including: • Air pollution: Particulate matter and harmful gases emitted by the kiln could irritate human and animals' respiratory systems and cause health problems. Biochar is known to produce black soot in the atmosphere which can cause harm to those who are near it. • Noise pollution: The noise from the kiln operation could disturb animals, causing stress, reduced productivity, and difficulty in sleeping or resting. • Light pollution: Excessive light pollution could disrupt animals' natural sleep -wake cycles, leading to stress and health problems. • Water contamination: Runoff from the kiln site could contaminate nearby water sources used by animals for drinking or grazing. • Fire risk: The kiln operation could pose a fire risk that could directly harm animals if it spreads to nearby pastures or habitats. The image of the proposed kiln factory speaks for itself. Such an industrial facility is incompatible with our residential and agricultural zoned areas, particularly in close proximity to heavily traveled roads and homes with livestock. Biochar has a place in the ecoclimate and is a sustainable resource. However, having a 24 -hour kiln operation in a neighborhood with many homes and animals is not acceptable. I am requesting that you deny the special use permit Case Number USR24-0019. I urge you to carefully consider the negative impacts of this project on both human health and the well- being of our animals. Thank you for your time and attention to this matter. I appreciate the work you do as Commissioners representing the best interests of your constituents. Sincerely, S haron A O'Neil Diana Aungst From: Rachel Brown <elbrown1366@gmail.com> Sent: Tuesday, September 17, 2024 11:15 AM To: Diana Aungst Subject NGL Water Solutions DJ LLC USR Case # USR24-0019 Follow Up Flag: Flag for follow up Flag Status: Flagged b z .O S EXHIBIT 6 Caution: This email originated from outside of Weld County Government. Do not click links or open attachments unless you recognize the sender and know the content is safe. Hello Diana, I am emailing you to protest the NGL Water Solutions DJ LLC USR request(Case # USR24-0019). This facility would decrease my quality of life greatly! It would be so awful to have to drive by this ugly smoke emitting place every time I left and came back to my home!! The pollution this facility would admit is also very very concerning! It could affect not only my animal's health but my health and the health of my family! It could also affect the health of the bird life in the area. There are eagles, herons, egrets, pelicans, several species of owls, and several species of ducks that live right by this proposed facility. This in no way seems like ORGANIC composting!! I am surprised that Weld county would ever consider this type of business organic composting and that it fits into an agricultural business! I also think it is immoral for NGL and this biochar company to try to put this business so close to people's homes just because they want to buy cheaper agricultural land and pay less property taxes! For these reasons this facility would greatly impact my property values and I am very much against this USR being passed! Thank you for your consideration in this matter. Rachel Brown 14510 County Rd 6 Fort Lupton, CO 1 Diana Aungst From: Jeri Yarbrough <yarbroughacres@icloud.com> Sent: Tuesday, December 12, 2023 7:21 PM To: Diana Aungst <daungst@weld.gov> Subject: Biochar data ID 5 EXHIBIT 7 Caution: This email originated from outside of Weld County Government. Do not click links or open attachments unless you recognize the sender and know the content is safe. Hi Diana , Tony Hale the neighbor to the east of me sent me this data, can you add to the file for the county. Thank you Jeri Yarbrough Sustainable Restoration of Soil Functionality in PTE Affected Environments: Biochar Impact on Soil Chemistry, Microbiology, Biochemistry, and Plant Growth Abstract Biochar can be useful for the functional recovery of soils contaminated with potentially toxic elements (PTEs), even if its effectiveness is variable and sometimes limited, and conflicting results have been recently reported. To shed some light on this regard, softwood -derived biochar was added at 2.5 (2.5-Bio) and 5.0% w/ w (5.0-Bio) rates to an acidic (pH 5.74) soil contaminated by Cd (28 mg kg -1), Pb (10,625 mg kg -1), and Zn (3407 mg kg -1). Biochar addition increased soil pH, available P and CEC, and reduced labile Cd, Pb, and Zn (e.g., by 27, 37, and 46% in 5.0-Bio vs. the unamended soil). The addition of biochar did not change the number of total heterotrophic bacteria, actinomycetes, and fungi, while it reduced the number of Pseudomonas spp. and soil microbial biomass. Dehydrogenase activity was reduced in amended soils (e.g., by ---60 and 75% in 2.5- and 5.0-Bio, respectively), while in the same soils, urease increased by 48 and 78%. Approximately 165 rRNA gene amplicon sequencing and the Biolog community -level physiological profile highlighted a significant biochar impact (especially at a 5% rate) on soil bacterial diversity. Tomato (but not triticale) yield increased in the amended soils, especially in 2.5-Bio. This biochar rate was also the most effective at reducing Cd and Pb concentrations in shoots. Overall, these results demonstrate that 2.5% (but not 5.0%) biochar can be useful to restore the soil chemical fertility of PTE -polluted soils with limited (or null) impact on soil microbial and biochemical parameters. Montevecchio dismissed minins site iSardinia, Italy) PTE-palluted soil 25% biochar 5.0% bloc lair Graphical Abstract PIE -polluted raining soil Ph 10,625 mg kg' Cd 28 rng 2n 3,407 rig Mg' Cd Pb Zn pH 5,74 Reduction at Pb, Cd and Zn ire sail Improvement of soil fertility parameters Increased soil t.IR€ activity Enhanced plant yield (L. escuientum) Increased bacterial diversity (at 5.0% rate) Reduced Cd and Pb in shoots (at 2.5% rate) Decreased abundance of Pseudornonas sr Declined soil microbial C (at 5.0% rate, Reduced sail QIlG activity Decreased plant yield (triticale) (at 5.0% 1. Introduction Soil pollution by potentially toxic elements (PTE; e.g., Pb, Zn, Cd, As, and Sb) is of growing concern worldwide due to its critical effects on soil biota, including plants, and its potential impact on public health [1,2,3]. Soils polluted by PTE cannot be used for agricultural purposes (due to the health risks mentioned above), not contributing to the provision of food or feed, and limiting the achievement of many of the United Nations Sustainable Development Goals (SDGs), e.g., zero hunger (SDG 2), no poverty (SDG 1), and decent work and economic growth (SDG 8) (https://sdgs.un.org/goals, accessed on 20 August 2023). Sustainable remediation of these soils is therefore urgently needed to limit PTE spread in the environment and attenuate their negative consequences for health and society. In this sense, remediation interventions can be fundamental to converting marginal lands (i.e., PTE -polluted areas) into productive ones, e.g., by cultivating high - income non-food crops. Adding organic amendments to PTE -polluted soils is one of the sustainable remediation options to increase soil fertility, reduce labile PTE (i.e., potentially bioavailable fractions), and reduce potential health risks [4,5]. In this context, biochar, i.e., the solid material deriving from the pyrolysis of different feedstock biomasses, can have relevant implications [6]. In particular, its large surface area, high pH, presence of different functional groups, relevant porosity, surface charge, cation exchange capacity (CEC), and abundance of recalcitrant C are responsible for effective immobilization of labile PTE in soil through a variety of mechanisms such as precipitation, specific and non-specific adsorption, and diffusion within pores [7,8,9,10,11]. Such PTE -immobilizing capacities are greatly influenced by the feedstock nature and pyrolysis conditions, among others [12]. A recent meta -analysis showed that biochar's effectiveness in reducing PTE bioavailability in polluted soils depended mainly on soil pH (after amendment), texture, aging time, and the pyrolysis temperature of biochar [13]. In the same study, other important drivers regulating the bioavailability of PTE were identified, such as PTE species in soil, biochar feedstock, and application rate. This implies that a detailed characterization of each biochar x soil combination is needed to develop tailored solutions for soil recovery. This is essentially supported by the scientific literature of the last 10 years, which, however, has not provided so far any conclusive solutions and/or well-defined guidelines for biochar use in different soil pollution scenarios (e.g., [14]). For instance, while softwood -derived biochar was effective at immobilizing As and Cu in an aqueous solution [8], Beesley at al. [15,16] reported increased mobilization of As and Cu after soil amendment with hardwood biochar. Moreover, while a large literature reports on the PTE -immobilization capacities of biochar (e.g., [17,18,19]), an increase of Cu, Cd, Ni, and Zn in soil solution after biochar amendment was reported by El-Naggar et al. [20]. Additionally, similar biochars added to different soils in comparable amounts and incubation times showed varying effectiveness of PTE immobilization, e.g., Cd immobilization by maize straw biochar (pyrolyzed at ~500 °C) in two alkaline soils reached 24% in one case and 71% in the other [12]. Again, this supports the view that a customized, or case -by -case, assessment of biochar effectiveness is required and that knowledge gaps on biochar use for the recovery of PTE -polluted soils still exist. Mother aspect requiring more research efforts concerns the biochar impact on the soil microbial community and its functioning. This is an important point, as plant growth and health greatly rely on belowground microbial communities [21,22]. Although many studies reported a positive impact of biochar on soil microbial abundance, diversity, and activity (e.g., [23] and references therein), others highlighted contrasting results [24,25], making it impossible to draw general conclusions on this point. For instance, Anders et al. [26] showed that soil microbial biomass did not change after the addition of different biochars, while Andres et al. [27] reported a significant reduction. In addition, Wang et al. [28] reported a reduction in the relative abundance of fungi and bacteria when high rates of maize straw biochar were applied to the soil. Decreased soil basal respiration was noticed by Domene et al. [29] after corn stover biochar addition at the 0.2-7.0% rate, while reduced microbial activity (i.e., N mineralization) was reported by Dempster at al. [30] with increasing biochar from eucalyptus. Finally, the addition of biochar (from oak and hickory hardwood sawdust) also resulted in a null influence on soil microbial community structure [31], while many other critical effects of biochar on soil biota have been discussed elsewhere [25,32]. For instance, biochar can reduce nutrient bioavailability, thereby limiting plant growth and agricultural yield (e.g., [19,33,34]). This possibility, which mainly depends on feedstock and amendment rate, should be carefully evaluated before biochar employment in soil recovery intervention, as plant growth (PTE phytostabilizing species in particular) can be essential to reducing labile PTE and their spread into the environment [18,35,36]. The aim of this study was therefore to gain new knowledge on the effectiveness of softwood biochar in the functional recovery of a PTE -polluted soil from the dismissed Montevecchio mine in Sardinia, where Zn and Pb were extracted from galena (PbS) and sphalerite (Zn,Fe)S for more than one century [37]. In particular, PTE mobility was evaluated through sequential extraction in the polluted soil and in the same soil amended with two biochar rates. Soil microbial and biochemical parameters (e.g., soil microbial biomass, number of culturable microorganisms, community -level physiological profile, enzyme activities, amplicon sequencing analysis) were also addressed in the same soils. Finally, the biochar impact on soil fertility, plant growth, and PTE uptake was considered using different plant species, i.e., triticale and tomato. 2. Materials and Methods 2.1. Soil Origin, Biochar, and Mesocosms Set Up The soil used in this study was sampled in the vicinity of the dismissed Montevecchio mine (39° 33' 35" N; 8° 25' 29" E) in Southwestern Sardinia (Italy). The mine was exploited for more than a century (1848-1991) to extract Pb and Zn from galena and sphalerite [37]. The mining area (i.e., Montevecchio-Ingurtosu) includes about 150 dumps, accounting for approx. 8 Mm3 of waste dumps and tailings. In addition, approx. 7 Mm3 of tailings are dispersed in a large area around the mining site [38]. Due to limited management and securing of dumps and tailings, the area is characterized by significant PTE pollution consequent to the weathering of metal sulfides. Different soil samples (upper 30 cm) were collected near the mining site, pooled in the laboratory (150 kg in total), and sieved to <2 mm before mesocosms were set up. The soil was acidic (pH 5.74) and had a sandy loam texture (USDA classification: 28% coarse sand, 41.5% fine sand, 15.8% silt, 14.7 clay; [39]). The softwood-biochar used in this study (from elder, beech, and poplar pyrolyzed at 700 °C) was kindly provided by Ronda S.p.A. (Zane, Italy). A detailed physico-chemical characterization of this biochar was previously described by Pinna et al. [8] and reported in Table 51. Briefly, the biochar was alkaline (pH 9.3) with a pHYzc = 5.0, had approx. 60% of total C, 85 mg kg -1 of available P, and a CEC of 19 cmol(+) kg -1. The content of total N and dissolved organic carbon (DOC) was low, i.e., 0.3% and 0.02 mg kg -1 respectively. Biochar acidity was mainly due to phenolic groups (2.1 cmol(+) kg -1) rather than carboxylic ones (0.14 cmol(+) kg -1), while Pb, Cd, and Zn were not detected. Triplicate mesocosms (approx. 15 kg each) were set up in plastic containers for control soil (C soil), soil amended with 2.5% biochar (2.5-Bio), and soil amended with 5.0% biochar (5.0-Bio). Such biochar rates were established based on previous studies carried out on soils with a PTE pollution status comparable to the one investigated here (e.g., [18,40D. Before addition to soil, biochar was sieved to <2 mm. Mesocosms were left to equilibrate for 3 months at 20-22 °C and a constant humidity level (i.e., 40% of their water holding capacity). During this time, they were mixed weekly to favor soil -amendment contact. 2.2. Soil Chemical Analyses After the contact period, physico-chemical analyses were carried out on duplicate soil samples from each mesocosm. Soil pH and electrical conductivity (EC) were determined in 1:2.5 and 1:5 soil -to - water suspensions; available P and cation exchange capacity (CEC) were determined using the Olsen and the BaCl2-triethanolamine methods, respectively, according to Gazzetta Ufficiale n. 84 [41]. Soil organic C and total N were determined using a Leco CHN628 CHN analyzer and a Soil LCRVI Leco part no. 502-697 as a calibration sample. DOC was quantified following Manzano et al. [19], while pseudo -total PTE (i.e., Pb, Cd, and Zn) was determined after microwave mineralization of soil samples (as previously reported) using a Perkin Elmer AAnalyst 400 HGA 900 atomic adsorption spectrometer (FAAS) for Zn and a Perkin Elmer AAnalyst 400 equipped with an HGA 900 graphite furnace (GFAAS) for Pb and Cd. The NIST-SRVI 2711 -certified reference soil was included for quality assurance. 2.3. Mobility of Pb, Cd, and Zn in Soil The mobility of Pb, Cd, and Zn in each mesocosm was evaluated (after the contact period) through the sequential extraction procedure described by Basta and Gradwohl [42]. Readily soluble and exchangeable fractions (labile PTE) were quantified after the extraction of duplicate soil samples (1 g each) from each mesocosm with 0.5 M Ca(NO8)2 solution, acid -soluble fractions, and those weakly complexed by soil colloids were quantified after extraction with 1 M NaOAc (pH 5); finally, surface- complexed and precipitated PTE fractions were quantified after extraction with Na2EDTA (pH 7). Residual PTE (i.e., very insoluble and occluded fractions) were quantified after microwave soil mineralization as described for pseudo -total PTE. After each extraction step, the soil suspensions were centrifuged (3500 rpm for 10 min), and the PTE concentration in the filtered supernatant (0.45 pm cellulose acetate filters) was determined using FAAS and GFAAS as already reported. 2.4. Culturable Microorganisms and Soil Microbial Biomass After the contact period, the number of total culturable heterotrophic bacteria, fungi, actinomycetes, and Pseudomonas spp. was determined in duplicate soil samples (10 g) from each mesocosm as previously described [2]. Briefly, soil samples were serially 10 -fold diluted using a 0.89% NaCl solution, and aliquots (100 uL) of the resulting suspensions were used to inoculate Petri dishes containing the following microbiological growth media: 1:10 Tryptone Soy Agar (for heterotrophic bacteria; Microbiol, Cagliari, Italy); Rose Bengal Chloramphenicol Agar (for fungi; Biolife, Monza, Italy); Actinomycetes Isolation Agar Glycerol (for actinomycetes; Difco, Milan, Italy); Pseudomonas Selective Agar (for Pseudomonas spp.; Microbiol, Cagliari, Italy). Colony counts were carried out after 48 h of incubation at 28 °C for heterotrophic bacteria and fungi and after 72 h at 28 °C for actinomycetes and Pseudomonas spp. Microbial counts were expressed as Loglo colony -forming units (CFU g-1 soil). Soil microbial biomass (SMB) was estimated in each mesocosm using the chloroform -fumigation extraction method, as reported by Nunan et al. [43]. In brief, duplicate soil samples (40 g) from each mesocosm were divided into two 20 g aliquots: one was immediately extracted with 80 mL of a 0.5 M K2504 solution after shaking (60 min) and filtering with Whatman No. 42 filter paper; the other was incubated for 24 h under vacuum with ethanol -free chloroform as described by ISO 14240-2 [44] and subsequently extracted as described for the unfumigated samples. Afterwards, the increase in UV readings at 280 nm (A280) of the fumigated vs. unfumigated extracts was used to estimate soil microbial biomass C, as previously reported [40]. The values of soil microbial biomass C were expressed as pg C kg -1 soil. 2.5. Molecular Analysis of the Soil Bacterial Community through 16S rRNA Gene Amplicon Sequencing 2.5.1. Bioinformatics After the contact time, the PowerSoil DNA isolation kit (Mo Bio Laboratories, Carlsbad, CA, USA) was used to extract DNA from soil samples (-500 mg) of each mesocosm. DNA extracts were provided to the Integrated Microbiome Resource sequencing center (Dalhousie University, Halifax, NS, Canada), and amplicon sequencing was performed according to their Illumina MiSeq 2x300bp in-house protocol for amplicons generated with the V4 -V5 515FB (5'- GTGYCAGCMGCCGCGGTAA-3')/926R(5'- CCGYCAATTYMTTTRAGTTT-3') primers [45,46]. The retrieved sequences were subjected to quality assessment and control with the dada2 v1.24.0 [47] pipeline using the R software v4.1.3 [48], and ASV matrices were obtained as follows. Sequence reads were trimmed at the first instance of very low bases (Phred Q values of 2) while screened from the read error -prone end towards the start. The remaining parts were rejected if the expected error rates were at most 2 or if the remaining read parts were shorter than 150 bp. Moreover, read - pairs where the reconstruction of the amplicon of origin via merging (allowing no mismatches) was not possible were removed. Finally, chimeric, non-specific, or off -target amplicons (non - prokaryotic, unclassified, mitochondrial, or chloroplast) were also rejected from downstream analysis. Classification of the ASVs into taxa was performed with the Bayesian Classifier [49] version of dada2 against the Silva v138 database using an 80% bootstrap cutoff value [50] . The retrieved phylogenetic markers were also analyzed for their functional potential with PICRUSt2 [51] using the default parameters. 2.5.2. Biostatistics The retrieved ASV and predicted microbial function matrices were used for a series of statistical analysis tasks. a -diversity indices representing members or functions of the studied microbial communities of various dominance levels were calculated with the Vegan v2.6-4 [52] and the Entropart v1.6-11 [53] R packages. Specifically, the observed richness (representing all communities), the Shannon index (representing the, at least, low -dominance community members), the Inverse Simpson index (representing the, at least, intermediate -dominance community members), and the Fisher's a index (representing the highly dominant community members) were calculated. Permutational multivariate analysis of variance (PERVIANOVA) and canonical analysis were performed with the vegan package of R to assess the effect of the biochar treatment on the microbial communities and their functions. Analysis of variance with the Tukey's post hoc test or their non -parametric equivalents (Kruskal-Wallis and the Wilcoxon rank sum analysis) was used for comparing a -diversity indices, while analysis for differentially abundant taxa between treatments was performed with the Kruskal-Wallis (k test -factor levels, with k > 2) and the Wilcoxon rank sum (pairwise) analysis. 2.6. Soil Enzyme Activities and Community Level Physiological Profile Dehydrogenase (DHG) and urease (URE) were quantified (after the incubation period) in duplicate soil samples from each mesocosm. Both enzyme activities were determined using the protocols described by Alef and Nannipieri [54]. Briefly, the DHG activity was determined colorimetrically (A480) as triphenyl formazan released after incubation of soil samples (10 g at 30 °C for 24 h) with triphenyl tetrazolium chloride, while URE was determined as ammonia released (A690) after incubation of soil samples (5 g at 37 °C for 2 h) with urea [54]. The Biolog community -level physiological profile (CLPP) was obtained for soil microbial communities extracted from the different mesocosms, as reported by Diquattro et al. [2]. In particular, soil microbial communities from the different mesocosms were inoculated in 96 -well Biolog (microtiter) Ecoplates (Biolog Inc., Hayward, CA, USA) containing a total of 31 C sources of environmental relevance (one in each well) and a blank well replicated three times. After recording the A590 readings for each well (every 24 h for 5 days), using a Biolog VIicroStationTM reader (Biolog Inc., Hayward, CA, USA), the following CLPP indexes were determined, i.e., the Average Well Color Development (AWCD), the Shannon -Weaver index (H), and the Richness (S) value. The AWCD, or the potential catabolic activity of the different soil microbial communities, was calculated as in Equation (1): AWCD=>31 i=1(Ri—C)/31AWCD=>i=131Ri—C/31 (1) where Ri is the absorbance value (A590) of each response well, C is the absorbance value of the control well, and 31 is the number of C substrates in the plate [52]. H; indicating the catabolic functional diversity (substrate use) of the different soil microbial communities, was calculated as in Equation (2): H'=-> (pi (Log pi))H'=-> pi Log pi (2) where pi is the absorbance ratio of each of the 31 substrates to the total absorbance value of the plate [55]. S was calculated as the number of C substrates used (A590 > 0.15) by the different soil microbial communities [56]. Standardized A590 values, i.e., [(RI C)/AWCD of the plate], were also subject to Principal Component Analysis (PCA) using the variance/covariance matrix [56] to allow for a more straightforward data interpretation of multidimensional data. 2.7. Plant Growth and PTE Uptake After the incubation time, the soil from each mesocosm was used to fill 2 pots (approx. 2 kg of soil each), which were planted with triticale (x Triticosecale Wittm. cv. Trimour) and tomato (Lycopersicon esculentum L. cv. Rio Grande) seeds. These species, characterized by different physiologies and taxonomically distant, were chosen as bioindicator organisms to fully evaluate the remediation effectiveness of biochar and not to test the possibility of growing food or feeding crops in the polluted soil. Ten and five plants of triticale and tomato were grown, respectively, in each pot (without fertilization) for 2 months at 20-22 °C. At harvest, plants were removed from pots, and roots and shoots were carefully washed. All plant heights were recorded, shoots and roots were separated, and their dry weight was determined after 10 days in the oven at 55 °C. To quantify PTE uptake, root and shoot tissues were mineralized using microwave (ultraWave, Milestone, Sorisole, Italy) and a digestion solution containing 2 mL of suprapure H2O2 and 4 mL of a mixture of HNO3 and ultrapure H2O (ratio 1:1). After mineralization, Pb, Cd, and Zn were determined using FAAS for Zn and GFAAS for Pb and Cd. Peach leaves (NIST-SRM 1547) were used as standard reference material for quality assurance. 2.8. Data Analysis Soil chemical, biochemical, and microbiological data are reported in tables and figures as mean values ± standard errors (SE). Data were analyzed to investigate differences due to the treatments applied (i.e., biochar at two different rates). All traits were evaluated for normality and homoscedasticity using the Shapiro and Bartlett tests, respectively. The variables that passed both tests were analyzed through ANOVA, whereas those that did not were analyzed through the Kruskal- Wallis test (p < 0.05). In Table S2, the statistical analysis adopted for each of the investigated traits was reported. All statistical analyses were carried out in R 4.2.1 [48]. 3. Results and Discussion 3.1. Influence of Biochar on the Chemical Characteristics of the Polluted Soil The main physico-chemical characteristics of the polluted soil used in this study are reported in Table 1. This latter soil had a sandy loam texture with an acidic pH and a low content of organic matter, total N, and DOC. However, available P and GEC values were high, but pseudo -total concentrations of Pb, Cd, and Zn were all abundantly exceeding the threshold values established by the Italian law for potentially contaminated soils devoted to commercial and/or industrial use (i.e., 1000, 15, and 1500 mg kg -1 for Pb, Cd, and Zn, respectively; [57]) or to agriculture (i.e., 100, 5, and 300 mg kg -1 for Pb, Cd, and Zn, respectively; [58]). Overall, these data suggest limited soil fertility, with N being the most limiting factor for agricultural yields [59], and with low pH and high PTE content adding more stress for plant establishment and growth, as well as for the soil microbial community [42,56,60]. The low DOC content also suggests some additional constraints on microbial growth and abundance in the studied soil. Table 1. Selected physico-chemical characteristics of the contaminated (C soil) and biochar- amended soils (2.5-Bio and 5.0-Bio). Mean values ± SE followed by different letters within a row denote statistically significant differences (p < 0.05). Table 1. Selected physico-chemical characteristics of the contaminated (C soil) and biochar- amended soils (2.5-Bio and 5.0-Bio). Mean values ± SE followed by different letters within a row denote statistically significant differences (p < 0.05). Physico-Chemical Characteristics C Soil 2.5-Bio 5.0-Bio Texture pH CE (pS cm -1) Organic matter (g kg -1) Total N (g kg -1) P Olsen (mg kg -1) CEC (cmol(+) kg -1) DOC (mg kg -1) Pb (mg kg -1) Cd (mg kg -1) Zn (mg kg -1) Sandy loam 5.74 ± 0.02 a 376±9a 32.67 ± 0.58 a 1.00 ± 0.0 a 31.53 ± 1.22 a 24.36 ± 0.02 a 13.79 ± 0.43 b 10.625 ± 2058 a 28.3 ± 0.4 a 3407 ± 140 a OD 6.35 ± 0.01 b 325±5b 34.67 ± 0.58 b 1.00 ± 0.0 a 32.43 ± 0.98 a 24.55 ± 0.08 b 12.51 ± 0.26 a 10.238 ± 372 a 27.2 ± 1.05 a 3291 ± 241 a 6.58 ± 0.01 C 333+4b 36.33±0.580 0.91 ± 0.0 b 35.73 ± 0.47 b 25.15 ± 0.42 C 12.04 ±0.12 a 10.064 ± 141 a 27.1 ± 1.07 a 3323 ± 120 a Biochar addition increased soil pH, which approached neutrality in 5.0-Bio (Table 1). This was due to biochar alkalinity (Table S1), and it is expected to have a positive impact on both soil physico- chemical properties, e.g., through the reduction of soluble Al`s+ and PTE, and soil microbial activities [61]. Also, the increase in available P (especially in 5.0-Bio) and CEC recorded in amended soils is deemed positive, as these latter are important soil fertility parameters. The biochar ability to increase soil CEC was previously reported and attributed to the presence of oxygen -containing functional groups on biochar surfaces (e.g., carboxylic and phenolic) able to retain cations [12]. Moreover, biochar's natural oxidation and/or its incubation with soil can further increase the formation of oxygenated groups [62], likely explaining the CEC values of amended soils. The high amount of available P in biochar (i.e., 85 mg kg -1 soil; Table S1) can finally explain its increase in the amended soils (especially in 5.0-Bio; Table 1). 3.2. Influence of Biochar on the Mobility of Pb, Cd and Zn in Soil Both rates of biochar had a great influence on PTE mobility, significantly reducing the concentration of labile (readily soluble and exchangeable) Pb, Cd, and Zn in the amended soils (Figure 1). For instance, labile Pb [extracted with Ca(NO3)2] reduced by approx. 76% in 5.0-Bio, while in the same soil, Cd and Zn reduced up to 27 and 37%, respectively (Figure 1). Weakly complexed Pb (extracted with NaOAc) reduced up to 46% in Bio-5.0, while Cd and Zn increased or remained unchanged, respectively (Figure 1). After biochar addition, the surface complexed and precipitated PTE (extracted with Na2EDTA) reduced in the case of Pb (up to —5%) and Zn (up to —26%) but remained unchanged for Cd. Very insoluble and occluded fractions (residual PTE) remained unaffected for Pb and Cd, while significantly increasing for Zn (up to —45%). Ph rrta%eel (nag kg1 :sofa) 80 60 o Ca(Najh D MID& 1 • NagilYTA ■ Residual i C' sell 2.5 Bio 5.10-Bik Cd released (rug k -I U 20 - 15 - 10 5 e woo 1750 - 1500 7 1250 1440 • 5.00 ▪ 75O 250 U a (` Soil a a 2 5-Tld C soil 2,5 -Kith Figure 1. Concentrations of Pb, Cd, and Zn extracted from contaminated control (C soil) and amended soils (2.5-Bio and 5.0-Bio) using the sequential extraction procedure. Color bars refer to the different extraction solutions. For each PTE and within the same extraction solution, different letters indicate significant differences between treatments (p < 0.05). During the three-month contact period, a PTE redistribution clearly occurred in amended soils (especially in 5.0-Bio), leading to a shift from more mobile and potentially bioavailable fractions [i.e., labile PTE extracted with Ca(NO3)2] to less mobile and poorly bioavailable ones (e.g., those extracted with Na2EDTA and/or residual). This was previously reported by other studies (e.g., [63D ) and is of outmost importance from a remediation perspective since labile PTE are the most impactful on plants and soil (micro)organisms [4,18,40]. Such biochar-driven PTE redistribution towards less bioavailable fractions can be due to a variety of mechanisms, such as: (i) Pb, Cd, and Zn partial precipitation as oxides or hydroxides following the significant pH increase in the amended soils [7]; (ii) the formation of insoluble PTE -phosphates or PTE -carbonates (e.g., the biochar used contained substantial available phosphate, Table 1; [8]); (iii) the formation of strong complexes between PTE and oxygenated functional groups of biochar (e.g., phenolic and carboxylic, Table 1; [64] ); (iv) PTE surface adsorption and diffusion within biochar pores [7,14]. 3.3. Influence of Biochar on Culturable Microorganisms and Soil Microbial Biomass The size of the targeted culturable soil microbial communities was mostly unaffected by biochar addition (Figure 2). The number of total heterotrophic bacteria, actinomycetes, and fungi did not change after soil amendment, while that of Pseudomonas spp. was reduced by approx. 10 -fold (Figure 2). This is interesting as in the very few studies focusing on the effect of biochar on soil culturable microorganisms, increased microbial numbers were commonly reported after amendment (e.g., [65,66,67]). Our results can be explained by the DOC values recorded in the amended and unamended soils: DOC represents an important source of C for soil microorganisms [68], and its marginal reduction in the amended soils, also reported by Manzano et al. [19] and explained by adsorption phenomena, did not allow an increase of culturable microorganisms, while it reduced the number of Pseudomonas spp. [69]. However, PAHs accumulated in biochar during pyrolysis could have contributed to such adverse effects against Pseudomonas spp. [24]. Both DOC reduction and PAH accumulation in amended soils could also explain the approx. 60% reduction of SMB recorded in 5.0-Bio (Figure 3). Similar results were reported by Andres et al. [27] after adding maize biochar to Mediterranean vineyards and by Dempster et al. [30] after using eucalyptus biochar in wheat cultivation. While the impact of the highest amount of soft -wood biochar was clear, at least vs. Pseudomonas spp. and SMB, its relevance for soil functioning is hardly predictable, although microbial biomass is recognized to play a relevant role in soil ecosystem functioning and productivity [70]. Total .helcrotropbk+c bacteria AC ri 110 wenn I0 7,4) 44 6.0 ;mw 40 40 10 i5 z0 LO t ora Q 8.0 7,0 6.0 5.0 4.0 3.14 1.0 01) C scM 2.t-ffo Log CET Etl, soil 7.0 6.0 5,0 4.0 3.0 .0 1.0 C soil t soL1 5 Vie 45.0_Olilo Figure 2. Number of culturable microorganisms in contaminated control (C soil) and amended soils (2.5-Bio and 5.0-Bio). For each microbial group, different letters indicate significant differences between treatments (p < 0.05). µg SIV -C" kg -1 sail 40 35 30 25 20 15 10 5 0 C soil 2.5-Bio 5.0=Bio Figure 3. Soil microbial biomass C (SMB-C) in contaminated (C soil) and amended soils (2.5- Bio or 5.0-Bio). Different letters indicate significant differences between treatments (p < 0.05). 3.4. Influence of Bio char on the Structure of Soil Bacterial Community ASV matrices were generated with dada2 as described in the materials and methods. Out of a total of 261,009 read pairs, a final amount of 47,618 high -quality sequences passed the quality control process and were used in the analysis (Table 53). Significant differences between the control soil and 5.0-Bio were observed in a -diversity indices, i.e., the observed richness S, the Shannon, and the inverse Simpson (Figure 4A). In the case of the Fisher's a index, which is more representative of the highly dominant ASVs, no significant differences resulted from the tests performed. Twelve phyla dominated the samples, with Acidobacteriae, a-Proteobacteria, Bacteroidia, y-Proteobacteria, Gemmatimonadetes, and Vicinamibacteria being the most dominant among those (Figure 4B). Principal coordinates analysis (PCoA) showed a partial separation of the treatments, mostly due to the 5% biochar treatment (Figure 4C). Differential abundance analysis showed that 5 ASVs were mainly responsible for these structural differences, belonging to Bacteroidota, Proteobacteria, and Acidobacteriota (Figure 4D). A Observed S Shang Irw. Simpson 500 4X cp. C CI 0 r I' a CsI 3'1'1 7 6 5 300 Ei3 iso a too fi 42 - Alai [Mk. 02 D we. 40 Fishes a too A SY000076 CAI t4 p a).on C iI[IIl 2_.5 -Bias 5-G11i —0 a A 9'C •:!iJO jr +bat+ r (PM eolbettecial 6.035 C song rob 2,5-WWob 5-BW, I 7` o S ()out kihi Or, CPS ASO ■ .. .. traciwg Ems . Sts xismatsamin Eta Wackettida a ctirectsita Ulloplosilten ItattOzcadotant, CLiitninintligotiaria ICinmancrisiacear Nitviercagitebtrait z a :i is Uttixports is aprrwrisnasenes MBir pi * • Aitcapracarae Phyi igeb iiN. In Atli j St ■ Plintatactrat IS . $00010,10W • ,- u-asects. fiAletratol14 8iit tlitataitoten ilitadoboolteretil pUMS c soil lib .. -� Dab Pit U It it *4 '.W 410 .0 AIV003257 p. i10 P 44 II"I+ 24-810 I b S -E 41 p 004 C SOW lot 401 Ifs 4st dtt Figure 4. Microbial community data analysis outputs for contaminated (C soil) and amended soils (2.5-Bio or 5.0-Bio). (A) a -diversity boxplots with ANOVA results and post hoc pairwise Tukey's analysis (a 0.05). (B) Barplots of the dominant taxa with taxonomy resolution as low as family level. (C) Principal coordinates analysis (PCoA) scatter plot generated using the Bray -Curtis dissimilarity, with the explained variance provided at each axis. (D) Barplots of the five ASVs showing differential abundance between the treatments (different letters indicate significant differences according to Kruskal and Wilcoxon rank sum tests for a of 0.05). * p < 0.05. These data indicated a positive influence of biochar, when used at the highest rate, on soil bacterial diversity. This was previously reported by other authors (e.g., [71,72]) and can be attributed to the highest reduction of labile PTE and the highest increase of soil pH, which occurred in 5.0-Bio. Both factors likely contributed to reducing the environmental pressure faced by microbial communities in the polluted soil, allowing for the appearance (and/or increase) of rare or intermediate -dominant bacterial taxa [4,71,73]. The significant abundance of Lysobacter in 5.0-Bio could also be relevant from an environmental perspective, as members of this genus produce antibiotics and can be useful in the control of plant diseases [74]. Statistical analysis of the inferred functions according to Picrust2 output was also performed (Figure 5). The results showed no significant differences in the a -diversity of the functions (Figure 5A). Major identified functional classes included Biosynthesis, Degradation/Utilization/Assimilation, Generation of Precursor Metabolite and Energy, and Macromolecule Modification (Figure 5B). PCoA showed a separation between the control soil and 2.5- and 5.0-Bio, with this latter treatment being more distant (Figure 5C). Pathways showing significant differences were those of the TCA cycle (Helicobacter type) and L-methionine, thiazole, and thiamine diphosphate biosynthesis, with all of them being reduced at an increasing biochar application rate. These data suggest that the observed changes in the bacterial community structure were likely paralleled by functional changes, which could have a role in adapting to changed environmental conditions (e.g., lower labile PTE, increased pH, reduced N and DOC content; Table 1). C r a Oesrrwd S T 1 -01 U t at. Shannon 4 C soil 2.'amo Sao ASll,1 i 1 d`w1 hi . 5. Inv, Simpson 3-11 12 B FLOWa T 1 tePh Co y 401 fr aDarraw& ragodds*as a.ILS ayaw Kan Cnl a a 2-5-840 Jtv aura ■a sitatawdePttterre: Its 4.414%11.1424~09 41 reds *Al i. Ilia, - Sea 1' t 1' 7 I I i- u 412 u• a2 a+ ill NI 1 1114 11/41 144 OE' Weis Amapa a ditti sal t_54k, Ins ft Ger Imam Ibulen I- Ames ad tam �- krio . .tPpm yr€ 'o�ff � i a can-[aa Ode' .-- w loofahs . *ow IndUps isaafi DIOS ad Ovid luddev INAmta Web PUSS* diaadiS idol Sao ilIWIltalimilifligeak Lt too wadi mutt' Oriman'Oupsian 1 SOW duo too : dos Imo limbo ��. NOM asilodip Colas. RI 0441•1 Pen*. dideaS dimenlismoworlidS tar 1st I FlP Li tarps 2: sist Whin. 'tl' Wig IM. 44i' Mr( isi<11:F4.24Wirialla'aft POI 44NWM S taffeta*" offliiinaolkageibierpolbie- R#1.-I i c SON 2L'IND ' b u.i* u e u s II II S a Figure 5. Microbial function analysis outputs according to Picrust 2 for contaminated (C soil) and amended soils (2.5-Bio or 5.0-Bio). (A) a -diversity boxplots of functions with ANOVA results and post hoc pairwise Tukey's analysis (a > 0.05; no statistically significant differences were identified). (B) Barplots of the dominant functions. (C) Principal coordinates analysis (PCoA) scatter plot generated using the Bray -Curtis dissimilarity, with the explained variance provided at each axis. (D) Barplots of the four differentially enriched pathways showing differences between the treatments (different letters indicate significant differences according to Kruskal and Wilcoxon rank sum tests for a of 0.05). 3.5. Influence of Biochar on Soil Enzyme Activities and Community Level Physiological Profile DHG activity in soil is generally reduced according to the amount of biochar added, while the opposite was found for URE. In particular, DHG reduced by approx. 60 and 75% in 2.5-Bio and 5.0-Bio, respectively, compared to control soil, while in the same soils, URE increased by 48 and 78% (Figure 6). DHG data seemed to indicate a negative biochar effect on soil microbial activity, and this was not obvious since a reduction of labile PTE (which occurred in amended soils; Figure 1) is commonly expected to increase DHG (e.g., [4,17,56]). As mentioned for culturable Pseudomonas spp., this could be due to a reduction of readily usable C sources in DOC (which occurred in amende d soils; Table 1) and/or to a direct toxic effect of biochar on soil microorganisms [24,25,32]. PAHs, but also other biotoxic compounds adsorbed and/or accumulated on biochar surfaces, e.g., environmentally persistent free radicals and/or catechol, can be responsible for microbial toxicity phenomena and the consequent reduction of DHG and SMB [32]. Interestingly, the DHG decrease recorded in amended soils could be seen as a confirmation of the reduction of the TCA pathway highlighted by Picrust2 (Figure 5C). 18 1,6 14 - 12 - 10 8 6 4 2 0 C son L;.-Bio 5.Q-E10 D16 25 a 0 0cet 15 Wa 5 0 URE a 9 9 C sail ?.5-fisr 5.0-liIu Figure 6. Dehydrogenase (DHG) and urease (URE) activities in contaminated (C soil) and amended soils (2.5-Bio or 5.0-Bio). For each enzyme activity, different letters indicate significant differences between treatments (p < 0.05). The increased URE activity observed in the amended soils, together with the reduction of total N content (Table 1), was likely indicative of a stimulation of urea hydrolysis due to biochar rather than an increased microbial content in amended soils (i.e., SMB reduced in 2.5- and 5.0-Bio; Figure 3). Such accelerated rate of URE activity in the presence of biochar was recently reported by Zhao et al. [75] and could be partly responsible for the N reduction observed in the amended soils (especially 5.0-Bio; Table 1). The increased URE observed in the amended soils can also be due to an increased microbial synthesis of the enzyme stimulated by a more limited N availability in these soils [76], which in turn can be explained by NO3-N and NH4-N adsorption by biochar, as previously observed [19]. The Biolog CLPP did not show significant differences between control and amended soils according to the AWCD, H', and Richness values (Figure S1). However, when C source consumption was analyzed by PCA, clear differences appeared. PCA, which accounted for approx. 80% of the total variance (in PC1 and PC2), highlighted substantial differences in the potential catabolic activity of the microbial communities (Figure 7). PC1 (approx. 55% of the total variance) mainly separated the different microbial communities and was correlated with the catabolism of the following substrates: P-methyl-D-glucoside (r= 0.76), D-xylose (r= —0.99), 2-hydroxy benzoic acid (r = 0.78), L- arginine (r = —0.79), and L-threonine (r = 0.77); while PC2 (approx. 24% of the total variance) was mainly correlated with the usage of a-cyclodextrin (r = 0.76), 4-hydroxy benzoic acid (r = 0.78) and a-ketobutyric acid (r = 0.79). These results support a relevant impact of biochar (and of the rate added) on the structure of the soil microbial community, as also highlighted by the molecular analysis (Figure 4 and Figure 5) and by recent studies (e.g., [23,24,28]). Overall, this kind of impact was somewhat expected given the profound changes that biochar exerted on soil physico-chemical properties and nutrient dynamics (e.g., this study and Li et al. [7]). The reduction of labile PTE in the amended soils could also have been co -responsible for the observed changes, e.g., by decreasing the abundance of PTE -resistant strains in treated soils and favoring the appearance of new ones with different catabolic capacities, as previously reported [4,5]. PTE -resistant strains in treated soils and favoring the appearance of new ones with different catabolic capacities, as previously reported [4,5]. 1,6 1.2 ?.5-Bio Q 0.8' I t 0.4 -3.0 -2.0 -1.0 0 0 1.0 2.0 3.0 fJr� `` 0.1 Si -0 s -1.2 PC 1 55.5000) Figure 7. PCA plot of standardized C source utilization data of microbial communities extracted from contaminated (C soil) and amended soils (2.5-Bio or 5.0-Bio). 3.6. Influence of Blochar on Plant Growth and PTE Uptake Plant growth was tested to gain a wider view of the role of biochar in restoring soil fertility in PTE - polluted soils. Interestingly, biochar had a different impact on the growth of triticale and tomato. The height of the former species, together with the respective shoot dry weight, were unaffected by biochar, while substantial increases were recorded for tomato (Figure S2 and Figure 8). The height of tomato plants increased by approx. 2.5- and 2.1 -fold for 2.5-Bio and 5.0-Bio, respectively (Figure S2), while shoot dry weight increased by approx. 8.0- and 4.5 -fold in the same soils (Figure 8). Moreover, the higher biochar rate had a negative effect on triticale root dry weight, while both rates had a positive effect on the weight of tomato roots, with 2.5-Bio revealing the most effective treatment (Figure 8). 60 .-. so co 110 or E o 30 bo ni 20 aie t 10 0 a c so a 40 8 X30 tID 4-U 3 lU C soil i _ a Tritiale root 2,:5=Bio Tomato root 5rOaBka C soil 2.5-81c SM-Bio 2 - 175 - I 150 -' r 125 1no -4r � 3 fa) 3 sIJ 0 200 Ts 175 Tic 150 125 Y[1n am 75 ezt 3 5.13 ll In Trhtlkale shoot 1 a C soil C soil 2.5-8its 5,0 -Rio I a I 2.5-Bio 5-0-Bio Tomato shoot t Figure 8. Root and shoot dry weight of triticale and tomato plants grown in contaminated (C soil) and amended soils (2.5-Bio or 5.0-Bio). For each parameter, different letters indicate significant differences between treatments (p < 0.05). Overall, these data highlight the importance of using different plant species to understand the biochar potentials in the recovery of soil fertility in PTE -polluted soils. Our results suggest a quite different tolerance/sensitivity of the two plants towards labile PTE (as evident from the comparison of plant growth in control soil) and a different adaptation to soil chemical characteristics, e.g., pH and total N. Tomato yield increased dramatically when labile PTE was reduced in the amended soils, while triticale did not (Figure 8), likely suggesting a higher PTE tolerance of the latter species that allowed substantial plant growth in the control soil. This is probably why triticale, likewise other grass species, has been used in different phytoremediation studies (e.g., [77,78,79,80]). Furthermore, S. lycoperslcum is very sensitive to soil acidity (and soluble Ala+ ), and the pH increase recorded in 2.5- and 5.0-Bio could have contributed to improving its growth in the amended soils [81]. Finally, the yield reduction observed for both plant species in 5.0-Bio compared to 2.5-Bio was likely due to excessive nutrient adsorption by biochar, which reduced plant growth, and/or to other biochar toxicity effects previously reported [24,25]. In the first case, combining biochar with fertilizers and/or using biochar enriched with nutrients could mitigate the nutrient depletion effects arising from excessive biochar rates [24]; in the second case, phytotoxic effects can be avoided using lower biochar amounts, e.g., ≤2.5% [25]. Also, biochar influence on PTE uptake differed depending on the plant species: the concentration of Pb and Cd in triticale roots increased in the amended soils (up to 36 and 100%, respectively, vs. control), while that of Zn was reduced (up to 76% vs. control; Table 2). These results could be explained by a higher and/or altered root activity in the amended soils (e.g., increased secretion of siderophore, organic acids, and other root exudates), which led to enhanced Pb and Cd mobilization from the soil and their subsequent uptake [79], as well as a reduced Zn uptake (which was also correlated with the reduction of labile Zn in the amended soils; Figure 1). Table 2. PTE uptake (mg kg -1, mean ± SE) by triticale and tomato plants grown in contaminated (C soil) and biochar-amended soils (2.5-Bio or 5-Bio). Mean values ± SE, followed by different letters within each column, denote statistically significant differences between treatments (p < 0.05). ND was not detected because of the limited availability of root biomass. es Table 2. PTE uptake (mg kg -1, mean ± SE) by triticale and tomato plants grown in contaminated (C soil) and biochar-amended soils (2.5-Bio or 5-Bio). Mean values ± SE, followed by different letters within each column, denote statistically significant differences between treatments (p < 0.05)_ ND was not detected because of the limited availability of root biomass. Triticale C soil 2.5-Bio 5.0-Bio C soil 2.5-Bio 5.0-Bio Pb Uptake (mg kg -1) Shoots 39.2 ± 0.3 b 38.3 ± 0.5 a 53.3 ± 0.2 c Roots 434.8 ± 21.5 a 593.7 ± 2.9 b 456.8 ± 25.3 ab Pb uptake (mg kg -1) Shoots 514.7 ± 22.8 C 89.2 ± 7.4 a 115.5 ± 9.2 b Roots ND 695.4 ± 20.3 b 616.8 ± 17.0 a Cd Uptake (mg kg -1) Zn Uptake (mg kg -1) Shoots 5.7±0.1 b 5.1 ± 0.1 a 7.9 ± 0.1 c Roots 30.3 ± 1.1 a 61.6 ± 1.1 c 52.6 ± 0.7 b Tomato Cd uptake (mg kg -1) Shoots 17.7 + 0.6 b 15.3 ± 1.1 a 24.9 ±0.2 c Shoots 631.1 ± 25.8 a 733.2 ± 5.0 c 683.4 ± 10.1 b Roots 1596.3 ± 8.3 C 1307.4 ± 19.7 b 928.0 ± 6.7 a Zn uptake (mg kg -1) Roots Shoots ND 2843.1 ± 22.3 c 133.5±2.1 b 879.1 ±86.5b Roots ND 4859.2 ± 28.3 b 104.2±1.7a 680.3±9.5a 3101.2±28.4a With regards to tomato, PTE uptake by roots was reduced in 5.0-Bio vs. 2.5-Bio (Table 2) in agreement with labile PTE in these soils (Figure 1; control root yield was not enough to quantify PTE uptake). Differently from triticale, these data support a clear positive influence of biochar on the fertility recovery of PTE -polluted soils, as highlighted elsewhere [5,18]. In both triticale and tomato plants, PTE was largely accumulated in the roots rather than the shoots (Table 2). Overall, biochar impact on PTE uptake by shoots was more limited in the case of triticale and, for both plants, confirmed a better effectiveness of 2.5-Bio rather than 5.0-Bio in reducing Cd and Pb concentrations in the aerial part. 4. Conclusions The results from this study showed that softwood biochar added at 2.5 and 5.0% rates was able to significantly reduce labile (and potentially bioavailable) Pb, Cd, and Zn in a PTE -polluted mining soil and to increase selected fertility parameters (e.g., soil pH, available P, and GEC). This is relevant from a practical viewpoint since it suggests reduced ecotoxicological effects in amended soils as well as increased functionality. However, soil microbiological and biochemical data did not support this view, with the exception of bacterial a -diversity (which increased in 5.0-Bio vs. control) and urease activity (which increased in both 2.5- and 5.0-Bio vs. control). These results raise some questions about the overall biochar impact on soil functionality, or at least the ideal amount that should be added to any soil. In this regard, 2.5-Bio appeared to be the most effective treatment able to combine soil chemical restoration with a limited impact on soil microorganisms (e.g., on Pseudomonas ssp.) and biochemical activity (DHG was repressed but URE was stimulated by 2.5- Bio). This was supported by plant growth data, which showed reduced tomato and triticale yields for 5.0-Bio vs. 2.5-Bio, likely due to excessive nutrient adsorption by biochar. Overall, our results showed that chemical data alone cannot be sufficient to predict the effect of biochar on soil functionality, while the measurement of several (micro)biological proxies and the use of different bioindicators, such as different plant species, can be helpful. Given the significant role of plants in shaping rhizosphere microbial communities and their activities (e.g., through their root exudates), further studies should focus on the impact of endemic plants on the microbial abundance and diversity in biochar-amended polluted soils. Supplementary Materials The following supporting information can be downloaded at: https://www.mdpi.com/article/10.3390/soilsystems7040096/s1, Figure 51: AWCD, H', and Richness values of contaminated (C soil) and amended soils (2.5-Bio or 5.0-Bio); Figure S2: height of triticale and tomato plants grown in contaminated (C soil) and amended soils (2.5-Bio or 5.0-Bio); Table Si: selected chemical properties of the biochar used in this study; Table S2: statistical analysis adopted for each of the investigated traits; Table S3: quality control (QC) of the received sequence data. Author Contributions Conceptualization, P.C. and G.G.; methodology, M.G., P.C., M.V.P., S.D., A.C., N.P.M., S.V. and G.G; formal analysis, M.G, M.V.P., A.C., N.P.M. and S.V.; investigation, P.C., M.V.P., S.D. and G.G.; resources, G.G.; data curation, M.G., M.V.P., S.D., A.C., N.P.M. and S.V.; writinr original draft preparation, G.G.; writinr review and editing, P.C. and S.V. All authors have read and agreed to the published version of the manuscript. Funding This research was supported by the Agritech National Research Center and received funding from the European Union Next-GenerationEU (PIANO NAZIONALE DI RIPRESA E RESILIENZA (PNRR) MISSIONE 4 COMPONENTE 2, INVESTIMENTO 1.4 D.D. 1032, 17 June 2022, CN00000022). This manuscript reflects only the authors'views and opinions; neither the European Union nor the European Commission can be considered responsible for them. James D. Stewardson 13918 County Road 4 Brighton, Colorado 80603-5730 14 October 2024 Weld County Planning & Zoning Ms. Diane Aungst, Planner P. O. Box 758 1402 N. 17th Avenue Greeley, CO 80632 RE: Record USR24-0019; Public Comment & Objection; Proposed Biochar Production Facility on Weld County Road 6 Dear Ms. Aungst, SUMMARY Please consider my and my family's request to deny approval of the above referenced Use by Special Review application from Biochar Now LLC, and please insure that the WC Commissioners are apprised of our objections to the proposed project. BACKGROUND My wife and I own a 175 acre farm along WCR 4, one mile south of the proposed facility; we have been residents of said farm since 1985. We, as Weld County residents, count on our County Government to foster & help maintain the quality, and especially the safety, of our community's environment. The ro osed location of the Biochar facility is in an established agricultural area, consisting of high - value value homes and farms that produce high quality agricultural products, such as animal feed & livestock. In reviewing the available application documents from Biochar Now, we are persuaded that the Biochar production facility would degrade the community environment in multiple ways, proposed would provide no obvious benefit to said community, the County or the State, and that approval of the USR Application that has been presented for its construction should therefore be denied. 1. Environmental noise levels The proposed facility would clearly emit assorted sounds at levels and durations significantly higher than those historically present in the surrounding community. This issue has obviously been given considerable attention by the applicant, as they have commissioned an extensive Facility Operational Noise Modeling Report. The Report itself seems to contain some inconsistencies internally as well as with other of the Application documents. On page 3 of the Noise Modeling Report the following statements are made: "The operation will occur only during the daytime. Therefore, the operational noise will be assessed against the Weld County Daytime noise limit of 55 dBA". These statements seem to be at odds with other statements in the Report and other Application documents which do not suggest restricting the operation of p the proposed facility to daytime hours. Additionally, in Paragraph 5. On Page 17 of the Noise p p Report referencing the Screener Operation, the "75dBA noise limit at all receptors" that is referenced is very loud, and if a noise level of this magnitude were to be present for up to 15 minutes of every hour, as referenced elsewhere in the Report, such noise would be extremely annoying to humans and animals in the area. We suggest that if such sound levels and durations were to occur at night no human with their house windows open and no outside animal within half a mile of the source would be able to sleep normally. As time & location sound monitoring is easily accomplished with currently available monitoring equipment, the absence of a sound monitoring protocol or a remedial action procedure in the Application should result in rejection of said Application. 2. Negative effect of increased access -road traffic We note that no study of the effects of additional truck vehicle traffic on WCR 6 has been submitted by the petitioner. According to one of the Biochar company representatives at the informational meeting which the company hosted on Saturday, October 12, 2024, no such study has been done. We suggest that the location of the proposed facility along the fragile, graveled section of WCR6 east of Highway 85 along with expected new truck traffic would result in a vastly increased generation of road dust during dry weather as well as rapid deterioration of the road surface during inclement weather. Failure of the Application to address this issue up front should be cause for its rejection. 