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HomeMy WebLinkAbout20012462.tiff GROUNDWATER MONITORING WORK PLAN VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COLORADO CGRS NO. 1-135-2755aa by CGRS,INC. 1301 Academy Court Fort Collins, Colorado 80524 800.288.2657 June 6, 2001 2001-2462 CGRS,Inc. Table of Contents 1.0 INTRODUCTION 1 1.1 Objectives 1 1.2 Background Information 1 2.0 PILOT STUDY 2 2.1 Project Start-up 2 2.2 Hydrology Determinations 2 2.3 Soil Borings 3 2.4 Monitoring Well Installation 3 2.5 Groundwater Level Measurements and Chemical Analyses 3 2.6 Water Quality &Hydrogeologic Monitoring 3 2.7 Aquifer Characterization 5 — 2.8 Contingency Plan and Abatement 5 3.0 ORGANIZATION AND STAFF ASSIGNMENTS 6 3.1 Project Personnel 6 3.2 Subcontractors 6 4.0 OVERVIEW-QUALITY ASSURANCE/OUALITY CONTROL 6 5.0 REMARKS 7 FIGURES Figure 1 -Site Location Map Figure 2-Registered Well Location Map Figure 3-Area Use and Site Condition Map ATTACHMENTS Attachment A-Methods and Procedures Attachment B -Quality Assurance Project Plan CGRS, Inc. GROUNDWATER MONITORING WORK PLAN VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COLORADO CGRS NO. 1-135-2755 1.0 INTRODUCTION This document presents the proposed work scope for the evaluation of coal ash burial in saturated media. This will be accomplished by conducting a pilot field program, which consists of burying 400 tons of coal ash in water table conditions in Weld County, Colorado. Rigorous water quality monitoring is proposed over a one-year period to determine long-term leachability characteristics of coal ash under natural conditions. Quarterly background water quality monitoring at the proposed test area is ongoing and has been conducted over a one-year period. The field investigation will be performed in conjunction with a variety of laboratory studies in order to evaluate potential liabilities or benefits associated with coal ash burial. Specifically, this project addresses issues associated with the reclamation of gravel quarries under saturated conditions. A variety of laboratory experiments were conducted in order to evaluate coal ash leaching potentials.This work is performed under the authorization of Varra Companies. — 1.1Obiectives The purpose of this project is to identify potential liabilities with the reclamation of gravel quarries with coal ash and to determine if coal ash meets the criteria for classification as an inert fill. Specific objectives for the Varra Coal Ash Burial Project are to determine: • Leaching characteristics of coal ash with respect to varying water quality conditions; • Permeabilities of various types of coal ash (bottom and fly ash); • Affects of coal ash burial on local hydrology and water quality; • Hydrogeologic properties of coal ash; and • Physical characteristics of coal ash in saturated media. 1.2 Background Information The study area is an active gravel quarry located in the NW 1/4, Section 31, Township 3 North, Range 68 West, 6i° P.M., Weld County, Colorado (Figure 1). The surficial geology of the area as documented by Colton, 1978, varies between wind blown deposits of clay, silt and sand and sandy to gravelly alluvium, which are Holocene in age. Colluvium consisting of bouldery to pebbly sandy silt and clay may contain and interfinger with alluvium of various ages. The depth to groundwater at the site generally varies between three and ten feet below ground surface (bgs). The inferred groundwater flow direction is to the northeast roughly parallel to the St. Vrain River drainage. The Pierre Shale underlies the unconsolidated alluvial CGRS, Inc. deposits in this area. The depth to bedrock in this area as documented by field observation varies between 15 and 30 feet below ground surface. A United States Geological Survey investigation documented groundwater occurrence and movement near the study area. Underflow calculations in the vicinity of the study area indicate that 600 acre-feet of water passes across a two mile section of the alluvial valley.If the average depth to bedrock varies between 20 and 30 feet below ground surface then the average hydraulic conductivity is calculated to vary between 97 and 147 feet per day. Assuming a hydraulic gradient of 0.0023 feet per foot and a porosity of 0.27, the seepage velocity(actual groundwater flow velocity)is estimated to vary between 0.83 and 1.25 feet per day. Water well records obtained from the Colorado Division of Water Resources indicate that one well may be located within one-quarter mile of the proposed test plot. The registered well owner is Dakolios Construction and the permitted use of the well is industrial. The location of registered wells within a half- - mile radius of the proposed test plot are depicted on Figure 2. Field verification of well locations and construction details, if available will be performed prior to project start-up. 2.0 PILOT STUDY 2.1 Project Start-up The project start-up will consist of developing a work plan and a site specific Health and Safety plan. All required permits will be obtained prior to conducting the investigation. Utility companies will be contacted for the location of all underground utilities prior to commencing investigative activities (telephone, sewer, electrical,cable television,natural gas lines,oil and gas pipelines,buried tanks and wells). 