3. Air & soil cleanliness No air or soil cleanliness monitoring is contemplated in the Application proffered by Biochar Now LLC, nor is there any stated means of controlling the type of or quality of incoming raw materials which may be reasonably expected to produce noxious emissions when burned. The burning of common coatings on waste wood such as lead based paints, various wood preservatives (including creosote), galvanized steel nails, coated assorted steel parts or assorted pl astics, as well as the burning of unspecified materials themselves are all known to potentially produce noxious fumes. The lack of any requirement for an incoming material acceptance/rejection procedure may therefore lead to the burning of noxious and potentially toxic incoming materials. From a search of articles available online, the burning of sewage sludge, barnyard & feedlot waste and other assorted plant waste is also common in this industry and has not been precluded by any statement in the referenced Application. The absence of a formal requirement for responsible handling of incoming materials as well as for the strategic monitoring of air emissions fatally flaws this Application in our opinion. 4. Soil & Ground water contamination. Any toxic air emissions will likely settle on the surrounding land areas as well as on above- ground agricultural water and its transport & storage structures, and would result in degradation of the quality and safety of those surrounding areas for humans as well as for any agricultural products exposed to it. Storage of toxic materials on the site of the proposed facility will also potentially contaminate the land on which it is stored, which contamination can migrate in the soil, contaminate adjacent properties and agricultural water sources, and be very difficult to remove. The apparent lack of effective standards or procedures for the handling of potentially toxic materials should result in the rejection of this Application. 5. Property tax revenues We believe that approval of the referenced project would result in a reduction of value of the surrounding farm/residential properties that would not be offset by increased tax revenues from the proposed new facility, and that the Application for construction of the Bio Char facility should be rejected on this basis alone. We also maintain that approval of the referenced Application would result in a net decrease in the production of high quality farm products in Weld County. Over the years that we have lived here we have observed that Weld County has produced large amounts of high quality agricultural products, a significant portion thereof that has provided feed and raw materials to established WC industries, such as dairy farms, animal feed lots, and meat packing plants; and that anything we might do that lessens the availability of feed for marketable and productive animals will be of negative value to those industries - consequently inhibiting their business health & future expansion potential. The Biochar Application does not contain any economic or tax analysis reflecting its potential value to the County or State; furthermore there is no assertion that the prospective Bio Char product would be sold or beneficially used in either Weld County or the State of Colorado. CONCLUSION We Weld County residents have historically relied on the County to protect our living and working environments from harmful and unwelcome degradations. Please continue that wholesome tradition by rejecting the subject Application. Sincerely, 7 Cs) G'G4'l4,1 jL.9 r James D. Stewardson Tel: 303-659-5509 (res) Tel: 303-570-2740 (cell) FAX: 303-659-5731 e-mail — jimstew@mesanetworks.net 9/17/2024 To: Weld County Department of Planning Services Diana Aungst From: Tony Hale 14760 County Road 6, Ft. Lupton, CO 80621 Re: Case #: USR24-0019 NGL Water Solutions DJ LLC Ms. Aungst: It has been brought to our attention via post card received and neighbors regarding the above referenced case involving NGL Water Solutions and Biochar Processing. For reference, our home is to the east bordering the proposed location of Biochar Processing. When NGL was proposing installing SWD wells on this reference property, we were assured that no other development would take place on this property. This new proposal feels like they are going back on what surrounding landowners were initially led to believe. We do NOT feel that installing a Biochar Processing facility would be in the best interest of anybody other than NGL and Biochar for the following reasons: 1) Air quality. We already struggle with current air quality due to two members of our household being diagnosed with asthma (utilizing inhalers) and allergies. One with severe problems during poor air quality times. His pediatrician has been consulted and agrees that this facility will be potentially harmful to his ability to breathe normally. Installing a facility that will emit m.oretair pollutants within a few hundred feet of our home can do nothing but negatively impact our health. While we realize that the end product from biochar technology has the ability to aid in emissions reduction with application, the production facility where it is created within this close proximity to where we live, would be harmful to us. 2) Agricultural land should stay agricultural land wherever and whenever possible. We have not seen, heard or been told why this facility needs to be at this location instead of current available appropriately zoned acreage. What is the reasoning that the Biochar facility must be at this location? This is an agricultural area and should remain as such. 3) The facility wilt GREATLY damage our home value. The most valuable asset of our home is the view to the west. With the facility installation and operation, that view will be removed and destroyed. 4) Traffic increase. This area is already seeing a large increase in traffic due to increasing population. Adding the Biochar Processing facility will only amplify the problem. In summary, our family strongly objects the proposal to grant this USR for the installation of a Biochar Processing facility. We are planning to utilize any and all resources available to us to oppose this installation to the fullest extent allowable. Thank you for taking your valuable time to acknowledge our concerns. Regards, Tony Hale CEIVED S 2 1 2i24 Weld County Planning Department ea�w for our world Case No: Name: Proposed Project: Planner: October 9, 2024 Page 1. of 10 Environmental and Animal Defense P I (720) 722 - 0336 I business@eadefense.org (4) I www.eadefense.org PUBLIC COMMENT & OBJECTION USR24-0019 NGL Water Solutions DJ LLC USR for uses similar to an organic composting (Biochar Processing) in the (A) Agricultural Zone District Diana Aungst Dear Ms. Aungst, Environmental and Animal Defense is a Colorado -based nonprofit focused on environmental and animal protection. We believe all communities have a right to a healthy environment and work to maintain and improve the places that are homes to our communities and wildlife. Here, we have drafted a comment on behalf of Jeri Yarbrough, who opposes the proposed project to issue a Use by Special Review to NGL Water Solutions DJ LLC for uses similar to an organic composting (Biochar Processing) in the (A) Agricultural Zone District adjacent to her property. For the reasons set forth in this comment, Weld County Planning Services should not approve the proposed project due to its violations of municipal law. INTRODUCTION Biochar appears to have net negative environmental impacts in Colorado. These impacts directly relate to the approval process under Use by Special Review. Where BioChar Now, the underlying company seeking this project application, touts its product's agricultural uses, study after study demonstrates that most temperate zone farmers, i.e. Coloradan farmers, are typically better off composting the material directly into agricultural soils rather than turning it into biochar before doing so. This incineration business will dump more pollution into the air, fail to preserve prime farmland, and otherwise contribute to ethically dubious agricultural practices. 501 S. Cherry Street, Suite 1100 Denver, CO 80246 Page 2 of 10 Environmental and Animal Defense ENVIRONMENTAL AND HEALTH IMPACTS Biochar, as described by Biochar Now, has limited applications ranging from odor control, bio-filtering, and purportedly agricultural use to boost crop yields. The problem is that there are extremely limited commercial uses that benefit Colorado, most of them related to absorbing toxins in soils. The fundamental problem is that biochar as a soil additive in temperate climates, which that vast majority of the United States is, does not have significant measurable benefits.1 Even studies that conclude that there are any soil health benefits in temperate climates do so reluctantly. For example, in one study, the authors concluded there were some benefits noted in temperate climates, but "the impact of biochar on crop productivity in temperate agroecosystems is unclear."2 Other studies that are able to find any soil benefits make clear that the findings are limited, stating "[t3 here was no significant effect of biochar on pH, soil organic carbon, hot water extractable soluble carbon, light fraction carbon, total nitrogen, bulk density, water stable aggregates, microbial biomass carbon, carbon substrate use, species richness, species diversity, crop root and shoot biomass, harvest index, nitrogen and phosphorus uptake, use efficiency, uptake efficiency and utilization efficiency."3 3 When studies look at biochar versus composts of the materials they state, "it cannot be concluded that biochar in general leads to more or longer -lasting beneficial effects in soils compared to straw or compost."4 In the absence of some specific soil toxicity issue, such as a specific objective to defluoride waters,5 where 1 See generally Simon Jeffery et al. Blocher boosts tropical but not temperate crop yields, ENVIRONMENTAL RESEARCH LETTERS (2017) blips: iopscience.iop.org article 10.1088 1748-9326 aa67bd1 ("Here we use a global - scale meta -analysis to show that biochar has, on average, no effect on crop yield in temperate latitudes, yet elicits a 25% average increase in yield in the tropics.") 2 Vicky Levesque, Maren Oelbermann, and Noura Ziadi. Biochar in temperate soils: opportunities and challenges. CANADIAN JOURNAL OF SOIL SCIENCE (2022), https://doi.org/10.11:19/cjss-2021-0047 3 R.W. Jiang, M.A. Mechler, M. Oelbermann, Exploring the effects of one-time biochar application with low dosage on soil health in temperate climates, SOIL SECURITY, VOLUME 12 (2023), https://doi.org/10.1016/j. oisec. 20 23.100101 4 Martin Siedt, Andreas Schaffer, Kilian E.C. Smith, Moritz Nabel, Martina RoB-Nickoll, Joost T. van Dongen, Comparing straw, compost, and biochar regarding their suitability as agricultural soil amendments to affect soil structure, nutrient leaching, microbial communities, and the fate of pesticides, SCIENCE OF THE TOTAL ENVIRONMENT, VOLUME 751 (2021), https://doi.org/10.1016/j.scitotenv.2020.141607 5 Rakesh Kumar, Prabhakar Sharma, Pawan Kumar Rose, Prafulla Kumar Sahoo, Prosun Bhattacharya, Ashok Pandey, Manish Kumar, Co -transport and deposition of fluoride using rice husk -derived biochar in saturated porous media: Effect of solution chemistry and surface properties, ENVIRONMENTAL TECHNOLOGY & INNOVATION, VOLUME 30 (2023), https://doi.org/10.1016/j.eti.2023.103056 ("biochar-mediated sand columns can be utilized for defluoridation.") Page 3 of 10 Environmental and Animal Defense biochar may slightly outperform other materials,6 there seems to be little compelling reason to use the substance. Put more bluntly, there has been little scientific development over the last decade, since the original market hype of biochar first reached is fervor, claiming it to be the next black gold, that evinces biochar has escaped its snake oil claims of fixing energy, food, and climate woes.' what biochar does do is generate criteria air pollutants as defined by the Clean Air Act.8 For example, "[d] epending on the nature of the biomass and the thermal processing, VOC content in biochar can reach 40%."9 Denver Metro has suffered from major air pollution issues over the last decade. It was only in July 2024 that the EPA reclassified Denver metro/ northern Front Range, including northern Weld County, from moderate to serious nonattainment area for ozone. The way to combat these pressing air pollution issues are, according to the Colorado Department of Public Health and the Environment, "reducing emissions of precursors to ozone formation nitrogen oxides (NOx) and volatile organic compounds (VOCs)."° It may be unsurprising that a facility that uses high heat to cook organic compounds generates volatile organic compounds, and are regularly regulated as incinerators that require Title V Clean Air Act Permits. 11 Ozone itself has significant negative impacts on agricultural production. Ozone "causes a variety of responses including visible injury, reductions in Rubisco activity, chlorophyll content and photosynthesis and alterations in stomatal conductance (gsto), alterations to carbon (C) allocation including decreased root: shoot ratios, and reductions in biomass and yield quantity and quality. A meta - analysis of studies on the effects of ambient versus pre -industrial 03 levels found wheat yield losses of 8.4% demonstrating a significant and consistent crop response 6 Supra at 4. ("Biochar is most effective in increasing the sorption capacity of soils" 7 Biochar: Black Gold or Just Another Snake Oil Scheme?, Rachel Smolker, EARTH ISLAND, (September 18, 2013), https://www.earthisland.org/journal/index.php/articles/entry/biochar black gold or just another sn ake oil scheme/?utin source=google&utm medium=paid&utm campaign=tfd dsa&gad source=l&g clid=Cj 0KCQjw9Km3BhDjARIsAGUb4nwINgZTYgf2defV2e- fF7O3nTpY6UtNu 1 SD Mz9CmZ1NjUz6-koLC8aAhVSEALw wcB 8 Bruce Springsteen, Georgine G. Yorgey, Geoffrey Glass, and Christos Christoforou, Air Pollutant Emissions and Air Emissions Permitting for Biochar Production Systems, https://wpcdn.web.wsu.edu/cahnrs/uploads/sites/44/Riomass2Biochar-Chapter1 2.pdf 9 Saletnik, B., Zagula, G., Bajcar, M., Tarapatskyy, M., Bobula, G., and Puchalski, C. Biochar as a multifunctional component of the environment —a review. APPLIED SCIENCE (2019), h.ttps://www.nuipi.comi2076-3417/9/6/1139 10 Federal ozone pollution standards and Colorado nonattainment areas, DEPARTMENT OF PUBLIC HEALTH & ENVIRONMENT, https://cdphe.coloradu.gov/nonattainment-federal-ozone-pollution- standards#:—:text=ln°ia202022%2C%20the%20EPA%20reclassified,2024%2D2026%20ozone%20seaso n%20data. 11 Supra at 8. Page 4 of 10 Environmental and Animal Defense to current ambient 03 concentrations."12 Ozone not only causes agricultural crop loses, but significant impacts on forests, including Ozone has also been found to increase forest susceptibility to drought, wind throw, as well as insect and pest attack (e.g. bark beetle, wood borer, fungal infection). 13 The US Environmental Protection Agency own Policy Assessment for the Review of the Ozone National Ambient Air Quality Standards makes all of these same conclusions. Ozone, the main component of smog, is a corrosive air pollutant that inflames the lungs, constricts breathing, and even kills people.14 Ozone -induced health problems can force people to change their ordinary activities, requiring children to stay indoors and forcing people to take medication and miss work or school.15 Ground -level ozone, commonly referred to as smog, is formed by the interaction of two pollutants, volatile organic compounds ("VOC") and nitrogen oxides ("NOx"), with sunlight.16 These pollutants can be emitted by upwind states and carried to downwind states, causing ozone pollution there.17 Ozone pollution causes severe health impacts, including increased emergency room visits and hospital admissions, as well as premature death.18 Children, the elderly, and people with respiratory conditions are most at risk from ozone pollution.19 Ozone also damages vegetation and forested ecosystems, causing or contributing to widespread stunting of plant growth, tree deaths, reduced carbon storage, and reduced crop yields.29 The damage includes tree -growth losses reaching 30-50% in some areas, and widespread visible leaf injury, including 25- 37% of sites studied in just one state.21 By harming vegetation, ozone can also damage entire ecosystems, leading to ecological and economic losses.22 Biochar Now celebrates on its website a feature from Denver 7 showcasing how it can utilize waste wood from bark beetle. But a biochar facility would contribute to the very problem that it's purporting to solve by making the bark 12 Lisa Emberson, Effects of ozone on agriculture, forests and grasslands, PHILOSOPHICAL TRANSACTIONS OF THE ROYAL SOCIETY A: MATHEMATICAL, PHYSICAL AND ENGINEERING SCIENCES, VOLUME 378, ISSUE 2183 (2020), https://dui.org/ 1U.1UU8Irsta. 2U 19.U3> i 13 Id. 14 See EPA, National Ambient Air Quality Standards for Ozone, 80 Fed. Reg. 65,292, 65,308 (Oct. 26, 2015); EPA, Integrated Science Assessment for Ozone and Related Photochemical Oxidants, at 2-20 to -24, Table 2-1 (Feb. 2013). 15 See, e.g., EPA, Policy Assessment for the Review of the Ozone National Ambient Air Quality Standards, at 4-12 (Aug. 2014). 16 Sierra Club U. United States EPA, 972 F.3d 290, 293-94 (3d Cir. 2020). 17 EPA v. EME Homer City Generation, L.P., 572 U.S. 489, 497 (2014). 18 EPA, National Ambient Air Quality Standards for Ozone, 73 Fed. Reg. 16,436, 16,440 (Mar. 27, 2008). 19 EPA, National Ambient Air Quality Standards for Ozone, 73 Fed. Reg. 16,436, 16,441 (Mar. 27, 2008). 20 EPA, Policy Assessment at 5-2 to -3; Science Assessment at 9-1. 21 EPA, Policy Assessment at 5-13; Science Assessment at 9-40. 22 80 Fed. Reg. at 65,370, 65,377. Page 5 of 10 Environmental and Animal Defense beetle infestations worse along the Front Range. 23 This negative ozone feedback loop may be beneficial to Biochar Now's business, but it is not beneficial to the health and environment of the Colorado Front Range. Market analysis of biochar use in the United States shows another troubling trend. The second most predominant use of biochar is as animal feed. 24 As the US Biochar initiative notes, however, "Biochar is not recognized in the US as an approved animal feed material by AAFCO. Biochar producers are encouraged to proceed cautiously and seek qualified legal advice before considering selling any biochar or biochar amended product as feed. " 25 In other' words, biochar, as a commercial product, is used primarily in agricultural systems in South America, with little to no benefit in Colorado, and its secondary most predominant use is as an unapproved and unregulated animal feed. It is no wonder Biochar Now does not list this use on its website as an application for which it sells its products, 26 even though it will undoubtedly be used in agricultural feeds anyway. Finally, large scale applications of biochar are not explored, and the product has little evidence of its utility in its largest scale applications. Most concerning of all, biochar is an effectively irreversible product. Once biochar is added to the soil it would become nearly impossible to remove. 27 This is particularly concerning where: "[m]ixed findings are often reported; however, the results suggest that high doses of biochar in clay soils are likely to decrease available water content, and surface application of biochar to sandy soils likely increases erosion and particulate matter emissions. Furthermore, biochar may increase the likelihood of excessive soil salinity and decreased soil fertility because of an increase in the pH of alkaline soils causing nutrient precipitation. Regarding the impact of biochar on (agro)chemicals and the role of biochar-borne toxic substances, these factors cannot be neglected because of their apparent undesirable effects on target and non -target organisms, respectively. ... Our current understanding of the overall effects of biochar on soil and soil biota and their mutual interactions is not clear because biochar can have positive, negative, or neutral effects. These mixed findings clearly illustrate that the complex interactions and resulting effects of biochar on soil biota have been inadequately studied. Conclusions drawn from mainstream biochar- promoting studies may be misleading given that biochar is perceived as a 1-23 Biochar Feature on Channel 7, BIOCHAR Now, available at hops://youtu.be/3zVgJ 1 K6eHM (last visited Oct. 9, 2024) 24 U.S. Biochar Market Size & Share Analysis Report, 2030, https://www.grandviewresearch.com/industry-analysis/us-biochar-market 25 Biochar and Livestock, US BIOCHAR INITIATIVE, https://biochar-us.org/biochar-and-livestock 26 Biochar Now Products, BIOCHAR Now, available at https://biucharnuw•.cum/products/ (last visited Oct. 9, 2024) 27 See Long-term experiment — Ichar, ASSOCIAZIONE ITALIANA BIOCHAR, available at https://ichar.org/index.php/long-term-experiement/ (last visited Oct 9, 2024) Page 6 of 10 Environmental and Animal Defense positive tool for improving soil quality without considering the overall picture, and possible negative effects are usually overlooked at all levels." 28 These negative impacts, combined with the following violations of local law, should warrant the rejection of this proposed project. VIOLATIONS OF MUNICIPAL LAW Pursuant to the Weld County Municipal Code, "uses by Special Review are USES which have been determined to be more intense or to have a potentially greater impact than the Uses Allowed by Right in a particular zone district..." W.C.M.C. § 23-2-200. In an application for a Special Review Permit, "the applicant has the burden of proof to show that the standards and conditions [within the zoning code] are met." W.C.M.C. § 23-2-220. This includes, but is not limited to: • That if the USE is proposed to be located in the A (Agricultural) Zone District, the applicant has demonstrated a diligent effort has been made to conserve PRIME FARMLAND in the locational decision for the proposed USE. W.C.M.C. § 23-2-220, § 23-2-230. • That there is adequate provision for the protection of the health, safety and welfare of the inhabitants of the NEIGHBORHOOD and the COUNTY. W.C.M.C. § 23-2-220, § 23-2-230. • Buffering or SCREENING of the proposed USE from ADJACENT properties may be required in order to make the determination that the proposed USE is compatible with the surrounding USES. Buffering or SCREENING may be accomplished through a combination of berming, landscaping and fencing. W.C.M.C. § 23-2-240. • Uses by Special Review in the A (Agricultural) Zone District shall be located on the least prime soils on the property in question unless the applicant can demonstrate why such a location would be impractical or infeasible. W.C.M.C. § 23-2-240. • The operation of the USES shall comply with the air quality regulations promulgated by the Colorado Air Quality Control Commission. W.C.M.C. § 23-2-250. • The operation of the USES shall comply with the noise standards enumerated in Section 25-12-101, et seq., C.R.S. W.C.M.C. § 23-2-250. 28 Martin Brtnicky, Rahul Datta, Jiri Holatko, Lucie Bielska, Zygmunt M. Gusiatin, Jiri. Kucerik, Tereza Hammerschmiedt, Subhan Danish, Maja Radziemska, Ludmila Mravcova, Shah Fahad, Antonin Kintl, Marek Sudoma, Niaz Ahmed, Vaclav Pecina, A critical review of the possible adverse effects of biochar in the soil environment, SCIENCE OF THE TOTAL ENVIRONMENT, VOLUME 796 (2021), https://doi.org/ 10.1016/i.scitotenv. 20 21.148 :) Page 7 of 10 Environmental and Animal Defense The USES shall not emit heat so as to raise the temperature of the air more than five degrees Fahrenheit at or beyond the LOT line. W.C.M.C. § 23-2-240. NGL Water Solutions LLC is seeking to obtain a Uses by Special Review permit so that Biochar Now, LLC may develop a facility on site. The permit application clearly states that the property is in the Agricultural Zone and being used for agricultural purposes. While there are 3 injection wells on the property, they are not operational, as stated in the project application. The property is primarily being used as farmland. The proposed use will develop 40 kilns and electrical controls, including backup kilns and electrical controls, a skid steer, a loader, and a modular office building on site, as well as a 100' x 100' concrete pad and graveled driving areas. An opaque metal fence approximately 8' high will be constructed around the facility. Inconsistency with the Weld County Comprehensive Plan Under the Comprehensive Plan, Weld County elected and appointed officials and staff are bound by adhering to the directions of the Land use goals and objectives, W.C.M.C. § 22-2-30. The first of those objections is to "Commit to the future of agriculture" and that "Land use changes should not inhibit agricultural production nor operations." However, this proposal would do just that. Ms. Yarbrough's property is directly to the south of the applicant's property, where she lives with her family and animals; operates a horse boarding facility; and grows hay. This proposed development will impact Ms. Yarbrough's private property rights, primarily to operate her business and to engage in agricultural operations, but also her private use and enjoyment of her home. Ms. Yarbrough has already been verbally advised by a realtor representing Biochar Now, LLC that once the site is operational she would no longer be able to engage in hay farming due to the effects of the site. Since the site would be operating 24/7, 365 days per year, Ms. Yarbrough would be forever unable to safely engage in her agricultural operations. It is incorrect for the applicant to state that this proposal respects private property rights, as it would directly infringe upon Ms. Yarbrough's use and rights in her own property. See W.C.M.C. § 22-2-10.B. Furthermore, as the development of the applicant property would violate the goal of Weld County to protect and respect the County's Agricultural Heritage. See W.C.M.C. § 22-2-10.A. Additionally, as part of Weld County's Right to Farm Statement, officials and staff are directed to ensure that "agricultural users of the land should not be expected to Page 8ot10 Environmental and Animal Defense change their long-established agricultural practices to accommodate the intrusions of urban users into a rural area? W. . . . § 22-2-30.A.4.a. The ordinance further provides a list of agricultural uses it desires to protect within the Right -to -Farm Statement. "Well -run agricultural activities will generate off -site impacts, including noise from tractors and equipment; slow -moving farm vehicles on rural roads; dust from animal pens, field work, harvest, and gravel roads; odor from animal confinement, silage, and manure; smoke from ditch burning; flies and mosquitoes; hunting and trapping activities; shooting sports, legal hazing of nuisance wildlife; and the use of pesticides and fertilizers in the fields, including the use of aerial spraying. It is common practice for agricultural producers to utilize an accumulation of agricultural machinery and supplies to assist in their agricultural operations." In the list of agricultural uses, it is clear that operating a charcoal burning facility is not an agricultural use, and therefore, clearly why a Use by Special Review permit is required for any charcoal burning operations. Finally, the proposed charcoal burning is clearly not directly related to agriculture. See '. .M. . § 23410. The applicant's own documents indicate that there are many uses for charcoal, agricultural use only being one of them. However, the charcoal will not be directly related to any agricultural use on the applicant property, nor seemingly could it be. Instead, it will be shipped to another location for processing and sorting for further sale to other outside facilities, most of which will be entirely outside Weld County.'' Thus, where Weld County so highly prioritizes continuing agricultural operations, it must acknowledge that this proposal is not consistent with the intent of the Agricultural Zone. Therefore, staff must adhere to the directives of the Comprehensive Plan and determine that this permit proposal does not conform with the Comprehensive P'lan's priority to conserve agricultural use. Inconsistency with Zoning Requirements and USR Permitting Process 1. Prime Farmland Under the county ordinances, any Use by Special Review permit runs demonstrate a diligent effort has been made to conserve prime farmland. Here, the applicant has done no such thing. The application states that "this property contains soil classified as farmland of statewide importance and prime farmland if irrigated." It also acknowledges that the property is currently flood irrigated. Therefore, the property contains prime farmland, and the applicant must show diligent efforts to conserve it. The applicant does not, and instead downplays the "small" nature of the site and insignificant reduction in farmland. The ordinance is clear: an applicant 29►, m land Health Impacts, supra. Page 9 of 10 Environmental and Animal Defense must demonstrate a diligent effort to conserve the farmland on site. That does not include any leeway for an applicant to merely opine on the significance of the reduction in farmland on site. The parcel is 33 acres. Pursuant to the plats, the intended facility will take up nearly the entirety remaining open land on the parcel. There is no document in the application that purports any other efforts to maintain prime farmland on the parcel. Indeed, the entire application demonstrates that the parcel will no longer be used for any farming operations whatsoever and does not include any description of diligence taken to conserve any prime farmland or agricultural operations. 2. Screening The applicant proposes to store raw material stockpiles 15' -- 20' in height directly across from Ms. Yarbrough's property and within visibility. The permit applicant's screening plan only plans for a minimum 8' tall solid, opaque metal fencing around the facility. There is nothing to indicate that the stockpiles themselves will be screened by any means. Thus, the facility is inconsistent with the screening requirements for Uses by Special Review. See W.C.M.C. § W.C.M.C. § 23-2-240. 3. Air Quality There is not a reliable demonstration that the applicant will adhere to the air quality regulations by the Colorado Air Quality Control Commission. As part of the application, there are 3 kiln emission results dating back to 2021. These results are 3 years old and provide no indication of current emissions compliance status, nor similarity to the kilns or process that is proposed for the applicant property. 4. Noise While the applicant sets forth a noise study, it is inconsistent with the applicant's questionnaire of proposed use. In the questionnaire, the applicant stated that operations would be continuous, 24/7, 365 days a year. In the noise study, it indicates that "the operation will only occur during the daytime. Therefore, the operational noise will be assessed against the Weld County Daytime noise limit of 55 dBA." This study is therefore insufficient. The applicant must evaluate noise against all noise limitations, because it is intended to be operated at all hours of the day, every single day. Conclusion In sum, there are multiple demonstrations of inconsistencies with the Weld County Comprehensive Plan and the Use by Special Review application requirement ordinances. Furthermore, this facility will infringe upon Ms. Yarbrough's right to ongoing agricultural operations on her own property. For these reasons, the Weld County Planning Services should reject the permit application. Page 10 of 10 Environmental and Animal Defense Thank you for your consideration. Sincerely, Alexa McKay, Esq. Jeremy McKay, Esq. Environmental and Animal Defense 501 S. Cherry St. Suite 1100 Denver, CO 80246 720-722-0336 amckay@eadefense.org jrnckay@eadefense.org Chelsea Luedke DVM, MS Heritage Equine Clinic Brighton, CO 303-578-5898 To Whom It May Concern, EXHIBIT ill I am writing to express my concerns about the proposed biochar facility being installed near Jeri Yarbrough's facility. While I understand the importance of sustainable energy projects, the proximity of this facility to her horses (our patients) poses significant risks to their long-term health and well-being. As an equine veterinarian, I have strong concerns about this possibility. Biochar production releases fine particulate matter and other pollutants into the air, which could lead to respiratory issues, compromised immune systems, and other chronic health problems in horses. These animals are highly sensitive to environmental changes, and any decline in air quality or the introduction of toxins could have devastating effects on their health. I urge the county to carefully consider the potential impact of this facility on the surrounding environment and the health of the horses in the area. I hope you will take these concerns into account and explore alternative locations that would not put animals and their caretakers at risk. Thank you for your attention to this important matter. Sincerely, ressec:-.7."`##". _ Dr. Chelsea Luedke allillmaann BIOCHAR NOW, LLC USE BY SPECIAL REVIEW (USR) SURROUNDING PROPERTY OWNER RESPONSE LETTER FEBRUARY 10, 2025 EXHIBIT b la .0 S 12 Biochar Processing CR 6, LLC is in receipt of the surrounding property owner letters, as submitted to Weld County Planning. In addition to the October 12, 2024 neighborhood meeting that was held in order to first address neighbors' concerns, this letter seeks to directly respond to the specifically stated concerns in order to demonstrate that the site is compliant with the USR standards, to actively mitigate potential nuisances and to correct any misstated assumptions about the project. Submitted Objections/Concerns Prime Farmland This singular, �35 acre site (consisting of 2 adjacent parcels) is owned by NGL, who does not own any other contiguous land holdings. Given the presence of the injection wells and the small lot size, productive, commercial agricultural operations on this property is highest and best use of the site and is impractical to presume that farming would be the long term land use on this property. It is evident by the many intensive industrial and oil and gas facilities in the area, such as the Discovery DJ - Boardwalk Compressor Station, located immediately northwest of the Sack Farm, the Chevron (PDC) oil and gas facility located immediately west of the Sack Farm, Wells Concrete facility located 0.5 miles to the west of the site and the Vestas production facility located 1 mile to the west of the site that multiple non-traditional agricultural operations have been considered and approved in the area. The balance of these facilities to the existing farmland and rural residences does not appear to be affected, as there are productive traditional agricultural operations located directly adjacent to the above stated examples and both appear to successfully exist. There should be no presumption that the Biochar facility would not be able to demonstrate similar compliance and ability to harmoniously operate. Disruption to historic agriculture There are claims that the facility will reduce and impact agricultural and animal operations. The facility helps to counter balance the impacts of large-scale agricultural and oil and gas activities across the County and serves the agricultural economy by reclaiming and restoring contaminated sites to productive farmland or rangeland, by the use of biochar. It also can be used to improve the economic output and health of animal production operations, thereby providing a stabilizing service to agricultural practices, ensuring a long term mix of land uses. This claim can be seen specifically in an SPO statement that the current use of the property, being alfalfa production, as managed under a lease between NGL and the farmer, will be lost as a result of this application. As NGL is the current property owner, they have decided that the best use of the property is a partnership, where Biochar will develop the subject facility on the site. Therefore, although Biochar will be the user of the site, the decision to transition from alfalfa production to a different use rests with the property owner. Page 1 of 9 Dust from the charcoal can cause cancer A neighbor submitted a 2013 study attempting to link Biochar Now production to increases of polycyclic aromatic hydrocarbons (PAH) to the production of biochar. It appears that the report was based on different/outdated technologies and operations. There are no hydrocarbons in Biochar Now's exhaust and their biochar has been tested and has no PAHs in the biochar. See the supplied PDF titled "PAH and PCB test results" Regarding dust, the conversion and movement of biochar does not create or release fine particulates or dust. The converted biochar material is solid and is roughly 2 to 10 inches in size and is not prone to becoming airborne. Even if this was the case, which it is not, the concept of produced biochar in dust form would be a priority to collect, as the losing of any product by wind would be disadvantageous to the company, who n aturally seeks to maintain the full extent of their product. The original USR application did not include any protective covering at the location where the transfer of biochar from kiln to container will occur, as other Biochar Now sites have successfully operated without this measure. The hoop structure at the Berthoud site is used for processing and sorting of biochar, which will not occur at this site. That being said, fugitive dust has n ot been a problem at the Berthoud but we are willing to include a hoop structure where the material transfer will occur for further mitigation, should there be a perception of risk. This inclusion would cause any material to remain contained in the structure. Should this staff believe this concession is beneficial, it can be included on the USR plan as a future improvement, to be constructed when needed. Air emissions Emissions test results have been supplied. There will be limited air emissions from this facility and based on other operation sites, this can be effectively mitigated through the proprietary technologies and processes of Biochar Now. We understand that an air permit issued by the CDPHE will guide and monitor the air emissions and any instance of non-compliance would be in violation of the development standards. Burning and unintended releases can cause contamination to the ground and water Biochar is used for water filtration. There is no liquid by-product from our production and no solid waste streams besides recyclable metal. Unconverted materials from a kiln cycle are separated and reintroduced into subsequent cycles. Other biochar production technologies produce liquid discharges. We will likely be u sing biochar to improve the water quality associated with the onsite stormwater. There are no release event potentials, besides the ability for a tote to tip. However, this Biochar process is not yet processed into finer specs, so the clean-up ability, if needed, would be straightforward. Standard emergency spill kit equipment will be kept on -site. Concerns about horse proximity to the biochar production There is apparent concern that horses located at a local equine boarding facility will be negatively impacted, which we disagree with. It is mentioned that stables will be 100 feet away from the Biochar operations. Per our USR map, it appears that her stables area will be over 500 feet from production and the property line is over 200 feet from the facility. With the proposed screening, air control efforts, noise mitigation, etc. there should be no acute effects on the horses. Page 2 of 9 Impact on wildlife It is unclear if Colorado Parks and Wildlife received a referral request. The application team independently contacted Erin Priest, Area 2 - District Wildlife Manager in an attempt to solicit feedback on the USR application. Following a response from Priest, the application was reviewed, at the prompting of the applicant team. As stated in the referral letter dated February 3, 2025, CPW has no concerns with this application, which indicates to the Biochar team that no adverse wildlife impacts are expected or required to be mitigated based on State -level agency assessment. Additionally, per the CPW High Priority Habitat Web Map Application, which displays a variety of species such as Bald Eagle nests, Cutthroat Trout, Burrowing Owls, and Mule Deer, the site is not located within any HPH corridors, habitats, ranges, or areas. Traffic around the bend at CR 6 We are open to working with the county but do not see this as a major concern as there will be minimal traffic to the site. If needed, we can put up guard rails along the north side of CR 6 to help mitigate any potential accidents for both the traveling public and Biochar traffic; this will improve the safety above the existing level and will benefit the community. We are willing to work with the county on additional road safety measures, to be detailed in the Improvements and Road Maintenance Agreement. There will be minimal traffic to the site. This traffic will also not be impacting most of the attendees to the community meeting as almost all of the traffic will be coming from the west and heading to the west (no impact to WCR 31) Lost income The concern that the proposed facility will be responsible for the loss of income from businesses located on adjacent lands is a presumption that cannot be predicted prior to operation. It is the intention of the operator to be a quality addition to the community, which currently contains a variety of low impact and intensive uses. In this way, we expect the value of the subject property to increase, which may also positively impact the value of surrounding properties. Noise pollution There are concerns with noise from the facility negatively impacting surrounding land uses. The proposed sound barriers/panels, as detailed in the Noise Report, which are a significant cost of the project, are proposed to bring noise into compliance with Agricultural noise levels. Given the noisiest parts of the operation will occur during daytime, such as truck access, heavy equipment operation, shredding, screening and sorting materials. Furthermore, the shredder and screens are mobile equipment pieces, which will only operate on -site less than one week per month, as these machines can prepare raw materials in batches, highly minimizing noise impacts. It should also be noted that heavy equipment will utilize low tone and frequency back up alarms, with no shrill or high-pitched noise. It should be noted that Biochar received a grant from CDPHE for the shredder, which may suggest its quality and conformance to CDPHE equipment standards. Light pollution There are concerns that light will disrupt the enjoyment and nature of surrounding properties. Lighting will be minimal as detailed in the supplied lighting plan. All lighting shall be downcast and shielded as detailed. Truck Page 3 of 9 lighting, as it enters the site, will be blocked from surrounding properties to the south and east by the proposed solid fence. Pole and building mounted lighting will be no taller than 20 -feet, and will not shine onto adjacent properties. Should there be a complaint on any specific light, the operator will promptly address and correct any instance of noncompliance. Screening There are suggestions that the application does not meet the Weld County Code - USR requirements for Screening. We respectfully disagree in that the proposed fence adequately screens the visual aspect of the facility from a human -scale vantage point. Additionally, as the fence is setback from the property line and the stockpiles are further within the fenced yard, the viewing angle to observe the stockpiles and/or equipment and operations will be slight, diminishing nearly all activity. Berming is being considered along the eastern portion of the facility area, to buffer the site from the residential property to the east. Staff is willing to work with the property owner to develop the extent of that berm, based on his preference, should the application be approved. Fire risk We will continue to address fire protection and suppression requirements with Brighton Fire Protection District. At the existing Berthoud facility, Biochar has been operating for N12 years and never had a reported fire issue. No fire issues have occurred at other sites. Drainage Per the Drainage Report, prepared by Civil Arts, regarding the impact of site development on upstream and downstream properties, they can certify that the impact of the site development on upstream and downstream properties are negligible because we are limiting the post -development discharge and volume to be equal to or less than the pre -development discharge rate and volume. The major drainage basin for the site will mimic the existing flow patterns of the historic drainage for the site. The site will continue to drain southwest to northeast. This proposed drainage system will conform with the goals, policies, and standards, outlined in Weld County Code, Chapter 8 - Public Works, Article XI - Storm Drainage. It also provides the required treatment and post development analysis. Compatibility The proposed development is highly suitable for this site, which is already occupied by the NGL injection well facility. Given the constraints imposed by the injection well facility —including both perceived and real limitations such as setback requirements —it is neither feasible nor realistic to develop this land for uses such as commercial farming or rural residential. Furthermore, the property owner no longer holds sufficient water rights for agricultural use, as they were sold to the neighboring Sack family. While the property to the south is currently leased on a month -to -month basis for farming by an entity with access to water rights, the fact remains that the existing owner —and any future owners —cannot farm this land without acquiring additional water rights. This limitation significantly reduces the viability of long-term agricultural use and supports the need for a more productive and sustainable economic development opportunity. Page 4 of 9 Additionally, prioritizing development on this site over raw, greenfield locations is a prudent land -use decision. Developing this facility in a more rural part of the county would be impractical due to increased transportation costs, distance from material suppliers, and the risk of further fragmenting business development. This project aligns with several key sections of the Weld County Comprehensive Plan, as outlined below: Section 22-2-10.C Promoting Economic Growth and Stability. Land use policies have a significant impact on economic conditions in the County and should be structured to encourage economic prosperity. To ensure the continued strength of Weld County's economy, land use processes and decisions based on this plan shall be consistent and promote fiscally responsible growth. ■ The Weld County Comprehensive Plan emphasizes the importance of land -use policies that encourage economic prosperity and fiscally responsible growth. The proposed facility aligns with these principles by: ■ Generating economic growth through construction, temporary employment, and ongoing facility operations. ■ Providing stable, long-term employment and reinforcing the success of existing Weld County businesses. ■ Strengthening the county's industrial ecosystem by expanding the footprint of an established business in a location that supports continued growth. Section 22-2-30.C.1: Transition between land use types and intensities with buffers. Uses that are incompatible with existing uses must be able to mitigate conflicts. While the proposed facility differs from some surrounding land uses, it can be made compatible through proper mitigation strategies. Biochar is committed to: ■ Implementing visual and physical buffers to minimize land -use conflicts. ■ Complying with all site requirements and operational standards to mitigate potential concerns from surrounding property owners. ■ Demonstrating over time that the facility is a beneficial addition to the area, coexisting harmoniously with neighboring uses. Section 22-2-40.A.5: Encourage agglomeration economies of synergistic businesses Proximity to key suppliers is critical for the success of this facility. The unique waste streams processed at this site are converted into a marketable product, which requires efficient access to raw materials. The proposed location offers key advantages: ■ Close proximity to major material sources such as Vestas. ■ Access to the CR-6 and US Highway 85 trucking corridor, ensuring efficient transportation and logistics. Land Use Constraints and Feasibility The viability of long-term agricultural use on this property is significantly limited due to the lack of sufficient water rights. While the adjacent property to the south is currently leased for farming by an entity with water rights, the current property owner —and any future owners —cannot farm this land without acquiring additional water rights, making agriculture an unsustainable long-term use. Given these limitations, the highest and best Page 5 of 9 use of the property is not farming, but rather a development that aligns with existing industrial and economic activities in the area. The proposed facility presents a logical and beneficial alternative that maximizes the potential of the site. Demonstrated Land Use Compatibility in Weld County The proposed facility aligns with the county's historic and current land -use patterns, particularly in unincorporated Weld County, where agricultural and oil -and -gas -related businesses have been dominant. While the facility may differ from immediate surrounding uses, it can achieve compatibility through impact mitigation and stakeholder engagement. ■ Within one mile of the site, there are at least eight (8) USR permits for agricultural and mineral resource development. ■ Beyond this radius, numerous USR and SPR permitted operations demonstrate a precedent for mixed - use compatibility. ■ The existing, main Biochar facility in Berthoud is located less than one-half mile from a large, incorporated urban subdivision, with a rocket engine testing facility in between the two. There are many instances across the County where dissimilar land uses can be suitably and appropriately located adjacent to one another as long as proper mitigation and education can be received by neighbors in order to achieve mutual understanding and coexistence. ■ Throughout Weld County, diverse land uses have coexisted through proper mitigation, education, and outreach efforts. By locating the proposed facility on this constrained site rather than a greenfield area, Weld County can balance economic development with responsible land use planning. This facility will not only support the county's business sector but will do so in a way that minimizes land use conflicts and ensures long-term operational sustainability. Site selection Selecting an appropriate site for the proposed facility required careful consideration of multiple factors, including access to raw materials, transportation infrastructure, regulatory requirements, cost, and overall feasibility. After evaluating numerous potential locations, this site emerged as the most viable option based on the following key criteria: 1. Proximity to Feedstock Supply A key factor in site selection was access to a consistent and reliable supply of feedstock. The site's proximity to major agricultural and manufacturing operations ensures an ongoing source of raw materials. ■ Vestas, located nearby, is projected to produce approximately 800 tons of waste wood per month, which serves as a valuable input for biochar production. ■ The U.S. Highway 85 corridor is home to multiple businesses that generate similar organic waste streams, reinforcing the strategic advantage of locating in this area. Page 6 of 9 2. Access to Transportation and Distribution Networks Efficient transportation access is essential for receiving feedstock and distributing finished biochar products to agricultural and energy -sector partners. ■ The site is conveniently located along County Road 6 and U.S. Highway 85, providing direct access to regional and interstate routes. ■ This connectivity reduces transportation costs and ensures efficient logistics for suppliers and end u sers. 3. Proximity to Agricultural and Energy Sector Operations As a facility supporting agriculture and oil and gas operations, this site is well -positioned near businesses that benefit from biochar's applications. ■ Biochar has direct benefits for soil health, carbon sequestration, and agricultural productivity, making this location ideal for distribution to local farms and agricultural businesses. ■ The site is also strategically located near energy -sector operations that require sustainable waste management solutions and environmental remediation applications. 4. Compatibility with Surrounding Uses While every site has nearby properties with different land uses, this location is well -suited for the proposed facility due to: ■ Existing agricultural, resource -based, and energy -related businesses that align with biochar's purpose and benefits. ■ The ability to implement screening and buffering measures to mitigate potential concerns from n eighboring landowners. ■ A location that avoids direct impacts on high -density residential communities, unlike other sites that were considered. 5. Compliance with Regulatory and Environmental Considerations ■ The facility will be designed to meet Colorado Department of Public Health & Environment (CDPHE) requirements for biochar production. ■ The site was carefully reviewed in relation to Disproportionately Impacted Communities (DIC) zones to e nsure responsible land use and environmental consideration. ■ Full DIC zoning information can be accessed via the CDPHE DIC Mapping Tool. 6. Cost and Economic Feasibility ■ The cost of land acquisition was a significant factor in site selection. This location offered a cost- effective balance between affordability and strategic benefits. ■ Development costs, including necessary screening, road access, and site preparation, were evaluated to ensure long-term feasibility. ■ This site was more economically viable than alternative locations that posed higher financial and logistical challenges. Page 7 of 9 7. Approval Process and Municipal Considerations ■ Weld County was identified as the preferred jurisdiction due to its strong support for agricultural and energy -sector businesses. ■ The project team considered approval timeframes and land -use compatibility, ensuring a reasonable and achievable path to operation. ■ Alternative sites faced greater challenges related to regulatory approvals, residential proximity, and infrastructure constraints. 8. Alignment with the Weld County Comprehensive Plan ■ The proposed facility supports Weld County's long-standing agricultural and energy industries by providing a resource that enhances soil productivity and promotes sustainable land management. ■ The project contributes to regional economic stability by repurposing organic waste into a beneficial product, reducing environmental impacts, and supporting agricultural resiliency. ■ The site is consistent with Weld County's goals of supporting value-added agricultural businesses and resource -based operations. While every site has neighboring properties, after a detailed review of potential locations, this site was selected as the most suitable for this operations due to its: ■ Proximity to key feedstock sources (Vestas, US -85 corridor businesses) ■ Access to transportation routes (CR-6, US -85, regional logistics infrastructure) ■ Alignment with agricultural and energy -sector needs ■ Strategic location with fewer land -use conflicts than alternative sites ■ Economic viability, development feasibility, and regulatory compliance ■ Consistency with Weld County's long-term land -use planning goals Agricultural Application Per received comments, the use, value and applicability of Biochar is extremely limited in Colorado and other temperate climates. Biochar disagrees with this assessment, as there are a variety of demonstrated agricultural applications as detailed below. Based on the proprietary processes developed by Biochar, the following benefits of the Biochar Now product are explained below: 1. Soil Improvement & Fertility ■ Enhances Soil Structure: Helps improve aeration, drainage, and water retention, making soils more resilient to drought and heavy rainfall. ■ Increases Cation Exchange Capacity (CEC): Improves nutrient retention, reducing leaching of essential nutrients like nitrogen and potassium. ■ Supports Microbial Activity: Creates a habitat for beneficial microbes, which aid in plant growth and disease resistance. Page 8 of 9 2. Water Management ■ Improves Moisture Retention: Especially beneficial in sandy soils that drain quickly and clay soils that become compacted. ■ Reduces Runoff & Erosion: Biochar helps stabilize soils, preventing nutrient and sediment loss during heavy rains. 