2.2 Hydrology Determinations A site-specific investigation will be conducted prior to pilot project. We anticipate that between three and four groundwater monitoring wells will be installed to determine local hydrology and water quality. The investigation at a minimum will determine local groundwater flow direction and rate, soil conditions, porosity and hydraulic conductivity. Groundwater quality will be determined by obtaining water samples from one monitoring well on a quarterly basis until the ash placement is completed. Analytical parameters will be identical to those presented in the column-leaching test. At least two samples will be analyzed prior to the pilot project. The results of the investigation will be presented in a report to all interested parties for approval. It is anticipated that up to ten wells will be installed to monitor variations in local aquifer characteristics as a result of coal ash burial. 2 CGRS,Inc. 2.3 Soil Borings Up to ten soil borings will be drilled by hollow stem auger techniques at locations depicted on Figure 3. Soil samples will be collected on five-foot intervals using a split-spoon sampler. Boring logs will be constructed and will include interpretations of soil characteristics, conditions encountered during drilling, sample locations,and any other observations pertinent to the soil boring operation. 2.4 Monitoring Well Installation Soil borings will be converted to two-inch diameter monitoring wells. The wells will be installed and screened from approximately five feet above the groundwater table to the vertical limit of the well. The monitoring wells will be constructed using two-inch diameter, flush threaded, schedule 40 PVC casing and factory slotted screen. Soil boring and groundwater monitoring methods and procedures are presented in Attachment A. 2.5 Groundwater Level Measurements and Chemical Analyses In soil borings completed as groundwater monitoring wells, the ground surface elevation of each boring and/or monitoring well will be surveyed to the nearest 0.01 foot, and referenced to an arbitrary datum if actual elevations cannot be determined. The areal location will be surveyed to the nearest 0.5 feet. _ Groundwater level measurements will be taken in the borings and wells by using an electrical water level indicator.This data will be used to construct a groundwater contour map, which will assist in characterizing groundwater flow direction and the hydraulic gradient of the water table surface. The hydraulic conductivity will be estimated by performing slug and/or aquifer testing. Prior to initiating the pilot project, groundwater quality samples will be obtained and analyzed for pH, TSS, TDS, and other relevant parameters identified in the laboratory leaching tests. Samples will be obtained from no less than one up-gradient and two down gradient wells.The anticipated locations of the monitoring wells are depicted on Figure 3.Typical monitoring well construction details are described in Attachment A. 2.6 Water Quality & Hydrogeologic Monitoring The effects on groundwater quality and hydrology as a result of coal ash burial will be evaluated by placing roughly 400 tons of coal ash within a trench at the location shown on Figure 3.The coal ash will be placed so that the water table intersects the coal ash and that any fluctuation of the water table will be within the coal ash bed. The coal ash will be buried in a trench measuring 10 feet in width, 100 feet in length and roughly 10 feet in depth. In order to evaluate hydraulic characteristics of bottom ash and fly ash, one-half of the trench will be filled with fly ash. A native soil divider will be left and the other half of the trench will be filled with bottom ash and fly ash. Bottom ash will be placed in the lower one-half of the saturated portion of the trench and fly ash 3 CGRS, Inc. will be placed to one foot below ground surface. Approximately one foot of native soil will be place over the entire trench. Variations in water quality will be verified through quarterly water quality monitoring for analytical parameters identified in the laboratory quality assurance plan (Appendix B).The results of the analyses will be submitted to the Colorado Department of Public Health and Environment, Division of Minerals and Geology and Weld County Health Department. Within one week of coal ash burial water quality samples will be obtained from all monitoring wells. Water quality samples will be obtained on a weekly basis for one month, then monthly till the end of the first quarter and then on a quarterly basis until project termination. Action Level (AL) wells will be placed between the ash and point of compliance(POC) wells. The distance of the wells will be 10, 25 and 40 feet from the trench. This staggered spacing will document water quality at various distances downstream from the trench. Water quality data will be used to validate analytical fate and transport models presented previously. The Al wells will provide early warning of possible adverse environmental impacts. However, the intent of the project is to determine if coal ash can be safely deposited in wet, high-energy environments. Analytical models predict that no standards will be exceeded at fifty feet downgradient of the trench, which is where the Division requires POC wells be placed. An exceedenance in water quality standards in AL wells should not constitute a violation of the permit. The petitioner reserves the right to terminate the project based on AL well water quality data. If a standard(s) is exceeded in an AL well no less than monthly monitoring will occur (in AL wells) to monitor possible adverse impacts at the POC wells. If a standard is exceeded in a POC well,the well will be re-sampled within one week of receiving analytical results. If the confirmation sample confirms the initial finding then the project will be terminated and the ash removed from the trench.The ash will be disposed of at an approved landfill as soon as the material reaches and acceptable moisture level. Background water quality data indicate that iron, lead, sulfate and nitrate have been measured at levels above established standards. Boron and nitrite have been measured at levels very close to established standards. Water samples will be obtained from wells placed in the trench. These data, as well as column leaching data, should establish the elements or compounds of concern. The determination that the ash has contributed to groundwater degradation shall be determined by the State's project manager with recommendations made by CGRS. 4 CGRS, Inc. 2.7 Aquifer Characterization In order to estimate the hydraulic conductivity (K) of the aquifer, a minimum of four slug tests will be conducted at monitoring wells deemed to be representative of the aquifer at the site and in the downgradient area. Water level measurements and times will be recorded using an InSitu Troll SP4000 pressure transducer. The test results will be input into standardized software, utilizing the Bouwer Rice Method, to determine hydraulic conductivity in the aquifer at each well. The average groundwater flow rate (v)can be estimated using the following equation: v= Ki/4) where: v=average groundwater flow rate(ft/day) K=hydraulic conductivity(ft/day) i=hydraulic gradient(ft/ft) =porosity (dimensionless). Permeability testing will be conducted in wells completed within the ash on a periodic basis to evaluate possible changes in hydraulic conductivity with time. 2.8 Contingency Plan and Abatement If adverse changes to water quality as predetermined by all interested parties are observed during testing, the coal ash will be immediately excavated and stored in a dry impoundment within the Varra property boundary. Native soils will be placed in the trench and water quality will be monitored on a monthly basis for the constituents of concern. Additional remedial activities, if needed, will be commensurate with the extent and degree of water quality degradation. The water quality monitoring schedule is rigorous and should allow for the detection of adverse environmental conditions long before any significant degradation could occur. If the project is terminated it is likely that the only corrective action that will be required is source removal and monitoring. Monitoring will be conducted until it can be demonstrated that points of exposure(POEs)are not subject to impact. Any other required remediation will be dependant on the physical and chemical characteristic of the contaminate of concern. Corrective action could include oxidant/reductant injection, permeable reactive barrier, groundwater pump and treat or any combination of the above. Analytical data generated from the column experiment indicates that boron and selenium are the most leachable elements (nonmetals). As such, it is likely that the most effective form of remediation would be groundwater recovery and treatment. Previous analytical studies show that a single well pumping less than 10 gpm would capture all groundwater bypassing the trench. Treatment for boron or selenium could be accomplished by ion exchange or reverse osmosis. Dilution with natural waters is also an option. 