3. Carbon Sequestration & Climate Benefits ■ Long -Term Carbon Storage: Acts as a stable carbon sink, locking away carbon for centuries. ■ Reduces Greenhouse Gas Emissions: Helps mitigate methane (CH4) and nitrous oxide (N2O) emissions from soils, particularly in agriculture. 4. Agricultural Productivity ■ Increases Crop Yields: Improves soil fertility and nutrient availability, leading to higher yields for crops such as corn, wheat, and soybeans. ■ Enhances Fertilizer Efficiency: Reduces the need for synthetic fertilizers, cutting costs and e nvironmental impact. 5. Compost & Manure Management ■ Improves Compost Quality: Biochar mixed with compost accelerates decomposition, retains n utrients, and reduces odor. ■ Reduces Nutrient Loss in Manure: Helps capture nitrogen, preventing ammonia volatilization and n itrate leaching. 6. Remediation & Pollution Control ■ Adsorbs Heavy Metals & Toxins: Can help clean up contaminated soils by binding pollutants. ■ Reduces Agricultural Runoff Pollution: Captures excess phosphorus and nitrogen, preventing waterway eutrophication. Page 9 of 9 ResearchGate See discussions, stats, and author profiles for this publication at: https://www.researchgate.net/publication/312453546 All biochars are not created equal and how to tell them apart Article • January 2009 CITATIONS 35 4 authors, including: Hugh Mclaughlin NextChar, LLC 9 PUBLICATIONS 109 CITATIONS READS 93 Frank Shields Keith Day Company, Inc. 5 PUBLICATIONS 58 CITATIONS SEE PROFILE SEE PROFILE All content following this page was uploaded by Hugh Mclaughlin on 14 August 2018. The user has requested enhancement of the downloaded file. All Biochars are Not Created Equal, and How to Tell Them Apart Version 2 (October 2009), which supercedes the digital reprint issued at the North American Biochar Conference, Boulder, CO — August 2009 Hugh McLaughlin, PhD, PE(1 ), Paul S. Anderson, PhD(2), Frank E. Shields(3) and Thomas B. Reed, PhD(4) (1) Corresponding Author: Director of Biocarbon Research, Alterna Biocarbon Inc.(hmclaughlin@alternabiocarbon.com) (2) "Dr. TLUD" - V.P of Chip Energy Inc., Specialist in micro -gasification (psanders@ilstu.edu) (3) Director of Biofuel & Ag Related Research for Control Laboratories Inc. (frank@compostlab.com) (4) Chairman and Chief Scientist, Biomass Energy Foundation (tombreed2009@gmail.com) ABSTRACT The use of charcoal as a soil amendment and for CO2 sequestration raises many questions about the characteristics of those "biochars" and their impacts on soils and organisms. This paper reviews and revises the analyses of the principal characteristics used to distinguish biochars, and presents a small survey of measured properties. Explicit terminology is proposed about "resident and mobile carbon and other matter" in biochars intended for addition to soils rather than for use as a fuel. Specific data are presented for commercial lump charcoals and Top -Lit UpDraft (TLUD) charcoals. Easy methods for informal testing of chars are presented to determine several key biochar characteristics. The major conclusions are: 1) Currently available biochars vary significantly in key properties, 2) Great attention should be taken to know the characteristics of any charcoals being added to soils, and 3) Reports of the responses (whether favorable or unfavorable) of plants and soils to biochar applications are of questionable value without corresponding knowledge of the characteristics of the applied biochars. 1. INTRODUCTION Biochar is a term used to designate charcoal or biocarbon destined for addition to soils. As such, biochar is both a class of materials capable of sequestering carbon (CO2 equivalents) in soils and an ambitious goal of improving long-term soil productivity. Soil improvements attributed to the 1 addition of biochar include increased moisture retention, improved air permeability, elevated cation exchange capacity, increased buffering of soluble organic carbon, and synergistic interactions with soil microbial populations. With many potential raw materials (called source feed -stocks) and multiple positive attributes, biochar remains an enigma. Its specific desirable properties are subject to debate and are the basis for ambitious ongoing research programs on what is important to the plants and soils. The goal of this paper is to review the key attributes of biochar and discuss the options for measuring said properties in any specific char that is being considered for addition to soil. Potential biochar sources include conventional lump charcoal, residual char from open biomass burning (including forest fires), char residuals from gasifying stoves and furnaces, byproducts or co -products from fast and slow pyrolysis technologies, and carbonized biomass and agricultural residues manufactured in dedicated processes for specific feed -stocks, including chicken litter and bio-solids. An informal but fairly exhaustive survey was made of readily available chars, and their differentiating chemical properties were measured. The trends and scatter in those measurements are discussed. Finally, options for informally testing candidate chars are presented. The unavoidable conclusion is that one knows what one is getting in a specific biochar only after the actual properties are measured, and never just because a supplier is claiming a product is suitable for use as a biochar. 2. BACKGROUND 2.1. What Biochar is Not Much of the current understanding of the properties of biochar is derived from studies centered on the phenomenon known as "Terra Preta" in the Amazonian rainforests. Unfortunately, because of the anthropogenic nature of the ancient Terra Preta sites, it is difficult to reconstruct the causes and effects that created the enduring soil productivity that modern biochar seeks to replicate and possibly improve. However, some insights can be gleaned from the properties of carbon -rich substances and their observed effect in soils. Biochar is carbon -rich, containing significant fractions of amorphous graphitic domains (as in "tiny pockets") and additional organic carbon properties discussed below. The graphitic domains within the biochar have been documented to be stable in the soil for millennia, including samples isolated from historic Terra Preta sites. Although one might postulate that the presence of the graphitic carbon atoms results in the unique biochar properties, the answer is "likely not." If the cause of improved soils were merely the presence of graphitic carbon atoms, then "carbon black" or "tire black" materials would perform similarly in the soil — which has never been observed. Neither have beneficial effects of coal residues in soil been observed in places where coal dust has been spilt over the ages. 2 Biochar also has properties and molecular structures that resemble activated carbon, a common industrial material that possesses unique adsorption properties for vapor and liquid phase organic molecules. As will be discussed, adsorption properties are believed to play a significant role in biochar phenomena, but adsorption effects alone do not account for the composite of observed biochar attributes. If adsorption alone were the dictating phenomenon, then powdered activated carbon would be the ultimate soil amendment — which is also not observed. For example, Norit, an international activated carbon company, does market a product known as "GroSafe", which is a fairly typical powdered activated carbon product (see http://www.norit- americas.com/pdf/GroSafe rev4.pdf). However, the technical literature explains its role in the soil to be for removing toxins, such as herbicides. As such, powdered activated carbon may be helpful in those locations where toxicity is present in the soil, but its efficacy does not extend to the other biochar attributes. Similar logic can be applied to many common carbon -rich substances, such as shredded tires and pulverized plastics, etc. — and none of them exhibit any properties even vaguely similar to those of biochar. To the contrary, detrimental impacts on plants and soils are often observed. As such, little can be inferred in desirable biochar properties by observations of other natural and synthetic carbon -rich materials. 2.2. What Biochar is Without intending to make a rigid definition, biochar can be broadly characterized as "thermally - modified biomass". This description is more of an acknowledgement of how the vast majority of existing biochar found in soils was formed than an actual requirement to qualify a material as biochar. The thermal modification of biomass is significant because it results in a pivotal property of biochar — the ability to persist in the soil by not being susceptible to biological decay. Persistence basically makes biochar a soil "catalyst", in the sense of facilitating reactions beneficial to the soil dynamics, and not a consumed raw material. Soil raw materials are substances like fertilizers and other components that are either assimilated by living systems (plants, soil microbes) or gradually transformed, such as in the case of the breakdown of peat moss, compost or manure in soils. In the absence of thermal modification, essentially all forms of biomass (plants, animals and microbes alike) are 100% biodegradable. This conclusion is based on the impossibility of the inverse: that some portion of biomass is not biodegradable. If a fraction of biomass were not biodegradable, no matter how de minimus, it would accumulate over the course of millions of years and easily be detected, perhaps even overwhelming the masses of renewable but biodegradable biomass. It is important to recognize that biomass and biodegradability exist and operate in a relatively narrow temperature range — roughly 50 degrees Celsius on either side of room temperature. Below that temperature range, biological processes grind to a halt, and above that temperature range, the biological organic complexes thermally denature and lose their ability to function. 3 Within this biologically active temperature range, unmodified biomass is in a constant state of flux — growing, drying, and being recycled. Essentially every repetitive, biologically -created chemical structure and bond system present in living matter can be broken down and reused by other living species. This is why thermal modification, as in the conversion of biomass into charcoal, is so critical for providing persistence of carbon in the soil by inhibiting its biological degradation. The specific thermal modification that converts biomass into biochar can be viewed from two closely related perspectives called "pyrolysis" and "carbonization". The pyrolysis perspective focuses on the chemical breakdowns that result in the liberation of pyrolytic gases. The carbonization perspective focuses on the chemical build-ups of the carbon atoms into solid structures. The bulk of pyrolysis and carbonization reactions occur in the temperature range from about 200 to 500 degrees C. One can think of pyrolysis and carbonization as simultaneous physical -chemical processes, changing the biomass into pyrolytic gases and charcoal. At sufficient temperatures, generally above 300 degrees C, carbonization modifies the chemical bonds within the remaining solid such that they are less likely to be consumed as foods by living systems. The chemical bond modifications consist of dehydration, conversion of aliphatic bonds into aromatic bonds, and the consolidation of those aromatic bonds into local graphene complexes (http://en.wikipedia.org/wiki/Graphene). Living systems use enzymes to facilitate individual chemical reactions, and enzymes are very specific to the unique structure of the chemical bond being transformed. Carbonization randomizes the chemical bonds, creates locally varying molecular structures, and creates a much larger percentage of stable graphene chemical bonds. This diversity of chemical structures and overall greater bond stability thwarts the ability of living systems to supply appropriate enzymes to transform the carbonized bond structures. In a sense, carbonization converts biomass into a new form, termed biochar, which is more difficult to digest for the microbes - especially if there are sources of more palatable uncarbonized biomass available. This raises a question: If a portion of carbonized biomass is immune to biological decay and if natural forest fires generate additional carbonized biomass on an ongoing basis, why isn't the world chock-full of accumulated persistent biochar? The basic reason is that there are very slow, non -biological, ambient temperature reactions between carbonized biomass and atmospheric oxygen, which slowly degrade exposed graphene bonds over the course of thousands to millions of years. As a result, long-term stable fossil carbon reservoirs of oil and coal are only found under anoxic conditions, buried deep in the earth and far from any oxygen. Even at ambient temperatures, oxygen is reactive with all carbon -carbon and carbon -hydrogen bonds, given enough time. 3. CONVERTING BIOMASS TO BIOCHAR Before delving into the qualities and measurable properties of available biochars, it is useful to briefly review the conversion process that transforms biomass into biochar. Since we are interested in the biochar, the residual solid, we will focus on the carbonization reactions. The 4 carbonization process will be described for the most common application, which is the conversion of wood -derived ligno-cellulosic biomass into charcoal, but the carbonization reactions apply to any carbon -rich previously -living material. Woods is primarily a combination of hemicellulose, cellulose and lignin, with trace resins and inorganic salts. While accurate, this description under -represents the molecular -level complexity of the plant structure, as depicted in Figure 1. FIGURE 1: PHYSICAL AND MICROSCOPIC STRUCUTURE OF WOOD Clain ! —1'00 ar) Wall cell layer Wood Physical Structure lignin cellulose .Q resinc-(9)A 1Psub1/4‘'-i hemicclMu9nsc hydro praline rich glyco proteins Wood Microscopic Structure From: http://www.techtp.com/Torrefaction for High Quality Wood Pellets.pdf, page 7 of 36 During carbonization, the various components of the biomass are modified by chemical transformations that occur within specific temperature ranges. All of these transformations are basically initiated by the instability of the individual chemical bonds within the biomass at the elevated temperatures involved in carbonization. Realizing that living things spend their entire formative and functional lives in a very narrow temperature range, it is not surprising there occurs a wholesale rearrangement of biomass as the temperature rises significantly above ambient. Consider the dramatic changes that occur when cooking an egg that becomes hard- boiled by simply raising the biomass to only 100 degrees Celsius for a short period time without the loss of moisture from inside the shell. Analogously, but at much higher temperatures, carbonization takes that thermal transformation process of biomass through many phases, as shown in Figure 2. As can be seen in Figure 2, all three of the major components of biomass (hemicellulose, lignin and cellulose) are thermally transformed between 200 and 300 degrees Celsius. Figure 2 depicts the principal decomposition reactions, where the individual constituents of the biomass 5 "devolatilize" and release a mixture of gases, known as volatiles, and "carbonize" to form a more carbon -rich residual solid, which is the char. FIGURE 2: THERMAL MODIFICATIONS OF WOOD CONSTITUENTS 250 200 -150 N� rni col I ulc ssel, Extensive Devolatillisation a n rd carbon innfic-in fLN Limited davob at i I visa ti o in and tatboilisatiore 40) dapolyrne rlsation and r-et+arndentation (C) drying Harnlael'iLila sa Ugnhn C glass transition; softening. (e - Cellulose Cellulose 300 250 200 150 1 0O 0 From: http://www.techtp.com/Torrefaction for High Quality Wood Pellets.pdf, page 9 of 36 With terms like depolymerization and devolatilization, the molecular -level science may seem much more complicated than the everyday applications of the phenomena. Figure 3 shows a simple example of the entire carbonization process — the burning of a wooden match. As the flame progresses along the wooden match, it heats the wood and drives off the volatiles, leaving the carbonized char as the residual solid. FIGURE 3: A MATCH CONVERTS WOOD INTO CHAR AS IT BURNS 4QQG c 1500° C 1000'C IN 6000 C 1 aN�f / + a 400° C /7%!;' Charcoal r s. 16 Air diffusion in plume r' Combustion Products Combustion of gas, tar, and soot Gases from soot Oil vapors crack to hydrocarbons and tar Oil vapor and gas tEptm of wood Wood Another common example of carbonization is the burning of dry wood, such as campfires - especially if the fire is quenched with water, saving the glowing charcoal from being turned to ash. A more dramatic example is the "toasting of marshmallows — gone wrong", where the roasting marshmallow catches fire and converts [carbonizes] into a residual mass of crispy char while the soft white center generates a fireball of volatiles that rapidly burn in the available oxygen from the air. Note that in all of the above cases, a solid charcoal remains, meaning that the reactions of the residual graphitic carbon atoms with oxygen, called char -gasification, is not taking place. If char -gasification occurs, the char is converted to ash and the carbon atoms are converted to gases, mainly carbon dioxide and lesser amounts of carbon monoxide. 4. DISSECTING BIOCHAR INTO PROXIMATES AND ULTIMATES 4.1. Overview One of the challenges in characterizing biochar as a class of materials is that it is new and unique in the world of material testing. Until biochar is understood sufficiently to establish the hierarchy of preferred properties, it will have to be characterized by established tests that were developed for other materials. One such standard set of tests is the ASTM procedures intended for the characterization of solid fuels, especially coals. These procedures can be applied to charcoal that is intended for burning and such testing yields appropriate measurements, as they relate to the burning of charcoal as a fuel. Two popular ASTM tests for coals, known as Proximate and Ultimate Analyses, measure how a specific coal or coal -like sample will perform when utilized in a solid fuel combusting process. Figure 4 summarizes the basic breakdown of the Proximate and Ultimate Analyses as developed for the characterization of coals. The principal shortcoming of using coal characterizations for biochar comes down to different destinations for the two materials. Coal is a fuel, and the ASTM coal tests measure properties that predict performance when used as fuel, especially the amount of available thermal energy. Biochar is a soil amendment that will not be subjected to high heat. As such, the coal tests are measuring properties of the biochar that would be relevant were it to be burned like coal, which is unlikely. Still, the basic partitioning of properties associated with coal analyses has merit in differentiating biochars, subject to some minor modification of the testing procedures and associated interpretation of the testing results, as will be discussed. FIGURE 4: PROXIMATE AND ULTIMATE ANALYSES OF COALS Proximate Analysis Determines (on an as -received basis) • Moisture content • Volatile matter (gases released when coal is heated). • Fixed carbon (solid fuel left after the volatile matter is driven off, but not just carbon). • Ash (impurities consisting of silica, iron, alumina, and other incombustible matter). Moisture Ash ti Fixed Carbon �1\ Volatile\ Matter i‘i Carbon Hydrogen Oxygen Nitrogen Ash Sulfur Source: U.S. DOE - EIA, Coal Data: A Reference, 1989. Ultimate Analysis Determines the amount of carbon, hydrogen, oxygen, nitrogen, and sulfur. • Btu - Heating value is determined in terms of Btu both on an as -received basis (including moisture) and on a dry basis. • The carbon is from both the volatile and fixed matter, not differentiated. From: http://www.coaleducation.org/ky_coal_facts/coal_resources/coal_properties.htm 4.2. Revising Testing Conditions to facilitate the Interpretation of the Data When coal is combusted, the incoming pulverized coal fuel enters the combustion chamber and virtually instantly is heated to over 1000 degrees Celsius. In that environment, the coal powder immediately dehydrates, releases all the volatiles that will vaporize at 1000 degrees Celsius, and the remaining mass consolidates into volatile -free "char" particles. The volatiles burn rapidly in vapor -phase reactions and the char particles burn like miniature charcoal briquettes, where the oxygen in the combustion air reacts on the surfaces of the particles in a diffusion -controlled regime often called "glowing combustion". Furthermore, any ash remaining after coal combustion has been exposed to temperatures as high as 2000 degrees Celsius, and never less than 1000 degrees Celsius. As such, the coal tests seek to partition the composite coal into moisture, "volatile matter" that vaporizes as the mass is heated up to 1000 degrees Celsius, "fixed carbon" representing the amount of incoming coal that converts into char and burns as such, and ash, in a form representative of what will remain after the combustion process. For these reasons, the volatile matter test heats the coal up to 950 degrees Celsius in an inert atmosphere and any matter that exits is considered volatile matter. The ash is liberated/generated by exposing the coal to air at 8 800 — 900 degrees Celsius until all the available carbon is reacted to carbon dioxide and any metal salts are converted to the corresponding metal oxides. The resulting ash accurately represents the ash that exits the coal combustion process under conditions of complete carbon burnout. It should be noted that the "Fixed Carbon" portion of the coal proximate analysis is not pure carbon; it is whatever is not ash and does not volatilize at 950 degrees Celsius. Coal proximate analyses are readily available from commercial laboratories and not too difficult to perform in any lab with a muffle furnace, appropriate crucibles and an analytical balance. Unfortunately, the partitioning of a biochar sample into coal proximate analysis fractions does not provide much insight into how biochar actually partitions when used as a soil amendment, that is, when the char is subjected to temperatures and conditions that are encountered in soils. Therefore, we propose and present below a modified thermal analysis methods to yield more insight into the metrics relevant to distinguishing one biochar from another. The modifications are adjustments of the temperatures utilized during testing to be more aligned with the temperatures encountered during pyrolysis and carbonization. The specific modifications presented here are not cast in stone and may well be further manipulated as better insights into pivotal biochar properties are developed. At this juncture, we are trying new things and seeing what can be measured and subsequently interpreted. To avoid confusion with the standard ASTM tests for coal, we call our methods "Modified Proximate Analysis" and "Modified Ultimate Analysis". When these analyses were performed and reported for this paper, we made the following changes in the analytical protocol: 1. The term "Fixed" is changed to be "Resident." Resident does not mean absolute permanence in the soils, but half-life of over 500 years seems to justify the "resident" terminology. Others have used the word "Recalcitrant," but that does not have a specific connotation and seems a bit esoteric. 2. The term "Volatile" is changed to be "Mobile," as in "being able to be removed, but not necessarily being made into a gas". Mobile means a lack of permanence, as in the case of hydrocarbons that can be digested by microorganisms. Others have used the word "Labile," but that has the same communication issues as "Recalcitrant". 3. The grouping "Fixed Carbon" was renamed "Resident Matter." The difference between "fixed" and "resident" has been explained above. The usage of the term "matter" is to allow a partitioning in the ultimate analysis test of the carbon fraction separate from the non -carbon fraction of the resident matter. In summary, Resident Carbon plus Resident H & O (plus typically inconsequential other chemical species) is equal to the total Resident Matter (formerly grouped as Fixed Carbon in the terminology of proximate coal analyses). 4. Similarly, "Mobile Matter" is the sum of "Mobile Carbon" and "Mobile H & O." 5. The threshold temperature for vaporizing the Mobile Matter away from the Resident Matter has been lowered to 450 degrees Celsius. 9 6. The ashing temperature, in the presence of air, is performed at 500-550 Celsius. This temperature range produces a Mobile Matter fraction that minimizes additional generation of volatiles by the incremental carbonization of the biochar sample, which occurs whenever a char is heated above the highest treatment temperature (HTT) that the char has previously experienced during production. The lower ashing temperature also avoids converting the alkaline hydroxides and carbonates into metal oxides, thereby potentially providing a more representative sample of the ash present in the biochar sample. The drying of the biochar samples remained the same as in the coal assay, with drying in the presence of air at 105 Celsius until stable sample weight is obtained. 4.3 Test Results Using the Modified Proximate Analysis Nineteen representative biomass and biochars were tested with the Modified Proximate Analysis and the results are shown in Figure 5. FIGURE 5: MODIFIED PROXIMATE ANALYSES OF CHARS 300 0 a. E cu V y- 0 C al CD 150 v 0 a. s a) 250 200 100 C 50 �❑ Water (gm/100 gms dry biochar) DAsh ■ Mobile Matter • Resident Matter II I w -,`A-' /\\ \ jl,,'"�all,,,0• rat ��*1\ O o° �t r or r,� , r` . rte* Gr �•c•• eow G�� °�t o• oe te•C\t Cs G cc? .j C�r o `` 2r o im` Off` �tc�tt• ''t'4�� rte ` �e �?�r# o C',r apt • O \O ��� es- & cc., t Q Oek to 4 .6 cob- ,oO O 2� 10 The sample set used for Figure 5 is not comprehensive of the universe of potential biochars and the data is from a single measurement of each sample. But the data serve to demonstrate the diversity of measured properties. Figure 5 has the main constituents of chars normalized to provide the portions on a dry sample basis, with residual water presented above the 100% level. Residual water is not an intrinsic component of a char, but is due to post -carbonization practices such as cooling with water addition or storage and transport conditions that allow hydroscopic chars to acquire moisture. The chars in Figure 5 appear in groups broadly representative of the major types of raw materials and chars. The three entries (A, B, C) on the left of Figure 5 are pre -carbonization materials and reveal very high mobile ("volatile") and corresponding low resident ("fixed") portions. The five grass pellet and straw chars contain elevated levels of ash associated with the potassium and phosphorus typical of grasses as compared to wood -derived chars. The two gasifier chars (I and J) reflect the specific conditions of the gasifier operation, with more aggressive conditions leading to higher ash levels as more of the carbon portion of the biomass is reacted away [char - gasified] into the vapor phase. The three middle chars (K, L, M) are from various raw materials and processes and reflect the specifics of the individual manufacturers. The six wood -derived biocarbons on the right are from a single carbonization process, so the variability is associated mostly with the source biomass. Wood -derived chars generally have low levels of ash, although elevated ash may appear in the char if the wood is contaminated with soil during harvesting and/or transportation to the biocarbon conversion facility. In general, the specifics of an individual char derive from a combination of the properties of the starting biomass and carbonization conditions, with most factors being within the control of the various biochar producers. 4.4. Test Results Using the Modified Ultimate Analysis The focus of ultimate analysis testing is to measure the individual chemical levels in the composite sample to gain further insight into specific properties that are of interest during the use of the substance. For coal, that means measuring the elements shown in the second half of Figure 4, with the goal of calculating the heating value or total energy content of the coal. The name "ultimate" is somewhat of an historical misnomer, because in a world prior to expensive analytical instruments, "ultimate analysis" techniques were much more work than the "proximate analysis" and were considered to be about as much as could be known about a sample of coal. The Modified Ultimate Analysis of biochars builds off the same analytical measurements as for coal, but since biochar is not intended for use as a fuel, we need to rethink what we are learning from the partitioning of the char into individual elements or chemical classes. Furthermore, depending on the source of the biomass for the char, there are some chemical species, particularly sulfur, that are unlikely to be present at significant levels in the resulting char, but are a major concern in coal. For this paper, a conventional analytical instrument, a LECO Corporation CN2000, was used to combust a small dried sample of char and to measure the level of carbon dioxide and nitrogen oxides in the off gases. By calibrating the instrument on known standards, the instrument calculates the weight percentages of carbon and nitrogen in the original sample. By coupling the 11 ultimate analysis with the proximate analysis, after subtracting out the moisture and ash levels in the sample, one can determine the relative portions of carbon, nitrogen and, by difference, any remaining organic fraction in both the mobile (volatile) and resident (fixed) matter. The remaining organic fraction represents the sum of the hydrogen, oxygen and sulfur in the sample. Since sulfur is expected to be present at negligible levels, the organic fraction is interpreted to represent the sum of the weight of hydrogen and oxygen in the sample. For clarity, it is labeled as "Resident H & O" and "Mobile H & O" in the figures. In addition to low sulfur levels, most chars exhibit low nitrogen levels, attributed to the loss of nitrogen from the char as either ammonia or oxides of nitrogen during the carbonization process. The figures do include "Resident N" and "Mobile N" measurements, but they are usually so minor that it is hard to visualize and can normally be neglected or included in the "H & O" portion of biochars derived from relatively clean biomass sources. As such, the major partitioning that emerges in the biochar "Modified Ultimate Analysis" is to divide the char sample into 1) the "Resident Carbon" portion of the Resident Matter, 2) the hydrogen and oxygen portion of the Resident Matter, called "Resident H & O", and the analogous 3) Mobile Carbon and 4) Mobile H & O portions of the Mobile Matter. Since the proximate analysis isolates a pure ash sample, it is also possible to evaluate 5) the acid -soluble ash and 6) acid -insoluble ash by acidifying the acid and recovering the acid -insoluble fraction. 7) Resident N and 8) Mobile N can also be detected, but are often in amounts too small to be of significance in plant and soil science. The ultimate analyses of the nineteen samples from Figure 5 are shown in Figure 6. It should be kept in mind that Figures 5 and 6 represent a very small set of samples, with only one or two samples representing whole classes of chars. As such, the reader is cautioned from drawing overly broad conclusions from such a limited number of actual analytical results. However, it is clear that the various components of the char samples can be dissected into a finer group of chemical partitions by use of "modified proximate and ultimate analyses" evolved from the analytical methods for coal. A word of caution is necessary with respect to the ash levels indicated in Figures 5 and 6. Figure 6 shows the total ash of Figure 5 broken into two fractions (acid soluble and non -soluble), and the acid soluble fraction is always the majority of the total ash from uncontaminated wood. One needs to question the origin of the acid soluble ash fraction, especially in biochar derived from clean wood. Most of the ash in clean wood is made up of phytoliths, which are silica that has gone up into the tree to provide structure and support, and cations (sodium, potassium, calcium and magnesium) that form neutral salts with available anions, such as bicarbonates, carbonates, bisulfates, sul fate s, sulfates, hydroxyl groups, etc. The concern is that the ashing conditions used in the analytical procedure may convert the cations from one salt form to another, whereby changing the molecular weight of the salt and weight contributed to the ash content of the biochar sample. For example, sodium hydroxide (molecular weight 40) could be converted to sodium carbonate (molecular weight 84) under the conditions of the ashing test. Thus, any sodium hydroxide would generate a weight of ash a little over twice the actual weight of sodium hydroxide in the original biochar. 12 O a E Cu N V 'r - O IS C O V Sn 0 a s O) FIGURE 6: MODIFIED ULTIMATE ANALYSES OF CHARS 100% 90% 80% 70% 60% 50% 40% 30% 20% 10% 0% milli III m • • e CI 4/ f< 0 Se > * \/ . fr O 4q4 O' 4Ce. eS ),t r 4ctV $S'7 �C,r�O C,tkti\ �` C,,r �,r kC' �C, :ell •etOOkt%e'% �tb- etP tb• •`oU Q� ���.`oc, .`oo .`�Q' Qv Qv �� �t �� ?otJ/f/c 0, Q,t �� �� C�� C7� ��� � sci � ■ Resident Carbon O Resident H & 0 O Resident Nitrogen ■ Mobile Carbon O Mobile H & 0 ■ Mobile Nitrogen DAsh (acid soluble) ® Ash (non -soluble) As such, it is recommended that the absolute magnitude of ash measurements in biochars be taken with the proverbial "grain of salt", especially the acid soluble fractions. Higher ash levels generally mean that higher levels of non -organic "something" are present in the char. What those ash constituents are, and whether they could impact local soil conditions, needs to be understood before utilization as a biochar. We suspect that much of what the tests show to be ash is actually closely held in the resident matter, therefore behaving in soils quite differently if applied as part of the biochar versus being applied as loose ash, with potentially significantly different rates of release and consequences over time on the soil, plants and microorganisms. Similarly, the pH of an ash sample can reflect the conditions of the ash formation during the analyses more than the actual pH of the original char at carbonization temperatures. Furthermore, the pH of fresh biochar samples may not accurately reflect their pH impact in the soils, especially after the biochar has equilibrated with atmospheric carbon dioxide, which converts many of the alkaline hydroxides into corresponding carbonates and shifts the pH lower. 13 5. ADDITIONAL PIVOTAL BIOCHAR PROPERTIES AND ANALYTICAL TESTS Two additional biochar properties are believed to be pivotal in the unique properties of biochar in the soil; these will be discussed at length. The two remaining biochar attributes are a challenge both to measure analytically and to understand their role in the soil. They are known as Cation Exchange Capacity, or CEC, and Adsorption Capacity. Conceptually, the former is the extent to which biochar has ion exchange properties and the later is the extent that biochar has activated carbon properties. Many biochars exhibit significant and measurable amounts of CEC and adsorption capacity, and these properties may lie at the heart of the unique and dynamic role of biochar in the soil. 5.1. Cation Exchange Capacity (CEC) Cation Exchange Capacity takes a sample of char and converts all the cations to one form, then displaces them with another cation, and finally quantifies the displaced cations to measure the CEC. The CEC method used for this paper consisted of the following procedure: A sample of dried char is shaken/centrifuged/drained three times with sodium acetate solution, then shaken/centrifuged/drained with 2-propanol three times. The alcohol rinse removes excess cations present in solution, but not bound to the char. The sodium -loaded char is then shaken/ centrifuged/drained with ammonia acetate solution three times. The total solution from the three ammonia acetate rinses is measured for sodium level and the CEC calculated in milli -equivalents per 100 grams of dry starting char. CEC is not a very common analytical test and exact procedures vary from lab to lab. As such, this analytical test will benefit from additional methods -development work. Better and more standardized CEC methods, specific for biochar, are anticipated in the future. Further complicating predicting the roll of CEC in a specific biochar is the documented development of additional CEC within the soil over time and depending on soil conditions (see "Oxidation of black carbon by biotic and abiotic processes", C.H. Cheng et al. / Organic Geochemistry 37 (2006) 1477-1488). As such, it is likely that measuring the CEC of a char determines the current level of the CEC property at the time of measurement, but does not indicate what additional CEC may come into existence in the future. 5.2. Adsorption Capacity Adsorption Capacity is another property that is poorly understood in biochar. One characteristic of the adsorption capacity phenomenon in chars is shown in Figure 7, where a sequence of chars, carbonized over a range of Higher Treatment Temperatures (HTT), shows a dramatic variation of measured BET surface area. [Note to readers: BET stands for Brunauer-Emmett-Teller, the three scientists that published the method in 1938. Although the BET measurement has some limitations that we discuss shortly, it is a useful measurement for this initial discussion of surface areas being impacted by increasing carbonization temperatures. Furthermore, the BET method is the historic measurement of surface area that appears frequently in the literature.] 14 FIGURE 7: VARIATION OF CHAR BET SURFACE AREA WITH HTT 450 400 11 350 300 250 U ct t -H U) 200 U AC 150 c 100 50 0 300 400 500 600 700 800 900 1000 Terminal pyrolysis temperature(C) From http://terrapreta.bioenergylists.org/files/TrainingManual.pdf - bamboo charcoal The qualitative phenomenon shown in Figure 7 has been confirmed for many chars and always occurs. Individual chars will exhibit a quantitatively different absolute surface area at any given temperature, but the characteristic rise and fall is highly reproducible. The development of surface area above 300 Celsius is attributed to the formation of localized graphene regions within the char as the residual solid becomes progressively more carbon -rich. The decline of surface area above 700 Celsius is attributed to "calcination" [high temperature treatment] of the developed graphene plates, resulting in the coalescence of the individual graphene regions into larger, denser, but less porous amorphous graphitic carbon complexes — similar to the char formed en route to making activated carbon. Because surface area and adsorption capacity are properties of the graphene portion of the char itself, the property is formed at the time the char is created and is unlikely to further develop in the char when placed into soils. The adsorption capacity of a char can deteriorate after creation, perhaps by having something either occupy the adsorption sites or physically blocking access to the adsorption capacity by coating the outside of the char particles. As such, measuring the adsorption capacity of a freshly made char yields the upper ceiling for the life of the char with respect to this property. In terms of what biochar contributes to soil dynamics, adsorption capacity is believed to contribute the bulk of the moisture retention and most of the capacity to buffer soluble organic compounds. . As such, these characteristics may be pivotal in the stimulation of the microbial populations in the soil by stabilizing the minimum moisture and carbon source levels in the soil 15 and elevating microbial survival rates during times of drought and shortages of other soluble carbon sources. Adsorption capacity is measured by "challenging" the char with a known substance, usually an organic vapor, and measuring the extent of uptake of the challenge gas under controlled conditions. The test is not a routine analytical method and the closest historic analytical method is the BET surface area assay. Unfortunately, the BET method is performed under conditions far removed from what occurs in the soil, with the BET method measuring the adsorption of nitrogen vapor in a partial vacuum at liquid nitrogen temperatures (minus 196 degrees Celsius). As such, BET measurements may not accurately predict, or even differentiate, the adsorption capacity of chars in typical biochar applications. The adsorption capacity test used for this paper is known as "GACS" or Gravimetric Adsorption Capacity Scan. The GACS method is similar to another esoteric method known as the GRPD test for activated carbon, which was developed, in turn, from a test known as TACTIC (developed by Calgon Carbon Corporation to study activated carbons.) The GACS assay is performed on a custom-built modified TGA (Thermo-Gravimetric Analyzer) and measures all the adsorption behavior of chars and activated carbons over a wide range of adsorption conditions. For the purposes of comparing chars, it is sufficient to subject all chars to the same adsorption conditions and measure the extent of adsorption. For this paper, the standard conditions were the weight percent uptake of R134a (1,1,1,2 tetra- fluoro-ethane — the refrigerant used in automobile air conditioners) by a dried sample of char at either 100 degrees Celsius or 125 degrees Celsius. The assay is basically a means of comparing relative adsorption capacities within a group of chars. GACS measurements may become a useful standard test for biochar classification, but currently there are fewer than ten such instruments in the world, so it does lack facile accessibility. Interested individuals are invited to contact the Corresponding Author for additional information about the GACS assay. Figure 8 shows the CEC and adsorption capacity of eleven chars and two wood -samples previously discussed in conjunction with Figures 5 and 6. Some samples from Figure 5 and 6 did not have both the CEC and adsorption capacity measurements available and those samples are not included in Figure 8. The CEC data is shown on Figure 8 at 10% of the measured CEC level to allow a common y-axis for both CEC in units of meq/100 grams and adsorption capacity in units of weight percent R134a @ 100 degrees Celsius. Figure 8 shows significant variation of both CEC and adsorption capacity in the selected eleven chars and two woods. All the samples tested showed good levels of CEC, but considering how few samples there are, one should not jump to conclusions about what does and doesn't lead to CEC in a char. 16 FIGURE 8: CEC AND ADSORPTION CAPACITY OF CHARS 10.00 9.00 8.00 7.00 6.00 5.00 4.00 3.00 2.00 1.00 0.00 O10% of CEC in meq/100 grams ■ Adsorption Capacity (wt% @ 100C) � G \ \. + O °�@ �<�� '` �G`�'ebt ��' ` � C t e ow �o `ti ,Qo Q° °i``0 C,r� C�'�� C.r�or cy °� t���. QG•�oG� 0.(‘, oo�� et,. 40) <4 l. qt. e co a� I `ate or �� °a �ca� ��� mac' Q• O Q;g C' i0 i Adsorption capacity showed more dramatic trends, with the two pre -carbonization materials having little or no adsorption capacity, as would be expected from the trend of the low - temperature side of Figure 7. The adsorption capacity of the chars in Figure 8 seems to reflect the specifics of different carbonization process more than the specific starting material. This is not unexpected considering the carbonization process creates the internal structures in the starting biomass as the volatiles are driven off and the solid char is formed. Furthermore, of the two examples of gasifier chars, Gasifier Char #1 used woody biomass as the fuel for gasification and represents a wood -gasifier char, whereas, Gasifier Char #2 was residual char from a char - gasifier. Of the chars shown in Figure 8, letters H, L, 0, P, Q & S were all produced in the same carbonization process and seem to share uniformly elevated levels of adsorption capacity. From this discussion in Section 5, we conclude that future research about CEC and adsorption capacity could indeed be fertile ground [pun intended]. 17 6. POTENTIAL SOURCES OF BIOCHAR 6.1. Overview Potential biochar sources include conventional lump charcoal, char residuals from gasifying stoves and furnaces, by-products from fast and slow pyrolysis technologies, residual char from open biomass burning (including forest fires), and carbonized biomass and agricultural residues (including chicken litter and biosolids) manufactured in dedicated processes. Figure 9 summarizes a few of the many characteristics that can be used to classify biochars. FIGURE 9. Table of Potential Sources of Biochar Type Issue Incidental Gasifier Other Modern Industrial Processes Traditional Application Fire Residual Lump Charcoal Biomass to Energy By -Product or Co -product Sole product Description (Highly generalized) Fireplace Forest Incineration fire Primitive Modem kilns kilns Downdraft Updraft Top -Lit (TLUD) UpDraft Traditional Specialized Fast Pyrolysis Bio-Gas Oil retort retort & Bio- Biocarbon for energy Biochar for soil Oxygen Present during carbonization Oxic - Uncontrolled Oxic or Anoxic Oxic Anoxic (usually) Anoxic or Oxic Commercially available for biochar? No. destructive. Basically Yes. Established product cooking — for Biochar is NOT primary objective. usually the Biochar is NOT primary initial usually in Initial efforts specific for making the goal efforts biocarbon It is not the intent of this section to make judgments about what constitutes the good and bad characteristics of biochars, nor to say which methods of pyrolysis are better than others. Our purpose is to alert the readers to the fact that fundamental differences exist between biochars because of the pyrolysis methods, even when the starting biomass is exactly the same. At industrial scales, unavailable to average people, technologies have existed for decades for the purpose of dry distilling wood and collecting the volatiles, such as "wood alcohol" or methanol. They are now discovering that the by-product of charcoal has increased value as an additional product called biochar. Other large -volume sources may become commercially available in the near future. 18 Each of the carbonization methods can be further differentiated as being either a continuous or batch process. Both types can produce good and not -so -good biochar. The difference between them is that continuous production systems, which tends to be larger in size, lend themselves to steady-state operation, if appropriate monitoring is performed and if the product specifications are what the biochar user desires. A batch system, which favors smaller and less complex equipment, allows the user to easily customize the pyrolysis process, but can produce wide fluctuations in some characteristics, especially if monitoring and process controls are not rigorous. Currently, of all these sources, there are only three that are realistically accessible to the individual interested in using biochar. One is purchasing conventional lump charcoal; the second is small-scale use of simple drum retorts; and the third is making your own char residuals from Top -Lit UpDraft (TLUD) gasifying stoves. 6.2. Lump Charcoal from Commercial Sources Conventional lump charcoal was a widespread product prior to WWII, but has been replaced by charcoal briquettes after the war. Currently, most charcoal briquettes are a mixture of powdered devolatilized coal, a small portion of raw or carbonized sawdust, and intentional ash additives - intended to create the "complete charcoal cooking experience." All that lovely white ash, indicating the coals are ready for cooking, is limestone, straight from the mine. Nowadays, lump charcoal is a boutique cooking fuel, which is gaining popularity and distributed almost anywhere outdoor cooking supplies are sold, including most hardware stores. It is generally made from clean wood scraps, such as residues from furniture making, and appears as solid lumps that still exhibit the grain of the original wood. While it is not inexpensive, lump charcoal is certainly affordable in the smaller quantities that a home garden might require to achieve recommended biochar levels in the soils of 3 to 10 weight percent of the soil mass in the root zone. However, an underlying issue remains: Is lump charcoal a good candidate for use as a biochar? Furthermore, there are many varieties of lump charcoal, as can be investigated by visiting a web site called www.nakedwhiz.com. The site reviews the cooking properties of lump charcoals, but was a valuable resource by supplying over a dozen various lump charcoals for testing. This data set was augmented by a large number of varietal charcoals from Real Montana Charcoal, which makes small batches of charcoal from individual wood species. Thus, an additional survey was made of how charcoal varies as a function of the wood species when made within the same basic production process. The lump charcoals were tested for total mobile matter, adsorption capacity, and relative density. The goal was to judge the relative variability of the charcoal properties and see if any one property could be inferred from another, such as lower density charcoals correlating with higher adsorption capacity per unit weight, etc. It should be noted that for this set of data, the Mobile Matter assay temperature was the coal volatile matter setpoint of 900 degrees Celsius, which removes a small increment of additional volatiles over the previously discussed 450 -Celsius setpoint now proposed for the biochar modified proximate and ultimate analyses. 19 Mobile matter is an important property in biochar for two reasons. First, there is evidence that mobile matter leaches into the soil and provides a soluble carbon source, which can cause a short-term nutrient deficiency for the plants by stimulating soil microbe growth that competes with the plants for available nitrogen. The mobile matter levels in lump cooking charcoal are a concern because the charcoal is expected to light without the addition of liquid charcoal starter. As such, in order to aid lighting, lump charcoal are often made under carbonization conditions that leave higher levels of low molecular weight volatiles in the charcoal and, thereby, achieve the desired lighting qualities. Second, the elevated amounts of mobile matter are likely to disappear within a single growing season and not contribute to the long-term properties of the soil. As such, mobile matter portion in biochar is bought and paid for, but represents less long-term value as a soil amendment. Water and ash provide similarly reduced long-term value in the biochar, but most people recognize that situation and purchase accordingly. In addition to the Mobile Matter assay, Adsorption Capacity was tested because that is a crucial property of biochar that is created at the time of manufacture and unlikely to improve over time. The results of testing 15 randomly selected commercial lump charcoals are shown in Figure 10. In general, the best of the lump charcoals had adsorption capacities comparable with the biocarbons shown on the right of Figure 8, when the adsorption data is compared at the same adsorption temperature (done by the corresponding author, data not presented here). Unfortunately, the average lump charcoal mobile matter was over twice the average level of 10% for biocarbons shown in Figure 8. Furthermore, it is apparent from Figure 10 that one cannot infer the mobile matter or adsorption capacities based on the relative bulk density, although there appears to be a weak inverse correlation of adsorption capacity and bulk density. Eighteen samples of Real Montana Charcoal were obtained and tested for adsorption capacity to see how the adsorption capacities vary from species to species of wood, holding constant the specific carbonization process. Figure 11 shows the Real Montana Charcoals adsorption capacity data, plotted in addition to the adsorption capacity data of Figure 10 for commercial lump charcoals. As shown in Figure 11, selecting within a single carbonization method does reduce the variability of both the relative density and the adsorption capacity. Considering that the average Real Montana Charcoal adsorption capacity was 70% higher than for the selection of lump charcoals, and that only one other lump charcoal significantly exceeded the average of the Real Montana family, it is clear that there is value to be realized by testing lump charcoals for desired properties. Or in other words, the adsorption capacities have been found to vary as much as 700% (a seven -fold difference) between samples of commercial charcoals, and therefore their application into soils as biochars should be conducted with forethought and caution, including measurement of their individual properties prior to soil application. 20 FIGURE 10: COMMERCIAL LUMP CHARCOAL PROPERTIES 35% 1 30% C.) L CD a 25% co C) t co 5 C) O S 20% 15% 10% 5% 0% 0.5 • • - R2=0.0177 • • • ••• ' • • R2=0.1659 0.7 0.9 1.1 1.3 1.5 1.7 Relative Bulk Density of the Lump Charcoal 1.9 7% 6% V 5% 'v r 4% c� caQca V 'Zr = r 3% Off/ 2' 0 Q � 13 RS 1% 0% 2.1 Mobile Matter wt% Linear (Mobile Matter wt%) • Adsorption Capacity at 125C Linear (Adsorption Capacity at 125C) FIGURE 11: REAL MONTANA CHARCOAL ADSORPTION CAPACITIES 9% 8% 7% U6% - a as m4°./ ct3% 12-'46 0 w2% -0 ca t-1 0% • Commercial Lump Charcoals Real Montana Charcoal family Lump —Linear (Commercial Charcoals) R2 = 8E-09 • Linear Montana Charcoal family) (Real Y) 711 • • • ♦ • LI IL r, • • • • • • • • • R2=0.1659 0.5 0.7 0.9 1.1 1.3 1.5 17 Adsorption Sample relative density 1.9 2.1 21 6.3. Charcoals from Small Retorts [anoxic] Pyrolysis of biomass is caused by heat, and does not require a flame. So "anoxic pyrolysis" [without oxygen] can occur and is the basis for charcoal/biochar creation via retorts that essentially bake the raw biomass to drive off volatiles and tarry gases. Many variations of small charcoal -making retorts appropriate for personal experimentation are discussed on the Internet, including: http ://www. hol on. se/folke/carbon/simplechar/simplechar. shtml http://www.youtube.com/watch?v=ahIX54facp0&feature=related http://www.biochar-international . org/technol ogy/producti on http://www.biochar.info/biochar.biochar-production-methods.cfml In these anoxic procedures, there must be some external heat source that will elevate the temperature of the raw biomass without flame contact. Several of these retorts cited above utilize the external burning of the pyrolysis gases, created and emitted from the inner retort chamber, as fuel to sustain the carbonization process. Each anoxic approach can make a variety of biochars and the biochar properties can vary from batch to batch and even within individual batches due to variations in local conditions. For example, temperatures differences between the walls and the center can yield different amounts of mobile matter remaining in the individual pieces of char. Similarly, a thick piece of wood in the center will require longer to carbonize than would smaller pieces closer to the heat sources, possibly leaving some torrified or even raw wood at the end of the process. Biochars created via anoxic small -retort processes have not been specifically tested for this paper, but their characteristics would probably be quite similar to those of commercial lump charcoal, implying significant variations depending on many operational variables. Although the small retort chars can be quite different from each other, one advantage is the char producer is typically also the field -tester. This creates the opportunity for correlating the operational variables and qualities of each batch of biochar with the desired soil performance. 6.4. Charcoal from Gasifiers (background note) Gasifiers are devices in which dry biomass is transformed into combustible gases and charcoal in a zone that is distinctly and controllably separate from where the volatile gases are combusted. An important note on terminology: To the general public and most biochar enthusiasts, the word "gasification" denotes both the creation of gases via pyrolysis of the biomass and the subsequent oxidation of solid hot charcoal/carbon to yield CO2 and CO gases. This latter char -consuming process is called "char -gasification" in this paper to avoid confusion with the pyrolytic gasification of the biomass, "wood -gasification", which yields char and wood -gas. There are several different types of "gasifiers" (referring to the devices, not the processes). In almost all of them, the raw biomass moves downward, first undergoing anoxic pyrolysis caused by heat rising from below and converting the biomass to char, and then experiencing char - gasification and the creation of the heat, leaving behind only ash. In those gasifiers, the making 22 of biochar generally requires the removal of the downward moving fuel at an appropriate time, place and temperature, depending on the desired charcoal characteristics. Because most gasifiers were created to consume the charcoal to maximize energy production, prior to the recent interest in biochar, the removal of any char is easier in some designs than in others, and the carbonization conditions that any surviving char experiences are not always the same. 6.5. Biochars from oxic Top -Lit UpDraft (TLUD) Pyrolytic Gasifiers One convenient gasifier source of biochar is the Top -Lit UpDraft (TLUD, pronounced "Tee- lud") pyrolytic stoves and biochar makers. They can be easily constructed and operated for small-scale production of biochar. Originated in 1985 by Dr. Thomas B. Reed, and with almost simultaneous independent development by Paal Wendelbo, the TLUD devices have always been intended as biomass - burning cook stoves. Therefore, by intention, Top -Lit UpDraft gasification has been demonstrated primarily at a small scale. The TLUD devices feature flaming pyrolysis, a unique combustion process that produces char at the same time as the pyrolytic wood gas is released from the biomass. Cooking is accomplished by secondary combustion of the pyrolytic gases. The value of the TLUD char has been largely ignored (except by Dr. Ronal Larson, whose prominent advocacy of char-from-TLUDs enabled subsequent development efforts) until the recent surge of interest in biochar. Recent efforts are focused on making larger TLUDs with the emphasis on biochar production, leaving the utilization of the heat as a secondary feature and the subject of ongoing development efforts. In the TLUD gasifiers, the fuel does not move (except by shrinkage when pyrolyzed). Instead, a "pyrolysis front" moves downward through the mass of fuel, converting the biomass to char. The name "Top -Lit UpDraft" denotes two key characteristics: The fire is ignited at the top of the column of biomass and the primary combustion air is coming upward through the fuel from the bottom of the biomass. The primary combustion air sustains the pyrolysis reactions occurring within the pyrolysis front. This mode of combustion is called "flaming pyrolysis", where biomass is converted to char and releases combustible volatiles, in contrast with "glowing pyrolysis" that is characteristic of the combustion of char. The tiny "flames" within the descending pyrolysis front are due to the combustion of a portion of the created pyrolysis gases, thereby generating the heat needed for propagating the pyrolysis front downward. Since the rate of heat generation is determined by the amount of available oxygen, the progression of the pyrolysis front is controllable by regulating the primary airflow. In a typical TLUD, the pyrolysis front moves downward 5 to 20 mm per minute, depending on the nature of the fuel and the amount of available primary air. Above the pyrolysis front, the created char accumulates and the oxygen -depleted air (mainly nitrogen, carbon dioxide, carbon monoxide and water vapor) sweeps the created pyrolytic gases to the secondary combustion zone. There, additional air is provided and the pyrolytic gases are burnt in a separate and very clean flame. These pyrolytic gases are tarry and long -chain hydrocarbons that, if not burned, would form a thick smoke. 23 Unique among the gasifiers, TLUDs operate in an oxic batch mode and do virtually all of the biomass pyrolysis or wood -gasification before doing appreciable char -gasification. The transition between the two phases is quite distinct, changing from a characteristic yellow -orange flame (from burning tarry gases) to a smaller bluish flame that denotes the burning of carbon monoxide. There are numerous variations of the TLUD technology. Each variation has its own unique history and intended application. Most of them are do not facilitate the creation and salvaging of the char, because they promote the burning of the char by providing char -gasification within the TLUD device. Almost unique among the TLUD gasifiers, the version named "Champion" (because it won a clean combustion award at Stove Camp 2005) is designed for easy removal of the fuel canister after the pyrolysis is completed, facilitating the collection of the char into a simple container to extinguish the hot char. Such a "snuffer box" could be as simple as a clay pot with a plate to cover it or any other airtight vessel that will smother the residual combustion. Figure 12 shows a vertical cross-section of the "Champion" TLUD stove. Information about and construction details for the Champion TLUD gasifier and the Wendelbo Peko Pe TLUD gasifier are on the Internet at: vwwv.bioenergylists.org/andersontludconstruction and www.bioenergylists.org/wendelbopekope. Additional references are: www.bioenergylists.org/andersontludcopm (Summary of emissions testing of TLUDs) www.bioenergylists.org/stovesdoc/Anderson/GasifierLAMNET.pdf (the "big picture") www.hedon.info/docs/BP53-Anderson-14.pdf (A paper entitled "Micro -gasification: What it is and why it works") www.woodgas.com (Website of Dr. Tom Reed and the Biomass Energy Foundation - BEF) www.bioenergylists.org (An extremely good website dealing will all types of cookstoves.) Also, conducting Internet searches on the names and topics associate with TLUDs will reveal substantial additional information. 24 FIGURE 12: Vertical section of the "Champion" TLUD Gasifier (2008) Pot Concentrator Lid 8 -in. Outer Cylinder 7.5 -in. x 12 -in Fuel Cylinder 6 -in. x Tin Can 6 -in. x 7 -in. Grate -- J Flame Secondary air enters := Riser Gases rise & charcoal forms from upper fuel while pyrolysis front progresses downward through the raw fuel. t, Handle of Concentrator Lid E 1 Handle of Gasifier Optional use of forced -air gives several cooking advantages Secondary Air Primary Air 6.6. Analyses of TLUD Biochars 6.6.1. Background and Procedures Research about biochars is barely beginning and structured studies of carbonization conditions and resulting char properties are rare. This Section 6.5 examines data from one biochar maker (a Champion TLUD cookstove) using one fuel (wood pellets) and operated only one time in each of two settings for the primary air supply. The findings, summarized from unpublished records, are still singular observations and offer potential generalizations similar to those of earlier Sections. Any apparently meaningful observations should be replicated before acceptance and usage in further studies. The purpose of this section is to utilize some of the proposed biochar analyses, report some very preliminary results, and suggest some hypotheses for the underlying causes of the observed trends about characteristics of biochar. Individuals using TLUD technology can easily replicate these studies. 25 A standard -size Champion TLUD (15 cm or 6 inch diameter of the fuel chamber) was modified to take temperature readings at five locations, as shown in Figure 13. Four K -type thermocouples were inserted into the center of the 22 -cm tall fuel pile at heights of 1, 7, 13, and 19 cm above the grate. The fifth one recorded temperatures of the secondary combustion flame at the top of an 18 cm riser; no cooking pot was in place. The fuel both times was 2500 grams of standard woodstove pellets. FIGURE 13: Configuration of the Champion TLUD for Temperature Measurements The first data set was with both primary and secondary air supplied by "Natural Draft", where the chimney effect of the rising hot combustion gases results in the air flows. The first TLUD run lasted 2 hrs 50 minutes functioned in pyrolysis mode, consistently produced 3 kW (,,11 MJ/hr) of thermal energy, and produced 566 g of biochar, (22.6 wt % yield). The second data set, demarcated as "Forced Draft", featured the primary combustion air supply boosted by a small blower. This TLUD run pyrolyzed for 1 hr 25 minutes, doubled the energy output, and yielded 350 g of biochar (14 wt % yield). In both cases, the biochar was carefully removed in six approximately equal layers, extinguished without adding water, allowed to cool, and bagged for analyses. "Layer One" was from the top of the cooled char, and "Layer Six" was closest to the grate. 26 Summary of observations during the tests: No visible smoke was observed during either of the test runs. Temperature readings at one -minute intervals revealed the approach of the pyrolysis front to each thermocouple, but the temperatures did not decrease after its passage. Typical temperatures at and above the pyrolysis front were recorded as 600C to 700C in the first data set, and 800C to 1000C in the second, but initial efforts at thermocouple calibration on a 400 degree Celsius hotplate showed them to be reading 100Cto 200 degrees high, and the error probably increased at higher temperatures. In previous independent experiments with accurate thermocouples, temperatures in the flaming pyrolysis zone of similar TLUD devices have been measured from 490°C to 700°C, increasing with increasing gas flow and faster pyrolysis. Therefore, the reported temperature trends should be considered qualitative and requiring replication with better equipment. 6.6.2. Modified Proximate Analyses of the Experimental TLUD Chars The modified proximate analyses of the six layers of each of the two data collections are presented in Figure 14. FIGURE 14: MODIFIED PROXIMATE ANALYSES OF TLUD CHARS 120 100 80 60 20 0 CO ��� ��� ��� ire �tb ire , ik1/4.1 /1": eke S`: ck`•' \K \d \d I d \d \a ���� ,��� de ,�,�Se ���a ��'06 �C'060 X006 1000 �006 �C'06 +16 +16 +16 C,2r \-\(e 4 kfl l�0 kO 4 kfl kfl D Water (gm/100 gms dry biochar) DAsh ■ Mobile Matter ■ Resident Matter J AL. i / e, el e, 4. QC tom ' t/IV tom ' t� ' t ikS' O O O O O O 27 Based on the trends shown in Figure 14, the following observations are noted: a. Moisture was measurable in eight of the 12 samples, even though every sample was air- cooled and bagged within six hours of the completion of the data collection. The moisture levels were small, less than two weight percent, and were attributed to water vapor adsorbed from the ambient air during cooling. b. The ash content of the chars created with higher heat forced draft run was approximately double that of those created with the lower heat natural draft study. This is compatible with the reduced yield of char by weight from the same amount of starting wood pellets. Unless ash is physically carried away within the flow of the gases, which was not the case in TLUDs, it will accumulate to the extent any gasification reduces the amount of remaining char. c. It is interesting that both cases, Layer 6 (the lowest level, with visibly more loose ash in the collection tray) did not measure higher percentages of ash than the other five layers. One explanation is that only the pyrolyzed pellets were tested and any loose ash was not included in the testing. This practice was adopted because loose ash tends to migrate down within the bed of char and the each layer may contain ash descending from all the layers above it. d. The mobile matter is roughly three -fold higher in the lower temperature natural draft chars than in the higher temperature forced draft data set. Considering the 38% reduction in total weight of char produced, the total mass of mobile matter are roughly five times greater in the first set than in the second set. e. The impression is that the percentage of mobile matter is slightly lower in the middle levels than at Layers 1 and 6 in both data sets. This phenomenon, and the other observations above, deserves further replication studies before less conjecture -inspired explanations should be attempted. 6.6.3. Modified Ultimate Analyses of TL UD Chars Except for the indication of the moisture content, all of the above observations can also be seen in the Modified Ultimate Analyses in Figure 15. (Future biochar studies could present reasons to omit the Proximate Analysis altogether because modern chemical analyses greatly facilitate the testing.) Based on the trends shown in Figure 15, several observations are most evident: a. Almost all of the ash is acid soluble; the non -soluble ash was barely detected. Furthermore, because of the purity of the wood pellets used as the biomass source, mobile and resident nitrogen were present at the analytical detection limit. All three trace compounds, non -soluble ash, mobile nitrogen and resident nitrogen, have been eliminated from Figure 15. The original data may be accessed by exploring the embedded spreadsheet on MS Word versions of this document. 28 b. The amount of mobile carbon is highly variable, being significant in only six of the twelve samples. This inconsistency merits further examination. FIGURE 15: MODIFIED ULTIMATE ANALYSES OF TLUD CHARS 100% 90% 80% a, 70% ca 60% a) 50% v L C, Q. 40% 30% 20% 10% 0% tic <O te.A e re e ec t���, tom ' ����t sce ��, V ° �O <V\S•C \)k Nit t Q ÷s# 01/4- 4)1/4' '1/4%.+ + e1, rb IX Co es 01 re (�Aek � tet, t� ' pit' acs' �� ' t� ebe , v� v �� a' • Resident Carbon 0 Resident H & 0 U Mobile Carbon 0 Mobile H & 0 ❑Ash (acid soluble) c. For the higher temperature forced draft pyrolysis, the percentages of Resident H & 0 are nearly double those of the lower temperature data sets. However, given the total weight production was 62%, it appears that the actual amounts (grams) of Resident H & 0 are not greatly changed by the higher temperatures d. The greatest impacts of the higher temperatures on the percentages shown are on the amounts of Resident Carbon. Not only are the percentages 0% to 17% lower (between corresponding levels), but there is also the 62% weight factor to consider. In general, the absolute amount of Resident Carbon is perhaps only 50% of the Resident Carbon in the lower temperature biochar. 29 e. There is a noteworthy difference between the resident carbon content of TLUD chars and the other tested chars. The other chars (shown in Figure 6) have resident carbon amounts from 55 to 75 percent. The TLUD chars from the top five layers of the lower temperature natural -draft dataset have an average resident carbon reading of 77%. The percentages are more variable (from 63 to 81%) for the higher temperature forced -draft dataset. 6.6.4. 1 he CEC and Adsorption Capacity of TLUD Chars The higher temperatures associated with the forced draft appear to have dramatic impacts on the CEC and adsorption capacity of the two sets of TLUD biochars, as shown in Figure 16. FIGURE 16: CEC AND ADSORPTION CAPACITY OF TLUD CHARS 10.00 9.00 8.00 7.00 6.00 5.00 4.00 3.00 2.00 1.00 0.00 �❑ 10% of CEC in meq/100g ■Adsorption Capacity (wt% @ 100C) — k Sri' N KC 0 At S v1) . vgo. ���e�� 'V en) Based on the trends shown in Figure 16, several observations are most evident: esti �V a. The surprisingly high adsorption capacity in Layer 6 of the lower -temperature natural draft biochars caused a review of the methodology, and a probable explanation of the data. When the pyrolysis phase finished on that batch of fuel, the operator attempted to extinguish the processes by cutting off all of the air (with oxygen) that could enter the TLUD. However, 50 minutes later the biochar was still very hot, and then the 6 levels of samples were removed. One plausible interpretation is that some small amount of air managed to enter and sustain some char - gasification during the 50 minutes, resulting in the lowest level of the char being subjected to the 30 higher temperatures and perhaps other un-identified processes. This might have also influenced Layer 5 chars, but the impact is less dramatic. Referring to Figure 15, the higher amount of mobile carbon might also be attributed to this delay in removal of the biochar from the TLUD device. The delay did not occur with the second batch of data sets, since the operator learned how to (very carefully) scoop out the hot char. b. The CEC readings of Layers 1 and 2 in the natural draft TLUD data are similar to the range of CEC readings reported in Figure 8 for the other tested biochars. The remaining TLUD chars had markedly lower CEC levels. Restated, ten of the twelve CEC readings on Figure 16 are lower than any of the readings on Figure 8. It is known that CEC levels can naturally increase in soils, so the long term consequences of these low values is not known and may not be of significance. c. The adsorption capacities for the TLUD biochars in Figure 16 overlay the data reported in Figures 8 and 10, generally in the range of 1% to 7%. However, the TLUD data reveal that the adsorption capacities of the second set of six levels are substantially higher (average = 5.8 wt %) than for the first set (average = 2.0 wt %, with Layer 6 excluded because of the post combustion air leak discussed in 6.5.4. a). The single difference in the TLUD runs was the forced air for the second set, resulting in higher pyrolysis temperatures. This near tripling of the adsorption capacity must be offset by the 62% weight yield. Combining these trends, per kilo of original raw biomass converted into biochar available to go to the soil, the second TLUD operation generated approximately double the total adsorption capacity. A further observation based on 6.6.4. b & c: Adsorption capacity and CEC comparisons within biochar production methods are not accurate without consideration of the char yields. Furthermore, when comparing the yields of charcoal produced by oxic processes (such as with TLUDs) and anoxic processes (such as by retorts), the external fuel utilized to sustain the anoxic pyrolysis needs to be taken into consideration and accounted for in the overall yield calculation. 6.6.5. Summary and Conclusions Concerning the Two TLUD Char Datasets TLUD devices can be made and used at home and small commercial settings. They are easy and inexpensive to construct and operate in several sizes from very small (1 -gallon) up to moderate (55 -gallon) devices. Small quantities of biochar can be made quickly for research. TLUDs can use a wide variety of feedstocks. The fuel pieces are generally smaller (being pellets, chips, briquettes, pucks, etc.). Well -dried feedstocks are recommended and TLUDs have less stable secondary combustion with wet fuels due to elevated moisture levels in the volatilized wood gases. TLUD (Top -Lit UpDraft) pyrolytic gasifiers produce biochar with reasonable characteristics that merit further consideration. They utilize "oxic" (flame -present) pyrolysis. The conditions for operating the TLUD devices can influence biochar properties — especially adsorption capacity. In the context of world cultures, the small sizes of TLUD cook stoves provide advantages for the poorest people to obtain household energy for cooking and space heating while also producing 31 biochar. By sheer numbers of possible users, large volumes of biochar are possible in developing countries, which would represent substantial soil benefits and carbon dioxide offsets. 7. OPTIONS FOR INFORMALLY TESTING CHARS As has been seen, there is a significant amount of variability within virtually every measured property in chars that aspire to be good biochars. As such, it takes more than just the claim of the seller to make a quality biochar, which leads us to recommend, "Buyer beware". This final section presents some fairly accessible tests that allow one to screen out highly undesirable biochar properties and, perhaps, assist in selecting the better biochar candidates. Moisture and ash are two ingredients found in every bag of biochar, yet they add little value to the long-term biochar performance. Both are fairly straightforward to measure and any candidate char should be tested for both. 7.1. Moisture Measuring moisture content is particularly straightforward and can be done even in a lowly toaster oven. A small sample of the char is placed into a closed but not sealed container, preferably metal, and heated to just above 100 Celsius in dry air for an extended period of time. The time is "until no additional weight loss is observed." (Heating overnight works great if your oven is appropriate for that many hours of use). A suitable container can be made out of a 4 oz tomato paste can, with the top removed using one of the newer -style can openers that slices the edge of the top lid so that it sets back in place on the rim and does not fall inside the can. The lid is to shield the char from the direct infrared heating of the toaster oven elements. An alternative is to cover the container with heavy-duty aluminum foil and poke a few slits in the cover. A standard oven thermometer, suitable for use inside the toaster oven, provides sufficiently accurate and reproducible temperature indications, since the thermostats of inexpensive toaster ovens are not actually precise. An inexpensive scale, accurate to 0.01 grams, is needed to weigh the samples before and after heating. Acceptable units are available on "ebay" for less than $20 that read to 0.01 grams up to 200 grams — the principal target market application is likely the illegal drug trade at the retail level. Alternatively, a kitchen scale with nearest gram accuracy can be used if the sample of char is appropriately larger (also requiring longer drying times). The analytical techniques require a bit of practice to achieve consistency and reproducibility, but half a dozen attempts will turn you into a seasoned analytical practitioner for measuring moisture content. In general, as produced, chars have less than 5% and never more than 10% residual moisture. If higher, you are being sold "char with water added". However, many biochars are highly hydroscopic, an important property in the soil, and will adsorb significant amounts of moisture if exposed to humid air. If you are using homemade chars, this is really not an issue because you probably know when the char was made and if it has been wetted or exposed to humid air. Since the water is not harming 32 anything in the ultimate performance of the biochar, the issue is that water should not be a significant component of a commercial product sold on a weight basis or requiring transportation over a long distance. 7.2. Ash Ash is also relatively straightforward to measure — this requires the same scale accuracy of 0.01 grams, a propane camping stove and a clean open top tuna fish or cat food "tin can" (avoid aluminum). The tin can needs to be heated once while empty to burn off any coatings on the container. Weigh the container after it cools. A half -centimeter layer of dried char is spread on the bottom of this clean dry tin can and the weight of the added char is noted. The open tin can is heated on the camping stove over an open flame that uniformly heats the entire bottom of the container. The contents are periodically stirred to facilitate ashing, taking care to not knock or blow away any of the ash. The process is continued until the tin can contains only gray to white ash residue. At no time should the contents of the tin can catch fire and burn with an open flame, since that carries ash away as particulates in the smoke. The ashed sample and tin can are weighed, then the ash removed and the weight of the tin can subtracted. The weight of ash on a dry char basis is calculated. Most chars made from clean wood sources have less than 5 weight percent ash, while agricultural residues, such as corn stover, may have significantly higher levels. It is tempting to worry about the ash constituents in chars. This concern is legitimate if one does not know the origin of the biomass utilized to produce the char. In most cases, the starting material is new clean wood or agricultural residues, and concerns about ash constituent are generally not justified. However, whenever the origin of the biomass is unknown, or the ash levels are significantly higher than 10 weight percent, it may be worth testing the ash for soil pH impact and the presence of metals. The former can be estimated using pH paper and will indicate how much the ash will act like lime in the soil. For acidic soils, additional alkalinity is welcome, but for high pH soils, additional liming may lead to poor crop performance. Testing for metals should be conducted by a qualified laboratory that can also help interpret the analytical results. 7.3. Adsorption Capacity Surprisingly, adsorption capacity is one test that is accessible to the home practitioner. It does take some practice and it helps if you obtain a sample of activated carbon to use as a standard reference. Small quantities of activated carbon are available at pet supply stores, since it is used in home aquarium filters. The approach is to prepare a very dry sample of the candidate char, and then "challenge" it to adsorb a known vapor source. The drying of the char is critical, because adsorbed water will artificially lower the observed adsorption capacity. The drying method described previously is used, but the recommended temperature is around 200 degrees Celsius. The reason for the higher drying temperature is shown in Figure 17, which shows the weight losses of seven different char samples as they are heated from room temperature to 300 Celsius in a nitrogen atmosphere. As can be seen, there is a plateau in the weight loss between 175 C and 225 Celsius, which corresponds with the desorption of the adsorbed water vapor and any light volatile compounds 33 such as methanol, acetic acid, acetaldehyde, etc., which also diminish the adsorption capacity of the char, resulting in an incorrectly lower measurement of the Adsorption Capacity. FIGURE 17: WEIGHT LOSS CURVES FOR A SET OF SEVEN CHARS 120% UO 118% CD 116% 114% 112% O C 110% L O.108% CO al 106% Ame ,O)104% v 102% 100% r Juniper Char - Process I Aspen char 5-08 SPF char 5-08 Juniper Char - Process II Gasifier Carbon -rich ash Cedar 2-09 Beech 11-05-08 drying wt losses due to wt loss 1— residual carbonization 0 50 100 150 200 Temperature Celsius 250 300 350 Prior to drying, the candidate char should be crushed and sieved to yield a coarse granular material, with granules between 1 and 5 mm in diameter. After the char is dried to approximately 200 degrees Celsius, it is cooled in a container with a sealed lid to avoid uptake of atmospheric moisture. Once cooled, a weighed clean dry tomato paste can is filled about one half way with dry granular char and weighed again. The "challenge gas, R134a, is obtained from any auto supply store in a 12 ounce cans. An R134a dispensing device, with a metering valve and supply tubing, is also required. Modify the dispensing device by cutting the flexible hose and screwing an inflation needle used to pump up soccer and basketballs into the cut end of the hose. Inject the R134a slowly into the bottom of the tomato paste can through a small hole drilled in the unopened end of the can. As the R134a is admitted into the char, some R134a will be adsorbed and the heat of adsorption will be released — the container may get warm to the touch. The addition of R134a should continue until the char will adsorb no additional challenge gas. In general, the R134a addition can continue until the temperature of char returns to the starting temperature, since the excess R134a will enter as a cold vapor and eventually cool the char mass. A simple insertion meat thermometer can improve the accuracy of determining the endpoint of the R134a addition. The container should be shaken periodically to assist the equilibration process by mixing the char contents. When completed, the weight of the container, char and adsorbed R134a allow the calculation of the percentage of weight increase caused by the R134a. 34 In general, chars with good adsorption capacities show a noticeable temperature rise and significant weight gain, such as ten or more percent of the weight of the original char when the sample temperature is near ambient. In contrast, chars with low adsorption capacities (zero to four percent) will show little temperature rise during R134a addition and essentially no weight gain due to the adsorption of R134a. Furthermore, the adsorption test conducted on activated carbon should yield very high percentage increases in weight and a noticeable temperature rise during R134a addition. The differences become obvious with relatively little practice. Note: The results obtained by this ambient -temperature method are not directly comparable with the reported GACS results obtained at 100 and 125 degrees Celsius, as discussed in conjunction with Figures 8, 10 and 11. Adsorption results at typical ambient temperatures are on the order of twice the levels observed at the 100-125 degree Celsius. 7.4. The "feel" of good char Properly carbonized wood forms a rigid, easily crushed material that lacks pockets of under - carbonized material. This material differs from the partially burned logs that linger after the campfire goes out. In addition, fully carbonized chars are also not particularly "greasy" to the touch. They are dirty and make copious amounts of black dust, but that dust will wash off one's hands with just water. If it takes significant amounts of soap to remove the char powder from the pores of the skin, then the char has significant amounts of mobile matter, with the associated concerns discussed previously. 7.5. Other tests Beyond these simple tests, it becomes difficult to accurately measure char properties outside a proper analytical lab. Attempting proximate and ultimate analyses without the proper analytical equipment is unlikely to yield any insightful results. It is expected that facilities that are currently testing soils for typical agricultural properties, such as fertilizer content, alkalinity, etc., will offer appropriate biochar characterization tests in the future as biochar becomes a more accepted soil component. 8. CONCLUSIONS and RECOMMENDATIONS FOR FUTURE EFFORTS A discussion of this length does not lend itself to a comprehensive summary and one will not be attempted here. If but one conclusion is allowed, it would be that chars can be characterized sufficiently to discriminate between individual samples with a resolution adequate to predict subsequent effects when utilized as biochar, the soil amendment. Unfortunately, the research to relate char properties, measured by any means, to soil performance is at its infancy. However, when those cause and effect relationships are discerned, the composite path from measurable char properties to predictable soil performance will be in place. In anticipation of the day when char properties can be projected onto soil performance, the following issues remain unresolved and deserve further investigation: 35 a. Characterization of the "mobile matter" and "resident matter" and how it relates to the carbonization process that generates the biochar. Pyrolysis processes produce a wide variety of carbonization conditions, both between commercial processes and even within individual operations. That variability manifests itself in the transformation of the organic portion of the biomass into biochar and, to a lesser extent, the modification of ash properties. Understanding how pyrolysis conditions influence the char properties (and how the formed chars impact soil performance) will create the hierarchy of carbonization processes for the production of biochar and guide the operation of individual processes to optimize biochar efficacy. For example, it is anticipated that anoxic retort processes will yield significantly different non- graphene organics than would be found in similar chars created under oxic conditions, with both the mobile matter and resident matter having different properties, impacts and fates in the soil. b. Identifying and standardizing unique analytical methods for biochars and establishing the appropriate interpretation of the results. Biochar is a unique class of materials and its roles in carbon sequestration and influence on soil dynamics fall outside the capabilities of analytical methods developed for other materials, namely coal. This discussion has been very heavy-handed in the modification of traditional ASTM tests along with the wholesale advocacy of alternate analytical methods. We have proposed potentially insightful interpretations of the results, and have stated our rationale for those changes. Specifically, all components of the modified proximate and ultimate analyses methods, along with the standardization of the CEC assay and measurement of adsorption capacities, need to be subjected to a timely review, optimization, and adoption by the biochar research community. c. The science of biochar as a small but enabling aspect of the impact of biochar on society. The improved soil productivity and carbon sequestration benefits of biochar achieve nothing unless implemented outside the ivory halls, and have little impact if restricted to the traditional pathways of technology development and distribution. TLUD technology represents one example of "distributed biochar production". Such "low tech — low capital" approaches, with implementation on a massive scale within existing non -affluent cultures, would yield immediate results and likely have more cumulative impact than the "patent -pending" improvements of centralized production. Clearly, the distributed programs need to be correctly orchestrated along with sustainable biomass procurement practices. But the programs actually do need to occur if biochar is to somehow make a difference to the plants, the farmers, the atmosphere, and the societies of this world. As such, the time for bickering, power plays, and haggling about the exact amount of carbon sequestration credits for a specific biochar addition should be pushed behind us. As Voltaire noted, "The perfect is the enemy of the good", but only if we let it. In closing, biochar is at "the end of the beginning" and has the potential to play a dynamic role in the future of humanity and its societies. Hopefully, this discussion provides a small nudge in the right direction. 36 View publication slats b .a 4 EXHIBIT 14 From: James Gaspard Date: Wed, Oct 2, 2024 at 9:45 PM Subject: Re: Referral comments for Brighton hearings To: Robert Demaree <bob.demaree@kw.com> Cc: Dylan Van Demar Michael Hall <pagoda.mapping@gmail.com>, Michael Dente <michael.dente@kw.com>, Bob Choate <BChoate@cp2law.com> The 2013 study is from Eastern Europe and the technologies historically used in that part of the world do not have emission requirements that exist in Colorado. All I know is there are no hydrocarbons in our exhaust and our biochar has been tested and has no PAHs in the biochar. See attached test report from the State of Oregon. Jordan was the person quoted and that was a statement she made to CSU in an alumni post by CSU. Biochar is used for water filtration. It is ironic that they think we pollute the water. There is no liquid by-product from our production. Other biochar production technologies produce liquid discharges. James Gaspard CEO Biochar Now Colorado Site Address: 19500 County Road 7, Berthoud, CO 80513 Mailing Address: P.O. Box 1832, Loveland, CO 8O539-1832 www.biocharnow.com PAH and PCB test results.PDF 205K e-Hardcopy 2.0 Automated Report Northern California ccmsrn LABORATORIES Technical Report for Walking Point Farms - Sherwood OR Walking Point Farms - Soil Testing WALKING POINT FARMS - SOIL TESTING Accutest Job Number: C32292 Sampling Date: 02/03/14 Report to: Walking Point Farms 15485 SW Scholls Drive Sherwood, OR 97140 chris@walkingpointtech. com ATTN: Chris Tenney Total number of pages in report: 17 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Tony Vega 408-588-0200 James J. Rhudy Lab Director Certifications: OR (CA300006) CA (08258CA) AZ (AZ0762) DoD ELAP (L -A -B L2242) This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. Northern California • 2105 Lundy Ave. • San Jose, CA 95131 • tel: 408-588-0200 • fax: 408-588-0201 • http://www.accutest.com Accutest Laboratories is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. t 1 of 17 ▪ ACCUTEST C32292 LABORATORIES Sections: Table of Contents -1- Section1: Sample Summary3 Section 2: Summary of Hits 4 Section 3: Sample Results 5 3.1: C32292-1: #1 GRAB 6 Section 4: Misc. Forms 9 4.1: Chain of Custody 10 Section 5: GC/MS Semi-volatiles - QC Data Summaries 12 5.1: Method Blank Summary 13 5.2: Blank Spike/Blank Spike Duplicate Summary 14 Section 6: GC Semi-volatiles - QC Data Summaries 15 6.1: Method Blank Summary 16 6.2: Blank Spike/Blank Spike Duplicate Summary 17 40, a C) S ■ 2 of 17 ▪ ACCUTEST C32292 LABORATORIES Accutest Laboratories Sample Summary Walking Point Farms - Sherwood OR Job No: C32292 Walking Point Farms - Soil Testing Project No: WALKING POINT FARMS - SOIL TESTING Sample Collected Number Date Time By Matrix Received Code Type Client Sample ID C32292-1 02/03/14 10:00 HB 02/06/14 SO Soil #1 GRAB Soil samples reported on a dry weight basis unless otherwise indicated on result page. MI f 3 of 17 ACCUTEST C32292 LABORATORIES Summary of Hits Job Number: Account: Project: Collected: C32292 Walking Point Farms - Sherwood OR Walking Point Farms - Soil Testing 02/03/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method Page 1 of 1 • C32292-1 #1 GRAB No hits reported in this sample. , 4of17 ACCL TEST C32292 LABORATORIES Section 3 Northern California ccmsrn LABORATORIES Sample Results Report of Analysis w IIM 5of17 ACCUTEST C32292 LABORATORIES Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: Lab Sample ID: Matrix: Method: Project: #1 GRAB C32292-1 SO - Soil SW846 8270C SW846 3550B Walking Point Farms - Soil Testing Date Sampled: 02/03/14 Date Received: 02/06/14 Percent Solids: 92.6 • Run #1 a Run #2 File ID Y24866. D DF 1 Analyzed By 02/07/14 MT Prep Date 02/07/ 14 Prep Batch Analytical Batch OP9529 EY1135 Run #1 Run #2 Initial Weight Final Volume 1.17g 1.0ml BN PAH List CAS No. Compound 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 218-01-9 53-70-3 206-44-0 86-73-7 193-39-5 90-12-0 91-57-6 91-20-3 85-01-8 129-00-0 CAS No. 4165-60-0 321-60-8 1718-51-0 Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a, h)anthr acene Fluoranthene anthene Fluorene Indeno(1, 2, 3-cd)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Surrogate Recoveries Nitrobenzene -d5 2-Fluorobiphenyl Terphenyl-d14 Result RL MDL Units ND 4600 2000 ug/kg ND 4600 2200 ug/kg ND 4600 1500 ug/kg ND 4600 920 ug/kg ND 4600 920 ug/kg ND 4600 920 ug/kg ND 4600 1200 ug/kg ND 4600 920 ug/kg ND 4600 920 ug/kg ND 4600 1100 ug/kg ND 4600 920 ug/kg ND 4600 2000 ug/kg ND 4600 1200 ug/kg ND 4600 2100 ug/kg ND 4600 2200 ug/kg ND 4600 2100 ug/kg ND 4600 1600 ug/kg ND 4600 920 ug/kg Run# 1 Run# 2 Limits 61% 15-101% 61% 15-104% 69% 56-123% (a) Reporting Limit increased due to sample matrix (charcoal powder). Q ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 11i 6 of 17 MI ACCDTEST C32292 LABORATORIES Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: Lab Sample ID: Matrix: Method: Project: #1 GRAB C32292-1 SO - Soil SW846 8082 SW846 3550B Walking Point Farms - Soil Testing Date Sampled: 02/03/14 Date Received: 02/06/14 Percent Solids: 92.6 • Run #1 a Run #2 File ID PP033558.D DF 1 Analyzed By 02/07/14 RV Prep Date 02/07/ 14 Prep Batch Analytical Batch OP9530 GPP1097 Run #1 Run #2 Initial Weight Final Volume 1.16g 10.0ml PCB List CAS No. 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 CAS No. 877-09-8 877-09-8 2051-24-3 2051-24-3 Compound Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Surrogate Recoveries Tetrachloro-m-xylene lene Tetrachloro-m-xylene lene Decachlorobiphenyl Decachlorobiphenyl Result ND ND ND ND ND ND ND Run# 1 70% 65% 98% 86% RL 930 190 930 470 930 470 930 470 930 470 930 470 930 190 Run# 2 MDL Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Limits 38-109% 38-109% 49-138% 49-138% (a) Reporting Limit increased due to sample matrix (charcoal powder sample). Q ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 11i 7 of 17 ACCUTEST C32292 LABORATORIES Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: #1 GRAB Lab Sample ID: C32292-1 Matrix: SO - Soil Project: Walking Point Farms - Soil Testing Date Sampled: 02/03/14 Date Received: 02/06/14 Percent Solids: 92.6 • General Chemistry Analyte Moisture, Percent Result RL Units DF Analyzed By Method 7.4 % 1 02/08/14 18:45 PH SM18 2540G RL = Reporting Limit � i 8 o 17 ▪ ACCUTEST C32292 LABORATORIES Section 4 ■ Northern California ccmsrn LABORATORIES Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody a MI , 9of17 ACCUTEST C32292 LABORATORIES a LABORATORIES Samplers's Name Accutest Sam'te ID Sample ID / Field Point / Point of Collection CHAIN OF CUSTODY 2105 Lundy Ave, San Jose, CA 95131 (408) 588-0200 FAX: (408) 588-0201 Client Purchase Order f _ MIN 10 Day 5 Day 3 Day Way 1 Day Same Day Emergency T/A data available VIA Labllnk Approved By'Date: Relinquished by Sung 1 liglettet-tk Relinquished by: 5 Relinquished by: Commercial "A" - Results only Commercial "8" - Results with QC summaries Commerical "t3+" - Results, QC, and chromatograms FULTI - Level 4 data package EDF torGeotracker [] EDO Format Provide EDF Global ID Provide EDF Logcode: FED -EX Track,9 j 71 °C1804)-- ttfe Order Control Accutest Quote Sample Custody must be documented below each time samples change possession, Including courierdelivery, Date T Wit)Received By: Relinquished By: f001/14 1C4r/ ) it 2�" '/`if l6m%'!ec Time: Date D e me Received By: 5 Relinquished By: 4 Accutest NC Job U: C Comments! Remarks Date Tune: whii1/4, / Date Time: Received Sy: Custody SealS ZZg GW- Ground l'Vater SW- Surface %Wier OW Or114.inc,Water (Percht rate Only) LAB USE ONLY 2 Received By: Received Sy; 4 D C32292: Chain of Custody Pagel of 2 • 10 of 17 'CCU -TES -17 C32292 LABORATORIES Miakccu-ras 17p Accutest Laboratories Sample Receipt Summary LABORATORIES Accutest Job Number: C32292 Date / Time Received: 2/6/2014 Client: WALKING POINT FARMS Cooler Temps (Initial/Adjusted): #1: (15.3/15); Cooler Security 1. Custody Seals Present: 2. Custody Seals Intact: Cooler Temperature 1. Temp criteria achieved: 2. Cooler temp verification: 3. Cooler media: 4. No. Coolers: Y or N Delivery Method: 3. COC Present: ❑ 4. Smpl Dates/Time OK Y or N IR2 Glass; No Ice 1 Quality Control _Preservation Y or N N/A 1. Trip Blank present / cooler: 2. Trip Blank listed on COC: 3. Samples preserved properly: 4. VOCs headspace free: Project: Walking Point Farms FedEx Airbill #' s: 797818710680 Y or N Sample Integrity - Documentation 1. Sample labels present on bottles: 2. Container labeling complete: 3. Sample container label / COC agree: Sample Integrity - Condition 1. Sample recvd within HT: 2. All containers accounted for: 3. Condition of sample: Sample Integrity - Instructions 1. Analysis requested is clear: 2. Bottles received for unspecified tests 3. Sufficient volume recvd for analysis: 4. Compositing instructions clear: 5. Filtering instructions clear: Y or N a Y or N Intact Y or N N/A O Comments Accutest Laboratories V:408.588.0200 2105 Lundy Avenue F: 408.588.0201 San Jose, CA 95131 www/accutest.com C32292: Chain of Custody Page 2 of 2 MIT 11 of 17 ACCUTEST C32292 LABORATORIES Section 5 Northern California ccmsrn LABORATORIES GC/MS Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Cif 11 12 of 17 ACCUTEST C32292 LABORATORIES Method Blank Summary Job Number: Account: Project: C32292 WPFORS Walking Point Farms - Sherwood OR Walking Point Farms - Soil Testing Page 1 of 1 Sample OP9529-MB File ID DF Analyzed By Y24862.D 1 02/07/14 MT Prep Date 02/07/14 Prep Batch Analytical Batch OP9529 EY1135 The QC reported here applies to the following samples: C32292-1 CAS No. Compound 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 218-01-9 53-70-3 206-44-0 86-73-7 193-39-5 90-12-0 91-57-6 91-20-3 85-01-8 129-00-0 Acenaphthene Acenaphthy lene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a, h)anthracene F luoranthene Fluorene Indeno(1, 2, 3 -cd)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene CAS No. Surrogate Recoveries 4165-60-0 Nitrobenzene -d5 321-60-8 2-Fluorobiphenyl 1718-51-0 Terphenyl-d14 Method: SW846 8270C Result RL MDL Units Q ND 500 220 ND 500 230 ND 500 160 ND 500 100 ND 500 100 ND 500 100 ND 500 130 ND 500 100 ND 500 100 ND 500 120 ND 500 100 ND 500 220 ND 500 130 ND 500 230 ND 500 240 ND 500 230 ND 500 170 ND 500 100 78% 75% 95% Limits 15-101% 15-104% 56-123% ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 13 of 17 ACCUTEST C32292 LABORATORIES Blank Spike/Blank Spike Duplicate Summary Job Number: C32292 Account: WPFORS Walking Point Farms - Sherwood OR Project: Walking Point Farms - Soil Testing Page 1 of 1 Sample OP9529-BS OP9529-BSD File ID DF Y24863. D 1 Y24864. D 1 Analyzed By 02/07/14 MT 02/07/14 MT Prep Date 02/07/14 02/07/14 Prep Batch OP9529 OP9529 Analytical Batch EY1135 EY1135 The QC reported here applies to the following samples: C32292-1 CAS No. Compound 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 218-01-9 53-70-3 206-44-0 86-73-7 193-39-5 90-12-0 91-57-6 91-20-3 85-01-8 129-00-0 Acenaphthene Acenaphthy lene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a, h)anthracene F luoranthene Fluorene Indeno(1, 2, 3 -cd)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Method: SW846 8270C Spike BSP BSP BSD BSD Limits ug/kg ug/kg % ug/kg % RPD Rec/RPD 2500 1970 79 1740 70 2500 2010 80 1760 70 2500 2270 91 2120 85 2500 2410 96 2260 90 2500 2480 99 2350 94 2500 2390 96 2290 92 2500 2410 96 2190 88 2500 2450 98 2230 89 2500 2410 96 2250 90 2500 2510 100 2310 92 2500 2500 100 2320 93 2500 2090 84 1840 74 2500 2480 99 2260 90 2500 1980 79 1790 72 2500 1970 79 1750 70 2500 1890 76 1730 69 2500 2230 89 2020 81 2500 2410 96 2330 93 CAS No. Surrogate Recoveries BSP 4165-60-0 Nitrobenzene -d5 321-60-8 2-Fluorobiphenyl 1718-51-0 Terphenyl-d14 83% 78% 97% BSD 74% 70% 95% Limits 15-101% 15-104% 56-123% 12 13 7 6 5 4 10 9 7 8 7 13 9 10 12 9 10 3 34-112/28 33-115/28 59-111/21 72-122/22 71-120/22 67-123/24 57-134/24 74-126/25 73-125/22 59-132/23 69-117/21 42-112/24 60-131/21 33-110/30 33-107/30 32-121/31 57-113/21 63-120/20 * = Outside of Control Limits. w N amt 14of17 ACCUTEST C32292 LABORATORIES Section 6 Northern California ccmsrn LABORATORIES GC Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries 0) 11 15 of 17 ACCUTEST C32292 LABORATORIES Method Blank Summary Job Number: Account: Project: C32292 WPFORS Walking Point Farms - Sherwood OR Walking Point Farms - Soil Testing Page 1 of 1 Sample OP9530-MB File ID DF Analyzed By PP033559.D 1 02/07/14 RV Prep Date 02/07/14 Prep Batch Analytical Batch OP9530 GPP1097 O) The QC reported here applies to the following samples: C32292-1 CAS No. Compound 12674-11-2 Aroclor 1016 11104-28-2 Aroclor 1221 11141-16-5 Aroclor 1232 53469-21-9 Aroclor 1242 12672-29-6 Aroclor 1248 11097-69-1 Aroclor 1254 11096-82-5 Aroclor 1260 CAS No. Surrogate Recoveries 877-09-8 877-09-8 2051-24-3 2051-24-3 Tetrachloro-m-xy lene Tetrachloro-m-xy lene Decachlorobiphenyl Decachlorobiphenyl Result ND ND ND ND ND ND ND 85% 83% 108% 90% Method: SW846 8082 RL MDL Units Q 100 100 100 100 100 100 100 Limits 20 50 50 50 50 50 20 38-109% 38-109% 49-138% 49-138% ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg t r _ i 16 of 17 ▪ ACCUTEST C32292 LABORATORIES Blank Spike/Blank Spike Duplicate Summary Job Number: C32292 Account: WPFORS Walking Point Farms - Sherwood OR Project: Walking Point Farms - Soil Testing Page 1 of 1 Sample OP9530-BS OP9530-BSD File ID DF PP033560.D 1 PP033561.D 1 Analyzed By 02/07/14 RV 02/07/14 RV Prep Date 02/07/14 02/07/14 Prep Batch OP9530 OP9530 Analytical Batch GPP 1097 GPP 1097 The QC reported here applies to the following samples: C32292-1 CAS No. Compound 12674-11-2 Aroclor 1016 11096-82-5 Aroclor 1260 CAS No. Surrogate Recoveries 877-09-8 877-09-8 2051-24-3 2051-24-3 Tetrachloro-m-xylene Tetrachloro-m-xylene Decachlorobiphenyl Decachlorobiphenyl Spike BSP BSP ug/kg ug/kg % 400 400 BSP 81% 77% 104% 86% 364 91 406 102 BSD 80% 77% 107% 89% Method: SW846 8082 BSD BSD ug/kg 361 90 415 104 Limits 38-109% 38-109% 49-138% 49-138% Limits RPD Rec/RPD 1 46-114/22 2 54-127/21 * = Outside of Control Limits. t f 17 of 17 ▪ ACCUTEST C32292 LABORATORIES Trinity/ Consultants MEMORANDUM To: Dylan Van Demark, Biochar Now Cc: James Gaspard, Biochar Now From: Carla Manzi, Trinity Consultants Date: February 12, 2025 RE: Biochar Now LLC: Proposed Biochar Production Facility at NGL Water Solutions County Road 6, Fort Lupton, Co - Process Description & Emissions Summary Trinity Consultants (Trinity) is preparing this memorandum on behalf of Biochar Now to provide an overview of the biochar manufacturing process and anticipated emissions from the proposed biochar production facility at the NGL Water Solutions County Road 6 property in Fort Lupton, Weld County, Colorado. Facility Overview Biochar Now plans to construct a new biochar production facility at the NGL Water Solutions County Road 6 property in Fort Lupton, Colorado. The proposed facility will manufacture biochar using a controlled heating process known as pyrolysis to convert raw wood into biochar while maintaining emissions below the Denver Metro — North Front Range (DMNFR) Title V permitting thresholds. The DMNFR area is currently classified as a severe nonattainment area for ozone. As such, the Title V major source thresholds are 25 tons per year (tpy) of NOx and VOC, and 100 tpy for all other criteria pollutants (CO, PM, and S02). The proposed facility will be similar to the company's existing Berthoud, Weld County, Colorado, operation, which already diverts thousands of tons of clean construction and demolition (C&D) waste wood from landfills by converting it into biochar. The Fort Lupton facility will further enhance these efforts, significantly increasing C&D recycling capacity in the Front Range while promoting environmental sustainability and protecting public health in Colorado. The proposed facility will operate as a synthetic minor source and will produce significantly lower NOx and VOC emissions than nearby industrial sources. Process Description Raw wood will be delivered by truck, sorted, shredded, and loaded into kilns, where it will undergo the pyrolysis process. Each kiln will be fitted with a natural gas -fired afterburner to maintain high temperatures and control emissions. Once pyrolysis is complete, the kilns are moved to a designated cooling area. The resulting biochar will then be transported to an enclosed building for unloading into trucks before being shipped off site for further processing, packaging, and distribution. Daily operations will be limited to maintain emissions below the DMNFR Title V permitting thresholds. 1. Raw Material Handling: Wood logs are received by truck, sorted, and stored before processing. The logs are then shredded and screened to reduce wood size before being loaded into kilns. 2. Pyrolysis in Biochar Kilns: Wood material is loaded into kilns. Each kiln is then fitted with a removable afterburner to control emissions from individual kilns. Pyrolysis within the kiln is initiated by a natural gas -fired kiln burner that is a component of the kiln itself. Once the pyrolysis is initiated, the kiln burner is turned off as the pyrolysis process is self-sustaining and does not require additional natural February 2025 Biochar Now LLC Fort Lupton Facility Page 2 of 5 gas combustion. The kiln's integral seal -cover lid is then opened, and the afterburner is used to control kiln emissions. 3. Biochar Cooling: After pyrolysis, kilns are cooled before unloading. There are no emissions from the kilns during the cool -down period. 4. Kiln Emptying: Once cooled, the biochar is transported to a kiln emptying area inside an enclosed building, where it is unloaded into a covered truck. The biochar is then hauled to the Berthoud facility for final processing, packaging, and distribution. Facility Emissions Overview The table below presents the estimated maximum PM, PMlo, PM2.5, fugitive PM, NOx, CO, VOC, and methanol emissions for the proposed facility. The emissions were calculated using the methodologies described below. The proposed facility will qualify as a synthetic minor source of emissions, similar to Biochar Now's existing biochar production facility in Berthoud. A synthetic minor source is a source that has potential emissions that exceed the major source threshold(s) but have implemented emission controls or some other federally enforceable limit to cap potential emissions below the Title V permitting thresholds. (Note that emission estimates are based on projected operations and are subject to change depending on final facility design.) Table 1 Maximum Estimated Emissions for the Fort Lupton Facility Pollutant Expected Actual Emissions Potential Emissions Potential Emissions (tons/yr) Before Controls (tons/yr) After Controls (tons/yr) PM 0.7 0.7 0.7 PM10 0.6 0.6 0.6 PM2.5 0.6 0.6 0.6 Fugitive PM 3.1 3.1 3.1 Fugitive PM10 1.1 1.1 1.1 NOx 24 24 24 CO 14 14 14 VOC 5.9 117 5.9 Highest (Methanol) Individual HAP 2,300 lbs/yr 46,000 lbs/yr 2,300 lbs/yr Emissions from the pyrolysis process: PM/PMio/PM2.5, NOx, CO, VOC, and methanol emissions from the biochar kilns are based on emission factors derived from a 2021 source test report conducted at Biochar Now's Berthoud facility (see attached 2021 Emissions Testing Report) and include an additional 25%-50% safety factor. The afterburner control efficiency of 95% was applied to all uncontrolled VOC and volatile hazardous air pollutant (HAP) emission rates. The table below presents a summary of the calculated emission factors for a single kiln. Biochar Now will limit the daily and annual kiln processing rates to remain below DMNFR Title V thresholds. February 2025 Biochar Now LLC — Fort Lupton Facility Page 3of5 Table 2 — Single Kiln Emission Factors Single Kiln Emission Factors Pollutant Stack Test Result i Emission Factor 2 Units PM ., 0.113 0.14 lb/ton processed Plyilo' 0.113 0.14 lb/ton processed PM2 5 ` 0.113 0.14 lb/ton processed NOX4 0.425 0.53 lb/hr V005 1.076 1.61 lb/ton processed CO6 0.219 0.33 lb/hr Methanol 0.212 0.32 lb/ton processed 1 Emission factors as measured m the afterburner stack. 2 All emission factors based on April 2021 stack test with multiplying factor as shown below. PM emission factor multiplier: 4 NOx emission factor mutiplier: VOC emission factor mutiplier: CO emission factor mutliplier: McOH emission factor multiplier: Multiplier Notes 1.25 1.25 1.50 1.5 1.5 Stack test factor is the maximum measured for any class of PM. Emissions measured at stack exit. See uncontrolled estimate below. Emissions measured at stack exit. See uncontrolled estimate below. ® Emissions from feedstock handling (shredding and kiln loading): PM/PM1o/PM2.5 emissions from feedstock handling (shredding and kiln loading) are calculated based on the maximum throughput of feedstock, and emission factors obtained from the table in the memorandum "Particulate Matter Potential to Emit Emission Factors from Activities at Sawmills, Excluding Boilers, Located in Pacific Northwest Indian Country", May 8, 2014, from Dan Meyer, US EPA Region 10. These emissions are expected to be insignificant. Emissions from kiln unloading: PM/PMio/PMz.s emissions from product handling are calculated based on published factors in AP -42 Section 11.19.2 — Crushed Stone Processing and Pulverized Mineral Processing. Emission factors in lb/ton are multiplied by the maximum material throughput in tons. These emissions are expected to be insignificant. ► Haul road emissions: Potential emissions from haul roads were calculated using the methods presented in AP -42, 5th Edition, Section 13.2.2 Unpaved Roads (Nov 2006) and are assumed to be similar to those from the existing Biochar Now plant in Berthoud. Air Quality Impact and Emissions Comparison The figures below show maps of the area surrounding the proposed site, highlighting NOx and VOC emissions from various surrounding facilities in tpy.1 The proposed biochar site is marked with an "X," and surrounding emission sources are represented by green circles of varying sizes, corresponding to their actual reported NOx and VOC emission levels. The maps also include a boundary to delineate the 15 km radius assessment area for air pollution sources relative to the proposed site. 1 Source: Colorado Department of Public Health and Environment (CDPHE). Air Quality Data. Available at: https://www.colorado.gov/airquality/ss map wm.aspx Search parameters: Proposed facility coordinates (Lat: 40.02804, Long: -104.78019), search radius of 15 km. February 2025 Biochar Now LLC — Fort Lupton Facility Page 4 of 5 As shown in the figures below, the proposed biochar facility, whose NOx emissions will be limited to below 25 tpy and around 6 tpy of VOC, will produce significantly lower NOx and VOC emissions than existing nearby oil and gas facilities, natural gas processing plants, and power plants. Figure 1: Actual NOx Emissions from Facilities Near the Proposed Site i Figure 2: Actual VOC Emissions from Facilities Near the Proposed Site February 2025 Biochar Now LLC Fort Lupton Facility Page 5 of 5 Odor Considerations In terms of odor control, Biochar Now does not anticipate odor concerns at the proposed facility. The existing Berthoud plant has not reported any obnoxious odor (or really any odor). While long-term storage sites might develop a subtle mildewy smell associated with wet wood, the proposed facility will operate with continuous processing; thus, long-term storage is not anticipated. Attachments ► Biochar Now — Berthoud, Colorado 2021 Emissions Source Test Report, Appendix D wn cseiV O> r=4`'' Hit SOURCE TEST REPORT 2021 EMISSIONS TESTING BIOCHAR NOW KILNS 56, 65 and 74 BERTHOUD, COLORADO Prepared For: Biochar Now P .O. Box 1832 Loveland, Colorado 80513 For Submittal To: Colorado Department of Public Health and Environment Air Pollution Control Division 4300 Cherry Creek Drive South Denver, CO 80246 P repared By: Montrose Air Quality Services, LLC 990 West 43rd Avenue Denver, Colorado 80211 Document Number: GP043AS-007255-RT-644 Test Dates: April 13th through 15th, 2021 S ubmittal Date: May 13th, 2021 MM U a Cfiter i_OP MONTROSE AIR QUALITY SERVICES Biochar Now Berthoud, Colorado 2021 Emissions Source Test Report REVIEW AND CERTIFICATION All work, calculations, and other activities and tasks performed and presented in this document were carried out by me or under my direction and supervision. I hereby certify that, to the best of my knowledge, Montrose operated in conformance with the requirements of the Montrose Quality Management System and ASTM D7036-04 during this test project. S ignature: Name: Jeff Goldfine Date: Title: May 13, 2021 Client Project Manager I have reviewed, technically and editorially, details, calculations, results, conclusions, and other appropriate written materials contained herein. I hereby certify that, to the best of my knowledge, the presented material is authentic, accurate, and conforms to the requirements of the Montrose Quality Management System and ASTM D7036-04. S ignature: Name: Timothy Wojtach Date: Title' May 13, 2021 Account Manager FACILITY CERTIFICATION I have reviewed this document and agree that the information contained herein is true, accurate, and complete, to the best of my knowledge. S ignature: Name: Date: Title' G P043AS-007255-RT-644 2 of 381 V\ I MONTROSE AIR QUAl ITY SERVI([S Biochar Now Berthoud, Colorado 2021 Emissions Source Test Report TABLE 1-2 SUMMARY OF AVERAGE EMISSIONS RESULTS - KILN 56 (KILN 2) APRIL 13th, 2021 Parameter/Units Average Results Filterable Particulate Matter (PM) lb/hr lb/ton Particulate Matter (PM1o) lb/hr lb/ton Particulate Matter (PM2.5) lb/hr lb/ton Total Particulate Matter (PM/PMIo/PM2.5) lb/hr lb/ton Opacity3 Nitrogen Oxides (NOX) lb/hr lb/ton Carbon Monoxide (CO) lb/hr lb/ton Total Hydrocarbons, as Propane (VOC) lb/hr lb/ton Methanol (MeOH) lb/hr lb/ton 3 Opacity results are calculated as the highest six -minute average observed. 0.00677 0.0562 0.00816 0.0677 0.00687 0.0570 0.0104 0.0862 0.0 0.425 3.53 0.179 1.49 <0.00497 <0.0412 <8.99 x 10-4 <7.47 x 10-3 G P043AS-007255-RT-644 8 of 381 fisAL MONTROSE AIR QUALITY SERVICES Biochar Now Berthoud, Colorado 2021 Emissions Source Test Report TABLE 1-3 SUMMARY OF AVERAGE EMISSIONS RESULTS - KILN 65 (KILN 1) APRIL 14th, 2021 Parameter/Units Average Results Filterable Particulate Matter (PM) lb/hr lb/ton Particulate Matter (PM1o) lb/hr lb/ton Particulate Matter (PM2.5) lb/hr lb/ton Total Particulate Matter (PM/PMIo/PM2.5) lb/hr lb/ton Opacity'. Nitrogen Oxides (NOX) lb/hr lb/ton Carbon Monoxide (CO) lb/hr lb/ton Total Hydrocarbons, as Propane (VOC) lb/hr lb/ton Methanol (MeOH) lb/hr lb/ton 4 Opacity results are calculated as the highest six -minute average observed. 0.0109 0.102 0.0121 0.113 0.0100 0.0941 0.0157 0.147 0.0 0.417 3.91 0.0598 0.561 <0.00426 <0.0400 <4.36 x 10-4 <4.09 x 10-3 G P043AS-007255-RT-644 9 of 381 fisAL MONTROSE AIR QUALITY SERVICES Biochar Now Berthoud, Colorado 2021 Emissions Source Test Report TABLE 1-4 SUMMARY OF AVERAGE EMISSIONS RESULTS - KILN 74 (KILN 3) APRIL 15th, 2021 Parameter/Units Average Results Total Particulate Matter (PM) lb/hr lb/ton Particulate Matter (PM1o) lb/hr lb/ton Particulate Matter (PM2.5) lb/hr lb/ton Total Particulate Matter (PM/PMIo/PM2.5) lb/hr lb/ton Opacity5 Nitrogen Oxides (NOX) lb/hr lb/ton Carbon Monoxide (CO) lb/hr lb/ton Total Hydrocarbons, as Propane (VOC) lb/hr lb/ton Methanol (MeOH) lb/hr lb/ton 5 Opacity results are calculated as the highest six -minute average observed. 0.00691 0.0604 0.0108 0.0942 0.00948 0.0828 0.0131 0.114 0.0 0.363 3.17 0.219 1.91 <0.00617 <0.0538 <0.00124 <0.0106 G P043AS-007255-RT-644 10 of 381 fisAL MONTROSE AIR QUALITY SERVICES PROJ-007255 Biochar Now Kiln #56 4/14/2021 EPA Method 2 Data Run # 1 Start Time 8:28 Stop Time 10:40 2 11:47 13:58 1 2 3 15:00 17:16 3 Average DS Pbar Pg Cp VA Pavg TS A Pg Md MS PS Ts(abs)VS Q Q Inputs Stack Diameter (inches) Barometric Pressure ("Hg) Stack Static Pressure ("H2O) Pitot Tube Coefficient (unitless) Avg. Velocity Head of Stack Gas V("H2O) Stack Gas Temperature (°F) Calculations Stack Area (ft2) Stack Static Pressure ("Hg) Stack Gas Molecular Weight, dry basis (lb/lb-mole) Stack Gas Molecular Weight, wet basis (lb/lb-mole) Absolute Stack Pressure ("Hg) Absolute Stack Gas Temperature (°R ) Stack Gas Velocity (ft/sec) Stack Gas Dry Volumetric Flow Rate (dscf/hr) Stack Gas Dry Volumetric Flow Rate (dscf/min) EPA Method 4 Data 24.0 25.12 -0.01 0.84 0.0881 1189 3.14 0.00 29.96 28.34 25.12 1649 9.63 25,307 422 1 24.0 24.0 25.12 25.12 -0.01 -0.01 0.84 0.84 0.1000 0.1001 1276 891 1118 3.14 3.14 0.00 0.00 29.87 29.90 28.31 28.92 25.12 25.12 1736 1351 1578 11.2 9.80 10.22 28,134 33,373 28,938 469 556 482 2 3 Average Vic Vm Y AH Tm Pm Tm Vwc(std) Vm(std) Bws Inputs Volume of Water Condensed (mL) Volume of Stack Gas Collected (dcf) Meter Calibration Factor (unitless) Pressure Differential Across Orifice ("H2O) Temperature at Gas Meter (°F) Calculations Absolute Pressure at Gas Meter ("Hg) Absolute Temperature at Gas Meter i°R) Volume of Water Condensed (scf) Sample Gas Volume (dscf) Stack Gas Moisture Content (%/100) 166.0 55.770 0.9912 0.64 33.0 25.17 493 7.81 49.78 0.136 EPA Method 3A, 7E, 10 and 25A Data 1 174.3 62.608 0.9912 0.76 50.0 25.18 510 8.20 54.04 0.132 121.1 74.913 0.9912 1.09 62.1 25.20 522.1 5.70 63.22 0.0827 2 3 153.8 64.430 0.9912 0.83 48.4 25.18 508 7.24 55.68 0.117 Average O2 (%vd) CO2 (%vd) NOx (ppmvd) CO (ppmvd) TVOC (ppmvw as C3H8) TVOC (ppmvd as C3H8) 9.54 9.87 96.4 220 2.10 2.43 Mass Emission Calculations (Using EPA Methods 1-4) 1 11.2 8.91 144 50.9 <1.0 <1.2 8.99 9.64 126 12.1 <1.0 <1.1 2 3 9.91 9.47 122 94.3 1.37 1.56 Average NO), (lb/hr) NO), (lb/ton raw feed) CO (lb/hr) CO (lb/ton raw feed) TVOC (lb/hr as C3H8) TVOC (lb/ton raw feed as C3H8) *Kiln processed 2,120 lb of raw feed in 8.80 hours 0.291 2.42 0.405 3.36 0.00703 0.0584 0.482 4.01 0.104 0.864 <0.00371 <0.0308 0.500 4.15 0.0293 0.243 <0.00416 <0.0346 0.425 3.53 0.179 1.49 0.00497 0.0412 G P043AS-007255-RT-644 88 of 381 Kiln # 56 Test Performed For: Source(s) Tested: Test Condition: Test(s) Performed: Run Number Biochar Now, LLC Testing Performed By: Berthoud Plant / Colorado Montrose Air Quality Services Kiln # 56 Pilot Batch Process of Treated Wood 5/202 Run 1 Run 2 Project Manager: Jeff Goldfine Run 3 Average Date of Run 4/14/21 4/14/21 4/14/21 Emission Test Run Time Began - Ended Oxygen Concentration Carbon Dioxide Concentration Isokinetic Sampling Rate Stack Temperature Stack Temperature Moisture Content Stack Gas Velocity Stack Gas Flow @ Actual Conditions Stack Gas Flow @ Standard Conditions Stack Gas Flow @ Dry Standard Conditions Batch Time Raw feed processed %(dry) %(dry) % °F °C % volume f/s acfm scfm dscfm hr lb 0828-1040 1147-1358 9.54 11.2 9.9 8.91 102.6 100.2 1189 1276 643 691 13.6 13.2 9.63 11.2 1,816 2,115 488 540 422 469 1500-1716 8.99 9.64 98.8 891 477 8.27 9.80 1,849 607 556 9.91 9.47 1118 604 11.7 10.22 1,927 545 482 8.80 2,120 Visible Emissions, Highest Six Minute Average 0.0 0.0 0.0 0.0 Particulate Concentration, Filterable Particulate Emissions, Filterable Particulate Emissions, Filterable gr/dscf lb/hr lb/ton 0.00245 0.00128 0.00132 0.00168 0.00885 0.00516 0.00628 0.00677 0.0735 0.0429 0.0522 0.0562 Particulate Concentration, Condensable Particulate Emissions, Condensable Particulate Emissions, Condensable gr/dscf lb/hr lb/ton 0.000775 0.00134 0.000561 0.000892 0.00280 0.00539 0.00268 0.00362 0.0233 0.0448 0.0222 0.0301 PKa Emissions, Total PM1a Emissions, Total lb/hr 0.00873 0.00885 0.00689 0.00816 lb/ton 0.0725 0.0735 0.0572 0.0677 PM2.5 Emissions, Total PM2.5 Emissions, Total lb/hr lb/ton 0.00705 0.00787 0.0585 0.0653 0.00569 0.00687 0.0473 0.0570 Particulate Concentration, Total Particulate Emissions, Total Particulate Emissions, Total gr/dscf lb/hr lb/ton 0.00322 0.00263 0.00188 0.00258 0.0117 0.0106 0.00896 0.0104 0.0967 0.0876 0.0744 0.0862 G P043AS-007255-RT-644 89 of 381 PROJ-007255 Biochar Now Kiln #65 4/13/2021 EPA Method 2 Data Run # 1 Start Time 8:11 Stop Time 10:34 2 11:57 14:09 1 2 3 15:25 17:45 3 Average DS Pbar Pg Cp VA Pavg TS A Pg Md MS PS Ts(abs)VS Q Q Inputs Stack Diameter (inches) Barometric Pressure ("Hg) Stack Static Pressure ("H2O) Pitot Tube Coefficient (unitless) Avg. Velocity Head of Stack Gas V("H2O) Stack Gas Temperature (°F) Calculations Stack Area (ft2) Stack Static Pressure ("Hg) Stack Gas Molecular Weight, dry basis (lb/lb-mole) Stack Gas Molecular Weight, wet basis (lb/lb-mole) Absolute Stack Pressure ("Hg) Absolute Stack Gas Temperature (°R ) Stack Gas Velocity (ft/sec) Stack Gas Dry Volumetric Flow Rate (dscf/hr) Stack Gas Dry Volumetric Flow Rate (dscf/min) EPA Method 4 Data 24.0 24.0 24.0 25.16 25.16 25.16 -0.01 -0.01 -0.01 0.84 0.84 0.84 0.0982 0.1301 0.1045 1068 1226 1162 1152 3.14 3.14 3.14 0.00 0.00 0.00 29.81 29.83 29.68 28.35 28.35 28.46 25.16 25.16 25.16 1528 1686 1622 1612 10.3 14.4 11.3 12.0 29,733 37,436 31,309 32,826 496 624 522 547 1 2 3 Average Vic Vm Y off Tm Pm Tm Vwc(std) Vm(std) Bws Inputs Volume of Water Condensed (mL) Volume of Stack Gas Collected (dcf) Meter Calibration Factor (unitless) Pressure Differential Across Orifice ("H2O) Temperature at Gas Meter (°F) Calculations Absolute Pressure at Gas Meter ("Hg) Absolute Temperature at Gas Meter i°R) Volume of Water Condensed (scf) Sample Gas Volume (dscf) Stack Gas Moisture Content (%/100) 165.5 62.464 0.9912 0.79 38.1 25.22 498.1 7.79 55.29 0.123 EPA Method 3A, 7E, 10 and 25A Data 1 223.6 85.899 0.9912 1.02 54.0 25.24 514 10.52 73.74 0.125 151.1 70.482 0.9912 1.06 51.5 25.24 511.5 7.11 60.81 0.105 2 3 25.23 508 8.47 63.28 0.118 Average O2 (%vd) CO2 (%vd) NOx (ppmvd) CO (ppmvd) TVOC (ppmvw as C3H8) TVOC (ppmvd as C3H8) 10.1 8.77 72.7 52.8 <1.0 <1.1 Mass Emission Calculations (Using EPA Methods 1-4) 1 11.0 8.68 116 11.9 <1.0 <1.1 11.4 7.68 127 14.4 <1.0 <1.1 2 3 10.8 8.38 105 26.4 <1.0 <1.1 Average NO), (lb/hr) NO), (lb/ton raw feed) CO (lb/hr) CO (lb/ton raw feed) TVOC (lb/hr as C3H8) TVOC (lb/ton raw feed as C3H8) *Kiln processed 2,040 lb of raw feed in 9.57 hours 0.258 2.42 0.114 1.07 <0.00388 <0.0364 0.519 4.87 0.0324 0.304 <0.00490 <0.0459 0.474 4.44 0.0327 0.307 <0.00400 <0.0376 0.417 3.91 0.0598 0.561 <0.00426 <0.0400 G P043AS-007255-RT-644 92 of 381 Kiln # 65 Test Performed For: Source(s) Tested: Test Condition: Test(s) Performed: Run Number Biochar Now, LLC Testing Performed By: Berthoud Plant / Colorado Montrose Air Quality Services Kiln # 65 Pilot Batch Process of Treated Wood 5/202 Run 1 Run 2 Project Manager: Jeff Goldfine Run 3 Average Date of Run 4/13/21 4/13/21 4/13/21 Emission Test Run Time Began - Ended Oxygen Concentration Carbon Dioxide Concentration Isokinetic Sampling Rate Stack Temperature Stack Temperature Moisture Content Stack Gas Velocity Stack Gas Flow @ Actual Conditions Stack Gas Flow @ Standard Conditions Stack Gas Flow @ Dry Standard Conditions Batch Time Raw feed processed %(dry) %(dry) % °F °C % volume f/s acfm scfm dscfm hr lb 0811-1034 1157-1409 1525-1745 10.1 11.0 11.4 10.8 8.77 8.68 7.68 8.38 97.0 103.0 101.3 100.4 1068 1226 1162 1152 576 663 628 622 12.3 12.5 10.5 11.8 10.3 14.4 11.3 12.0 1,946 2,707 2,130 2,261 566 713 583 621 496 624 522 547 - 9.57 2,040 Visible Emissions, Highest Six Minute Average OA 0.0 0.0 0.0 0.0 Particulate Concentration, Filterable Particulate Emissions, Filterable Particulate Emissions, Filterable gr/dscf lb/hr lb/ton 0.00413 0.00152 0.00155 0.00240 0.0175 0.00815 0.00692 0.0109 0.165 0.0765 0.0650 0.102 Particulate Concentration, Condensable Particulate Emissions, Condensable Particulate Emissions, Condensable gr/dscf lb/hr lb/ton 0.000753 0.00127 0.000989 0.00101 0.00320 0.00681 0.00443 0.00481 0.0300 0.0639 0.0415 0.0451 PKo Emissions, Total PM1a Emissions, Total lb/hr 0.0149 0.0123 0.00906 0.0121 lb/ton 0.140 0.115 0.0850 0.113 PM2 5 Emissions, Total PM25 Emissions, Total lb/hr lb/ton 0.0116 0.0107 0.109 0.101 0.00775 0.0100 0.0727 0.0941 Particulate Concentration, Total Particulate Emissions, Total Particulate Emissions, Total gr/dscf lb/hr lb/ton 0.00488 0.00280 0.00254 0.00341 0.0207 0.0150 0.0113 0.0157 0.195 0.140 0.106 0.147 G P043AS-007255-RT-644 93 of 381 PROJ-007255 Biochar Now Kiln #74 4/15/2021 EPA Method 2 Data Run # 1 Start Time 10:20 Stop Time 12:44 2 13:50 15:58 1 2 3 16:58 19:04 3 Average DS Pbar Pg Cp VA Pavg TS A Pg Md MS PS Ts(abs)VS Q Q Inputs Stack Diameter (inches) Barometric Pressure ("Hg) Stack Static Pressure ("H2O) Pitot Tube Coefficient (unitless) Avg. Velocity Head of Stack Gas V("H2O) Stack Gas Temperature (°F) Calculations Stack Area (ft2) Stack Static Pressure ("Hg) Stack Gas Molecular Weight, dry basis (lb/lb-mole) Stack Gas Molecular Weight, wet basis (lb/lb-mole) Absolute Stack Pressure ("Hg) Absolute Stack Gas Temperature (°R ) Stack Gas Velocity (ft/sec) Stack Gas Dry Volumetric Flow Rate (dscf/hr) Stack Gas Dry Volumetric Flow Rate (dscf/min) EPA Method 4 Data 24.0 24.0 24.0 24.92 24.92 24.92 -0.01 -0.01 -0.01 0.84 0.84 0.84 0.0986 0.1063 0.0945 1233 1273 1019 1175 3.14 3.14 3.14 0.00 0.00 0.00 29.76 29.78 29.66 28.00 28.20 28.49 24.92 24.92 24.92 1693 1733 1479 1635 11.0 12.0 9.79 10.94 27,576 29,787 29,650 29,004 460 496 494 483 1 2 3 Average Vic Vm Y off Tm Pm Tm Vwc(std) Vm(std) Bws Inputs Volume of Water Condensed (mL) Volume of Stack Gas Collected (dcf) Meter Calibration Factor (unitless) Pressure Differential Across Orifice ("H2O) Temperature at Gas Meter (°F) Calculations Absolute Pressure at Gas Meter ("Hg) Absolute Temperature at Gas Meter i°R) Volume of Water Condensed (scf) Sample Gas Volume (dscf) Stack Gas Moisture Content (%/100) 200.3 62.438 0.9912 0.79 46.2 24.98 506 9.43 53.87 0.149 EPA Method 3A, 7E, 10 and 25A Data 1 173.6 61.457 0.9912 0.74 48.4 24.97 508 8.17 52.79 0.134 142.0 68.993 1.0071 0.91 48.5 24.99 509 6.68 60.23 0.100 2 3 0.128 Average O2 (%vd) CO2 (%vd) NOx (ppmvd) CO (ppmvd) TVOC (ppmvw as C3H8) TVOC (ppmvd as C3H8) 11.5 8.09 104 192 2.64 3.10 Mass Emission Calculations (Using EPA Methods 1-4) 1 11.7 8.22 125 109 <1.0 <1.2 11.0 7.62 85.2 16.8 1.27 1.41 2 3 11.4 7.98 105 106 <1.64 <1.89 Average NO), (lb/hr) NO), (lb/ton raw feed)) CO (lb/ton raw feed) CO (lb/hr) TVOC (lb/hr as C3H8) TVOC (lb/ton raw feed as C3H8) *Kiln processed 2,000 lb of raw feed in 8.73 hours 0.342 2.98 0.385 3.36 0.00979 0.0855 0.444 3.88 0.235 2.05 <0.00394 <0.0344 0.302 2.63 0.0361 0.315 0.00477 0.0417 0.363 3.17 0.219 1.91 <0.00617 <0.0538 G P043AS-007255-RT-644 96 of 381 Kiln #74 Test Performed For: Source(s) Tested: Test Condition: Test(s) Performed: Run Number Biochar Now, LLC Berthoud Plant / Colorado Kiln #74 Pilot Batch Process of Treated Wood 5/202 Run 1 Run 2 Testing Performed By: Montrose Air Quality Services Project Manager: Jeff Goldfine Run 3 Average Date of Run Emission Test Run Time Began - Ended Oxygen Concentration Carbon Dioxide Concentration Isokinetic Sampling Rate Stack Temperature Stack Temperature Moisture Content Stack Gas Velocity Stack Gas Flow @ Actual Conditions Stack Gas Flow @ Standard Conditions Stack Gas Flow @ Dry Standard Conditions Batch Time Raw feed processed %(dry) %(dry) °F °C % volume f/s acfm scfm dscfm hr lb 4/15/21 1020-1244 11.5 8.09 102.0 1233 667 14.9 11.0 2,078 540 460 4/15/21 1350-1558 11.7 8.22 92.5 1273 690 13.4 12.0 2,260 573 496 4/15/21 1658-1904 11.0 7.62 106.0 1019 548 10.0 9.79 1,846 549 494 11.4 7.98 1175 635 12.8 10.9 2,061 554 484 8.73 2,000 Visible Emissions, Highest Six Minute Average °I0 0.0 0.0 0.0 0.0 Particulate Concentration, Filterable Particulate Emissions, Filterable Particulate Emissions, Filterable gr/dscf lb/hr lb/ton 0.00263 0.0104 0.0906 0.00152 0.00646 0.0565 0.000922 0.00390 0.0341 0.00169 0.00691 0.0604 Particulate Concentration, Condensable Particulate Emissions, Condensable Particulate Emissions, Condensable gr/dscf lb/hr lb/ton 0.00112 0.00440 0.0384 0.00237 0.01007 0.0879 0.000948 0.00401 0.0350 0.00148 0.00616 0.0538 PM1a Emissions, Total PM1a Emissions, Total lb/hr lb/ton 0.0113 0.0991 0.0144 0.126 0.00663 0.0579 0.0108 0.0942 PM2.5 Emissions, Total PM25 Emissions, Total lb/hr lb/ton 0.00938 0.0819 0.0132 0.115 0.00589 0.0514 0.00948 0.0828 Particulate Concentration, Total Particulate Emissions, Total Particulate Emissions, Total gr/dscf lb/hr lb/ton 0.00375 0.0148 0.129 0.00389 0.0165 0.144 0.00187 0.00792 0.0691 0.00317 0.0131 0.114 G P043AS-007255-RT-644 97 of 381 2/3/25, 4:20 PM Keller Williams Realty, Inc. Mail - EA Defense opposition to Brighton facility Robert Demaree <bob.demaree@kw.com> EA Defense opposition to Brighton facility James Gaspard Sat, Feb 1, 2025 at 4:44 PM To: Robert Demaree <bob.demaree kw.com> Cc: Dylan Van Demark , Michael Dente <michael.dente@kw.com>, Michael Hall <pagoda.mapping@gmai .com> I am not wasting much time responding to this letter. The issue is the authors know nothing about what they are talking about. They simply were paid to google articles that cut in their favor without understanding that "all biochars are not created equal". Attached is a paper that was published in 2009 that stated that most basic premise. The attached article should be our basic response. Every article they cite is from biochar technologies around the world that have nothing in common with our patented technology. None of the biochars created in the technologies they cite have similar properties that we have in our biochar. All those technologies in the papers they cited were fast pyrolysis or gasifiers. They have nothing to do with the carbon we produce. The discussions about lack of markets or lack of efficacy do not apply to the carbon we produce. We have a market for our carbon. We meet all CDPHE guidelines for our emission permits, so their comments about emissions are irrelevant to us. We meet all noise requirements, etc. Basically, when they start their list with the heading "violations of municipal law" they should be disciplined as attorneys for misrepresentations. The best they could have said was "possible violations of municipal law", but then none of the listed issues applies to our technology and we have operated for 14 years in the State of Colorado legally permitted by all relevant agencies. James Gaspard CEO Biochar Now Colorado Site Address: 19500 County Road 7, Berthoud, CO 80513 Mailing Address: P.O. Box 1832, Loveland, CO 80539-1832 www.biocharnow.com . .II All biochars are not created equal - Hugh and Frank.pdf 1352K https://mail.google.com/mail/u/0/?ik=a76626f293&view=pt&search=all&permmsgid=msg-f:1822893040568157588&simpl=msg-f: 1822893040568157588 1/1 CDPHE Disproportionately Impacted Communities Map https://www.arcgis.com/apps/mapviewer/index.html?layers 7d0cf560blle41 foa4d323c4e6c9oe Ob We need to stay out of these areas as part of the site selection process for CDPHE air permits Nonattainment area More restrictive air quality control area by CDPHE EXHIBIT i17 Layers x Get started You can explore maps, add layers, and more without signing in. To save your work, sign in before creating your map. Learn more about Map Viewer CDPHE Disproportionately Impacted Communities (ARCHIVED Version September 20 1) X R 06 N 107th St rfIle _J r Broornfieild BroonifieLd ni W 120b- W 117th Ave i 66 Firestone Frederick: •—e I � r I, 5251 1 F 128th Ave E 160th Ave r t. / Barr Lake State Park Highway 52 irty tti a Ft Hlud tsCon CDPHE Disproportionately Impacted .. . a ft C6 c Properties x Cbetween layers in the map. Information Symbology tise the selector above to switch CDPHE Disproportionately Impacted Communities (ARCHIVED Version September 2021) f Appearance Blending ir Normal Transparency 0% 0 A a Layers x Get started You can explore maps, add layers, and more without signing in_ To save your work, sign in before creating your map. Learn more about Map Viewer CDPHE Disproportionately Impacted Communities ((ARCHIVED Version September 2021) O Add M i M b Highway 52 k co creek Wattenberg. 27 U, ist County Road 4 County Road 2 1/2 County Road 31 a -Pit-1Jt County Road 12 County Road 31 EE PtOU , 1unoj 5184 Jr A Smith Mound Mathews Ave SE Re°d Aiuno , County Road a County Road 6 GAI n3 H- County Road 35 - —E 168th *4 a �reb�+k n..r r — — E -168th -Ave — — — —E 1.68th-Are 521 LE peed Munoz County Road 3) Courn q 1 CDPHE Disproportionately impacted ... Properties X County•f Esri, NASA, NGA, USES, FE.MA. City of Fort Lupton, CO, Esri, T omTor , Garmin., SateGraph, G,eo T echnologies, Inc METI/NASA, US__ __ Powered by Esri lase the selector above to switch between layers in the map. Information Symbology CDPHE Disproportionately Impacted Communities (ARCHIVED Version September 2021) f Appearance Blending ir Normal Transparency 0% 0 25% 50% 75% V teje _ it a l itt s i 'a flan a win Lakes Buena i 4:Denver Metro/Nc:rtk'i Front Range 8 -Hour Ozone NoriattainrnentArea Red reather"' -:Lak.es-• _..xa�' �s Nutional ., Grassland : Wood Iar..dt Palle wt, ,C, Colorado ,61 rN_nq Pawnee art Mcrqanc Brush a Lin 0 Huyo St€. III nJ 0 - Akron R _ F Ia�jI.erSeib' EXHIBIT NEIGHBORHOOD MEETING NOTICE In tit .0 18 Dear neighbor, Biochar Now is in process of permitting a conversion facility on the subject property, shown below, located south of and adjacent to CR 6 and approximately 0.25 miles west of CR 31. As part of this process, we want to reach out to the nearby property owners to explain the proposed operation and answer any questions you may have. It is our desire to respectfully integrate into your community and to mitigate impacts of our operation. Please consider attending an informal neighborhood meeting, to be held at the: Fort Lupton Public and School Library Fort Lupton Community Room 2 370 S Rollie Ave, Fort Lupton, CO 80621 10:00 Aid, SATURDAY, OCTOBER 12, 2024 The goals of this meeting are to: • Explain biochar and the proposed on -site operations. • Provide you with details about the project, including the permitting processes. • Address concerns and answer questions that you may have about the project. We hope to see you there! NEIGHBORHOOD MEETING DETAILS On September 24, 2024, the applicant team mailed notice to the surrounding property owners identified on the Weld County Property Portal 500 -foot buffer report, listed below. BROWN RACHEL E LIVING TRUST 4510 COUNTY ROAD 6 FORT LUPTON. CO 806218216 HALE TONY LYNN 4760 Cc: U NTY ROAD I F=)RT LI_!PT 'N.'.1O 80621821b NGL WATER SOLUTIONS DJ LLC 865 ALBION ST STE 400 DENVER, CO 802204809 FAUDOA FERNANDO •ii 45/12 C O l_1 N TY ROAD 6 FORT LUPTON: C€=> >801;.2'182.' 6 YARBROUGH JERI E 451, t r=:, U N TY ROAD 6 FORT LUPTON_, CO 806218216 SACK GEORGE A. 4323 cod._l NT's' ROAD 6 FORT LUPTON. CC) 8062/82/5 This meeting was intended to provide the community with accurate information and to assist in addressing any concerns in a positive manner. Included in this document is a copy of the mailed letter and the attendance sheet. MEETING MINUTES The following topics were discussed: ■ What is Biochar, what will occur on this property, our desire to integrate into the area ■ Co -permitting efforts with NGL & OGED for injection wells; USR & WOGLA timeline • Mitigation efforts and options to reduce perceived land use conflicts ■ Irrigation practices and business impacts • Air emissions & pollution questions ■ Decrease in property values and quality of life ■ Site selection & compatibility complaints • General environmental health and contamination concerns • Stockpile heights and on -site equipment types ■ Kiln operated process and temperature ■ History of traffic incidents on CR 6 and possibility of increase NEIGHBORHOOD MEETING ATTENDANCE SHEET 10:00 AM, SATURDAY, OCTOBER 12, 2024 Name EmaRR SheJdie to\ettn 01 1\161 bOtioey000vieji(possi I Q)\iefl 5 \atr✓icc7hti1e9ryia.-il .C° SAG fee ,,u-dsM SUeQSreLAOLCW\ if Litt /Qc 'gall Y114le IYd le COril Alla tat K(c 't'v&c�7 Y/€ ( al 2MY-CA sk- c -a0 Qra-avvicaLs62-1-- foN/<.. 9 auk I. C W CV\CknC4 cz Yit eacut± V p%Ka( ouGHs'•cr&-SeP lei fr. �e "ilk 0 I ell i 1r 2arbeirh 0 36DallYYLou /57n%y�v611Z di � �v+-rso J to en Nnegi beer � a3 Colleen K. O'Neil, Ed.D. October 6, 2025 EXHIBIT 19 Dear Weld County Commissioners and Weld County Planners Aungst and Snyder: On behalf of myself and my family, I am writing, again, to express my strong opposition to the proposed NGL Biochar Project (Case No. USR24-0019) located near 14512 County Road 6, Fort Lupton, CO 80621. We are asking that you deny this request. My family, consisting of myself, my mom and my brother live in three separate homes approximately 2,500 feet from this proposed site. This operation would fundamentally change the character of our agricultural community and pose direct risks to human health, animal safety, and environmental quality. It has been brought to our attention that the same company operates another biochar facility in Berthoud, Colorado, which has an extensive record of air -quality violations documented by the Colorado Department of Public Health and Environment (CDPHE). The highlevel violations appear below and will be further outlined by Alexa McKay, Esq. at the hearing. • 2020 Compliance Advisory (Case No. 2020-126): CDPHE found that Biochar Now exceeded permitted emission limits for nitrogen oxides (NOx) and carbon monoxide (CO). Testing showed kiln emissions reaching 0.180 lb/hr NOx and 1.25 lb/hr CO, compared to permitted limits of 0.14 lb/hr NOx and 0.12 lb/hr CO. These rates translate to annual emissions of up to 120 tons per year of CO, which is more than ten times the legal limit • 2023 Early Settlement Agreement (Case No. 2023-051): Biochar Now again violated its permit, exceeding allowed emissions of NOx, VOCs, and CO, and operating well beyond its permitted hours of engine use. The company paid $31,500 in penalties to the State of Colorado for these violations. • 2023 Title V Permit Application (CDPHE #23OPWE558): In its own filing, Biochar Now acknowledged that its Berthoud plant qualifies as a major stationary source of air pollution under the federal Clean Air Act due to NOx emissions exceeding 25 tons per year, placing it in the highest category for regulation within the Denver Metro —North Front Range ozone non -attainment area. These violations and the company's ongoing status as a major source demonstrate a pattern of emissions control problems that directly contradict assurances that such operations are safe. Weld County Case No. USR24-0019 Page l 1 Colleen K. O'Neil, Ed.D. Health and safety implications Biochar kilns release carbon monoxide, fine particulates (PM 2.5), volatile organic compounds (VOCs), and nitrogen oxides (NOx). These are all pollutants known to worsen respiratory conditions, harm cardiovascular health, and contribute to ground -level ozone formation. These pollutants pose documented health risks to people and animals living nearby. Fine particulate exposure in livestock has been linked to respiratory irritation, reduced performance, and stress responses. For people, long-term exposure increases risks of asthma, lung disease, and heart conditions. My brother and my mom are one of those individuals that will drastically be affected by these emissions. My mom, at 84 years old, just battled lung cancer. And, while she is winning that battle today, emissions from this facility could certainly cause further damage. My brother is wheelchair bound and diagnosed with lung and heart sarcoidosis. These emissions will almost certainly cause secondary issues and could further exacerbate an already deadly condition. Given that the proposed site sits within a dry, wind -prone agricultural zone, emissions and airborne dust could easily drift across neighboring properties, directly affecting families, pets, and livestock. The 24 -hour operation and transport traffic also raise serious fire -safety and air -quality concerns. Request While biochar has beneficial uses, its production requires industrial -scale combustion. Siting a continuous -burn kiln facility in a rural residential area less than half a mile from homes, barns, water sources, and animals is inappropriate. The company's compliance history shows repeated failure to operate within safe emission limits despite multiple opportunities to correct violations. For these reasons, we respectfully request denial of Special Use Permit Case No. USR24-0019. This operation presents unacceptable environmental, health, and safety risks to nearby residents and animals, and its approval would contradict Weld County's responsibility to protect public welfare and uphold air -quality standards. Thank you for your time, diligence, and continued commitment to representing the best interests of Weld County residents. Weld County Case No. USR24-0019 Page 12 Colleen K. O'Neil, Ed.D. Sincerely, Colleen K. O'Neil, Ed.D. e: colleenkoneil@gmail.com p: 970-302-9517 On behalf of self, Colleen O'Neil, 1865 County Road 31, Fort Lupton, CO, and Robert O'Neil, 1869 County Road 31, Fort Lupton, CO, and Sharon O'Neil, 14952 County Road 6, Fort Lupton, CO BioChar Now Kiln Image Addendum Weld County Case No. USR24-0019 Page 13 COLORADO Department of Public Health & Environment AIR POLLUTION CONTROL DIVISION b .0 a EXHIBIT 20 COMPLIANCE ADVISORY CASE NO. 2017-123 AIRS NO. 123-9E2C INSPECTION DATES: May 24, 2017 July 11, 2017 TEST DATES: September 6-8, 2017 U.S. CERTIFIED MAIL NO. 7016 2710 0000 3004 8588 MAILING DATE: November 22, 2017 SOURCE CONTACT: Jim Geist IN THE MATTER OF BIOCHAR NOW, LLC This Compliance Advisory provides format notice, pursuant to § 25-7-115(2), C.R.S., of alleged violations or noncompliance discovered during the Air Pollution Control Division's ("Division") inspection and/or review of records related to Biochar Now, LLC's Facility identified below. The Division is commencing this action because it has cause to believe that the compliance issues identified below may constitute violations of the Colorado Air Pollution Prevention and Control Act ("the Act") and its implementing regulations. Please be aware that you are responsible for complying with applicable State air pollution requirements and that there are substantial penalties for failing to do so. Pursuant to the enforcement authority provided the Division by § 25-7-115, C.R.S., any person who violates the Act, its implementing regulations or any permit issued thereunder may be issued an order for compliance that can include permit revocation and assessment of penalties of up to $15,000 per day of such violation in accordance with § 25-7-122, C.R.S. The issuance of this Compliance Advisory does not in any way limit or preclude the Division from pursuing additional enforcement options concerning this inspection/review. Also, this Compliance Advisory does not constitute 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe John W. Hickenlooper, Governor I Larry Wolk, MD, MSPH, Executive Director and Chief Medical Officer COLORADO Air Pollution Control Division Deriartrrent of Putt Health 6 Environment a bar to enforcement action for violations not specifically addressed in this Compliance Advisory. Failure to respond to this Compliance Advisory by the date indicated at the end of this Compliance Advisory may be considered by the Division in the subsequent enforcement action and the assessment of penalties. Furthermore, the Division's enforcement process contemplates a full and final resolution of the compliance issues herein addressed, and those that may result from further review, in a timely manner. If at any time throughout the process of reaching such a resolution the Division determines that the Parties cannot agree to the dispositive facts, compliance requirements and/or penalty assessments (if any) associated with this Compliance Advisory, or a resultant enforcement action, the Division may exercise its full enforcement authority allowed under the law. Biochar Now, LLC ("Biochar") owns and operates a biochar production facility at 19500 County Road 7, Berthoud, Weld County, Colorado ("Facility"). The Facility is subject to the terms and conditions of Colorado Construction Permit Number 15WE1395 Issuance #1, Initial Approval issued to Biochar on March 8, 2016 ("Issuance 1"); Colorado Construction Permit Number 15WE1395 Issuance #2, Initial Approval issued to Biochar on July 11, 2016 ("Issuance 2"); Colorado Construction Permit Number 15WE1395 Issuance #3, Initial Approval issued to Biochar on March 13, 2017 ("Issuance 3"); Standards of Performance for New Stationary Sources, Subpart A - General Provisions ("Subpart A"), and Subpart IIII—Standards of Performance for Stationary Compression Ignition Internal Combustion Engines ("Subpart IIII"); Colorado Air Quality Control Statutes; and Colorado Air Quality Control Commission ("AQCC") Regulations. I. ALLEGED VIOLATIONS AND FACTS On May 24, 2017 and July 11, 2017, Mr. Jeffrey Bishop, of the Division, inspected the Facility. On September 6-8, 2017, compliance testing was conducted at the Facility. Mr. Bishop observed the testing on September 6, 2017. Based on Mr. Bishop's inspections, and a review of records related to the Facility including the test report received by the Division on October 13, 2017, the Division has identified the following compliance issues: A. Pursuant to Issuance 1 and Issuance 2, Condition 1 and AQCC Regulation Number 3, Part B, § III.G.1, Biochar shall submit a Notice of Startup to the Division no later than fifteen days after commencement of operation under the permit. Biochar commenced operations under Issuance 1 on March 28, 2016, and submitted an NOS as required on April 4, 2016. Biochar relocated, then re -commenced operations on August 15, 2016 under Issuance 2, for which it submitted an NOS as required on July 28, 2016. Although Biochar 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.8ov/cdphe John W. Hickenlooper, Governor I Larry Wolk, MD, MSPH, Executive Director and Chief Medical Officer 2 COLORADO Air Pollution Control Division L'epartrrent of P..itzlrr Health & Emuoninot submitted timely NOS forms, both submissions incorrectly indicate that the diesel engines listed in the permit (AIRS Points 004 and 005) are in operation at the Facility. Based on statements made by the source and observations made at the inspections, AIRS Points 004 and 005 were not installed and have never operated at the Facility. Instead, Biochar installed and operated unpermitted diesel engines at the Facility. Biochar failed to submit accurate NOS to the Division, violating Issuance 1 and Issuance 2, Condition 1 and AQCC Regulation Number 3, Part B, § III.G.1. B. Pursuant to Issuance 2 and Issuance 3, Condition 2 and AQCC Regulation Number 3, Part B, § III.G.2, Biochar shall self -certify compliance with the permit conditions within one hundred and eighty (180) days after commencement of operations or issuance of the permit, whichever is later. The deadline to complete self -certification for Issuance 2 was January 7, 2017. The deadline to complete self - certification for Issuance 3 was September 9, 2017. Biochar has not completed self -certification at this time. Biochar failed to complete self -certification, violating Issuance 2 and Issuance 3, Condition 2 and AQCC Regulation Number 3, Part B, § III.G.2. C. Pursuant to Issuance 2, Condition 4, 21, and 22 and AQCC Regulation Number 3, Part B, § III.G.2, Biochar shall, within one hundred and eighty (180) days after commencement of operation or issuance of the permit, whichever is later, complete all initial compliance testing and sampling as required in the permit and submit the results to the Division as part of the self -certification process. i. Pursuant to Issuance 2, Condition 21, Biochar shall demonstrate compliance with the opacity requirements of Permit Number 15WE1395 Condition 13 using EPA Method 9 to measure opacity from three kiln/afterburner units (AIRS Point 001) within one hundred and eighty (180) days of the permit issuance. The deadline to complete opacity testing on AIRS Point 001 for Issuance 2 was January 7, 2017. Biochar did not conduct initial opacity testing on AIRS Point 001 until May 24, 2017. Biochar failed to complete the EPA Method 9 opacity observation on AIRS Point 001 within the 180 day time limit, violating Issuance 2, Condition 21. ii. Pursuant to Issuance 2, Condition 22, Biochar shall demonstrate compliance with the annual emission limits listed in Permit Number 15WE1395, Condition 8, within one hundred and eighty (180) days after commencement of operations or permit issuance, whichever is later. To do so, Biochar must 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.8ov/cdphe John W. Hickenlooper, Governor I Larry Wolk, MD, MSPH, Executive Director and Chief Medical Officer 3 COLORADO Air Pollution Control Division L'epartrrent of P..itzlrr Health & Emuoninot conduct testing on a total of 3 kiln/afterburner units (AIRS Point 001) to measure the emission rates, on an hourly basis, over the entire process duration. The deadline to complete the emissions testing on AIRS Point 001 for Issuance 2 was January 7, 2017. Biochar did not conduct initial emissions testing on AIRS Point 001 until May 24, 2017. Biochar failed to complete the initial emissions testing on AIRS Point 001 within the 180 day time limit, violating Issuance 2, Condition 22. D. Pursuant to Issuance 2, Conditions 5 and 19; and AQCC Regulation Number 3, Part B, § III.G.7, Biochar shall, within one hundred and eighty (180) days after commencement of operation or issuance of the permit, whichever is later, submit an operation and maintenance (O&M) plan and record keeping format demonstrating how Biochar will maintain compliance with the requirements of the permit. The deadline to submit the OEtM plan and record keeping format for Issuance 2 was January 7, 2017. Biochar did not submit an O&M plan u ntil August 18, 2017, and did not submit a record keeping format u ntil September 8, 2017. Biochar failed to submit the OEtM plan and record keeping format within 180 days, violating Issuance 2, Conditions 5 and 19, and AQCC Regulation Number 3, Part B, § III.G.7. E. Pursuant to Issuance 1 and Issuance 2, Conditions 6 and 27 and Issuance 3, Conditions 6 and 29, Biochar shall, within thirty (30) days after commencement of operation or issuance of the permit, whichever is later, mark the permit number on the subject equipment for ease of identification. The deadline to mark the subject equipment for Issuance 1 was April 7, 2016. The deadline to mark the subject equipment for Issuance 2 was August 10, 2016. The deadline to mark the subject equipment for Issuance 3 was April 12, 2017. At the inspections on May 24, 2017 and July 11, 2017, Mr. Bishop observed that the kilns (AIRS Point 001) were marked with a permit n umber. No other equipment was marked as required. Biochar failed to mark permit numbers on all subject equipment, violating Issuance 1 and Issuance 2, Conditions 6 and 27 and Issuance 3, Conditions 6 and 29. F. Pursuant to Issuance 2 and Issuance 3, Condition 7, Biochar shall, within one hundred and eighty (180) days after commencement of operation or issuance of the permit, whichever is later, submit the manufacturer, model number, and serial number (equipment information) of the subject equipment. The submission deadline for Issuance 2 was January 7, 2017. The submission deadline for Issuance 3 was September 9, 2017. Biochar did not submit the equipment information until September 22, 2017. Biochar failed to submit the 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.8ov/cdphe John W. Hickenlooper, Governor I Larry Wolk, MD, MSPH, Executive Director and Chief Medical Officer 4 COLORADO Air Pollution Control Division L'epartrrent of P..itzlrr Health & Emuoninot equipment information within 180 days, violating Issuance 2 and Issuance 3, Condition 7. G. Pursuant to Permit Number 15WE1395, Condition 8, annual emissions from the kiln (AIRS Point 001) must not exceed 2.89 tons of PM1 o and 1.59 tons of PM2.5. The results of the September 6-8, 2017 testing conducted on equipment identified as Kiln 5, Kiln 26, and Kiln 35 showed average emissions of 3.26 tons per year of PMio and 3.24 tons per year of PM2.5. Biochar failed to comply with the PM1 o and PM2.5 annual emission limits for AIRS Point 001, violating Permit Number 15WE1395, Condition 8. H. Pursuant to Issuance 3, Condition 12, Biochar shall process only "clean" wood as defined in the permit. The permit states that clean lumber and wood waste do not include pressure treated wood or manufactured wood products that contain adhesives or resins. Biochar stockpiled and used as fuel prohibited materials including processed wood, pressed wood, and construction pallets that failed to meet the definition of "clean." Biochar processed wood that did not meet the definition of "clean" as defined in the permit, violating Issuance 3, Condition 12. Pursuant to Subpart 1111, § 60.4204(b), the diesel engines operating at the Facility must comply with the Tier 4 interim specifications. Based on information provided by Biochar in its July 18, 2017 APEN application for AIRS Point 008, the Isuzu diesel generator engine does not meet the Tier 4 interim specifications. Biochar failed to ensure that its diesel engine complies with the Tier 4 interim specifications, violating Subpart 1111, § 60.4204(b). J. Pursuant to Permit Number 15WE1395, Condition 18 and AQCC Regulation Number 3, Part B, § III.D.2, I. D.2, Biochar is located in an ozone non -attainment area and is subject to Reasonably Available Control Technology (RACT) requirements. The RACT requirements for Biochar are comprised of compliance with Permit Number 15WE1395 Conditions 10, 12, 14, and 15. As discussed in Paragraph H above, Biochar violated the terms of Permit Number 15WE1395Condition 12. Biochar failed to comply with RACT requirements, violating Permit Number 15WE1395, Condition 18 and AQCC Regulation Number 3, Part B,§III.D.2. K. Pursuant to § 25-7-114.1, C.R.S. and AQCC Regulation Number 3, Part A, § II.A, no person shall allow emission of air pollutants from any facility, process, or activity which constitutes a stationary source from which air pollutants are to be emitted unless and until an Air 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.8ov/cdphe John W. Hickenlooper, Governor I Larry Wolk, MD, MSPH, Executive Director and Chief Medical Officer 5 COLORADO Air Pollution Control Division L'epartrrent of P..itzlrr Health & Err:uonrrn=t Pollution Emission Notice (APEN) has been filed with the Division. Biochar installed and operated two diesel engines at the Facility prior to submitting APENs, violating § 25-7-114.1, C.R.S. and AQCC Regulation Number 3, Part A, § II.A. Biochar submitted the APENs for the diesel engines on July 18, 2017. L. Pursuant to § 25-7-114.2, C.R.S. and AQCC Regulation Number 3, Part B, § I I.A.1, no person shall commence construction of any stationary source without first obtaining or having a valid construction permit from the Division. Biochar installed and continues to operate two diesel engines at the Facility without obtaining a valid construction permit, violating § 25-7-114.2, C.R.S. and AQCC Regulation Number 3, Part A, § II.A.1. It is important to resolve the above -referenced issues as soon as possible. Therefore, the Division encourages Biochar to immediately identify those compliance issues that are not in dispute and to rectify those issues before the upcoming Compliance Advisory meeting. In accordance with § 25-7-115(3)(a), C.R.S., the Compliance Advisory meeting will be held within thirty (30) days of the Division's issuance of the Compliance Advisory in this matter. The Division also requests that Biochar provide the Division with a brief written response to the alleged violations ("Source Response"). The Source Response should identify the undisputed compliance issues and, if an alleged violation is disputed, the basis for the dispute. The Division requests that Biochar provide the Source Response, to the attention of Jeffrey Bishop, no later than ten business days before the Compliance Advisory meeting. At the u pcoming meeting, the Division will confirm the actions taken to rectify the u ndisputed compliance issues and proceed with unresolved matters as outlined below. If you have any questions regarding this Compliance Advisory, the Division's enforcement processes, or any related issues, please refer to the APCD Enforcement Manual located at https: / /www.colorado.gov/pacific/sites/default/files/AP- EnforcementandComplianceGuide.pdf and/or contact the Division personnel identified below. I I . COMPLIANCE ADVISORY MEETING Biochar is requested to contact the Division and schedule a meeting to: ➢ Discuss the disputed Compliance Advisory issues and answer any remaining questions you may have; ➢ Submit information necessary to successfully show that the deficiencies and noncompliance issues (or any portion of them) are not violations of Colorado's air pollution laws; and 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe John W. Hickentooper, Governor I Larry Wolk, MD, MSPH, Executive Director and Chief Medical Officer 6 COLORADO Air Pollution Control Division Department of F&ibIr. Healrh & Err:ironrreent Establish a mutually acceptable schedule and guidelines for the full and final resolution of any remaining deficiencies and noncompliance issues in a timely manner. Please contact the compliance officer identified below by no later than November 30, 2017 to schedule a meeting with the Division to discuss the Compliance Advisory. The Division currently anticipates that the meeting will take place during the week of December 11, 2017. Sarah Goff, Enforcement Advisor (303-692-6331) cc: Shannon McMillan, APCD Paul Carr, APCD Arch Crouse, APCD Michael Stovern, EPA (Region VIII) File Jeffrey Bishop, APCD Beth Pilson, APCD Heather Wuollet, APCD Tom Roan, Attorney General's Office 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.8ov/cdphe John W. Hickenlooper, Governor I Larry Wolk, MD, MSPH, Executive Director and Chief Medical Officer 7I COLORADO Air Pollution Control Division L'epartrrent of P..itzlrr Health & Emuoninot COLORADO Department of Public Health & Environment AIR POLLUTION CONTROL DIVISION COMPLIANCE ADVISORY CASE NO. 2020-126 AIRS NO. 123-9E2C TESTING DATES: October 8-9, 11, and 14, 2019 U.S. CERTIFIED MAIL NO. 7017 0660 0000 0139 3786 MAILING DATE: June 16, 2020 SOURCE CONTACT: Jim Geist IN THE MATTER OF BIOCHAR NOW, LLC This Compliance Advisory provides format notice, pursuant to § 25-7-115(2), C.R.S., of alleged violations or noncompliance discovered during the Air Pollution Control Division's ("Division") inspection and/or review of records related to Biochar Now, LLC's Facility identified below. The Division is commencing this action because it has cause to believe that the compliance issues identified below may constitute violations of the Colorado Air Pollution Prevention and Control Act ("the Act") and its implementing regulations. Please be aware that you are responsible for complying with applicable State air pollution requirements and that there are substantial penalties for failing to do so. Pursuant to the enforcement authority provided the Division by § 25-7-115, C.R.S., any person who violates the Act, its implementing regulations or any permit issued thereunder may be issued an order for compliance that can include permit revocation and assessment of penalties of up to $15,000 per day of such violation in accordance with § 25-7-122, C.R.S. The issuance of this Compliance Advisory does not in any way limit or preclude the Division from pursuing additional enforcement options concerning this inspection/review. Also, this Compliance Advisory does not constitute a bar to enforcement action for violations not specifically addressed in this Compliance Advisory. 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Polis, Governor I Jill Hunsaker Ryan, MPH, Executive Director Failure to respond to this Compliance Advisory by the date indicated at the end of this Compliance Advisory may be considered by the Division in the subsequent enforcement action and the assessment of penalties. Furthermore, the Division's enforcement process contemplates a full and final resolution of the compliance issues herein addressed, and those that may result from further review, in a timely manner. If at any time throughout the process of reaching such a resolution the Division determines that the Parties cannot agree to the dispositive facts, compliance requirements and/or penalty assessments (if any) associated with this Compliance Advisory, or a resultant enforcement action, the Division may exercise its full enforcement authority allowed under the law. Biochar Now, LLC ("Biochar") owns and operates the Berthoud Plant, a Biochar production facility located at 19500 Weld County Road 7, Weld County, Colorado ("Facility"). The Facility is subject to the terms and conditions of the Colorado Construction Permit Number 15WE1395, Issuance 4, Final Approval, issued to Biochar on April 25, 2018 ("Permit Number 15WE1395"), Colorado Air Quality Control Statutes, and Colorado Air Quality Control Commission ("AQCC") Regulations. I. ALLEGED VIOLATIONS AND FACTS On October 8-9, 11, and 14, 2019, compliance testing was conducted at the Facility. Testing was conducted on the exhaust stack of four kilns (AIRS Point 001): 7, 8, 21, and 40. The testing on October 8, 2019 (Kiln 40) was observed by Jeffrey Bishop, of the Division. On November 20, 2019, the Division received the test report. Based on the Division's observations made during testing and a review of records related to the Facility, including the test report received on November 20, 2019, the Division has identified the following compliance issues: A. Pursuant to Permit Number 15WE1395, Condition 4, the afterburners must be maintained and operated to ensure satisfactory performance. The permitted kiln emission factors are 0.14 pounds per hour ("lb/hr") NOx and 0.12 lb/hr CO. Compliance testing conducted on October 8, 2019 indicated Kiln 40 NOx emissions of 0.180 lb/hr and CO emissions of 1.25 lb/hr. Testing conducted October 9, 11, and 14, 2019 indicated 3-Kiln1 NOx emissions of 0.238 lb/hr. From September 8, 2017 (date of last passing test) to present, Biochar has failed to operate the afterburners to ensure the permitted kiln emission factors for NOx and CO are achieved, and therefore, Biochar has failed to operate the afterburners to ensure satisfactory performance, violating Permit Number 15WE1395, Condition 4. 1 Average of test results for Kilns 7, 8, and 21. 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Polls, Governor 1 Jill Hunsaker Ryan, MPH, Executive Director B. Pursuant to Permit Number 15WE1395, Condition 14, Biochar must demonstrate continued compliance with the annual kiln emission limits listed in Condition 2 by completing a source compliance test every two years. The average of 3 kiln/afterburner emission rates must demonstrate compliance with the annual emission limits listed in Condition 2. Any compliance test conducted to show compliance with an annual emission limitation must have the results projected up to the annual averaging time by multiplying the test results by the allowable number of operating hours for that averaging time. The permitted kiln emission limits are 13.5 tpy NOx and 11.6 tpy CO. Compliance testing conducted on October 8, 2019 indicated Kiln 40 NOx emissions of 17.34 tpy and CO emissions of 120.45 tpy. Testing conducted October 9, 11, and 14, 2019 indicated 3 -Kiln NOx emissions of 22.93 tpy. From September 8, 2017 (date of last passing test) to present, Biochar has failed to demonstrate continued compliance with the annual kiln NOx and CO emission limits, violating Permit Number 15WE1395, Condition 14. It is important to resolve the above -referenced issues as soon as possible. Therefore, the Division encourages Biochar to immediately identify those compliance issues that are not in dispute and to rectify those issues before the upcoming Compliance Advisory meeting. In accordance with § 25-7-115(3)(a), C.R.S., the Compliance Advisory meeting will be held within thirty (30) days of the Division's issuance of the Compliance Advisory in this matter. The Division also requests that Biochar provide the Division with a brief written response to the alleged violations ("Source Response"). The Source Response should identify the undisputed compliance issues and, if an alleged violation is disputed, the basis for the dispute. The Division requests that Biochar provide the Source Response, to the attention of Jen Schoennagel, no later than ten business days before the Compliance Advisory meeting. At the upcoming meeting, the Division will confirm the actions taken to rectify the undisputed compliance issues and proceed with unresolved matters as outlined below. If you have any questions regarding this Compliance Advisory, the Division's enforcement processes, or any related issues, please refer to the APCD Enforcement Guide located at https: / /www.colorado.gov/pacific/cdphe/inspections-and- enforcement and/or contact the Division personnel identified below. I I . COMPLIANCE ADVISORY MEETING Biochar is requested to contact the Division and schedule a meeting to: Discuss the disputed Compliance Advisory issues and answer any remaining questions you may have; 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Polls, Governor I Jill Hunsaker Ryan, MPH, Executive Director ➢ Submit information necessary to successfully show that the deficiencies and noncompliance issues (or any portion of them) are not violations of Colorado's air pollution laws; and ➢ Establish a mutually acceptable schedule and guidelines for the full and final resolution of any remaining deficiencies and noncompliance issues in a timely manner. Please contact the Enforcement Advisor identified below by no later than June 23, 2020 to schedule a meeting with the Division to discuss the Compliance Advisory. The Division currently anticipates that the meeting will take place during the week of July 13, 2020. Jen Schoennagel, Enforcement Advisor (303-692-3233) To ensure meaningful communication with all Coloradans, the Division offers free language services. Please let us know if we can provide an interpreter for anyone attending the Compliance Advisory meeting. cc: Shannon McMillan, APCD Paul Carr, APCD Heather Wuollet, APCD Ben Cappa, APCD Michael Stovern, EPA (Region VIII) Jeffrey Bishop, APCD Beth Pilson, APCD Tom Lovell, APCD Tom Roan, Attorney General's Office File 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Polls, Governor I Jill Hunsaker Ryan, MPH, Executive Director 4 DocuSign Envelope ID: E847CFE1-56E9-4034-8FO4-1 E3A1356B029 COLORADO Department of Public Health & Environment June 7, 2023 SENT VIA ELECTRONIC MAIL Jordan Gaspard Biochar Now, LLC 19500 Weld County Road 7 Berthoud, CO 80513 Re: Proposed Early Settlement Agreement in the Matter of BIOCHAR NOW, LLC AIRS No.: 123-9E2C Case No.: 2023-051 Dear Jordan Gaspard: Biochar Now, LLC ("Biochar Now") owns and operates the facility located at 19500 Weld County Road 7, Berthoud, Weld County, Colorado ("Facility"). The Facility is or was subject to the terms and conditions of the Colorado Construction Permit Number 15WE1395 Issuance 5, issued to Biochar Now, LLC on October 29, 2020 ("Permit Number 15WE1395 Issuance 5"); Colorado Construction Permit Number 15WE1395 Issuance 6, issued to Biochar Now, LLC on July 5, 2022 ("Permit Number 15WE1395 Issuance 6"); Colorado Air Quality Control Statutes; and Colorado Air Quality Control Commission ("AQCC") Regulations. The following Facility equipment is relevant to this enforcement action: AIRS Point Permit Number Equipment Description 0071 15WE1395 Diesel fuel -fired Make: John Deere generator Diesel, engine: Model: 4045TF285, S/N: 20107179, Design rate: 78 horsepower, Relocation date: 2015 1 The engine associated with AIRS Point 007 was taken offline on July 27, 2022 and replaced by a temporary engine. Biochar Now submitted an Air Pollutant Emission Notice ("APEN") on November 16, 2022 requesting that the replacement engine be made permanent and the original engine be canceled in accordance with the Alternative Operating Scenario ("AOS"). The replacement engine (AIRS Point 009) began operation on August 1, 2022. 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.cotorado.gov/cdphe Jared Potis, Governor I Jill Hunsaker Ryan, MPH, Executive Director DocuSign Envelope ID: E847CFE1-56E9-4034-8FO4-1 E3A1356B029 009 15WE1395 Diesel fuel -fired generator engine: Make: Isuzu, Model: BP-4LE2X, S/N: 7253219, Design rate: 59 horsepower On September 12, 2022, Danielle Serna, of the Weld County Department of Public Health Et Environment ("WCDPHE"), a duly delegated representative of the Colorado Air Pollution Control Division ("Division"), inspected the Facility. Based on the inspection, and a review of records related to the Facility, the Division issued a Compliance Advisory to Biochar Now on March 31, 2023. On May 3, 2023, the Division and Biochar Now met to discuss the issues identified in the Compliance Advisory. Based upon a review of the inspection, records related to the Facility, and the information provided by Biochar Now, the Division has determined the following: A. Pursuant to Permit Number 15WE1395, Issuances 5 and 6, Condition 2, emissions of air pollutants from AIRS Point 007 must not exceed the limitations in the permit. Compliance with the annual limits must be determined on a rolling twelve (12) month total. The table below details rolling 12 -month periods with exceedances of AIRS Point 007 emissions of NOx, VOC and CO during the compliance period. B. AIRS Point 007 Rolling 12 -Month Emissions (tons per year) Month Period Rolling Ending (2022) 12 - NOx VOC CO January 2.1 1.1 2.2 February 2.1 1.2 2.2 March 2.3 1.3 2.4 April 2.3 1.3 2.4 May 2.5 1.4 2.6 June 2.4 1.3 2.5 July 2.3 1.2 2.4 August 2.2 1.2 2.3 September 2.1 1.2 2.2 Permitted Limit 2.0 1.1 2.1 Biochar Now failed to limit NOx, VOC, and CO emissions from AIRS Point 007 to the permitted limits during the rolling 12 -month periods listed above, violating Permit Number 15WE1395, Issuances 5 and 6, Condition 2. Pursuant to Permit Number 15WE1395 Issuance 5, Condition 6 and Permit Number 15WE1395, Issuance 6, Condition 4, Biochar Now must limit the diesel consumption at AIRS Point 007 by limiting the 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Potis, Governor I Jill Hunsaker Ryan, MPH, Executive Director DocuSign Envelope ID: E847CFE1-56E9-4034-8FO4-1 E3A1356B029 operation of the engine to 6,388 hours per year. Compliance with the annual AIRS Point 007 process rates must be determined on a rolling twelve (12) month total. The table below lists rolling 12 -month periods with exceedances of the AIRS Point 007 annual operating parameter. AIRS Point 007 Rolling 12 -Month Diesel Consumption Rolling 12 -Month Ending Period Hours of Operation (2022) January 6,603 February 6,813 March 7,312 April 7,428 May 7,817 June 7,715 July 7,223 August 6,678 September 6,505 Permitted Limit 6,388 *Operation of replacement engine under AOS Biochar Now failed to limit the hours of operation during the rolling 12 -month periods listed above, violating Permit Number 15WE1395 Issuance 5, Condition 6 and Permit Number 15WE1395, Issuance 6, Condition 4. The Colorado Air Pollution Prevention and Control Act, at § 25-7-122(1)(b), C.R.S., specifies the penalty for such violations. The monetary amount of the Division's settlement offer specified below takes into account, among other factors, the magnitude and severity of the violation, cooperation of the company, as well as the prior history of violations of air quality requirements associated with any of the company's facilities/operations in the State of Colorado (including a company's parent or subsidiary relations, if applicable). Settlement offers are based on the evaluation of the same factors and criteria in all cases. Based upon Biochar Now's cooperation, and its efforts to bring its operations into compliance with the regulations and permit conditions identified above, the Division acknowledges that Biochar Now has appropriately and adequately addressed all compliance issues identified above. In the interest of settling the matters cited herein, the Division therefore offers the following settlement in accordance with the Division's settlement policy. 1. Payment of a reduced penalty in the sum of Thirty -One Thousand Five Hundred Dollars ($31,500.00). Payment of the penalty precludes further enforcement by the Division for the above -described violations against Biochar Now. The Division retains its authority to take enforcement actions based on 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Potis, Governor I Jill Hunsaker Ryan, MPH, Executive Director DocuSign Envelope ID: E847CFE1-56E9-4034-8FO4-1 E3A1356B029 any and all violations not specifically described above. Payment of Thirty -One Thousand Five Hundred Dollars ($31,500.00) shall be made in three equal payments of Ten Thousand Five Hundred Dollars ($10,500.00) on or before the following dates: a. First payment shall be made by July 15, 2023. b. Second payment shall be made by September 15, 2023. c. Third payment shall be made by November 15, 2023. 2. The Division's willingness to accept installment payments is expressly conditioned upon Biochar Now's continued payments in accordance with the schedule set forth above. Should Biochar Now fail to make any installment payment, the entire administrative penalty, at the option of the Division, shall become due and payable to the Division ten (10) days after the Division notifies Biochar Now that the balance of the administrative penalty is due. 3. Entering into this settlement shall not constitute an admission of violation of the air quality laws, or the alleged facts relating thereto, nor shall any third party infer it to be such an admission in any administrative or judicial proceeding. However, Biochar Now agrees not to challenge the factual or legal determinations herein, the Division's authority to bring, or the court's jurisdiction to hear, any action, insofar as it pertains to the matters contained herein, to enforce the terms of this settlement agreement. The described violation will constitute part of Biochar Now's compliance history for any purpose for which such history is relevant. This letter constitutes an offer of settlement and is not a demand for payment. Please contact me if you wish to discuss this offer of settlement. We remain willing to consider any information you wish to submit related to the violation. Please be advised, however, that the offer of settlement contained in this letter is predicated on resolving this matter within fifteen (15) days of the date of this settlement proposal letter. If you elect to continue the negotiation of this matter beyond that date, this offer shall be deemed withdrawn, and any penalty mitigation built into this settlement proposal may be revoked. If you require additional time to evaluate this settlement proposal or discuss remaining issues with the Division, however, please contact me regarding your request for an extension of the offer. Any extension of the offer, if agreed to by the Division, must be confirmed, in writing, by the Division. If the above terms are acceptable to you, please have the appropriate person sign and return this letter. Penalty checks shall be made payable to the Colorado Department of Public Health and Environment, and mailed to: Air Pollution Control Division Attn: Heather Wuollet 4300 Cherry Creek Drive South 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Potis, Governor I Jill Hunsaker Ryan, MPH, Executive Director DocuSign Envelope ID: E847CFE1-56E9-4034-8FO4-1 E3A1356B029 APCD-SS-B1 Denver, Colorado 80246-1530 This offer of settlement, upon being fully endorsed by both the Division and Biochar Now, shall constitute full and final resolution of the noncompliance issues identified herein and in the Compliance Advisory issued to Biochar Now. You may write or call to request a settlement conference if you wish to discuss the matter with representatives of the Division's compliance staff. If we do not receive a response from you within fifteen (15) days of the date of this letter, we will assume that you are not interested in resolving this matter as outlined above. Please call Heather Wuollet, at 720-515-0279, if you have any further questions regarding this matter. Sincerely, �— DocuSigned by: 17DC47B9 Shannon c Wan Compliance and Enforcement Program Manager I certify that I am authorized by Biochar Now to execute this settlement agreement and bind Biochar Now, and any affiliated entities, to the terms and conditions of this agreement. I have read the above settlement and agree to the terms and conditions of this offer. Name: James Gaspard Title: ceo DocuSigned by: jaktAGS ASp �LEgEF5UFFFl7"4Q4... Signature Telephone Number (303) 882-3561 6/8/2O23 cc: Shannon McMillan, APCD Paul Carr, APCD Heather Wuollet, APCD Ben Cappa, APCD Michael Stovern, EPA (Region VIII) Jason Long, APCD Date Danielle Serna, WCDPHE Beth Pilson, APCD Tom Lovell, APCD Jeffrey Bishop, APCD Robyn Witte, Attorney General's Office File 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Potis, Governor I Jill Hunsaker Ryan, MPH, Executive Director 12/27/23, 10:32 AM State.co.us Executive Branch Mail - Initial TV Completeness Letter: Biochar Now, LLC- Berthoud Plant; OP: 23OPWE558 STATE OF COLORADO Burns - CDPHE, Andrew <andrew.burns@state.co.us> Initial TV Completeness Letter: Biochar Now, LLC- Berthoud Plant; OP: 23OPWE558 1 message Burns - CDPHE, Andrew <andrew.burns@state.co.us> Wed, Dec 27, 2023 at 10:28 AM To: "jordan.gaspard@biocharnow.com" <jordan.gaspard@biocharnow.com> Dear Madam, Please find the completeness letter attached. Thank you, Andrew Burns Title V Permit Engineer COLORADO Air Pollution Control Division Department or Publ;c Health b Environment 4300 Cherry Creek Drive S., Denver, CO 80246 Andrew.Burns@state.co.us I www.colorado.gov/pacific/cdphe/hm 23OPWE558 Timeliness Determination.pdf 161K https://mail.google.com/mail/u/0/?ik=adc4f6be35&view=pt&search=all&permthid=thread-a: r-9135895218719816432&simpl=msg-a:r54932094757662... 1/1 COLORADO Department of Public Health & Environment December 27, 2023 Jordan Gaspard Managing Director Biochar Now, LLC 19500 Weld County Road 7 Berthoud, Colorado, 80513 RE: SUBJECT: Biochar Now, LLC - Berthoud Plant, FID: 123 - 9E2C, OP: 23OPWE558 Application for Title V Operating Permit Dear Jordan Gaspard: We have received your application for an Operating Permit for the above referenced facility on November 3, 2023. Please take note of the following information related to the processing of your application: Application Shield An operating permit application is due within one year after a source becomes subject to the Title V Operating Permit program. An administratively complete application received on or before the due date entitles the source to an application shield under the provisions of Regulation No. 3, Part C, Section II.B. . B. According to the Title V application, Biochar Now - Berthoud Plant, an existing facility located in the ozone non -attainment area, became subject to Title V permitting requirements upon the reclassification of the Denver Metro Area/North Front Range region to "Severe" non -attainment, which occurred on November 7th, 2022. The facility is a major stationary source for the following criteria pollutants: NOx (39.8 tpy), as it exceeds the "Severe" ozone non -attainment major stationary source thresholds of 25 TPY for the pollutant. As this source became subject to Title V due to an operation of law, per Colorado Regulation No. 3, Section III.B.2, B.2, the due date is one year after the effective date of the reclassification, making the due date November 7, 2023. A complete Title V Operating Permit application was submitted for the facility on November 3, 2023. The Operating Permit application submitted on November 3, 2023 for the above referenced facility has been determined to be administratively complete in accordance with the requirements of Colorado Regulation No. 3, Part C, Sections III . B, C, and D. Since a complete application was submitted prior to the regulatory deadline, the application shield is hereby granted and is effective as of November 3, 2023. Fees Colorado Regulation No. 3, Part A Section VI .A.1 requires the division to charge fees to "...recover the direct and indirect costs incurred by the Division in processing permit applications, issuing permits, and in 4300 Cherry Creek Drive S., Denver, CO 80246-1530 P 303-692-2000 www.colorado.gov/cdphe Jared Polls, Governor I Jill Hunsaker Ryan, MPH, Executive Director conducting a compliance monitoring and enforcement program. Such fees shalt apply without regards to whether a permit is issued, denied, withdrawn, or revoked." with respect to processing applications and issuing permits, fees wilt be charged for time spent reviewing the application and drafting the permit and associated basis document, including researching regulatory and technical issues related to the application and permit draft as applicable. Chargeable time also includes peer and supervisor review of drafts, as well as time spent by permit engineers and division management in meetings, phone calls, and responding to emails. The hourly permit processing fee is $119.00 beginning on July 1, 2021. Please see https: / /cdphe.colorado.gov/air-emissions/emissions-and-permitting-fees for additional information about fees. The Colorado Legislature has directed the Division to inform sources if the time spent processing an application wilt exceed 30 hours. The Division has determined that the time required to process your application for renewal of the operating permit wilt exceed 30 hours. Based on our experience in processing operating permits, we estimate that the total time required to process your application will be between 50 and 200 hours. This letter fulfills the Division's obligation to inform you that the processing time for your operating permit renewal wilt exceed 30 hours and to provide you with an estimate of the processing time. Please note that the Division utilizes a quarterly billing system for all operating permits. The bills you receive will reflect chargeable time for the previous quarter. Timeline The Division has eighteen months after a complete application is received to either approve or disapprove the application for an operating permit (Regulation No. 3, Part C, Section IV.C). Required Additional Information The next step in reviewing the application is the Technical Review. If the Division determines that additional information is necessary to evaluate or take final action on an application, a request will be made in writing for the information and a reasonable deadline for a response set. If the applicant fails to provide the requested information or does not meet the deadline, the application shield wilt be revoked and the Division wilt be unable to continue with the processing and issuance of the permit (Colorado Regulation No. 3, Part C, Section IV. D). Please note that in accordance with Colorado Regulation No. 3, Part C, Sections IV.B.3 3 and 4 that it is the sources' responsibility, without notification, to supplement the permit application in the event that errors or omissions are discovered after the permit application submittal. Additional information must be signed and certified by the responsible official as to its completeness and accuracy. Please do not hesitate to contact us if you have any questions at 303-692-3100 or cdphe_aped _title _v@state.co.us. Sincerely, The Title V Intake Team Stationary Sources Program Air Pollution Control Division 12/27/23, 10:33 AM State.co.us Executive Branch Mail -Additional Information Request: Biochar Now, LLC- Berthoud Plant; OP: 23OPWE558 STATE OF COLORADO Burns - CDPHE, Andrew <andrew.burns@state.co.us> Additional Information Request: Biochar Now, LLC- Berthoud Plant; OP: 23OPWE558 1 message Burns - CDPHE, Andrew <andrew.burns@state.co.us> Wed, Dec 27, 2023 at 10:32 AM To: "jordan.gaspard@biocharnow.com" <jordan.gaspard@biocharnow.com> Dear Madam, Your application failed to include a concurrence letter along with your complete EJ Summary. While your application is considered administratively complete per the guidance of the "Air Pollution Control Division Guidance for Incorporating Environmental Justice into Permitting" memo published in July of 2023, the concurrence letter is required to supplement the application when completed. If you have not yet received your concurrence letter, a copy of the letter of concurrence from the Division's EJ Permitting Specialist must be submitted to the title V email box (cdphe_apcd_title_v@state.co.us) within two weeks of receiving the letter of concurrence. If you have received your concurrence letter, a copy of the letter must be submitted to the title V email box within two weeks of receiving this request. Note that this does constitute a request for additional information per Colorado Regulation No. 3, Part C, Section IV.D. Failure to comply with this request will result in the revocation of application shield, if granted. If, for whatever reason, you are unable to comply with the aforementioned deadline, please notify the division in writing before the deadline has passed, complete with a rationale and an alternative deadline. Thank you, Andrew Burns Title V Permit Engineer COLORADO Air Pollution Control Division Department of Pubhc F-Cet th Er Environment 4300 Cherry Creek Drive S., Denver, CO 80246 Andrew.Burns@state.co.us I www.colorado.gov/pacific/cdphe/hm https://mail.google.com/mail/u/0/?ik=adc4f6be35&view=pt&search=all&permthid=thread-a: r-3208547623957036797&simpl=msg-a:r24002085062980... 1/1 TrinityConsultants � 1391 N Speer Blvd, Ste 350, Denver, CO 80204 / P 720.638.7647 / trinityconsultants.com November 2, 2023 Submitted electronically to cdphe apcd title V@state,cosus Colorado Department of Public Health and Environment Air Pollution Control Division — Title V Division 4300 Cherry Creek Drive South, APCD-SS-B1 Denver, Colorado 80246-1530 RE: Biochar Now, LLC CDPHE APCD AIRS ID: 123-9E2C Initial Title V Operating Permit Application To whom it may concern, ACB AIRS: 123-9E2C Permit #: 23OPWE558 Rcvd: 11/3/2023 On behalf of Biochar Now, LLC, Trinity Consultants is submitting the enclosed initial Title V Operating Permit application for the Biochar Now Berthoud Plant (Berthoud Plant) located at 19500 Weld County Road 7 Berthoud, CO 80513. The Berthoud Plant operates under Colorado Department of Public Health and Environment (CDPHE) Air Pollution Control Division (APCD) Construction Permit 15WE1395, Issuance 6, issued on July 5, 2022. Weld County is within the boundaries of the Denver Metro -North Front Range (DMNFR) nonattainment area, which was reclassified on November 7, 2022, as severe non -attainment for the 8 -hour ozone standard. This reclassification lowered the Title V permitting thresholds for NOx and VOC for facilities in the DMNFR from 50 to 25 tons per year (tpy). Biochar Now submitted a modification to 15WE1395 in March 2023 to reduce potential NOx emissions below 25 tpy but a revised permit with enforceable limits less than the major source threshold will not be issued prior to the effective reclassification date of November 7, 2023. As a result, an initial Title V application is being submitted to maintain the permit application shield for a timely application. Biochar Now will withdraw the initial Title V permit application once the synthetic minor construction permit is issued. Per CDPHE guidance, submittal of previously submitted and approved emission calculations and APEN forms for sources included in this initial Title V application are not required since no changes to authorized limits are being requested. If you have any questions, or require any additional information on this submittal, please contact me at giwaszek@trinityconsultants.com or via phone at (303) 349-4673. Sincerely, tee -r- 4uce-gai George Iwaszek Principal Consultant cc: Dylan Van Demark, Biochar Now Jordan Gaspard, Biochar Now INITIAL TITLE V PERMIT APPLICATION Biochar Nowt-., Biochar Now, LLC Prepared By: George Iwaszek — Principal Consultant Kendall Maffet — Consultant Matthew Petrosky — Associate Consultant TRINITY CONSULTANTS 1391 N Speer Blvd, Suite 350 Denver, CO 80204 (720) 638-7647 November 2023 Trinity/ Consultants TABLE OF CONTENTS 1. EXECUTIVE SUMMARY 2. PROCESS DESCRIPTION 3. CAM APPLICABILITY APPENDIX A. TITLE V FORMS APPENDIX B. FACILITY PLOT PLAN APPENDIX C. EJ SUMMARY 1-1 2-1 3-1 A-1 B-1 C-2 Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants i 1. EXECUTIVE SUMMARY The Biochar Now Berthoud Plant (Berthoud Plant) located at 19500 Weld County Road 7 Berthoud, CO 80513 in Weld County. The Berthoud Plant operates under Colorado Department of Public Health and Environment (CDPHE) Air Pollution Control Division (APCD) Construction Permit 15WE1395, Issuance 6, issued on July 5, 2022. Weld County is within the boundaries of the Denver Metro -North Front Range (DMNFR) nonattainment area, which was reclassified on November 7, 2022, as severe non -attainment for the 8 -hour ozone standard and in attainment/unclassified for all criteria pollutants. This reclassification lowered the Title V permitting thresholds for NOx and VOC for facilities in the DMNFR from 50 to 25 tons per year (tpy). Biochar Now submitted a modification to 15WE1395 in March 2023 to reduce potential NOx emissions below 25 tpy but a revised permit with enforceable limits less than the major source threshold will not be issued prior to the effective reclassification date of November 7, 2023. As a result, an initial Title V application is being submitted to maintain the permit application shield for a timely application. Biochar Now will withdraw the initial Title V permit application once the synthetic minor construction permit is issued. Table 1. Facility PTE Emissions Summary (tons/year) Emission Source TSP PMio PM2.5 SO2 NOx VOC CO Kilns (AIRS 001) 1.5 1.0 0.7 0.0 20.2 2.9 1.3 Unpaved Roads (AIRS 006) 3.1 1.1 0.0 0.0 0.0 0.0 0.0 49 kW Engine (AIRS 009) 0.5 0.5 0.5 0.4 6.5 0.5 1.4 58 kW Engine (AIRS 010) 0.5 0.5 0.5 0.4 6.6 0.5 1.4 TOTAL 5.5 3.0 1.6 0.9 33.2 4.0 4.2 Severe NAA NNSR/Title V 100 100 100 100 25 25 100 Thresholds Facility Severe Site NAA -Wide NNSR/ Emissions Title < V YES YES YES YES NO YES YES Thresholds PSD Thresholds 250 250 250 250 - - 250 Facility PSD Thresholds Site -Wide Emissions < YES YES YES YES - - YES Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants 1 2. PROCESS DESCRIPTION Biochar Now is a pioneer in the biochar industry with strong engineering, manufacturing, sales, and administrative personnel focused on making and selling quality biochar on a very large scaler. Biochar is a black charcoal -like material containing carbon and ashes that is produced from burning organic material such as agricultural, grass, and forest wastes. The Facility is classified under Standard Industrial Classification (SIC) code 2861 (Gum and Wood Chemicals). At the Berthoud Plant, most emissions come from kiln operations (AIRS 001). The NOx emissions associated with kiln operations are associated with burning different fuels to power the kiln. The Facility receives power from two generators (AIRS 009 and AIRS 010) and has permitted fugitive emissions from unpaved roads (AIRS 006). In addition, the Facility also has insignificant sources such as shredding/loading and packaging. 1 https://biocharnow.com/about/ Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants 2-1 3. CAM APPLICABILITY The Compliance Assurance Monitoring (CAM) rule applies to each pollutant -specific emission unit (PSEU) at a major source that is required to obtain a Part 70 permit if the PSEU meets all of the applicability criteria outlined in 40 CFR 64.2(a) as follows: a) The unit is subject to an emission limitation or standard for the applicable regulated air pollutant (or a surrogate thereof), other than the exemptions in this subpart; b) The unit uses a control device to achieve compliance with any emission limitations or standards; and c) The unit has a potential pre -control device emissions (as defined in this subpart) of the applicable regulated air pollutant that are equal to or greater than 100 percent of the amount, in tons per year, required for the source to be classified as a major source. There are no permitted boilers at the Berthoud Plant per their most recent 2022 CDPHE Construction Permit, and therefore, the Facility is not subject to CAM. Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants 3-1 APPENDIX A. TITLE V FORMS The following forms are included in this section. General Facility Forms: O P -50 - OP -1o0 OP -101 O P -102 O P -103 OP -105 Title V Operating Permit Application Form - General Facility & Contact Information Form - Source and Site Description Form - Plant Wide Criteria Air Pollutants Form - Plant Wide Hazardous Air Pollutants Form - Insignificant Activities Form Source Specific Forms: ► Kilns (AIRS ID 123/9E2C/001) • OP -312 — Kiln Operations Form • OP -400 — Compliance and Monitoring Form Der Unpaved Haul Roads (AIRS ID 123/9E2C/006) • OP -310 — Fugitive Particulate Matter Form • OP -400 — Compliance and Monitoring Form 49 kW RICE (AIRS ID 123/9E2C/009) • OP -302 — Reciprocating Internal Combustion Engine Form • OP -400 — Compliance and Monitoring Form 58 kW RICE (AIRS ID 123/9E2C/010) • OP -302 — Reciprocating Internal Combustion Engine Form • OP -400 — Compliance and Monitoring Form Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants A-1 General Facility Forms Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants A-2 S COLORADO Air Pollution Control Division Department of Public Health Er Environment Title V Operating Permit Application Form This form must be included with any application submittal to the Title V Operating Permit Unit Form OP -50 Title V Operating Permit Number: Initial Plant AIRS ID 123 - 9E2C Number: 1. Instructions Included on the Colorado Air Pollution Control Division Website is an instruction sheet (Form OP -50A) for this application form. Refer to the instruction sheet or contact the Division with questions. Attach a cover letter describing the purpose of the application package if more room is needed. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Permit Application Type (check all that apply) Initial Renewal in a cover - letter. Identify any requested changes below or x Si nificant Modification g Administrative ownership, Modification correct typographical (e.g. error, transfer of etc.) Minor Modification source wishes - to use The the Minor Modification procedures under worksheet Colorado Regulation (Form OP No. -201) 3, must Part also be C, Section completed X. if a Notification Unit (APCD of PS Construction Memo 09-01, Scenario Permit Exempt #7) Contact Contact, Update and/or (Responsible Billing Contact) Official, Permit Supplemental Information (describe): Click here to enter text. Other (describe): Click here to enter text. 3. General Description - Include brief description describing the purpose of the application package. If more detail is needed, provide in cover letter. General Description of package Biochar Now, LLC is submitting this initial Title V Operating Permit application because the facility is a new Title V source due to the reclassification of the Denver Metro -North Front Range (DMNFR) nonattainment area as severe non -attainment for the 8 -hour ozone standard, which lowered the Title V permitting thresholds for NOX and VOC for facilities in the DMNFR from 50 to 25 tons per year. There are no requested changes to the facility equipment or emissions associated with this application. Form Revised August 2023 Page 11 of 5 COLORADO Department of Public Health Et Environment a COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -50 4. Section "Operating complete Forms Included 5.D application. Permit for submittal in the Form instructions. Applicability Submittal - Check Also Matrix" the included for forms more that on direction the will Division be submitted webpage on which with is a forms to the guidance include application. document to comprise Refer labeled a to OP -300 General Emission Unit, Quantity: Number x_l OP -50 Application x_l OP -100 Facility Identification OP -301 Boiler, Furnace, and Process Heater, Quantity: Number x_l OP -101 Site Information x OP -302 Engine, Quantity: 2 x_l OP -102 Plant Wide Criteria Emissions OP -303 Tanks, Quantity: Number x_l OP -103 Plant Wide HAP Emissions OP -304 Turbine, Quantity: Number OP -104 Permit Shield, Quantity: Number OP -305 Coating, Painting, Fiberglass, and Solvent Use, x OP -105 Insignificant Activities Quantity: Number OP -201 Minor Modification OP -306 Dehydrator, Quantity: Number OP -202 Oil and Gas OP -307 Amine, Quantity: Number OP -202.1 Additional Storage Vessels g Quantity: - Number OP -308 Liquid qQ Loadout, Quantity: Number Y OP -309 Fugitive VOC, Quantity: Number OP -202.2 Additional Dehydrators, Quantity: Number OP -310 Fugitive Particulate Matter, Quantity: Number OP -311 Incinerator, Quantity: Number OP -202.3 Additional SI Engines, Quantity: Number J OP -312 Kiln, Quantity: 1 OP -202.4 Additional CI Engines, OP -313 Landfill Quantity: Number OP -314 Separator p and Natural Gas Venting, g Quantity: Y : Number OP -202.5 Additional Fugitive Emissions, Quantity: Number OP -315 Routine or Predictable Emissions OP Additional Sweetening Units, OP -315.1 Routine or Predictable Emissions, .202.6 Quantity: Number Quantity: Number OP -202.7 Additional Combustion, x OP -400 Compliance and Monitoring (Note that each OP - Quantity: Number 300 series form), Quantity: form must 3 have an corresponding OP -400 OP -203 CAM, Quantity: Number 5. Additional Information A. Initial and Renewal Applications x Check this box if you are submitting an initial or renewal application. For all other application types, proceed to Section 5.B. If you are submitting an initial or renewal application, provide the application due date. See Colorado PS - Memo 09-01 and PS Memo 22-01 for help with Title V Operating Permit application due dates. Application Due Date: 11/7/2023 Basis for Application Due Date (Initial Permits Only): New Title V source due to reclassification of the Denver Metro/North-Front Range Nonattainment area to severe nonattainment area. B. APEN Attachments New/revised APENs are required if the facility is requesting a modification that requires a new APEN or changes information on a previously submitted APEN. Note that as of the updates made to Colorado Regulation No. 3 effective February 14, 2021, APEN copies are no longer required to be submitted with applications. New or revised APENs have been included with this submittal (filing fees must be included). Form Revised August 2023 Page 12of 5 COLORADO Department of Public Health Et Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -50 C. Check Confidential/Trade pages PS the Memo application following including 98-01 for includes Secret box confidential acceptable if any confidential Information confidential/trade information confidential information must information secret clearly on information the be submittals. following labeled has as confidential. pages: been Click submitted here with to this application. text. The See This enter D. Submittal Division is requiring one electronic copy submittal emailed to the Air Pollution Control Division to The cdphe_apcd_title_V@state.co.us. The date received by the Division will be the date the complete electronic submittal is received with signatures as stated in (1) below. submittal must contain the following: The 1. The which source shall must contain submit either a complete PDF copy of a the scanned full application ink signature. including all signature pages digital signatures or 2. Forms must also be submitted individually in word format (either .doc or .docx) For electronic submittals, it is suggested that the permittee place multiple files in a compressed zip file before attaching to the email, use optimize/enhance tools in Adobe to reduce size of pdf files, or send multiple emails if there are problems with file sizes. If a source is not able to complete an electronic application as stated above, the permittee should contact the Division at cdphe_apcd_title_V®state.co.us to determine how to submit the application. Included on the APCD website is a sample V Initial application (for an oil and gas exploration and Title production facility) and a general instruction document for using the V forms. Reference either of these Title documents for further guidance and examples of a complete submittal. [UPDATE] Note that as of April 2023, The Division is no longer requiring hardcopy submittals of the V Title application forms. E. Oil and Gas Sources If this facility is associated with Oil Et Gas activities, Form OP -202 must be completed if the facility is submitting an initial application or the facility is requesting changes to oil and gas equipment and must be submitted for the application to be considered complete. Oil and Gas SIC codes include, but are not limited to, 1311, 1321, and 4922. Form OP -202 has been included with this application. facility is not an oil and gas facility, and/or the facility is not requesting any changes to the oil and gas x This equipment. F. Modeling If an emission unit will have to go through a modeling determination as part of a permit action, APCD-114 and the APCD Permit Modeling Unit's (PMU) determination must be completed and attached to the application. For information about the modeling process, see the page titled "Air Quality Modeling Guidance for Permits" on the Division webpage. Form APCD-114 along with PMU's Determination has been completed and attached. This application did not trigger the need for a PMU determination or APCD-114 form [x G. Environmental Justice III.C.14) As of July 15, and 2023, a letter an of environmental concurrence justice from the summary (See Division's Colorado Environmental Regulation Justice group No. 3, Part is required C, Section to be submitted with all Title V initial and renewal applications, and minor or significant modification applications. For more information about the Division's Environmental Justice process and to access the reporting tool, see the pages titled "New Environmental Justice Report Tool for Air Quality Regulation 3" and "Air Pollution Control Division Guidance for Incorporating Environmental Justice into Permitting" on the Division Webpage (links are included on the OP -50A Instruction Document). The environmental justice summary report, required aerial or satellite image, and supplemental IX environmental justice summary information has been completed, submitted to the Division's Environmental Justice group, and a copy is attached. Form Revised August 2023 Page I3of5 COLORADO Department of Public Health Et Environment 111 COLORADO Air Pollution Control Division Department of Public Health & Environment Form OP -50 The letter of concurrence from the Division's Environmental Justice group is completed and attached. If the letter of concurrence is not attached, explain: Biochar Now has not yet received the letter of concurrence after submitting the EJ Summary to the Division. This application does not trigger the need for an environmental justice summary report or letter of concurrence because it is the following application type (check the box below): Administrative Permit Amendment APEN exemption/Permit exemption/Insignificant activity Contact Update (RO, contact person, and/or billing contact update) Supplement to previously submitted application Other, explain: Click_: here to enter text. I 6 Signature of Responsible Official WARNING: statement, of A. B. C. a Statement I I applicable applicable applicable applicable have certify certify certify certify Any representation, here here reviewed and person of inquiry, that that that that Completeness complete. of requirements, assurance requirements, of requirements. requirements, and to to Facility the the Facility the the this I enter facility facility enter who may facility facility certify monitoring. application Compliance Compliance knowingly, or be described described text, described described text certification punished that including except except the in Status for Status for as in its statements in in in in compliance defined the the in, accordance this this this this entirety With With following air air following air air or in omits Federal pollution pollution State pollution pollution and, and § certification 18-1-501(6), with information emissions -Only emissions material based and the permit permit Enforceable permit permit State on requirements unit(s) unit(s) information provisions information contained application application application application C. Enforceable OS., identified identified Conditions makes f from § and in is is is is 25-7 this and fully fully Conditions fully fully any this belief any below: below: I application in in in in false application 22.1, applicable compliance compliance compliance compliance formed material C.R.S. after are is true, with with with with guilty x reasonable accurate Certification I x all compliance all Click Certification x all all Click misdemeanor Responsible Name Official or Others Jordan Gaspard Title Managing Director Signature2 c/ , Date t�t , . , -. . text. , 1F or the fol[ow�ng applications, a signature of a Legally Authorized Person (not a vendor or consultant) is acceptable: Notification of Construction Permit Exempt Unit, Billing contact update, Responsible Official update, and Supplemental Information submittal. For these application types,PP PP a Legally Authorized Person must only certify with Section 6.A (6.B and 6.C certifications are not needed). Form Revised August 2023 Page 14of5 • COLORADO Department of Public • --'. Health 8 Environment �M�:�� Air Pollution Control Division COLORADO Form OP -50 CDPHE TM Department of Public Health & Environment 2Either a wet or electronic signature is required here. Form Revised August 2023 Page 15 of 5 COLORADO Department of Public Health Et Environment COLORADO Air Pollution Control Division Department of Public Health & Environment General Facility Information Form Form OP -100 Title V Operating Permit Number: Initial Plant AIRS ID 123 - 9E2C Number: 1. Instructions Included on the Colorado Air Pollution Control Website is an instruction sheet (Form OP -100A) for this application form. Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Facility Name and Physical Address Company Name Biochar Now, LLC Facility Name Berthoud Plant Address 1 19500 Weld County Road 7 Address 2 Inter facility address line 2, if applicable. City Berthoud County Weld State and Zip Code 80513 3. Parent Company Name and Mailing Address Name Biochar Now, LLC Address 1 19500 Weld County Road 7 Address 2 Enter Parent Facility Address line 2, if applicable. City Berthoud State and Zip Code Colorado, 80513 4. Billing/Accounts Payable for Title V Operating Permit Fees Invoices immediately applications. other construction associated Division are issued with upon permit The fees annual Division any quarterly can change processing) be pollutant may updated to send to recover avoid or emissions. invoices via by costs additional an following via Air associated Pollution the email penalties instructions and/or with Emission due processing US to Notice on Mail. nonpayment. the Update (for annual hourly V the emission Operating Billing contact fees contact associated fee Permit information invoice information with for fees for Title Contact Name Jordan Gaspard Managing Director Title Email Jgaspard@biocharnow.com (970) 593-9100 Telephone Address 19500 Weld County Road 7, Berthoud, CO 80513 Form Revised August 2023 Page 11 of \e3lj X90/ COLORADO Department of Public Health 8 Environment COLORADO Air Pollution Control Division Department of Public Health & Environment Form OP -100 5. Responsible Official - See instruction sheet for information on Responsible Official requirements. Name Jordan Gaspard Title Managing Director Email jgaspard@biocharnow.com (970) 593-9100 Telephone Address 19500 Weld CR7, Berthoud, CO 80513 6. Permit Contact Person Name Jordan Gaspard Managing Director Title Email jgaspard@biocharnow.com (970) 593-9100 Telephone Address 19500 Weld CR7, Berthoud, CO 80513 7. Correspondence Options - Select the correspondence option associated with the processing of the Title V Operating Permit for the facility. x x x Permit Contact Person Only Copy Responsible Official (formal letters only) Copy Responsible Official (include all files, draft permits, etc.) 8. Facility Information A. Business of facility: Activity Biochar production facility B. SIC Code: 2861 C. NAICS Code: 325194 D. Is located nonattainment area the facilit (NAA)? in a y E. If check designated nonattainment pollutant(s) yes on the D, CO x Ozone PM1 o Other (specify): Click here to If included enter the defined 27, yes northern Part for text ozone, in in A.? the Colorado . portion 2015 is this of 8 -hour Regulations facility Weld located County O3 NAAQS 7 and in as 24- N Yes No Yes x No F. Is of section this accidental facility 112(r)(7) subject release of the to of the hazardous Clean provisions air Air Act?: governing pollutants contained prevention in Yes IX No If yes, has a RMP been registered? Yes No G. Is subject Acid the Rain facility to the H. If a new yes complete or on G, is Yes x No Yes No Form Revised August 2023 Page 12of4 COLORADO Department of Public Health 8 Environment COLORADO Air Pollution Control Division Department of Public Health & Environment Form OP -100 Provisions of renewal Acid Title IV? included? Rain application permit 9. approvals incorporated number, List of date, Permits and exemptions and and - construction what List all unit/process (Federal issued to permits and this that is State) facility. covered need air This to by pollution section be incorporated each permit. permits includes Attach (including construction into the additional operating grandfathered permits pages permit. units), already if necessary. List the plan Permit Number Date Last Issued Units/Processes Covered by Permit 15WE1395 Jul 5, 2022 y Process diesel fuel kilns, -fired various unpaved generator engines haul roads, two (2) Enter Number. Click here to enter text. Click here to enter text. Enter Number. Click here to enter text. Click here to enter text. Enter Number. Click here to enter text. Click here to enter text. Enter Number. Click here to enter text. Click here to enter text. Enter Number. Click here to enter text. Click here to enter text. Enter Number. Click here to enter text. 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Click here to enter text. Enter Number. Click here to enter text. Click here to enter text. Form Revised August 2023 Page 13of4 COLORADO Department of Public Health 8 Environment COLORADO Air Pollution Control Division Department of Public Health & Environment Form OP -100 10. Prevention of Significant Deterioration (PSD) and Non -Attainment New Source Review (NANSR) A. Is Deterioration 100 II.A.25.a.(1)) this tons facility a (PSD) per year? listed (See source for which Colorado for the the source Regulation purposes of would 3, be Part Prevention considered A, Section of Significant major at Yes 'XI No If here yes, describe: to enter Click text. B. Is Prevention ≥ 250 this facility • of Tons/Year a major •�• Significant or 100 stationary Tons/Year source • Deterioration if (PSD) listed for the source) program? purposes p p (Potential of the • to • Emit Yes x No Ifyes, Click text. enter here pollutants: to enter C. Is Attainment above II.A.25.b) this .A.25. facility thresholds b) New a major Source stationary listed in Review (NANSR) Colorado source Regulation for program? the 3, purposes (Potential Part of D, Section the to Non- Emit x Yes No If NOx yes, enter pollutants: 11. Reporting Facilities are required to submit semiannual Monitoring and Deviation reports and annual Compliance Certifications (these reports are included as appendices in the operating permit). For the calendar year reporting period (see below), reports are required by the end of the month following the end of the semiannual or annual periods respectively; e.g., Monitoring and Deviation reports would be due on July 31 and January 31, and the Compliance Certification would be due on January 31. The applicant may elect to alter the reporting date ranges below. Note that the requested reporting periods must be every 6 months for the Monitoring and Deviation report, and every 12 months for the compliance certification. Xi *Calendar year periods as follows: Monitoring and Deviation report: January 1 - June 30, July 1 - December 31 Compliance Certifications: January 1 - December 31 Reporting periods will align with issued permit i.e. if the operating permit is issued in May, annual compliance period will be May 1 - April 30 *Alternate reporting period (specify): Click here to enter text . *Note that if the applicant selects one of these options and the permit is issued on any month other than January or July, there will be shortened reporting periods to "catch up" to the default period. The applicant will be informed of any shortened periods with the issuance letter. Form Revised August 2023 Page 14 of 4 \e3lj X90/ COLORADO Department of Public Health 8 Environment COLORADO Air Pollution Control Division Department of Public Health & Environment Source and Site Description Form OP -101 Title V Operating Permit Number: Initial Plant AIRS ID 123 - 9E2C Number: 1. Instructions Included on the Colorado Air Pollution Control Website is an instruction sheet (Form OP -101A) for this source and site description form. Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Site Description Describe the units to be permitted and the activities at the facility. If additional space is needed, attach an additional description. The facility accepts clean waste wood (logs, pallets, etc.) that is shredded (insignificant activity) and processed in sealed kilns to produce biochar by heating the waste wood in a low -oxygen, controlled temperature ambient to drive off volatile compounds, leaving a carbonaceous "skeleton". Kiln emissions are controlled by a combustion afterburner. Biochar product is packaged (insignificant activity) for shipment offsite. Power at the site is provided by diesel fuel generators. Haul roads result in low -levels of fugitive particulate emissions. 3. Site Information Site Location Description (Include instructions needed to drive to remote sites not identified by street addresses) 19500 Weld County Road 7 Berthoud, CO 80513 Neighboring state(s) and Tribal programs within a 50 mile radius of the facility (check all that apply) x Arizona Utah Wyoming New Mexico Southern Utes Nebraska Kansas Oklahoma Texas Class I and II Federal areas within a 100 kilometer radius of the facility (check all that apply) To find this information, use the link to the data viewer provided in the instruction sheet. Form Revised August 2023 Mount Zirkel Wilderness Flat Tops Wilderness West Elk Wilderness La Garita Wilderness Mesa Verde National Park Great Sand Dunes National Park Florissant Fossil Beds National Monument Dinosaur National Monument Page I 1 of 2 x x Rawah Wilderness Rocky Mountain National Park Eagles Nest Wilderness Maroon Bells Snowmass Wilderness Black Canyon of the Gunnison Wilderness Weminuche Wilderness Great Sand Dunes National Preserve Colorado National Monument COLORADO Department of Public Health 8 Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -101 Uncompahgre Mountain Wilson Mountain Required (check Safety all that Equipment apply) Xi Hard Hat ❑ Hearing Protection x Safety Shoes Flame Retardant Clothing x Gloves H2S Monitor Other (describe): Click here fX E e Protection y ❑ to enter text. Collocation Information Is this facility collocated with another facility? Yes x No If yes, AIRS ID(s): list other Click facility operating here permit to enter text. number(s) (if applicable) and 4. Required Attachments - The following must be attached in order for the application to be considered administratively complete: Facility Plot Plan (plan view) - The Division will not accept blueprint sized drawings • Include all buildings occupied by or located on the site of the facility and any outdoor process layout • Identify location of emission units ❑ Process Flow Diagram (PFD) (if applicable) • Identify emission units X Form Revised August 2023 Page 12 of 2 COLORADO Department of Public Health & Environment a COLORADO Air Pollution Control Division Department of Public Health & Environment Plant Wide Criteria Air Pollutants Form OP -102 Title V Operating Permit Number: Initial Instructions Complete the following emissions summary for criteria air emissions at this facility. Included on the Colorado Air Pollution Control Website is an instruction sheet (Form OP -102A) for this form. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. Classification Is this facility considered to be a single source with another facility? Yes x No If yes, list other facility operating permit number(s) and plant AIRS ID(s): Click to enter text . If the facility associated with this Operating Permit application is considered a single source with another facility, fill out the following table for emissions associated with this Operating Permit application only; do not include any emissions from other facilities. Air Pollutant Uncontrolled Potential to Emit (tpy) Controlled Potential to Emit (tpy) Particulates (PM/TSP) 5.8 5.5 PMio 3.2 3.0 PM2.5 1.7 1.6 Sulfur Dioxide (502) 0.9 0.9 Nitrogen Oxides (NOx) 33.2 33.2 Volatile Organic Compounds (VOC) 59.5 4.0 Carbon Monoxide (CO) 4.2 4.2 Ozone (03) PTE PTE Lead PTE PTE Fluorides PTE PTE Total Reduced Sulfur PTE PTE Reduced Sulfur Compounds PTE PTE Hydrogen Sulfide (H2S) PTE PTE Sulfur Acid Mist PTE PTE Municipal Waste Combustor Organics PTE PTE Municipal Waste Combustor Metals PTE PTE Municipal Waste Combustor Acid Gases PTE PTE Form Revised August 2023 Page I1of1 COLORADO Department of Public Health Et Environment S COLORADO Air Pollution Control Division Department of Public Health Er Environment Plant Wide Hazardous Air Pollutants Form OP -103 Title V Operating Permit Number: Initial Instructions Complete the following emissions summary for all hazardous air emissions at this facility. Included on the Colorado Air Pollution Control Website is an instruction sheet (Form OP -103A) for this form. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. Classification (1) Is the facility considered a major source of hazardous air pollutants (HAPs) (Over 10 tons per year of a single HAP or 25 tons per year of combined HAPs)? Yes x No (2) Is the facility considered a single source with a facility that is a major source of HAP or where combined emissions make the facility a major source of HAPs? Yes x No If yes, list other facility permit number(s) and plant AIRS ID(s): Click here to enter text If the facility associated with this Operating Permit application is considered a single source with another facility, fill out the following table for emissions associated with this Operating Permit application only; do not include any emissions from other facilities. Hazardous Name Air Pollutant CAS Number Uncontrolled to Emit (Enter Potential Units) Controlled Emit (Enter Potential Units) to Benzene 71-43-2 1.87E-03 1.87E-03 108-88-3 8.20E-04 8.20E-04 Toluene Xylene 1330-20-7 5.71E-04 5.71E-04 Methanol 67-56-1 23.52 1.18 Formaldehyde 50-00-0 2.37E-03 2.37E-03 HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE HAP Name CAS Number PTE PTE Form Revised August 2023 Page I1of1 COLORADO Department of Public Health Et Environment S COLORADO Air Pollution Control Division Department of Public Health & Environment Insignificant Activities Form OP -105 Title V Operating Permit Number: Initial Plant AIRS ID Number: 123-9E2C 1. Instructions Included on the Colorado Air Pollution Control Website is an instruction sheet (Form OP -105A) for this insignificant activities form. Refer to the instruction sheet or contact the Division with questions. Review the exemptions listed and determine if any of the insignificant activities described operate at the facility. In the "additional information" column, using the checkboxes, indicate "Yes" or "No" if this insignificant activity operates at the facility. If "Yes", complete any additional questions that and/or fill out any associated tables. If more space is needed in the table(s), attach additional information. Note that the Operating Permit exemptions listed below do not apply if the emission unit is subject to any specific federal or state applicable requirements such as a New Source Performance Standard (NSPS) , National Emission Standard for Hazardous Air Pollutants (e.g. MACT), and/or Colorado Regulation No. 7, No. 24, No. 25, and No. 26, etc. Units subject to specific federal or state applicable requirements must submit the proper application forms and have the applicable requirements reflected in the Operating Permit. See Colorado Regulation No. 3, Part C, Section II.E for more details. Potential to Emit (PTE) for insignificant activities is typically estimated using the maximum design/emission rate of the emission unit operating at 8760 hours per year, or 500 hours/year for emergency engines. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Exemptions 2.A. Starred Insignificant Activities Sources activities an the sufficient insignificant are production required are marked record activity rate of keeping to with the include source an activity. verifying a list asterisk category that of in insignificant owner the Colorado based exemption on or the operator activities Regulation size applies. of of No. the these in activity, their 3, individual Part permit applications C, Section emissions emission II.E. levels points if from the asterisk must the insignificant denotes activity maintain or The The Insignificant g Activity Regulatory Citation Additional Information *Units APEN with de emissions less minimis - criteria pollutants. p than Re 3, II.E.3.a g Section Part ulation C, Yes No Ix_l Name of Unit PTE (indicate pollutant only) highest Location Shredding/Kiln Wood Loading PM: 0.20 ton/yr Location Biochar Et Packaging Sizing PM: 0.08 ton/yr y Location Unit PT Location Unit PTE Location Unit PTE Location Unit PTE Location Form Revised August 2023 Page 11 of 7 COLORADO Department of Public Health Et Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -105 Unit PTE Location `Research laboratories. Re Regulation 3, Section II.E.3.i g Part . E. 3.i C, Yes No x *If yes, is it of a small pilot ten thousand pounds scale of test Yes and material No that process less than per year? *If actual yes, is it less than six emissions less than pollutant or ten pounds months pollutant? five of Yes hundred any in duration non -criteria No with controlled pounds of any criteria reportable *Disturbance development, exceed acres for and six of purposes twenty-five that do months in surface areas of land that do not contiguous not exceed duration. Regulation 3, Part C, Section II.E.3.j Yes No x Describe: Click here to enter text. *Each burning smokehouse internal that than British that individualpiece equipment, combustion uses gaseous has a or equal thermal generators design to five units of fuel other and engines, fuel, and rate less million per hour. than Regulation 3, Part Section II.E.3.k C, Yes No x Name of Unit Design Rate (MMBtu/hr) Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location *Petroleum associated combusting containing exce approved having of any five p tin uncontrolled pollutant tons industry no by with natural hydrogen trace the per of flares, refineries, gas sulfide amounts, COGCC emissions less year. not and than Regulation g 3, Part Section II.E.3.m C, Yes No x Describe: Click here to enter text. *Chemical containers five throughput five not wastewater production hundred have an gallons associated and gas facilities processing. that storage annual less per that hold gallons, than with production or wastewater tanks less average day, either commercial accept or than that twenty- and are oil oil for Regulation 3, II.E.3.n Part C, Section Yes No X Chemical Storage Capacity (gal) Location Tanks Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Form Revised August 2023 Page 12of 7 COLORADO Department of Public Health & Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -105 *Landscaping housekeeping or less than size (lawnmowers, snow devices ten blowers, and site equal to horsepower in p trimmers, etc.). Regulation g 3, Part Section II.E.3.bb C, Yes No ❑ x 10,000 6750 equipment loading sites year production day exploration *Crude basis. gallons averaged loading that barrels or that than condensate oil loading at sites rate does Condensate equipment and splash of submerge 16308 exploration of on condensate where not crude an production fill less barrels per year. truck the exceed oil annual truck at than fill of and less per per Regulation 3, Part C, Section II. E.3.ee Yes No ❑ x Describe: Click here to enter text. `Chemical chemicals exceed containers, storage are storage capacity g P five thousand stored and areas where y does in closed gallons. where total not Regulation g 3, Part Section II. E.3.mm C, Yes No ❑ x Chemical Storage Areas Capacity (gal) p y Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location Unit Capacity Location *Venting natural gas cylinders, of gas, one gallon of butane compressed with or or a capacity less. propane Regulation 3, Part Section II.E.3.bbb C, Yes No x Describe: Click here to enter text. `Fuel attainment solely vehicles throughput four averaged attainment/maintenance recovery than gallons by Regulation order must Regulation equipment hundred storage five to for utilize where annually. an on capacity, take areas company is gallons ozone all hundred Number this and Stage Number in the no more tanks as exemption. dispensing ozone operated -owned daily Sources 1 and required per vapor greater 7 24], fuel than day, in area fifty [Now in Regulation g 3, Part Section II.E.3.ccc C, Yes No x Equipment Daily Throughput (gal/day) Fuel Fuel Location T e yp Unit Throughput Type Location Unit Throughput Type Location Unit Throughput Type Location Unit Throughput Type Location Unit Throughput Type Location Unit Throughput Type Location Is the equipment subject Yes to No NESHAP CCCCCC? Form Revised August 2023 Page 13of7 #1:4;6".,"%45,4 Hse . COLORADO Department of Public Health Et Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -105 `Storage (1) than (2) (i) (iii) (iv) a equal (Reid vapor the Annual four (ii) As through oil/water to vapor following gallons; liquid the Fuel turbine pressure tanks fuels that hundred throughput following: psi stored 6; oils pressure meeting criteria: and 1-D, #1 fuels 4 - mixture less of diesel thousand 2-D, - is #6; 1 all of is less one of or 4- - GT with or fuel .025 Regulation 3, Part C, Section II.E.3.fff . E. 3. fff No II Yes Ix Capacity (gal) Throughput (gal/yr) yp Type of Liquid Stored Location Tank The Diesel An Unit Capacity Throughput Type Location Unit Capacity Throughput Type Location Unit Capacity Throughput Type Location Unit Capacity Throughput Type Location Unit Capacity Throughput Type Location GT; than of Unit Capacity Throughput Type Location Unit Capacity Throughput Type Location Unit Unit Capacity Throughput Type Location Surface mine seventy fewer of year. A plan sources. other activities mining activities that thousand tons product material fugitive dust control is required for such q Crushers, screens processing equipment are not included this exemption. or per and in Regulation g 3, Part Section II.E.3. qqq C, No I Yes x Describe: Click here to enter text. Chemical stora a tanks. g Regulation 3, Part C, Section I. E.3.eeee Does your facility have exceed ten thousand sulfuric five hundred acid No storage gallons tanks not to capacity? Yes x Does your facility have sodium hydroxide No storage tanks? Yes (x Tanks Capacity (gallons) Liquid of Stored Location Type Unit Capacity Type Location Unit Capacity Type Location Unit Capacity Type Location Unit Capacity Type Location Unit Capacity Type Location Unit Capacity Type Location *Any with condensate are production owned same barrels condensate a manifold per year person, production and per year storage rate or operated storage together g of less and rate or 730 that are tanks less located tank of or that with barrels are by the 730 a Regulation 3, Part C' Section II.E.3. gggg Ix No D Yes Tanks Throughput (bbl/yr) Location Unit Throughput Location Unit Throughput Location Unit Throughput Location Unit Throughput Location Unit Throughput Location Form Revised August 2023 Page 14of 7 COLORADO Department of Public Health & Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment at exploration and production sites. Form OP -105 Unit Throughput Location Are any of these tanks subject to NSPS K, Ka, or Kb? ❑ Yes ❑ No LB. Co mmon Insignificant Activities The Division strongly suggests reporting the following common insignificant activities. However, it is not required to complete this section. Using the checkboxes, indicate "Yes" if this insignificant activity operates at the facility. If "Yes", complete any additional questions that and/or fill out any associated tables. Units with emissions less than APEN de minimis - non -criteria pollutants. Regulation 3, Part Section II.E.3.b C, Yes Name of Unit PTE (indicate pollutant only) highest Location Unit Example- HF: 100 lbs/yr Location Unit Example- Acrolein: p lbs/yr 50 Location Unit PTE Location Unit PTE Location Unit PTE Location Fire laces P recreational or outside. used purposes, for inside Regulation 3, Part C, Section II.E.3.d E.3.d Yes ❑ Emissions construction, residential including all structures used place of residence, including devices. or buildings home from, or alteration of structures, or other primarily as a and heating Regulation 3, Part C, Section II.E.3.h Yes ❑ Internal powering P combustion gportable engines drilling rigs. Regulation 3, Section II.E.3.1 Part C, Yes ❑ Open P burning activities. Regulation 3, Part C, Section I I. E.3.q Yes ❑ Aerosol can usage. g Regulation 3, Part C, Section II.E.3.0 Yes ❑ Form Revised August 2023 Page 15 of 7 COLORADO Department of Public Health Et Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -105 Storage provided Regulation IV of liquefied vessel with than sixty Now No. 24, Part met, the Colorado where butane, petroleum thousand Number a capacity requirements B, propane, gas gallons, q rements 7, Section Regulation Section applicable. or in a of less of II] are Regulation 3, II g Part Section . E.3.zz C, Yes ❑ Storage than lubricating tanks forty lubricating of capacity less thousand gallons of oils or waste oils. Regulation 3, Part C, Section II.E.3.aaa Yes design to buildings Each individual burning gaseous rate ten units used equipment fuel, million per solely for and less British hour, for personal piece that than and heating of fuel that uses has a or equal thermal that is comfort. Regulation 3, Part C, Section I I . E. 3. ggg Yes ❑ Describe: Click here to enter text. Stationary internal combustion engines. Regulation 3, Part C, Section II.E.3.nnn Do you have power portable Yes drilling rigs? ❑ Do you have emergency more than two power hundred Yes generators fifty hours that per operate year? no Do you have engines that have less than five tons per year horsepower of uncontrolled actual emissions or manufacturer's site -rated less than fifty? Yes Name of Unit PTE (indicate pollutant only) highest Horsepower Unit Example- NOx: 100 lbs/yr Horsepower Unit Example - Acrolein: 50 lbs/yr Horsepower Unit PTE Horsepower Unit PTE Horsepower Are any of these engines or subject NSPS Yes JJJJ? to No NESHAP ZZZZ, NSPS IIII, ❑ Gasoline stations located in ozone attainment areas. Regulation 3, Part Section II.E.3.ppp C, Yes ❑ Form Revised August 2023 Page 16of 7 COLORADO Department of Public Health Et Environment S COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -105 impoundment evaporation exce accept produced commercial wastewater Surface water p tions oil wastewater and oil and of gas water and water storm ponds, im for of facilities production gas p (including non oundment tanks) processing. storage production water -potable with that the and of Regulation 3, Section . II.E.3.yyy Part E.3.yyy C, Yes Source Wet applicability included Federal notwithstanding Part screening Performance Regulations, 60, in Subpart the of operations the Code the Standards New of 40, Regulation 3, Section II . g Part E.3.ffff C, Yes Are these screening operations Yes No subject to NSPS OOO? Title OOO. 2.C. Other Insignificant Activities Use the space below to report any other noteworthy insignificant activities that the facility would like listed in the permit. Include the name of the exemption, regulation citation (from Regulation 3, Part C, Section II.E), name of unit, and any other information the facility would like to add. Attach additional pages as needed to report other insignificant activities. Click here to Click here to enter Click here to enter citation. Reg Click here to additional information. enter enter unit 3 exemption name. name. Form Revised August 2023 Page 17 of 7 COLORADO Department of Public Health Et Environment Source -Specific Forms Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants A-3 S COLORADO Air Pollution Control Division Department of Public Health Er Environment Kiln Operation Form OP -312 Title V Operating Permit Number: Initial AIRS ID Number: 123 - 9E2C - 001 1. Instructions Included on the Colorado Air Pollution Control Division Website is an instruction sheet (Form OP -312A) for this kiln form. Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Kiln Information Facility (example: Identifier S001) N/A Kiln Information Manufacturer Model Serial Number Shop Built N/A N/A Dates Date Date Date commenced commenced last modified/reconstructed: construction: operation: 2015 March 8, Click 2016 here to enter text. Construction Underlying Permit IX] Yes No Permit Number: 15WE1395, Issuance 6 Exemptions information): List any state exemptions Click that here to apply enter to this unit text. (See Instruction Sheet for more 3. Kiln Characteristics General Description equipment of Kilns used to process clean wood to produce biochar product 0.125 (each kiln) Maximum Burner (MMBtu Rating / hr) (Check Design all Information that apply) Tunnel (Continuous) Kiln x Periodic (Batch) Kiln Pulse -Fired Combustion System Standard Combustion System Flue Gas Recirculation Reduced Air Preheating Low-NOx Burners Other (describe): Click here to enter text. Firing Information Temperature Approximate total Range: < 500 time for F (kiln cycle: interior); 12 hr/kiln afterburner: 1000 - 1500 F. 4. Primary Fuel Information Type of (See Secondary Primary Below Fuels) Fuel for 0 Other (specify): Propane ❑ Coal ❑ Natural Gas ❑ Fuel Oil Form Revised August 2023 AIRS ID: 123 - 9E2C - 001 Page 11 of 5 COLORADO Department of Public Health Fr Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -312 Fuel Information Fuel Heat (Btu/lb Heat Content coal): Content. Fuel Heat Content Btu/scf : 2300 ( ) Fuel (Btu/gal): Content. Heat Content Heat Click enter additional information that helpful permitting process. here may to be in the % Ash Ash Sulfur Sulfur Content. content: Content. content: % Sulfur content: Sulfur Content. % Sulfur content: Sulfur Content. Grade of Fuel Oil: Grade of Oil. Type of Natural Gas: Type of Coal: ❑ Anthracite Pipeline Quality Bituminous Subbituminous Field Quality Lignite Other Permit Throughput Limitation 16,800 MMBtu/yr 5. Secondary Fuel Information XI Check this box if the kiln does not have a secondary fuel and leave this section blank. Type of Secondary Fuel ❑ Other (specify): Enter fuel. ❑ Coal ❑ Natural Gas ❑ Fuel Oil Fuel Information Fuel Heat (Btu/lb Btu/lb Heat Content coal): Content. Fuel Heat Content (Btu/scf): Heat ) Content. Fuel Heat Content (Btu/gal): Heat Content. Click enter additional information that helpful permitting process. here to may be in the %Ash Ash Sulfur Sulfur Content. content: Content. content: Sulfur content: Sulfur Content. % Sulfur content: Sulfur Content. Grade of Fuel Oil: Grade of Oil. T e of Coal: Type Type of Natural Gas: ❑ Anthracite Pipeline Quality Bituminous Field Quality Subbituminous Other Lignite Click here to enter throughput and specify units. Permit Throughput Limitation Additional Information Indicate to when enter secondary text. fuels are used (i.e. startup, backup, etc.): Click here 6. Processing Information Permit and/or Hours (specify Throughput Limitation units) Raw Material Finished Hours Limitation (if applicable): Products (if (if applicable): applicable): 11,200 ton/yr clean - 2500 tons Click here biochar/yr to wood enter hours . Form Revised August 2023 AIRS ID: 123-9E2C-001 Page I2of5 COLORADO Department of Public Health £t Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -312 Design (specify Process Rate units) 1 ton clean wook/kiln Additional Information Process 32 kilns operating per day 7. State and Federal Regulations Rule Applicability How will you comply with this Regulation? 40 Subpart CFR Part JJJJJ 63 Click here to enter text. Subject x Not Subject 40 Subpart CFR Part 63 RRRRRR ❑ Subject Click here to enter text. x Not Subject 40 CFR Subpart Part 63 LLL Click here to enter text. ❑ Subject x Not Subject 40 CFR Subpart Part 60 F ❑ Subject Click here to enter text. x Not Subject Colorado No. Regulation 26 Part B Section II.A Subject Click here to enter text. x Not Subject Reasonably Available Control Technology See Permit 15WE1395, Issuance 6, Condition 9 X Subject For Point 001, application of afterburners to be RACT for this Not Subject source. Note equipment that the applicant in a nonattainment may be asked or attainment/maintenance to provide a RACT analysis if new or modified area. (RACT) Compliance Monitoring Assurance (CAM) If subject, addressed attach Form OP -203 CAM unless CAM has already in the permit or a CAM plan is not due yet. been Subject X Not Subject Colorado No. Requirements Regulation 1 Opacity p y These requirements are identified in Form OP -400. q x Subject Not Subject Other (specify) Click here to enter text. Colorado 1 Regulation PM Requirements No. Colorado Regulation 1 SO2 Requirements No. ❑ Subject Subject Not Subject Not Subject Colorado Regulation No. 6 PM Requirements Colorado Regulation No. 6 SO2 Requirements ❑ Subject Subject ❑ Not Subject Not Subject 8. Control Device Information Is any emission control equipment or practice used to reduce emissions? If yes, describe control device(s) below: x Yes No Control Device Description Afterburner stacks Pollutant PM PM10 PM2.5 SO2 NOx VOC CO Lead Enter Other Form Revised August 2023 AIRS ID: 123-9E2C-001 Page 13of 5 COLORADO Department of Public Health £t Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -312 Control Efficiency I Text Text Text Text Text 95% Text Text Text Controlled Enter Enter Enter Enter Enter Enter Enter Enter Individual HAP: Methanol HAP HAP HAP HAP HAP HAP HAP HAP Control EfficiencyI 95% Text Text Text Text Text Text Text Text 9. Primary Fuel Criteria Pollutant Emission Information Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Source (e. . g manufacturer, source Factor AP test, -42, etc. Uncontrolled Potential Emit (tpy) -to- Permitted Limitation (tpy) PM 0.27 EF lb /ton Stack 1.49 1.49 Testing PM10 0.18 EF lb/ton Stack 1.02 1.02 Testing PM2.5 0.13 EF lb/ton Stack 0.71 0.71 Testing SO2 EF EF EF Units EF Source PTE Limit NOx 0.30 EF lb/hr Stack Testing 20.16 20.16 VOC 10.44 0.522 lb/ton Stack 58.46 2.92 Testing CO 0.02 EF lb/hr Stack 1.34 1.34 Testing Lead EF EF EF Units EF Source PTE Limit Enter Pollutant EF EF EF Units EF Source PTE Limit 10. Primary Hazardous Air Pollutant (HAP) Emission Information Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Factor Source (e.g. AP -42, manufacturer, source test, etc. Uncontrolled Potential -to- Emit (tpy) Permitted Limitation (tpy) Methanol 4.20 0.21 lb/ton Stack 23.52 1.18 Testing Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit 11. Secondary Fuel Criteria Pollutant Emission Information Check this box if the unit does not have a secondary fuel and leave this section blank. xi Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Factor Source (e.g. AP -42, manufacturer, Uncontrolled Potential -to- Emit (tpy) Permitted Limitation (tpy) Form Revised August 2023 AIRS ID: 123-9E2C-001 Page 14of 5 COLORADO Department of Public Health £t Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -312 source test, etc. PM _L' Li EF Units EF Source PTE Limit PM10 - EF Units EF Source PTE Limit PM2.5 EL{' EF EF Units EF Source PTE Limit SO2 EF EF EF Units EF Source PTE Limit NOx EF EF EF Units EF Source PTE Limit VOC EF EF EF Units EF Source PTE Limit CO EF EF EF Units EF Source PTE Limit Lead EF EF EF Units EF Source PTE Limit Enter Pollutant EF EF EF Units EF Source PTE Limit 12. Secondary Fuel Hazardous Air Pollutant (HAP) Emission Information Check this box if the unit does not have a secondary fuel and leave this section blank. >1 Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Source (e.g. AP manufacturer, source test, Factor -42, etc. Uncontrolled Potential -to- Emit (tpy) Permitted Limitation (tpy) Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit 13. Compliance and Monitoring I have filled out and attached Form OP -400 Compliance and Monitoring with all known applicable requirements for this emission unit: xl Yes 0 No 14. Required Attachments The following must be attached in order for the application to be considered administratively complete (unless previously submitted): Emission Calculations Manufacturer Specifications or Contract Guarantee for Control Equipment (if applicable) Form Revised August 2023 AIRS ID: 123 - 9E2C - 001 ge 15of5 COLORADO Department of Public Health Fr Environment S COLORADO Air Pollution Control Division Department of Public Health & Environment Compliance and Monitoring Form OP -400 Title V Operating Permit Number: Initial AIRS ID Number: 001 - 9E2C - 001 1. Instructions Complete this form and attach it to the completed corresponding OP -300 series form for the applicable emission unit. Each OP -300 series form must be accompanied by a Compliance and Monitoring form (OP -400). Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. . B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Emission Unit Information Facility (example: Identifier 5001) Kilns 3. Applicable Requirements Identify recordkeeping, attach each additional applicable and descriptions. reporting requirement requirements, for the emission and the unit, basis any for the associated requirement. compliance If monitoring, more space is needed, Emission Limitations (tpy, lb/hr, lb/MMBtu, gr/dscf, etc.) TSP: PM PM NOx: VOC: CO: -10: -2.5: 1.5 1.3 1.0 20.2 2.9 0.7 tpy tpy tpy tpy tpy tpy Opacity Visible periods exceed using In a. shall, control maintenance include, procedures, addition, At EPA all to emissions of 30% times, practices startup, Method the but opacity the is and extent procedures including not following inspection must 9. for limited process for (Reference: practicable, minimizing not more exceed modification, requirements periods are to, of than being monitoring the be emissions. Regulation of twenty six source. minutes start-up, maintained used of will or results, percent Regulation (Reference: adjustment Determination Number be in shutdown, and based any (20%) opacity operated sixty 1, Number on Regulation opacity of Section and information observations, consecutive of control 6, malfunction, in whether II.A.1. during .A.1. a Part manner Number equipment A, or available normal minutes. 6t 4.) Subpart not review the consistent 6, acceptable Part visible facility, operation to of Opacity A, operating the A. General emissions with General and Division, must operating of good the control and be Provisions, Provisions source. must air which determined maintenance equipment pollution and not may apply During from Form Revised August 2023 AIRS ID: 001 - 9E2C - 001 Page I1of4 COLORADO Department of Public Health Fr Environment TM 40 CFR 60.11 b. No article, machine, equipment, or process shall be used to conceal an emission that would otherwise constitute a violation of an applicable standard. Such concealment includes, but is not limited to, the use of gaseous diluents to achieve compliance with an opacity standard or with a standard that is based on the concentration of a pollutant in the gases discharged to the atmosphere. (S 60.12) COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Operational Limitation(s) (hrs/yr, MMscf/yr, lb/yr, etc.) Clean wood processing rate: 20,075 tons/year Natural gas/propane consumption: 23.62 MMscf/year (Based on a fuel's heat value of 1,020 Btu/scf) Other Requirements List all other applicable requirements for this emission point. RACT Regulation Number 2 Regulation Number 3, Part B, II.A.4 Regulation Number 3, Part B, Regulation Number 3, Part B, IV. E. Regulation Number 3, Part B, III.A.4 Regulation Number 3, Part B, III.G.7. Regulation Number 3, Part D, V.A.7. B The owner or operator must demonstrate continued compliance with the annual Kiln emission limits listed in condition 2 by completing a source compliance test every two years. The test must be conducted no earlier than 21 months after the last compliance test and must be completed prior to 27 months after the last compliance test. (The last compliance test was conducted in September 2017) This test must be conducted on a total of 3 kiln/afterburner units to measure the emission rate(s) over the entire process duration for the pollutants listed below in order to demonstrate compliance with the annual emission limits listed in Condition 2. The average of the emissions rates for the 3 tests must be used to show compliance with the emission requirements. The test protocol must be in accordance with the requirements of the Air Pollution Control Division Compliance Test Manual and must be submitted to the Division for review and approval at least thirty (30) days prior to testing. No compliance test shall be conducted without prior approval from the Division. Any compliance test conducted to show compliance with a monthly or annual emission limitation must have the results projected up to the monthly or annual averaging time by multiplying the test results by the allowable number of operating hours for that averaging time (Reference: Regulation Number 3, Part B. III.G.3): Form Revised August 2023 AIRS ID: 001 - 9E2C - 001 Page 12of4 COLORADO Department of Public Health Fr Environment S COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Particulate Matter (PM10 and PM2.5, filterable and condensable) using EPA approved methods. 4. Monitoring Requirements Complete the following monitoring questions about the emission unit. Continuous Emission Monitoring Requirements? Yes x No Pollutant(s) Requirement(s): or Parameter(s): Click Click here to here to enter text. enter text. Continuous Emission Monitoring System (CEMS) Predictive Emission Monitoring System (PEMS) Continuous Emission Rate Monitoring System (CERMS) Other (describe): Click here to enter text. Periodic Compliance Testing? lXJ Yes No Pollutant(s): Frequency: Date of last Every Division PM: PM10, 21 -approved - 27 PM2.5 months test: from November previous 11, test. 2021 Other? Yes x No Describe: Frequency: Click Click here to enter text. here to enter text. 5. Compliance Status and Commitment Indicate the compliance status of the emission point as of the date of submittal: x In compliance with all applicable requirements Not in compliance (fill out Section 6 below if schedule of compliance is required) For applicable requirements this emission point is currently in compliance with: x_l The emission point will continue to comply with these requirements For applicable requirements that will become effective during this permit term: The emission point will comply with these requirements in a timely basis x 6. Schedule of Compliance Complete this section if "Not in compliance" was answered in Section 5 and a schedule of compliance is required. Also, complete this section if the applicant is required to submit a schedule of compliance by an applicable requirement. Attach copies of any judicial consent decrees, compliance orders on consent, or Form Revised August 2023 AIRS ID: 001 - 9E2C - 001 Page 13of4 COLORADO Department of Public Health Fr Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 administrative orders, etc. for this requirement. Applicable (Description Requirement and Citation) Click here to enter text. Reason for Noncompliance Click here to enter text. Narrative Description Compliance Will Achieved be How Click here to enter text. Provide a schedule of corrective leading action(s), including an enforceable to compliance, including a date for sequence of actions final compliance. with milestones, Corrective Action Date to be Achieved Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. First Progress Report Frequency of Submittals will be Submitted Thereafter: on: Click here to enter text . Click here to enter text . Form Revised August 2023 AIRS ID: 001 - 9E2C - 001 14 of 4 COLORADO Department of Public Health Fr Environment a COLORADO Air Pollution Control Division Department of Public Health Er Environment Fugitive Particulate Matter Sources Form OP -310 Title V Operating Permit Number: Initial AIRS ID Number: 123 - 9E2C - 006 1. Instructions Included on the Colorado Air Pollution Control Division Website is an instruction sheet (OP -310A) for this form. Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section I i. B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Information Facility Identifier (example: S001) Unpaved Haul Roads Dates Commenced Commenced construction: Click here to enter text. operation: Click here to enter text. Underlying Construction Permit Yes 15WE1395 XI ❑ No Permit Number: Description General Description of Fugitive Dust Sources: Unpaved Haul Roads 3. State and Federal Regulations 40 Subpart CFR Part OOO 60 Subject Click here to enter text. x Not Subject 40 CFR Subpart Part 60 p Y Subject Click here to enter text. [X Not Subject Colorado No. Regulation 1 Section III.D ❑ Subject Click here to enter text. x Not Subject If applicable subject, attach most current approved Fugitive Particulate Emission Control Plan if Colorado No. Requirements 1 Regulation Opacity P y These requirements are identified in q Form OP -400. x Subject Not Subject Other (specify) Click here to enter text. 4. Criteria Pollutant Emission Information Pollutant Potential -to -Emit (tpy) Permitted Limitation (tpy) PM 3.1 3.1 PM10 3.1 3.1 PM2.5 PTE Limit Form Revised August 2023 AIRS ID: 123 - 9E2C - 006 Page I lof4 COLORADO Department of Public Health Fr Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -310 5. Topsoil Xl Check this box if removal/stockpile of topsoil does not occur at this facility and proceed to Section 6 Removal Stockpile(s) Topsoil Removed Daily: Tons Maximum Stored Tons Stored Annual: Tons Controls Controls ❑ Watering Moist Material Chemical Stabilizer ❑ Enclosure Complete Water Spray (select one) Partial Revegetation Other: Specify Other: Specify 6. Overburden xl Check this box if removal/stockpile of overburden does not occur at this facility and proceed to Section 7 Removal Stockpile(s) Equipment Used for Removal: Equipment Maximum Stored Tons Stored Tons Daily: Tons Dragline Removed Annual: Tons Controls ❑ Watering Drop Height: Feet Chemical Stabilizer Scraper Hours Daily: Hours Enclosure ❑ Complete Operated Annually: Hours (select one) Partial Moist Material Revegetation Controls Water Spray Other: Specify Other: Specify 7. Drilling a Blasting xl Check this box if drilling/blasting does not occur at this facility and proceed to Section 8. Otherwise, select all activities that occur below. ❑ Drilling ❑ Blasting Number Holes of Drilled Daily: Number of Holes Number of Blasts Daily: Number of Blasts Annual: Number of Holes Annual: Number of Blasts Controls Blast Area (acres) Acres Water Injection Blasting Material Type of Blasting Material Bag Collectors Blasting Used Material Daily: Specify Units Other: Specify Annually: Specify Units Form Revised August 2023 AIRS ID: 123 - 9E2C - 006 Page 12of4 COLORADO Department of Public Health £r Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -310 8. Raw Material xl Check this box if removal and/or stockpile of raw material does not occur at this facility and proceed to Section 9. Removal Stockpile(s) Material Removed Daily: Tons Maximum Stored: Tons: Tons Stored Annual: Tons Size (acres): Acres Max Drop Height Feet Controls ❑ Watering Specific Content Moisture o Percent ( ) Chemical Stabilizer ❑ Compacting of Piles Controls ❑ Moist Material ❑ Enclosure Complete Water Spray (select one) Partial Revegetation ❑ Other: Specify ❑ Other: Specify 9. Conveyors a Transfer Points xi Check this box if conveying and/or transfer of material does not occur at this facility and proceed to Section 10. Conveying Material Conveyed Daily: Tons Annual: Tons Controls Enclosure one) Complete ❑ (select Partial Other: Specify Transfer Points Number of Number of Transfer Points Transfer Points Controls ❑ Watering Chemical Stabilizer Enclosure Complete (select one) ❑ Partial Other: Specify 10. Material Transport xl Check this box if material transport does not occur at this facility and proceed to Section 12. Vehicle 1 Vehicle 2 Vehicle 3 Vehicle 4 Material Transport: Tons /year Road (select Type one) Traveled on Paved Paved Paved Paved Unpaved Unpaved Unpaved Unpaved Haut Vehicle Capacity Tons Tons Tons Tons Haul Vehicle Empty Weight Tons Tons Tons Tons Trips/Day Trips/Day Trips/Day Trips/Day Max Number of Trips Per day Road Length (avg. one way) Miles Miles Miles Miles Speed Limit on Road MPH MPH MPH MPH Additional Material Transport if needed Form Revised August 2023 AIRS ID: 123 - 9E2C - 006 Page 1 3of4 COLORADO Department of Public Health £r Environment COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -310 Vehicle 5 Vehicle 6 Vehicle 7 Vehicle 8 ❑ Paved Paved Paved Paved Road T e Traveled on yp ❑ Unpaved Unpaved ❑ Unpaved Unpaved Haul Vehicle Capacity Tons Tons Tons Tons Haul Vehicle Empty Weight Tons Tons Tons Tons Trips/Day Trips/Day Trips/Day Trips/Day Max Number of Trips Per day Road Length (avg. one way) Miles Miles Miles Miles Speed Limit on Road MPH MPH MPH MPH Controls Used Watering Graveled Chemical Stabilizer Unpaved XI None ❑ As Needed XI No Yes: Type X1 No ❑ Yes ❑ Frequent: Times /Day Paved Street Sweeping: xl No ❑ Yes 11. Compliance and Monitoring I have filled out and attached Form OP -400 Compliance and Monitoring with all known applicable requirements for this source: x Yes ❑ No 12. Required Attachments The following must be attached in order for the application to be considered administratively complete (unless previously submitted): Emission Calculations Fugitive Particulate Emission Control Plan (If applicable) Form Revised August 2023 Page 14 of 4 AIRS ID: 123 - 9E2C - 006 COLORADO Department of Public Health £r Environment S COLORADO Air Pollution Control Division Department of Public Health & Environment Compliance and Monitoring Form OP -400 Title V Operating Permit Number: Initial AIRS ID Number: 001 - 9E2C - 006 1. Instructions Complete this form and attach it to the completed corresponding OP -300 series form for the applicable emission unit. Each OP -300 series form must be accompanied by a Compliance and Monitoring form (OP -400). Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. . B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Emission Unit Information Facility (example: Identifier 5001) Haul Roads 3. Applicable Requirements Identify recordkeeping, attach each additional applicable and descriptions. reporting requirement requirements, for the emission and the unit, basis any for the associated requirement. compliance If monitoring, more space is needed, Emission Limitations (tpy, lb/hr, lb/MMBtu, gr/dscf, etc.) FUG FUG PM: PM -10: 3.1 1.1 tpy tpy Opacity Visible periods exceed using In a. shall, control maintenance include, procedures, addition, At EPA all to emissions of 30% practices startup, Method times, the but opacity the extent procedures is and including not following inspection must 9. for limited process for (Reference: practicable, minimizing not more exceed modification, requirements periods are to, of than being monitoring the be emissions. Regulation of twenty six source. minutes start-up, maintained used of will or results, percent Regulation (Reference: adjustment Determination Number be in shutdown, and based any (20%) opacity operated sixty 1, Number on Regulation opacity of Section and information observations, consecutive of control 6, malfunction, in whether II.A.1. during .A.1. a Part manner Number equipment A, or available normal minutes. 6t 4.) Subpart not review the consistent 6, acceptable Part visible facility, operation to of Opacity A, operating the A. General emissions with General and Division, must operating of good the control and be Provisions, Provisions source. must air which determined maintenance equipment pollution and not may apply During from Form Revised August 2023 AIRS ID: 001 - 9E2C - 006 Page I1of4 COLORADO Department of Public Health Fr Environment TM 40 CFR 60.11 b. No article, machine, equipment, or process shall be used to conceal an emission that would otherwise constitute a violation of an applicable standard. Such concealment includes, but is not limited to, the use of gaseous diluents to achieve compliance with an opacity standard or with a standard that is based on the concentration of a pollutant in the gases discharged to the atmosphere. (S 60.12) COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Operational Limitation(s) (hrs/yr, MMscf/yr, lb/yr, etc.) N/A Other Requirements List all other applicable requirements for this emission point. Regulation Number 2 Regulation Number 3 4. Monitoring Requirements Complete the following monitoring questions about the emission unit. Continuous Emission Monitoring Requirements? Yes X No Form Revised August 2023 Page 12 of 4 AIRS ID: 001 - 9E2C - 006 COLORADO Department of Public Health Fr Environment S COLORADO Air Pollution Control Division Department of Public Health Et Environment Pollutant(s) or Parameter(s): Click here to enter text. Requirement(s): Click here to enter text. Continuous Emission Monitoring System (CEMS) Predictive Emission Monitoring System (PEMS) Continuous Emission Rate Monitoring System (CERMS) Other (describe): Click here to enter text. Form OP -400 Periodic Compliance Testing? Yes x No Pollutant(s): Click here to enter text. Frequency: Click here to enter text. Date of last Division -approved test: Click here to enter text . Other? Yes x No Describe: Click here to enter text. Frequency: Click here to enter text. 5. Compliance Status and Commitment Indicate the compliance status of the emission point as of the date of submittal: In compliance with all applicable requirements Not in compliance (fill out Section 6 below if schedule of compliance is required) For applicable requirements this emission point is currently in compliance with: x The emission point will continue to comply with these requirements For applicable requirements that will become effective during this permit term: The emission point will comply with these requirements in a timely basis x x 6. Schedule of Compliance Complete required. applicable administrative Also, this requirement. section complete orders, if "Not Attach etc. this in section for this compliance" copies requirement. if of the applicant any was judicial answered is required consent in Section to submit decrees, 5 and a compliance a schedule schedule of of orders compliance compliance on consent, is by an or (Description Applicable Requirement and Citation) Click here to enter text. Reason for Noncompliance Click here to enter text. Narrative Compliance Description Achieved Will be How Click here to enter text. Provide a schedule of corrective leading action(s), to compliance, including an enforceable including a date for sequence final compliance. of actions with milestones, Corrective Action Date to be Achieved Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Form Revised August 2023 AIRS ID: 001 - 9E2C - 006 Page 13of4 COLORADO Department of Public Health Fr Environment a COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Click here to enter text Click here to enter text. Click here to enter text. Click here to text. enter Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. First Progress Frequency Report of Submittals will be Submitted Thereafter: on: click Click here here to enter text to enter text. . Form Revised August 2023 AIRS ID: 001 - 9E2C - 006 14 of 4 COLORADO Department of Public Health Fr Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Reciprocating Internal Combustion Engine Form OP -302 Title V Operating Permit Number: Initial AIRS ID Number: 123 - 9E2C - 009 1. Instructions Included on the Colorado Air Pollution Control Website is an instruction sheet (Form OP -302A) for this engine form. Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Engine Information Facility (example: Identifier S001) N/A Engine Information Manufacturer Model Serial Number Isuzu BP-4LE2X 7253219 Dates Manufacture Order Date First Date Date engine operation commenced last date: Click was P modified/reconstructed: date: first date: 2019 here August construction: located g to enter to Colorado: 1, 2022 Click Click text. here 2019 here to enter text. to enter text. Construction Underlying Permit Yes Permit 15WE1395 (if applicable): Click here to enter type and package. X ❑No Permit General Number: Exemptions List . information): any state exemptions that Click here to apply enter to this engine (See Instruction Sheet text. for more 3. Engine Characteristics Function X Standard ❑ Peaking Power ❑ Emergency ❑ Fire Pump Black Start Other (specify) Click here to enter text. Engine Characteristics (Check all that apply) Spark Ignition x Compression Ignition Dual Fuel Lean Burn Rich Burn x Turbocharged g Low NOx Design g 2 -Stroke 4 -Stroke Air Fuel Ratio Controller (AFRC) Permitted Maximum Hours 7,500 hr/yr Horsepower Nameplate Site -rated Horsepower Horsepower: P 66 (if applicable): 66 General Description of Equipment One of two primary power generators that provide electrical power to the site. Form Revised August 2023 AIRS ID: 123 - 9E2C - 009 Page I1of4 COLORADO Department of Public Health £t Environment S COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -302 Should the Division include an alternative operating scenario (AOS) in the permit? x Yes Date of last AOS replacement (if applicable): August 1, 2022 Last AOS replacement type (if applicable): Temporary x Permanent No 4. Fuel Information Types of all Fuels that (check apply) x Diesel Natural Gas Propane Landfill Gas Other (specify): Click here to enter text . Permit Throughput Limitation 25,171 gal/yr (gal/hour Fuel Consumption or scf/hour) 3.4 gal/hr Brake Specific Consumption applicable) Fuel (if BSFC (Btu/hp-hr): 7,000 Fuel (specify Heat Content units) 137,000 Btu/gal Displacement Displacement Number of Cylinders: (specify 4 units, typically L/cyl or cc): 0.54 L/cyl 5. State and Federal Regulations Rule Applicability How will you comply with this Regulation? 40 Subpart CFR P Part 63 ZZZZ Subject Not Subject Comply with requirements of NSPS IIII. IX] 40 CFR Subpart Part 1111 60 Subject Not Subject See - - - - - - Permit Emissions Oxides Emissions per Emissions grams All (1) (2) maximum Compliance of or the All configured, specifications manufacturer. If the that backpressure shall the in the 15WE1395, hp fuel Sulfur Have Division engines filter notifies a engine be -hour. per fuel combined used readily a kept of of of content must hp aromatic minimum shall specifications for and operated, Non Carbon Particulate -hour. shall is the Issuance accessible and limit of inspection control equipped be -Methane any shall shall be installed owner meet instructions compound of Monoxide cetane demonstrated corrective the not not devices and 6, Matter the or provided location with engine Condition Hydrocarbons exceed upon operator following exceed index maintained with shall content provided a action shall request. must diesel a is and 3.5 15 of by by backpressure approached. not when 7 not 40 be grams specifications: ppm. maintaining the taken exceed of made according particulate and exceed or installed, by 35% supplier the have the available after Nitrogen per by high 3.7 engine a Records hp 0.30 volume. to monitor -hour. grams copies on the filter, the -site to x Form Revise August 2023 AIRS ID: 123 - 9E2C - 009 Page 12of4 COLORADO Department of Public Health Fr Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -302 backpressure that the high monitor backpressure has notified limit is the approached. owner or operator 40 Subpart CFR Part 60 JJJJ ❑ Subject Click here to enter text. x Not Subject Colorado No. 26 Regulation Part B Subject Click here to enter text. x Not Subject Reasonably Control (RACT) Technology Available See Permit 15WE1395, Issuance 6, Condition 9 x Subject - Compliance with the requirements of NSPS Subpart IIII was Not Subject assumed to be RACT for this source. Note equipment that the applicant in a nonattainment may be asked or attainment/maintenance to provide a RACT analysis if area. new or modified Compliance Assurance Monitoring (CAM) If subject, addressed attach in the permit Form OP or -203 CAM unless CAM a CAM plan is not due has already yet. been Subject x Not Subject Colorado No. Requirements 1 Regulation Opacity These requirements are identified in Form OP -400. X Subject Not Subject Other (specify) Click here to enter text. Colorado Regulation No. 1 PM Requirements Colorado 1 SO2 Requirements Regulation No. Subject XI Subject ❑ Not Subject x Not Subject Colorado Regulation No. 6 PM Requirements Colorado Regulation 6 SO2 Requirements No. Subject x Subject Not Subject x Not Subject 6. Control Device Information Is any emission If yes, describe control control equipment device(s) or below: practice used to reduce emissions? Yes No ❑ x Control Description Device Click here to describe control device. Pollutant PM PM10 PM2.5 SO2 NOx VOC CO Lead Enter Other Control Efficiency I Text Text Text Text Text Text Text Text Text Controlled HAP Individual All HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Control Efficiency I Text Text Text Text Text Text Text Text Text 7. Criteria Pollutant Emission Information Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Factor Source (e.g. AP -42, manufacturer, source test, etc. Uncontrolled Potential Emit t (tpy) -to- Permitted Limitation t ( pY) Form Revise August 2023 AIRS ID: 123 - 9E2C - 009 Page 13of4 COLORADO Department of Public Health £t Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -302 PM 2.20E-03 EF lb/hp-hr AP -42 0.46 0.46 PMio 2.20E-03 EF lb/hp-hr AP -42 0.46 0.46 PM2,5 2.20E-03 EF lb/hp-hr AP -42 0.46 0.46 SO2 2.05E-03 EF lb/hp-hr AP -42 0.43 0.43 NOx 3.10E-02 EF lb/hp-hr AP -42 6.49 6.49 VOC 2.51E-03 EF lb/hp-hr AP -42 0.53 0.53 CO 6.68E-03 EF lb/hp-hr AP -42 1.40 1.40 Lead EF EF EF Units EF Source PTE Limit Enter Pollutant EF EF EF Units EF Source PTE Limit 8. Hazardous Air Pollutant (HAP) Emission Information Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Factor Source (e.g. AP manufacturer, source etc. -42, test, Uncontrolled Potential Emit(tpy)t -to- Permitted Limitation ( py) Formaldehyde 1.18E-03 EF lb/MMBtu AP -42 1.73E-03 1.73E-03 Acetaldehyde 7.67E-04 EF lb/MMBtu AP -42 1.12E-03 1.12E-03 Acrolein 9.25E-05 EF lb/MMBtu AP -42 1.36E-04 1.36E-04 Benzene 9.33E-04 EF lb/MMBtu AP -42 1.37E-03 1.37E-03 Hexane EF EF EF Units EF Source PTE PTE 4.09E-04 EF lb/MMBtu AP -42 6.00E-04 6.00E-04 Toluene Xylene 2.85E-04 EF lb/MMBtu AP -42 4.18E-04 4.18E-04 1,3 -Butadiene 3.91E-05 EF lb/MMBtu AP -42 5.73E-05 5.73E-05 PAH 1.68E-04 EF lb/MMBtu AP -42 2.46E-04 2.46E-04 Total Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit 9. Compliance and Monitoring I have filled out and attached Form OP -400 Compliance and Monitoring with all known applicable requirements for this emission unit: xi Yes No 10. Required Attachments The following must be attached in order for the application to be considered administratively complete (unless previously submitted): Emission Calculations Manufacturer Specifications or Contract Guarantee for Control Equipment (if applicable) Form Revise August 2023 AIRS ID: 123 - 9E2C - 009 Page 14of4 COLORADO Department of Public Health £t Environment S COLORADO Air Pollution Control Division Department of Public Health & Environment Compliance and Monitoring Form OP -400 Title V Operating Permit Number: Initial AIRS ID Number: 001 - 9E2C - 009 1. Instructions Complete this form and attach it to the completed corresponding OP -300 series form for the applicable emission unit. Each OP -300 series form must be accompanied by a Compliance and Monitoring form (OP -400). Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. . B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Emission Unit Information Facility (example: Identifier 5001) 49 kW RICE 3. Applicable Requirements Identify recordkeeping, attach each additional applicable and descriptions. reporting requirement requirements, for the emission and the unit, basis any for the associated requirement. compliance If monitoring, more space is needed, Emission Limitations (tpy, lb/hr, lb/MMBtu, gr/dscf, etc.) PM: PM PM SO2: NOx: VOC: CO: -10: -2.5: 0.46 0.4 6.5 0.5 1.4 0.46 0.46 tpy tpy tpy tpy tpy tpy tpy Opacity Visible periods exceed using In a. shall, control maintenance include, procedures, addition, At EPA all to emissions of 30% times, practices startup, Method the but opacity the extent is and procedures including not following inspection must 9. for limited process for (Reference: practicable, minimizing not more exceed modification, requirements periods are to, of than being monitoring the be emissions. Regulation of twenty six source. minutes start-up, maintained used of will or results, percent Regulation (Reference: adjustment Determination Number be in shutdown, and based any (20%) opacity operated sixty 1, Number on Regulation opacity of Section and information observations, consecutive of control 6, malfunction, in whether II.A.1. during .A.1. a Part manner Number equipment A, or available normal minutes. 6t 4.) Subpart not review the consistent 6, acceptable Part visible facility, operation to of Opacity A, operating the A. General emissions with General and Division, must operating of good the control and be Provisions, Provisions source. must air which determined maintenance equipment pollution and not may apply During from Form Revised August 2023 AIRS ID: 001 - 9E2C - 009 Page I1of4 COLORADO Department of Public Health Fr Environment TM 40 CFR 60.11 b. No article, machine, equipment, or process shall be used to conceal an emission that would otherwise constitute a violation of an applicable standard. Such concealment includes, but is not limited to, the use of gaseous diluents to achieve compliance with an opacity standard or with a standard that is based on the concentration of a pollutant in the gases discharged to the atmosphere. (S 60.12) COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Operational Limitation(s) (hrs/yr, MMscf/yr, lb/yr, etc.) 6,378 hrs/yr Other Requirements List all other applicable requirements for this emission point. RACT Regulation Number 2 Regulation Number 3 NSPS IIII 4. Monitoring Requirements Complete the following monitoring questions about the emission unit. Continuous Emission Monitoring Requirements? Yes X No Form Revised August 2023 Page 12 of 4 AIRS ID: 001 - 9E2C - 009 COLORADO Department of Public Health Fr Environment S COLORADO Air Pollution Control Division Department of Public Health Et Environment Pollutant(s) or Parameter(s): Click here to enter text. Requirement(s): Click here to enter text. Continuous Emission Monitoring System (CEMS) Predictive Emission Monitoring System (PEMS) Continuous Emission Rate Monitoring System (CERMS) Other (describe): Click here to enter text. Form OP -400 Periodic Compliance Testing? Yes x No Pollutant(s): Click here to enter text. Frequency: Click here to enter text. Date of last Division -approved test: Click here to enter text . Other? Yes x No Describe: Click here to enter text. Frequency: Click here to enter text. 5. Compliance Status and Commitment Indicate the compliance status of the emission point as of the date of submittal: In compliance with all applicable requirements Not in compliance (fill out Section 6 below if schedule of compliance is required) For applicable requirements this emission point is currently in compliance with: x The emission point will continue to comply with these requirements For applicable requirements that will become effective during this permit term: The emission point will comply with these requirements in a timely basis x x 6. Schedule of Compliance Complete required. applicable administrative Also, this requirement. section complete orders, if "Not Attach etc. this in section for this compliance" copies requirement. if of the applicant any was judicial answered is required consent in Section to submit decrees, 5 and a compliance a schedule schedule of of orders compliance compliance on consent, is by an or (Description Applicable Requirement and Citation) Click here to enter text. Reason for Noncompliance Click here to enter text. Narrative Compliance Description Achieved Will be How Click here to enter text. Provide a schedule of corrective leading action(s), to compliance, including an enforceable including a date for sequence final compliance. of actions with milestones, Corrective Action Date to be Achieved Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Form Revised August 2023 AIRS ID: 001 - 9E2C - 009 Page 13of4 COLORADO Department of Public Health Fr Environment a COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Click here to enter text Click here to enter text. Click here to enter text. Click here to text. enter Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. First Progress Frequency Report of Submittals will be Submitted Thereafter: on: click Click here here to enter text to enter text. . Form Revised August 2023 AIRS ID: 001 - 9E2C - 009 14 of 4 COLORADO Department of Public Health Fr Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Reciprocating Internal Combustion Engine Form OP -302 Title V Operating Permit Number: Initial AIRS ID Number: 123 - 9E2C - 010 1. Instructions Included on the Colorado Air Pollution Control Website is an instruction sheet (Form OP -302A) for this engine form. Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Engine Information Facility (example: Identifier S001) N/A Engine Information Manufacturer Model Serial Number Kohler KD13404TCR/22N 5133303960 Dates Manufacture Order Date First Date Date engine operation commenced last date: Unknown was modified date: date: first 11/2021 construction: /reconstructed: (rental) located October to Colorado: 23 11/2021 2023 N/A 2021 Construction Underlying Permit Yes o 15WE1395 (if applicable): Click here to enter type and package. x ll N Permit General Number: Permit Exemptions List any state exemptions that apply information): Click here to enter to this engine (See Instruction Sheet for more text. 3. Engine Characteristics Function x Standard Peaking Power Emergency Fire Pump Black Start Other (specify) Click here to enter text. Engine Characteristics (Check all that apply) Spark Ignition x Compression Ignition Dual Fuel Lean Burn Rich Burn x Turbocharged g Low NOx Design g 2 -Stroke XI 4 -Stroke Air Fuel Ratio Controller (AFRC) Permitted Maximum Hours 5,445 hr/yr Horsepower Nameplate Site -rated Horsepower: 78 Horsepower (if applicable): P 78 General Description of Equipment One of two primary power generators that provide electrical power to the site. Form Revised August 2023 AIRS ID: 123-9E2C-010 Page I1of4 COLORADO Department of Public Health £t Environment S COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -302 Should the Division include an alternative operating scenario (AOS) in the permit? x Yes Date of last AOS replacement (if applicable): October 23, 2023 Last AOS replacement type (if applicable): Temporary x Permanent No 4. Fuel Information Types of all Fuels that (check apply) x Diesel Natural Gas Propane Landfill Gas Other (specify): Click here to enter text . Permit Throughput Limitation 21,630 (gal/hour Fuel Consumption or scf/hour) 4 gal/hr Brake Specific Consumption applicable) Fuel (if BSFC (Btu/hp-hr): 7,000 Fuel (specify Heat Content units) 137,000 Btu/gal Displacement Displacement Number of Cylinders: (specify 4 units, typically L/cyl or cc): 0.84 L/cyl 5. State and Federal Regulations Rule Applicability How will you comply with this Regulation? 40 Subpart CFR P Part 63 ZZZZ Subject Not Subject Comply with requirements of NSPS IIII. IX] 40 CFR Subpart Part 1111 60 Subject Not Subject See - - - - - - Permit Emissions Oxides hour. Emissions per Emissions grams All (1) (2) maximum Compliance of or the All configured, specifications manufacturer. If the that backpressure the in the 15WE1395, fuel Sulfur Have engines hp Division filter notifies a -hour. per fuel engine combined used readily a of of of hp content aromatic must minimum shall specifications for and operated, Non Carbon Particulate -hour. shall is the limit Issuance accessible and inspection control equipped be -Methane shall shall be installed owner meet instructions compound of Monoxide cetane demonstrated the not not devices and or 6, Matter the location provided with engine Condition Hydrocarbons exceed upon operator following exceed index maintained with shall content provided a shall request. must diesel a is and 3.0 15 of by by backpressure approached. not when 7 not 40 be grams specifications: ppm. maintaining the exceed of made according particulate and exceed or installed, by 35% supplier the have the available Nitrogen per by high 3.7 engine a Records kilowatt- 0.22 volume. to monitor grams copies on filter, the -site to x Form Revise August 2023 AIRS ID: 123 - 9E2C - 010 Page 12of4 COLORADO Department of Public Health Fr Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -302 shall backpressure that the be kept high of any monitor backpressure corrective has notified action limit is taken after the the owner or operator approached. 40 CFR Subpart Part JJJJ 60 ❑ Subject Click here to enter text. x Not Subject Colorado No. Regulation 26 Part B ❑ Subject Click here to enter text. x Not Subject Reasonably Control Available Technology See Permit 15WE1395, Issuance 6, Condition 9 [X Subject - Compliance with the requirements of NSPS Subpart IIII was ❑ Not Subject assumed to be RACT for this source. (RACT) Note equipment that the applicant may in a nonattainment be asked or to provide a RACT analysis if attainment/maintenance area. new or modified Compliance Monitoring Assurance (CAM) If subject, addressed attach in the Form OP -203 CAM unless CAM permit or a CAM plan is not due has already yet. been Subject x Not Subject Colorado No. Requirements 1 Regulation Opacity P Y x Subject These requirements are identified in Form OP -400. q ❑ Not Subject Other (specify) Click here to enter text. Colorado 1 PM Regulation No. Requirements Colorado Regulation 1 SO2 Requirements No. Subject x Subject ❑ Not Subject xl Not Subject Colorado 6 PM Regulation Requirements No. Colorado Regulation No. 6 SO2 Requirements Subject Fry Subject Not Subject x Not Subject 6. Control Device Information If Is any emission yes, describe control equipment control device(s) or below: practice used to reduce emissions? Yes No ❑ >< Control Description Device Click here to describe control device. Pollutant PM PM10 PM2.5 SO2 NOx VOC CO Lead Enter Other Control Efficiency I Text Text Text Text Text Text Text Text Text Controlled HAP Individual All HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Enter HAP Control Efficiency I Text Text Text Text Text Text Text Text Text 7. Criteria Pollutant Emission Information Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Factor Source (e.g. AP -42, manufacturer, source test, etc. Uncontrolled Potential -to- Emit t (tpy) Permitted Limitation t ( PY) Form Revise August 2023 AIRS ID: 123-9E2C-010 Page 13of4 COLORADO Department of Public Health £t Environment COLORADO Air Pollution Control Division Department of Public Health Et Environment Form OP -302 PM 2.20E-03 EF lb/hp-hr AP -42 0.47 0.47 PMio 2.20E-03 EF lb/hp-hr AP -42 0.47 0.47 PM2,5 2.20E-03 EF lb/hp-hr AP -42 0.47 0.47 SO2 2.05E-03 EF lb/hp-hr AP -42 0.43 0.43 NOx 3.10E-02 EF lb/hp-hr AP -42 6.56 6.56 VOC 2.51E-03 EF lb/hp-hr AP -42 0.53 0.53 CO 6.68E-03 EF lb/hp-hr AP -42 1.41 1.41 Lead EF EF EF Units EF Source PTE Limit Enter Pollutant EF EF EF Units EF Source PTE Limit 8. Hazardous Air Pollutant (HAP) Emission Information Pollutant Uncontrolled Emission Factors Controlled Emission Factors Emission Factors Units Emission Factor Source (e.g. AP manufacturer, source etc. -42, test, Uncontrolled Potential Emit t (tpy) -to- Permitted Limitation t ( py) Formaldehyde 1.18E-03 EF lb/MMBtu AP -42 6.36E-04 6.36E-04 Acetaldehyde 7.67E-04 EF lb/MMBtu AP -42 4.13E-04 4.13E-04 Acrolein 9.25E-05 EF lb/MMBtu AP -42 4.98E-05 4.98E-05 Benzene 9.33E-04 EF lb/MMBtu AP -42 5.03E-04 5.03E-04 Hexane EF EF EF Units EF Source PTE Limit 4.09E-04 EF lb/MMBtu AP -42 2.20E-04 2.20E-04 Toluene Xylene 2.85E-04 EF lb/MMBtu AP -42 1.54E-04 1.54E-04 1,3 -Butadiene 3.91E-05 EF lb/MMBtu AP -42 2.11E-05 2.11E-05 PAH 1.68E-04 EF lb/MMBtu AP -42 9.05E-05 9.05E-05 Total Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit Enter HAP EF EF EF Units EF Source PTE Limit 9. Compliance and Monitoring I have filled out and attached Form OP -400 Compliance and Monitoring with all known applicable requirements for this emission unit: xi Yes No 10. Required Attachments The following must be attached in order for the application to be considered administratively complete (unless previously submitted): Emission Calculations Manufacturer Specifications or Contract Guarantee for Control Equipment (if applicable) Form Revise August 2023 AIRS ID: 123-9E2C-010 Page 14of4 COLORADO Department of Public Health £t Environment S COLORADO Air Pollution Control Division Department of Public Health & Environment Compliance and Monitoring Form OP -400 Title V Operating Permit Number: Initial AIRS ID Number: 001 - 9E2C - 010 1. Instructions Complete this form and attach it to the completed corresponding OP -300 series form for the applicable emission unit. Each OP -300 series form must be accompanied by a Compliance and Monitoring form (OP -400). Refer to the instruction sheet or contact the Division with questions. Any form with missing information may be determined administratively incomplete and may result in inability to grant the application shield of Regulation No. 3, Part C, Section II.B. . B. Renewal and modification applications for equipment already included in the Title V permit are allowed to only complete portions of the form affected by the modification. Note that if using copy and paste; the applicant must paste as plain text. See "General Instructions" document for more details. 2. Emission Unit Information Facility (example: Identifier 5001) 58 kW RICE 3. Applicable Requirements Identify recordkeeping, attach each additional applicable and descriptions. reporting requirement requirements, for the emission and the unit, basis any for the associated requirement. compliance If monitoring, more space is needed, Emission Limitations (tpy, lb/hr, lb/MMBtu, gr/dscf, etc.) PM: PM PM SO2: NOx: VOC: CO: -10: -2.5: 0.47 0.4 6.6 0.5 1.4 0.47 0.47 tpy tpy tpy tpy tpy tpy tpy Opacity Visible periods exceed using In a. shall, control maintenance include, procedures, addition, At EPA all to emissions of 30% times, practices startup, Method the but opacity the extent is and procedures including not following inspection must 9. for limited process for (Reference: practicable, minimizing not more exceed modification, requirements periods are to, of than being monitoring the be emissions. Regulation of twenty six source. minutes start-up, maintained used of will or results, percent Regulation (Reference: adjustment Determination Number be in shutdown, and based any (20%) opacity operated sixty 1, Number on Regulation opacity of Section and information observations, consecutive of control 6, malfunction, in whether II.A.1. during .A.1. a Part manner Number equipment A, or available normal minutes. 6t 4.) Subpart not review the consistent 6, acceptable Part visible facility, operation to of Opacity A, operating the A. General emissions with General and Division, must operating of good the control and be Provisions, Provisions source. must air which determined maintenance equipment pollution and not may apply During from Form Revised August 2023 AIRS ID: 001 - 9E2C - 010 Page I1of4 COLORADO Department of Public Health Fr Environment TM 40 CFR 60.11 b. No article, machine, equipment, or process shall be used to conceal an emission that would otherwise constitute a violation of an applicable standard. Such concealment includes, but is not limited to, the use of gaseous diluents to achieve compliance with an opacity standard or with a standard that is based on the concentration of a pollutant in the gases discharged to the atmosphere. (S 60.12) COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Operational Limitation(s) (hrs/yr, MMscf/yr, lb/yr, etc.) 5,445 hr/yr Other Requirements List all other applicable requirements for this emission point. RACT Regulation Number 2 Regulation Number 3 NSPS IIII 4. Monitoring Requirements Complete the following monitoring questions about the emission unit. Continuous Emission Monitoring Requirements? Yes X No Form Revised August 2023 Page 12 of 4 AIRS ID: 001 - 9E2C - 010 COLORADO Department of Public Health Fr Environment S COLORADO Air Pollution Control Division Department of Public Health Et Environment Pollutant(s) or Parameter(s): Click here to enter text. Requirement(s): Click here to enter text. Continuous Emission Monitoring System (CEMS) Predictive Emission Monitoring System (PEMS) Continuous Emission Rate Monitoring System (CERMS) Other (describe): Click here to enter text. Form OP -400 Periodic Compliance Testing? Yes x No Pollutant(s): Click here to enter text. Frequency: Click here to enter text. Date of last Division -approved test: Click here to enter text . Other? Yes x No Describe: Click here to enter text. Frequency: Click here to enter text. 5. Compliance Status and Commitment Indicate the compliance status of the emission point as of the date of submittal: In compliance with all applicable requirements Not in compliance (fill out Section 6 below if schedule of compliance is required) For applicable requirements this emission point is currently in compliance with: x The emission point will continue to comply with these requirements For applicable requirements that will become effective during this permit term: The emission point will comply with these requirements in a timely basis x x 6. Schedule of Compliance Complete required. applicable administrative Also, this requirement. section complete orders, if "Not Attach etc. this in section for this compliance" copies requirement. if of the applicant any was judicial answered is required consent in Section to submit decrees, 5 and a compliance a schedule schedule of of orders compliance compliance on consent, is by an or (Description Applicable Requirement and Citation) Click here to enter text. Reason for Noncompliance Click here to enter text. Narrative Compliance Description Achieved Will be How Click here to enter text. Provide a schedule of corrective leading action(s), to compliance, including an enforceable including a date for sequence final compliance. of actions with milestones, Corrective Action Date to be Achieved Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. Form Revised August 2023 AIRS ID: 001 - 9E2C - 010 Page 13of4 COLORADO Department of Public Health Fr Environment a COLORADO Air Pollution Control Division Department of Public Health Er Environment Form OP -400 Click here to enter text Click here to enter text. Click here to enter text. Click here to text. enter Click here to enter text. Click here to enter text. Click here to enter text. Click here to enter text. First Progress Frequency Report of Submittals will be Submitted Thereafter: on: click Click here here to to enter enter text . text . Form Revised August 2023 AIRS ID: 001 - 9E2C - 010 14 of 4 COLORADO Department of Public Health Fr Environment APPENDIX B. FACILITY PLOT PLAN Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants B-1 APPENDIX C. EJ SUMMARY Biochar Now, LLC / Initial Title V Permit Application Trinity Consultants C-2 From: Matthew Petrosky Sent: Wednesday, November 1, 2023 4:04 PM To: cdphe_apcd_ejreports@state.co.us Cc: George lwaszek; jgaspard@biocharnow.com Subject Biochar Now Initial Title V EJ Summary Attachments: Biochar Now Environmental Justice Report (2023-1101).pdf Hello, I am submitting the attached Environmental Justice Summary on behalf of Biochar Now, LLC, for their Initial Title V Application. Included in the attachment is a PDF of the facility's Environmental Justice Report, answers to the Supplemental Information Google Form, and an aerial map of the facility. Please reach out with any questions. Thank you, Matt Petrosky Associate Consultant P 720.638.7647 I M 814.691.1227 Email: Matthew.Petrosky@trinityconsultants.com 1391 North Speer Blvd, Suite 350 I Denver, Colorado 80204 Trinity trans u« ants Connect with us: LinkedIn / Facebook / Twitter / YouTube / trinityconsultants.com Stay current on environmental issues. Subscribe today to receive Trinity's free EHS Quarterly. Trinity Consultants -S 1391 N Speer Blvd, Ste 350, Denver, CO 80204 / P 720.638.7647 / trinityconsultants.com October 31, 2023 DELIVERED VIA ELECTRONIC MAIL ONLY Colorado Department of Public Health and Environment Air Pollution Control Division (APCD) 4300 Cherry Creek Drive South, APCD-SS-B1 Denver, CO 80246-1530 RE' Environmental Justice Summary - In Support of Initial Title V Application, AIRS 123-9E2C Biochar Now, LLC — Berthoud Plant Dear Sir or Madam: On behalf of Biochar Now, LLC, Trinity Consultants is submitting the enclosed Environmental Justice Summary (EJ Summary) for the Biochar Now Berthoud Plant at 19500 Weld County Road 7, located in Census Block Group 081230021032 in Weld County. Biochar Now operates under Construction Permit 15WE1395, Issuance 6, with enforceable limits for NOx emissions greater than 25 tons per year. The reclassification of the Denver Metro -North Front Range (DMNFR) nonattainment area to severe non -attainment for the 2008 8 -hour ozone standard on November 7, 2022, lowered major source thresholds for NOx and VOC emissions for facilities in the DMNFR from 50 to 25 tons per year. Biochar Now submitted a modification to 15WE1395 in March 2023 to reduce potential NOx emissions below 25 tpy but a revised permit with enforceable limits less than the major source threshold will not be issued prior to the effective reclassification date of November 7, 2023. As a result, an initial Title V application is being submitted to maintain the permit application shield for a timely application. Biochar Now will withdraw the initial Title V permit application once the synthetic minor construction permit is issued. This EJ Summary is a required element of the initial Title V application. Facilities that are located in more than one (1) census block group must submit an EJ summary for each census block group within which they are operating. Since Biochar Now is located in one (1) census block group, only one (1) EJ Summary is required and is being supplied. The EJ Summary shows that Biochar Now is not located in a Disproportionately Impacted (DI) Community for any EJ metrics pursuant to Regulation No. 3, Part B, Section III.5.c. Further, this application does not entail an increase in any emissions. Therefore, Biochar Now is not subject to enhanced monitoring and/or modeling requirements for the initial Title V application. The EJ Summary consists of the following attachments: (1) An "Environmental Justice Report" (EJ Report) in Attachment A generated using Colorado EnvioScreen; (2) An Environmental Justice Summary Supplemental Information Form in Attachment B; and (3) Per Regulation No. 3, Part B, Section III.B.5.b, documentation of "Occupied Areas" within one mile of Biochar Now as shown in a Google Earth aerial image in Attachment C. CDPHE - Page 2 October 2023 If you have questions regarding this submittal, please contact me at (814) 691-1227 or by email at matthew.petrosky@trinityconsultants.com. Sincerely, TRINITY CONSULTANTS Matthew Petrosky Associate Consultant CC: Dylan Van Demark, Biochar Now Jordan Gaspard, Biochar Now George Iwaszek, Trinity Consultants CDPHE - Page 3 October 2023 Attachment A. Environmental Justice Report COLORADO Air Pollution Control Division Department of Public Health Ey Environment Air Quality Regulation (Reg.) 3 Environmental Justice Report Applicant Information Company Name: Biochar Now, LLC Facility Name: Berthoud Plant Plant AIRS ID Number: 123/9E2C Permit Type: Construction Permit / Initial Title V Operating Permit Permit Number: 15WE1395 Facility location used for generating the report: 40.282 , -104.9938 Environmental Justice Summary Weld County Census Block Group 081230021032 Air Quality Reg. 3 Disproportionately Impacted (DI) Community No Air Quality Reg. 3 Community Type Not Disproportionately Impacted Low-income Population People of Color Population Limited English Proficiency Population Housing Cost Burdened Population CO EnviroScreen Percentile Score Environmental Justice Overview 26.4% 46.06 Environmental Exposures Percentile Score 66.48 The environmental exposures score represents a community's exposure to certain environmental risks relative to the rest of the state. The score ranges from 0 to 100, with higher scores indicating higher burden. The environmental exposures score does not cover all pollutants; it is the average of data on diesel particulate matter, traffic proximity, ozone, PM 2.5, air toxics, other air pollutants, lead exposure risk, drinking water violations, and noise. Environmental Effects Percentile Score 63.31 Report Created: Friday, October 27, 2023 CO EnviroScreen Version 1.0 1/7 The environmental effects score represents how many hazardous or toxic sites are in a community relative to the rest of the state. The score ranges from 0 to 100, with a higher score indicating higher burden. The score is the average of data on proximity to mining, oil and gas operations, impaired surface waters, wastewater discharge facilities, Superfund sites, facilities that use hazardous chemicals, and facilities that generate, treat, store, or dispose of hazardous wastes. Climate Vulnerability Percentile Score 65.97 The climate burden score represents a community's risk of drought, flood, extreme heat, and wildfire compared to the rest of the state. The score ranges from 0 to 100, the higher the score, the higher the burden. Sensitive Populations Percentile Score 49.07 The sensitive populations score captures how at risk a community is to environmental exposures and climate impacts as it relates to health. For example, air pollution has stronger impacts on older and younger people, and people with chronic conditions such as asthma. The score ranges from 0 to 100, with a higher score being worse. The score is calculated using data on asthma hospitalization rate, cancer prevalence, diabetes prevalence, heart disease prevalence, life expectancy, low birth weight rate, mental health, population over 65, and population under 5. Demographics Percentile Score 23.08 The demographics score represents a community's social and economic vulnerabilities. The score ranges from 0 to 100, with a higher number representing a higher vulnerability. It is calculated using data on people living with disabilities, housing cost burden, educational attainment, limited English proficiency, income, and race and ethnicity. Report Created: Friday, October 27, 2023 CO EnviroScreen Version 1.0 2/7 Pollution and Climate Indicators Indicator Original Unit of Measure Percentile Air Toxics Emissions distance weighted measure of estimated air toxics emissions 99.24 Diesel Particulate Matter micrograms per cubic meter 42.89 population weighted duration (in weeks) of resolved and unresolved Drinking Water Regulations 83.49 health based violations from active community public water systems Fine Particle Pollution (PM 2.5) micrograms per cubic meter 73.9 Impaired Streams and Rivers average impairment and assessment status of streams 76.74 Risk percentage of housing units built before 1960, as an indicator of Lead Exposure 66.19 potential exposure to lead Noise decibles A 18.49 Other Air Pollutants distance weighted measure of estimated other air pollutant emissions 98.64 Ozone parts per billion 39.92 Proximity to Hazardous Waste Facilities distance weighted count of hazardous waste facilities within 5 km 39.89 distance weighted measure of the total number of active coal, hard Proximity to Mining Locations 83.46 rock, and construction materials mining permits Proximity to National Priorities List . distance weighted count of proposed or listed NPL sites with 5 km Sites 34.15 Proximity to Oil and Gas distance weighted measure of the total number of active oil and gas locations 99.04 Proximity to Risk Management Plan Sites distance weighted count of RMP facilities within 5 km 52.49 Traffic Proximity and Volume amount of vehicular traffic nearby, and distance from roads 27.26 Wastewater Discharge Indicator toxic chemical concentrations in stream segments per km 65.34 Drought sum of weekly total percent of an area experiencing a severe, extreme, or exceptional drought 22.93 Extreme Heat Days average number of high heat days between May and September from 2016 to 2020 86.01 Floodplains percentage of each geographic area where there is at least a one percent chance of flooding annually 77.8 Wildfire Risk mean wildfire hazard potential within each geographic area as determined by the US Forest Service, 2021 67.86 Report Created: Friday, October 27, 2023 CO EnviroScreen Version 1.0 3/7 Health and Social Indicators Indicator Orignial Unit of Measure Percentile Asthma Hospitalization Rate rate of hospitalization per 100,000 people 40.09 Cancer Prevalence percent of adults 67.74 Diabetes Prevalence percent of adults 36 Heart Disease in Adults percent of adults 88.93 Life Expectancy years 16.39 Low Birth Weight percent of singleton births 9.02 Mental Health Indicator percent of adults 45.25 Population over 64 years of age percent of total population 65.29 Population under 5 years of age percent of total population 69.65 Disability percent of total population 27.07 Housing Cost Burdened percent of total population 40.14 Less Than High School Education percent of total population 25.26 Linguistic Isolation percent of total population 54.42 Low Income percent of total population 30.39 People of Color percent of total population 12.09 Understanding the Data The values shown in the Pollution and Climate Indicator and Health and Social Indicator tables are percentiles. Percentiles are a way to see how one area compares to other areas in Colorado. Percentile values range from 0 - 100. A higher score indicates higher burden. Specifically, the percentile tells you the percentage of places in Colorado that have a lower score than the selected location. For example, an area with 85 percentile score for the noise indicator, ranks in the top 15% of areas impacted by noise in Colorado. That means that 85% of the other Census Block Groups in Colorado have a lower score for noise impacts. Number of Census Black Groups Percentile Score (Norma[ distribution for visuQlzation purposes only) Burden 85th Percentile 15% Set The data in the report comes from Colorado EnviroScreen version 1.0. Developed in 2022 by CDPHE and Colorado State University, EnviroScreen maps the overlap of environmental exposures and effects, climate vulnerability, sensitive Report Created: Friday, October 27, 2023 CO EnviroScreen Version 1.0 4/7 populations, and demographics to better understand environmental injustice and environmental health risks in Colorado. For more detailed information on the data sources used in Colorado EnviroScreen Version 1.0 see the technical documentation. On the first page of the report, red text highlights if values for a census block group meet or exceed the criteria for definition of Disproportionately Impacted Community for Air Quality Regulation 3. On subsequent pages of the report, red text highlights indicators in the top percentiles for Colorado that may warrant additional consideration during the permitting process. The Environmental Justice Report is not intended to show individual health risk or exposure. In the Environmental Justice Summary on the first page, values shown in red indicate a census block group that meets or exceeds the following criteria to qualify as a Disproportionately Impacted (DI) Community for Air Quality Reg 3: - Over 40% of households are low-income (meaning they are at or below 200% of the federal poverty level), - 40% of the population identify as people of color, - 50% of households are housing -cost burdened (meaning they spend more than 30% of household income on housing costs), or - 20% of the population is linguistically isolated (meaning no adults in a household speak English well). A census block group that meets or exceeds any of these percentages is labeled as a Socioeconomically Vulnerable Community (SVC). The CO EnviroScreen Percentile Score, which is also found on the first page of the Environmental Justice Report, is written in red if it is above the 80th percentile. A census block group with a CO EnviroScreen Score above the 80th percentile is labeled as a Cumulatively Impacted Community (CIC). In other sections of the Environmental Justice Report, including the Environmental Justice Overview, Pollution and Climate Indicators, and Health and Social Indicators sections, indicator and component scores over the 80th percentile are also highlighted in red. The 80th percentile threshold is used in most cases to flag census block groups that have indicators and groups of indicators (components) that are in the top 20% of census block groups in Colorado. These indicators and components are flagged because they may warrant further review in the permitting process by the permit applicant and/or the Division staff reviewing the permit. As explained on page 11 of the User Guide, for most indicators, the indicator is highlighted in red if it is above the 80th percentile to indicate that the census block group where the facility is located faces higher risks based on that indicator compared to other Colorado communities. However, less than 20% of census block groups in Colorado have oil and gas facilities or mining locations. Accordingly, all census block groups in Colorado score above the 80th percentile for proximity to these two types of facilities because even having zero facilities puts a community in the top 20%. Accordingly, the Environmental Justice Report highlights a census block group in red if it is above the 85th percentile for mining facilities and above the 90th percentile for oil and gas facilities. This ensures that only census block groups with a greater number of facilities than the statewide average of zero are highlighted on the EJ Report. On the first page of the report, red text highlights if values for a census block group meet or exceed the criteria for definition of Disproportionately Impacted Community for Air Quality Regulation 3. On subsequent pages of the report, red text highlights indicators in the top percentiles for Colorado that may warrant additional consideration during the permitting process. The Environmental Justice Report is not intended to show individual health risk or exposure. In the Environmental Justice Summary on the first page, values shown in red indicate a census block group that meets or exceeds the following criteria to qualify as a Disproportionately Impacted (DI) Community for Air Quality Reg 3: - Over 40% of households are low-income (meaning they are at or below 200% of the federal poverty level), - 40% of the population identify as people of color, Report Created: Friday, October 27, 2023 CO EnviroScreen Version 1.0 5/7 - 50% of households are housing -cost burdened (meaning they spend more than 30% of household income on housing costs), or - 20% of the population is linguistically isolated (meaning no adults in a household speak English well). A census block group that meets or exceeds any of these percentages is labeled as a Socioeconomically Vulnerable Community (SVC). The CO EnviroScreen Percentile Score, which is also found on the first page of the Environmental Justice Report, is written in red if it is above the 80th percentile. A census block group with a CO EnviroScreen Score above the 80th percentile is labeled as a Cumulatively Impacted Community (CIC). In other sections of the Environmental Justice Report, including the Environmental Justice Overview, Pollution and Climate Indicators, and Health and Social Indicators sections, indicator and component scores over the 80th percentile are also highlighted in red. The 80th percentile threshold is used in most cases to flag census block groups that have indicators and groups of indicators (components) that are in the top 20% of census block groups in Colorado. These indicators and components are flagged because they may warrant further review in the permitting process by the permit applicant and/or the Division staff reviewing the permit. As explained on page 11 of the User Guide, for most indicators, the indicator is highlighted in red if it is above the 80th percentile to indicate that the census block group where the facility is located faces higher risks based on that indicator compared to other Colorado communities. However, less than 20% of census block groups in Colorado have oil and gas facilities or mining locations. Accordingly, all census block groups in Colorado score above the 80th percentile for proximity to these two types of facilities because even having zero facilities puts a community in the top 20%. Accordingly, the Environmental Justice Report highlights a census block group in red if it is above the 85th percentile for mining facilities and above the 90th percentile for oil and gas facilities. This ensures that only census block groups with a greater number of facilities than the statewide average of zero are highlighted on the EJ Report. Report Created: Friday, October 27, 2023 CO EnviroScreen Version 1.0 6/7 Colorado EnviroScreen does: - Show which areas in Colorado are more likely to have higher environmental health injustices. - Identify areas in Colorado where government agencies can prioritize resources and work to reduce pollution and other sources of environmental injustice. - Provide information to empower communities to advocate to improve public health and the environment. - Identify areas that meet the updated definition of "Disproportionately Impacted Community" under House Bill 23-1233 adopted a definition that applies to all state agencies, including CDPHE. - Identify areas where the Air Quality Regulation (Reg.) Number 3, which governs permitting in disproportionately impacted communities, applies. - Identify areas that meet the prior definition of "Disproportionately Impacted Community" under the Colorado Environmental Justice Act (HB21-1266). Colorado EnviroScreen does not: - Define a healthy or unhealthy environment. - Establish causal associations between environmental risks and health. - Define all areas that may be affected by environmental injustice or specific environmental risks. - Provide information about an individual person's health status or environment. - Take all environmental exposures into account. - Tell us about smaller areas within a census block group that may be more vulnerable to environmental exposures than other areas. - Provide information about non -human health or ecosystem risks. Additional Resources Frequently Asked Questions: Environmental Justice Report Tool for Air Quality Regulation 3 Air Pollution Control Division's Small Business Assistance Program CDPHE Environmental Justice Program Colorado EnviroScreen Version 1.0 Reports, Guides, and Resources Folder Report Created: Friday, October 27, 2023 CO EnviroScreen Version 1.0 7/7 CDPHE - Page 4 October 2023 Attachment B. Environmental Justice Summary Supplemental Information Form This information was also submitted online using the Environmental Justice Summary Supplemental Information for Air Quality Regulation 3 Online Submission Form but is provided here as an overview of the description of the proposed permit application and a summary of engagement to be conducted by the permit applicant with the surrounding community. From: Goodie Forms To: Matthew Petrosky Subject: Environmental Justice Summary Supplemental Information for Air Quality Regulation 3 Date: Tuesday, October 31, 2023 1:07:37 PM Thanks for filling out Environmental Justice Summary Supplemental Information for Air Quality Regulation 3 Here's what was received. I_nvironmental Justice Summary Sunlemental Information for Air Quality Re.ulation 3 Air Pollution Control Division Background: Under Colorado's Air Quality Regulation 3, an Environmental Justice Summary ("EJ Summary") is required for all applicable permit applications. This EJ Summary consists of: 1. Environmental Justice Report ("EJ Report" - submitted separately as an email attachment to cdphe_apcd_ejreports@state.co.us). 2. Environmental Justice Summary Supplemental Information Form (this form). 3. Any additional supporting documentation (such as map images). You must submit a complete EJ Summary to the Air Pollution Control Division (APCD) for review and approval before submitting your main permit application. You will then receive a letter of concurrence from the Division's Environmental Justice in Permitting Specialist. The Environmental Justice Summary, including the Environmental Justice Report, is part of the permit record. If the main permit application does not include a letter of concurrence, it may be rejected as incomplete. Additional information is available on the EJ Report Tool website. Note: If a modeling determination (form APCD-11 4) is required for this emission source, you should submit your modeling determination request at the same time you submit the Environmental Justice Summary by following the instructions on form APCD-114. If you are unsure whether a modeling determination is required for this emission source, please consult the Air Pollution Control Division's website. Note: Small businesses can contact the Air Pollution Control Division's Small Business Assistance Program for assistance: cdphe_apcd_sbap@state.co.us. For information about which businesses qualify for assistance as a small business, visit the program's website. A copy of your responses will be emailed to you upon form submission. Email matthew.petrosky@trinityconsultants.com Section 1: Background Information (Company/f=acility) Company name Biochar Now, LI_C Facility name (If the facility does not have a name, enter the company name.) Berthoud Plant Facility location (street address or coordinates) 19500 Weld County Road 7, Berthoud, CO 80513 Census block group(s) in which the facility is located (this information is found in the facility's Environmental Justice Report) 081230021032 Which type of air permit will you be applying for? Initial Title V Permit O Title V Permit Renewal or Modification OGeneral Permit OUnsure OOther: Has this facility previously received an official permit or exemption letter from the Air Pollution Control Division (APCD)? 0 0 Yes No Unsure Section 1: Background Information (Company/Facility) What is the AIRS ID of this facility? (The AIRS ID number will be listed on the permit or exemption letter. It is seven or ten digits, usually written "XXX-XXXX" or "XXX-XXXX-XXX")..F,, 123-9 E2C What is the permit number or exemption number? 15WE1395 Section 2: Company/Facility Contact Information Company representative name Jordan Gaspard Company representative phone number (970) 443-4896 Company representative email address jgaspardbiocharnow.corn Company representative name #2 (optional) Company representative phone number #2 (optional) Company representative email address #2 (optional) Section 3: Environmental Justice Requirements The Environmental Justice Report Tool and how-to instructions are available on the Air Pollution Control Division's website. Please run a report for your facility to answer the questions below. Based on the Environmental Justice Report generated, is this facility located in a Disproportionately Impacted (ICI) Community? 0 Yes No Section 4: Description of Proposed Permit Application Will this facility emit any Affected Pollutants? (Check all that apply.) Volatile organic compounds (VOCs) Nitrogen oxides (NOx) Particulate matter ≤2.5 microns in diameter (PM2.5) Benzene Toluene Ethyl benzene Xylene Unsure Not applicable JI Describe the proposed permit application, including the estimated emission rates (in tons per year) of any and all Affected Pollutants. For each Affected Pollutant, clearly state whether the estimated emissions would be a net increase, net decrease, or no change. If estimated emission rates of Affected Pollutants will remain the same, please still provide those estimates below. Please provide this information even if your facility is not located in a Disproportionately Impacted Community. (Note: Please do not send this information as additional attachments. Provide the information requested as a short plain language summary below.) There will be a 0 tpy change for all pollutants. Is the proposed permit application for a new source or modification to an existing source that will increase emissions of Affected Pollutants in a Disproportionately Impacted Community? 0 Yes No Describe any mitigation measures and/or changes to the proposed emission sources that were made based on the results of the facility's Environmental Justice Report and Summary, if any (such as enhanced monitoring, recordkeeping, and/or reporting). (Note: If you prefer to send this as an email attachment to cdphe_apcdejreports@state.co.us, write "Will send via email." If the facility is not located in a Disproportionately Impacted Community, write "N/A.") N/A Describe any emission reduction strategies that were considered in relation to the Colorado EnviroScreen indicator data, if any (i.e., information in the facility's Environmental Justice Report). (Note: If you prefer to send this as an email attachment to cdphe_apcd_ejreports@state.co.us, write "Will send via email." If the facility is not located in a Disproportionately Impacted Community or no such mitigation measures or changes were made, write "N/A.") N/A Describe any changes that were made to the originally -planned source equipment or operations based on engagement with and assessment of the Disproportionately Impacted Community, if any. (Note: If you prefer to send this as an email attachment to cdphe_apcd_ejreports@state.co.us, write "Will send via email." If the facility is not located in a Disproportionately Impacted Community or no such changes were made, write "N/A.") N/A I acknowledge that, if applicable, I provided complete answers to the questions above in this section OR I will submit a summary of the information requested in the questions above to cdphe_apcd_ejreportsOstate.co.us. _r Yes Section 5: Public Outreach For facilities located in Disproportionately Impacted Communities, the Air Pollution Control Division encourages thoughtful and culturally -sensitive enhanced public outreach by the facility to keep communities informed and engaged with the latest information. This includes any engagement with members of the Disproportionately Impacted Community who reside within one mile of the proposed Affected Construction Source or frequent an Occupied Area within one mile of the proposed Affected Construction Source, unless the Occupied Area is under the control of the proposed Affected Construction Source's owner/operator. You can explore community engagement, outreach, and public participation tips and best practices on CDPHE's vvebsite. Did the owner/operator of the facility conduct or plan to conduct enhanced community outreach to the impacted community prior to submitting the main permit application? 0 Yes No Provide a summanj of community outreach the owner/operator of the facility conducted, or plans to conduct, if any. (Note: If you prefer to send this as an email attachment to cdphe_apcd_ejreports®state.co.us, write "Will send via email." If the facility is not located in a Disproportionately Impacted Community or no such engagement will be conducted, write "N/A.") , N/A Describe any other considerations intended to facilitate the fair treatment and meaningful involvement of Disproportionately Impacted Community members, if any. (Note: If you prefer to send this as an email attachment to cdphe_apcd_ejreports@state.co.us, write "Will send via email." If the facility is not located in a Disproportionately Impacted Community or no such considerations have been implemented, write "N/A.") N/A I acknowledge that, if applicable, I provided complete answers to the questions above in this section OR I will submit a summanj of community outreach the facility conducted, or plans to conduct, to cdphe_apcd_ejreports®state.co.us. . Yes Section 6: Acknowledgements and Supplement Submission To submit a complete Environmental Justice Summary to the Division, email the following documents to cdphe_apcd_ejreports@state.co.us beforeoraftersubmitting this onlineform. Facility's Environmental Justice Report generated by the Environmental Justice Report Tool. 2. If this facility is located in a Disproportionately Impacted (DI) Community, a summary of any community outreach activities conducted or planned as mentioned in Section 5. a Any additional supporting documentation (such as aerial or satellite map images). I acknowledge that I will submit a complete Environmental Justice Summary to the Air Pollution Control Division prior to submitting the main permit application. Yes I acknowledge that, if applicable, I must also submit a completed Form APCD- 114 prior to submitting the main permit application. (Information on Form APCMD-114 can be found here). Yes I acknowledge that I must submit an aerial or satellite image of the location of the facility as documentation of any Occupied Areas not within Owner/Operator control within one mile of the Source, to cdphe_apcd_ejreports@state.co.us. Instructions on how to submit this image are available on the Air Pollution Control Division's website. Yes Create your own Google Form Report Abuse CDPHE - Page 5 October 2023 Attachment C. Aerial Image of the Facility Office Office and Processing Generators Propane Tan Processing System 14 Operational Emission Stacks Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 1 of 17 Enforcement Case Summary Report Without Comments Criteria: Action Achieved date is between Jul 1 2020 12:00AM - Sep 30 2020 11:59PM Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 2 of 17 Enforcement Case Summary Report Without Comments Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2015-080 IR/MEP Reg 7 violations 031-2126 BAYSWATER EXPL - REG 7 & 0000 REPORTING 8/25/2015 9/1/2020 Action Achieved Penalty SEP 9/1/2020 79,200 EFV2 9/1/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2019-126 Failure to connect vapor recovery 777 Xtreme Petroleum LLC 8/1/2019 Action Achieved Penalty CO 8/20/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2019-150 Failure to control emissions 059-0627 STINKER STORES - STINKER #339 9/3/2019 Action Achieved Penalty COC 9/3/2020 9,450 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2019-152 Failure to control emissions 031-1438 STINKER STORES - STINKER #314 9/3/2019 Action Achieved Penalty COO 9/3/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2019-161 Failure to provide records, APEN violation 123-0491 R & B SUPERMARKET - GASOLINE & GROCERY 9/13/2019 Action Achieved Penalty CO 8/20/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2019-192 Failure to control emissions, APEN violation 005-1080 7 -ELEVEN, INC. - NO 21493 11/25/2019 7/1/2020 Action Achieved Penalty EFV2 7/1/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2019-193 Failure to control emissions, throughput, emissions, and APEN violations 031-1467 7 -ELEVEN, INC. - NO 13194 11/25/2019 7/1/2020 Action Achieved Penalty EFV2 7/1/2020 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 3 of 17 Enforcement Case Summary Report Without Comments Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-009 Emissions and work practice violations 017-0191 TUMBLEWEED MIDSTREAM - N MAYFIELD C.S. 1/23/2020 8/20/2020 Action Achieved Penalty EFV2 8/20/2020 WL 8/20/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-013 Monitoring and control device requirement violations 103-0291 ENTERPRISE GAS PROC - MEEKER GAS PLANT 2/3/2020 7/2/2020 Action Achieved Penalty EFV2 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-015 Failure to control emissions 031-1445 STINKER STORES - STINKER #342 2/5/2020 10/15/2020 Action Achieved Penalty COC 9/3/2020 0 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-022 Emissions, throughput, and APEN violations 031-1916 CIRCLE K STORE # 2709842 2/28/2020 9/6/2020 Action Achieved Penalty EFV2 9/6/2020 C O C 8/20/2020 26,325 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-023 Failure to control emissions, APEN violation 005-1274 CIRCLE K STORE # 2709879 2/28/2020 Action Achieved Penalty C O C 8/24/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-024 APEN violation 001-1302 CIRCLE K STORE # 2709850 2/28/2020 9/6/2020 Action Achieved Penalty EFV2 9/6/2020 C O C 8/20/2020 Case# Case Description AIRS ID Plant/Location 2020-025 APEN violation 001-1304 CIRCLE K STORE # 2709889 Case Opened 2/28/2020 Case Closed 9/6/2020 Action Achieved Penalty Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 4 of 17 Enforcement Case Summary Report Without Comments EFV2 9/6/2020 i COO 8/20/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-026 Failure to provide records, APEN violation 005-1245 CIRCLE K STORE # 2709898 2/28/2020 9/6/2020 Action Achieved Penalty EFV2 9/6/2020 COO 8/20/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-027 Failure to control emissions, emissions, throughput, and APEN violations 035-0674 CIRCLE K STORE # 2709905 2/28/2020 Action Achieved Penalty COC C 8/20/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-028 APEN violation 005-0540 CIRCLE K STORE # 2709880 2/28/2020 9/6/2020 Action Achieved Penalty EFV2 9/6/2020 COO 8/20/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-029 Failure to control emissions, APEN, and permitting violations 005-0972 J&S PETRO - DRY CREEK GAS AND SNACK 3/2/2020 9/8/2020 Action Achieved Penalty EFV2 9/8/2020 Case# Case Description AIRS ID Plant/Location 2020-030 Permit and APEN violations 059-2031 KUM & GO, L.C. - #319 Action Achieved Penalty Case Opened Case Closed 3/13/2020 8/19/2020 EFV2 8/19/2020 COO 8/11/2020 9,275 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-033 Emissions, monitoring, and reporting violations 101-0252 GCC RIO GRANDE - PUEBLO CEMENT PLANT 3/24/2020 7/20/2020 Action Achieved Penalty EFV2 7/20/2020 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 5 of 17 Enforcement Case Summary Report Without Comments Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-036 Testing, monitoring, and work practice violations 013-0003 CEMEX CONSTRUCTION MATERIALS - LYONS 3/26/2020 8/10/2020 Action Achieved Penalty EFV2 8/10/2020 AS 7/21/2020 42,000 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-038 Emissions, monitoring, work practice and reporting violations 075-0029 STERLING ENERGY INVESTMENTS - YENTER GP 3/26/2020 7/15/2020 Action Achieved Penalty EFV2 7/15/2020 AS 7/6/2020 18,200 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-039 Testing, monitoring, reporting, and work practice violations 081-0350 GREAT DIVIDE DISPOSAL FACILITY 3/27/2020 10/8/2020 Action Achieved Penalty AS 9/28/2020 3,448 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-041 Emissions, throughput, work practice, monitoring, recordkeeping and 123-9E0F PLATTE RIVER MIDSTREAM -LUCERNE WEST STAT APEN violations 4/6/2020 7/1/2020 Action Achieved Penalty EFV2 7/1/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-042 APEN and permitting violations 001-1400 KUM & GO, L.C. - STORE #940 4/6/2020 Action Achieved Penalty COC 8/11/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-043 Failure to control emissions, permit and APEN violations 123-9760 KUM & GO, L.C. - STORE #973 4/6/2020 Action Achieved Penalty COC 8/11/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-044 Emissions, work practice, monitoring, and APEN violations 123-0057 KMCGEE FT LUPTON/PLATTE VALLEY/LANCASTER 4/15/2020 10/7/2020 Action Achieved Penalty Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 6 of 17 Enforcement Case Summary Report Without Comments AS 9/29/2020 47,425 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-046 Emissions violations 123-9009 DCP OPERATING CO - SULLIVAN C.S. 4/16/2020 7/20/2020 Action Achieved Penalty EFV2 7/20/2020 AS 7/7/2020 10,500 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-048 Recordkeeping, reporting, and APEN violations 117-0017 SUMMIT COUNTY LANDFILL 4/16/2020 7/14/2020 Action Achieved Penalty EFV2 7/14/2020 AS 7/7/2020 5,600 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-070 Emission limit violations, failure to install control device 123-9E99 ROCKY MOUNTAIN MIDSTREAM - FT LUPTON GAS 4/16/2020 Action Achieved Penalty C O C 7/28/2020 21,000 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-071 Testing and reporting violations 017-0209 TUMBLEWEED MIDSTREAM - LADDER CREEK C.S. 4/16/2020 8/12/2020 Action Achieved Penalty EFV2 8/12/2020 AS 8/5/2020 3,500 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-084 Monitoring and APEN violations 045-1234 CAERUS PICEANCE - J16W/M16W PROD FACILIT 4/21/2020 7/14/2020 Action Achieved Penalty EFV2 7/14/2020 AS 7/10/2020 3,675 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-087 Monitoring, record keeping, and APEN violations 073-0146 NIGHTHAWK PRODUCTION -CRAIG 4-4 4/23/2020 Action Achieved Penalty COO 9/16/2020 1,925 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 7 of 17 Enforcement Case Summary Report Without Comments Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-090 APEN and permitting violations 059-0605 CITAULA BROTHERS 6 - CONVENIENCE PLUS 5/6/2020 7/6/2020 Action Achieved Penalty EFV2 7/6/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-101 Visible emissions from flare - INOV 123-9E20 WHITING OIL & GAS - RAZOR 33 CENTRAL 5/26/2020 8/24/2020 Action Achieved Penalty EFV2 8/24/2020 EFNH N H 8/19/2020 AS 8/24/2020 8,050 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-102 Emissions, throughput, and work practice violations 001-1332 DILLON COS - KING SOOPERS FUEL FAC #081 6/1/2020 7/2/2020 Action Achieved Penalty EFV2 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-108 Failure to control emissions, APEN violation 005-1100 BYERS THRIFT - BYERS SINCLAIR 6/15/2020 8/19/2020 Action Achieved Penalty EFV2 8/19/2020 AS 8/13/2020 3,150 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-121 Work practice,monitoring, recordkeeping, and APEN violations 005-1471 OMNI-X U.S.A . 6/15/2020 8/3/2020 Action Achieved Penalty EFV2 8/3/2020 AS 7/28/2020 5,425 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-122 Emissions and monitoring violations 001-0611 DENVER AUTO AUCTION 6/15/2020 9/16/2020 Action Achieved Penalty EFV2 9/16/2020 EFV4 9/16/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 8 of 17 Enforcement Case Summary Report Without Comments 2020-123 Emission limit violation - stack test 103-0028 NATURAL SODA LLC 6/15/2020 8/4/2020 Action Achieved Penalty EFV2 8/4/2020 AS 7/29/2020 2,800 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-126 Emission limit violations - stack test 123-9E2C BIOCHAR NOW, LLC - BERTHOUD PLANT 6/15/2020 Action Achieved Penalty 000 8/20/2020 5,250 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-127 Failure to complete test, notify Division of test 123-9C89 BONANZA CREEK - PRONGHORN 24-7 BOOSTER 6/15/2020 10/1/2020 Action Achieved Penalty AS 9/29/2020 22,750 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-129 Open thief hatch - INOV 123-9A75 K.P. KAUFFMAN - FACILITY #7 6/18/2020 Action Achieved Penalty EFNH N H 9/14/2020 NOV 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-131 Emissions and control efficiency requirement violations - stack test 087-0111 STERLING ENERGY - JACKSON LAKE GAS PLANT 6/29/2020 10/1/2020 Action Achieved Penalty CA 7/13/2020 AS 9/23/2020 35,000 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-132 APEN and permit violations 001-2243 MAVERIK, INC - #549 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 0 AS 8/10/2020 5,600 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-133 APEN and permitting violations 001-2244 MAVERIK, INC - #495 7/1/2020 9/21/2020 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 9 of 17 Enforcement Case Summary Report Without Comments Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-134 APEN and permitting violations 001-2245 MAVERIK, INC - #540 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-135 APEN and permitting violations 001-2246 MAVERIK, INC - #544 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-136 APEN and permitting violations 005-1753 MAVERIK, INC - #490 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-137 APEN and permitting violations 005-1754 MAVERIK, INC - #525 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-138 APEN and permitting violations 005-1755 MAVERIK, INC - #579 7/1/2020 9/21/2020 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 10 of 17 Enforcement Case Summary Report Without Comments Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-139 APEN violation 029-0115 MAVERIK, INC - #463 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-140 APEN and permitting violations 035-0791 MAVERIK, INC - #479 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description 2020-141 APEN violation AIRS ID Plant/Location Case Opened Case Closed Action Achieved Penalty 041-2174 MAVERIK, INC - #494 7/1/2020 9/21/2020 EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description 2020-142 APEN violation AIRS ID Plant/Location Action Achieved Penalty EFV2 9/21/2020 041-2175 MAVERIK, INC - #566 Case Opened Case Closed 7/1/2020 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-143 APEN violation 041-2176 MAVERIK, INC - #602 7/1/2020 9/21/2020 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 11 of 17 Enforcement Case Summary Report Without Comments Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-144 APEN and permitting violations 069-0582 MAVERIK, INC - #520 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-145 APEN violation 077-0640 MAVERIK, INC - #482 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-146 APEN violation 077-0641 MAVERIK, INC - #418 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-147 APEN violation 077-0642 MAVERIK, INC - #500 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-148 APEN violation 077-0643 MAVERIK, INC - #400 7/1/2020 9/21/2020 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 12 of 17 Enforcement Case Summary Report Without Comments Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-149 APEN violation 077-0644 MAVERIK, INC - #417 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-150 APEN violation 083-0115 MAVERIK, INC - #497 7/1/2020 9/21/2020 Action Achieved Penalty EFV2 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-151 APEN and permitting violations 123-A0FD MAVERIK, INC - #609 Action Achieved Penalty 7/1/2020 9/21/2020 EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description 2020-152 APEN violation AIRS ID Plant/Location Action Achieved Penalty EFV2 9/21/2020 083-0116 MAVERIK, INC - #275 Case Opened Case Closed 7/1/2020 9/21/2020 CA 7/2/2020 AS 8/10/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-153 APEN violation 087-0126 MAVERIK, INC - #480 7/1/2020 9/21/2020 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 13 of 17 Enforcement Case Summary Report Without Comments Action Achieved Penalty EFV2 9/21/2020 AS 8/10/2020 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-154 APEN, permitting, and control plan requirement violations 123-9DA6 PAWNEE WASTE - PAWNEE WASTE E&P LANDFILL 7/1/2020 Action Achieved Penalty CA 7/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-155 Failure to repair leaks, APEN and permit violations 123-0015 DCP OPERATING CO - SPINDLE GAS PLANT 7/2/2020 Action Achieved Penalty CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-156 Emissions, reporting, recorkeeping, and testing violations 001-2202 CRESTONE PEAK - BIG SANDY 3-65 36-31 1D 7/2/2020 9/29/2020 Action Achieved Penalty EFV2 9/29/2020 AS 9/29/2020 8,750 CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-157 Emissions limit violation -stack test 123-9FDB REP PROCESSING LLC - PIERCE GAS PLANT 7/2/2020 10/26/2020 Action Achieved Penalty CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-158 Visible emissions, testing, monitoring, recordkeeping and reporting violations 123-9F9C ROCKY MOUNTAIN MIDSTREAM - DISCOVERY MUS 7/2/2020 Action Achieved Penalty CA 7/2/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-159 Failure to control emissions, self -certify 031-2422 RUDEETAI - SPEER SHELL 7/10/2020 9/22/2020 Action Achieved Penalty Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 14 of 17 Enforcement Case Summary Report Without Comments EFV2 9/22/2020 i CA 7/13/2020 AS 9/11/2020 3,500 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-160 MACT, emissions, permitting, work practice and APEN violations 123-0107 DCP OPERATING CO - LUCERNE 1 GAS PLANT 7/13/2020 Action Achieved Penalty EF45 7/13/2020 NOV 7/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-161 Emission limit violation, APEN and fee payment violations - stack test 001-0559 CONSERVATION SERVICES 7/23/2020 Action Achieved Penalty CA 7/27/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-162 APEN and permitting violations - self audit immunity 123-A03A MALLARD EXPLORATION - CINNAMON TEAL FED 8/10/2020 8/11/2020 Action Achieved Penalty EFV2 8/11/2020 EFV4 8/11/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-163 Visible emissions, recordkeeping, and work practice violations 005-1712 CRESTONE PEAK - STATE LA PLATA 5-65 8/10/2020 Action Achieved Penalty EFV2 8/11/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-164 Monitoring and recordkeeping violations -self audit immunity 123-9DF7 AKA ENERGY GROUP - SPEER GAS PLANT 8/11/2020 8/13/2020 Action Achieved Penalty EFV2 8/13/2020 EFV4 8/13/2020 Case# Case Description 2020-176 Reporting violations AIRS ID Plant/Location Action Achieved Penalty 041-0091 COLORADO SPRINGS UTIL. - CLEAR SPRING RA Case Opened 8/12/2020 Case Closed Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 15 of 17 Enforcement Case Summary Report Without Comments CA 8/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-177 Emissions and monitoring violations 123-9010 DCP OPERATING CO - GODFREY BOTTOM C.S. 8/12/2020 Action Achieved Penalty CA 8/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-178 Emission limit violations 123-7168 HIGHPOINT - PETERSON 5-63-30 SWNE 8/12/2020 10/28/2020 Action Achieved Penalty CA 8/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-179 APEN, recordkeeping and failure to provide records violations 005-0279 QUALITY CLEANERS 8/12/2020 10/12/2020 Action Achieved Penalty CA 8/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-180 Emission limit violation - aborted stack test 123-9C84 NOBLE ENERGY - ROHN STATE LD4 ECONODE 8/12/2020 Action Achieved Penalty CA 8/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-181 Odor violation 101-1195 STAYCON - CRAFT CONCENTRATES 8/12/2020 Action Achieved Penalty CA 8/13/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-182 Emissions, throughput, APEN and permitting violations 123-0090 DCP OPERATING CO - MEWBOURN 9/10/2020 9/16/2020 Action Achieved Penalty EFV2 9/16/2020 WL 9/16/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-183 Emissions, throughput, and work practice violations 123-9 FA E HIGHPOINT OPERATING -CIRCLE B 5-61-27 CS 9/16/2020 Action Achieved Penalty Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 16 of 17 Enforcement Case Summary Report Without Comments CA 9/21/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-184 Emissions, monitoring, and reporting violations 043-0001 HOLCIM (US) INC. PORTLAND PLANT 9/16/2020 Action Achieved Penalty EF45 9/2/2020 CA 9/17/2020 EF64 9/14/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 2020-186 Emissions and control device violations - stack test 059-1988 COORSTEK, INC. - CENTER FOR ADVANCED MAT 9/17/2020 Action Achieved Penalty CA 9/21/2020 EFNH N H 8/16/2020 Case# Case Description AIRS ID Plant/Location Case Opened Case Closed 3 2020-187 Monitoring and work practice violations 123-1351 KERR-MCGEE GATHERING - IONE C.S. 9/17/2020 Action Achieved Penalty CA 9/18/2020 Case# Case Description J AIRS ID Plant/Location Case Opened Case Closed 2020-193 Emissions, work practice, and reporting violations 059-0409 ARCOSA LWB LLC - LIGHTWEIGHT - BOULDER 10/26/2020 Action Achieved Penalty INFS 8/14/2020 Case Totals Open 27 Closed 62 Total 89 Thursday, November 5, 2020 6:20 PM Colorado Air Compliance Tracking and Inventory System Page 17 of 17 Enforcement Case Summary Report Without Comments Action/Penalty Summary Action Number Penalty SEP - SUPPLEMENTAL ENVIRONMENTAL PROGRAM 1 79,200 AS - SETTLEMENT 17 229,373 COC - STATE CONSENT AGREEMENT ISSUED 6 73,225 Total: 24 381,798 Angela Snyder From: Sent: To: Cc: Subject: Jeremy McKay <jmckay@eadefense.org> Tuesday, October 7, 2025 12:12 PM Diana Aungst; Angela Snyder Alexa McKay USR24-0019 EXHIBIT D 21 3 This Message Is From an Untrusted Sender You have not previously corresponded with this sender. Use extra caution and avoid replying with sensitive information, clicking links, or downloading attachments until their identify is verified. To the Weld County Planning Commission, On behalf of Ms. Yarbrough, Environmental and Animal Defense offers this brief supplemental comment in connection with the documents it sent via email to the planning commission on October 6, 2025. Weld County is a severe nonattainment area under the Clean Air Act. Biochar Now's other facility in Berthoud, which it references as support for this project, put in a Title V major source air pollution operating application under the Clean Air Act due to current VOC and NOx emissions from the facility. This is the same type of permit a coal fired powered plant would require. That facility has also been subject to multiple enforcement actions by the CDPHE for violations at that facility. While that other facility has also put in an application for a synthetic minor source permit, it should be noted that Biochar Now has proposed one way to reduce its emissions to meet the criteria for that permit, run fewer of its kilns for fewer hours. This is because Biochar Now's kilns generate harmful emissions at predictable rates. To stay under the Title V threshold, Biochar Now can only run so many kilns for so long. The Berthoud facility is relevant because the applicant relies upon it so heavily in its request for this permit. There are no 1 assurances in the project record that indicate the same results will not occur at this facility as in Berthoud. There are extensive studies showing the significant harms caused by these types of pollutants, and Environmental and Animal Defense has already offered this information into the record. Nothing has been offered by the applicant to contradict these concerns, nor refute the impacts on equine health, or to show Mrs. Yarbrough's continued ability to conduct her agricultural practices. The applicant should offer real data to support its claims and should have been transparent about its other facility. Instead, the applicant has tried to obscure the fact that it will generate harmful emissions by hiding behind an empty sales pitch about its "patented technologies." We urge the planning commission to consider these supplemental documents in combination with our previous submission. Sincerely, Jeremy McKay, Staff Attorney Environmental and Animal Defense Get Outlook for iOS Hello