5 CGRS, Inc. 3.0 ORGANIZATION AND STAFF ASSIGNMENTS 3.1 Project Personnel Mr. Joby Adams of CGRS will serve as project coordinator and contact to Varra Companies. Dr. James Warner (CSU Groundwater Program Leader) of Colorado State University will provide senior technical review. Mr. Chester Hitchens of CGRS will serve as field coordinator and will be responsible for supervising drilling activities and will perform or supervise water quality sampling. 3.2 Subcontractors Subcontracted services for this project will include Drilling Engineers of Fort Collins, Colorado, and Technology Laboratories,Inc.,of Fort Collins,Colorado. Drilling Engineers will be responsible for drilling soil borings and completing the borings as groundwater monitoring wells.Technology Laboratory will analyze groundwater samples for the analytes of concern. 4.0 OVERVIEW- QUALITY ASSURANCE/QUALITY CONTROL Quality assurance (QA) is a management system for ensuring that all information, data, and decisions _ — resulting from the project are technically sound and properly documented. Quality Control (QC) is the functional mechanism through which quality assurance achieves its goals. Quality control programs, for example, define the frequency and methods of checks, audits, and reviews necessary to identify problems and dictate corrective action to resolve these problems, thus ensuring data of high quality. Thus, a QA/QC program pertains to all data collection,evaluation, and review activities that are part of the project. The use of qualified personnel for conducting various portions of the project is of paramount importance to an effective QA/QC program. This pertains not only to qualified QA/QC specialists, but also to specialists in other fields, including hydrogeologists, air quality specialists, soil scientists, analytical chemists and other scientific and technical disciplines. The project manager should ensure that qualified specialists, primarily individuals with the proper education, training, and experience, including licensed or certified professionals, are directing and performing the various project activities. The same general principles apply to selection of contractors and/or outside laboratories. Another important aspect of the QA/QC program is the communication between the QA/QC organization and the project manager. Regular appraisal by the project manager of the quality aspects related to the ongoing project data-gathering efforts provides the mechanism whereby the established objectives may be met. 6 CGRS, Inc. QA/QC procedures should provide details relating to the schedule, information to be provided, and the mechanism for reporting to the project manager. Reports to the project manager should include: • Periodic assessment of measurement data accuracy,precision, and completeness; • results of performance audits; • Results of system audits; • Significant QA/QC problems and recommended solutions; and • Resolutions of previously stated problems. The individual responsible for preparing the periodic reports should be identified. These reports should contain a separate QA/QC section that summarizes data quality information. The Quality Assurance Project Plan is presented as Attachment C. 5.0 REMARKS The scope of work is based upon current available information and our understanding of this project. As the project develops, changes to the project scope of work may be required. If changes in the scope of work are dictated by the needs of the project,these changes will be presented prior to implementation. This report was prepared by CGRS,INC. M` Dateo62/ / Joby L Adam P.G. Princip 1/Hydrogeologist Reviewed by: -44b, )� u, role Date 6/7/G/ Chester Irtchens,P.G. Senior Hydrogeologist 7 ; o 1 •N'.\ _V---->" \\N•Th 4906 .° ' :14 -7 C-----)1/ (-tett ���III O in = �• �/ch �g50 il � r,C J 4950 •it '4894 4 78 • '' 478 r I,. O ii -"a' --� _ — j5 N crm p \ 1 e ,I, J / I —��J �_ <.Aft; `� /I. SDitch \—, 0 II D� 1 / 1.1,0 , „--,_— 'i T- 29 p 50 i � � ii I Y 9 // Y II J Oli Y60 4. o ° / O / SITE 4897 ii, __ LOCATION _.. - _ \ • _..—_ - - - --- v' '11 ► M _ . II .. YYYY��� s 48,0 1 : - / z:\ 3 ?I II •y850 \ _ . I Y . _lam///1 9. `•I St Vrain Sch II -•U'J J� '�.•. aeoz ,',,tI IR- 'r} B� P -:1}__ 4 — / Po 4809 o %v f e/ B II �/ n 491 r • ° 4833 ' o 480. r" ///��� \ / —��\ __oe _- u avo BzJ / �} 1 _ N FIGURE 1 i _,OWANDA QUADRANGLE VARRA COMPANIES COLORADO-WELD Co SITE LOCATION MAP - COAL ASH STUDY AREA I 7 5 SERIES PROJECT NO. PREPAVED BY C G RS 1-135-2755 JLA y,7J,r COLORADO GROUNDWATER H.....-..- 0.1 DATE 07/02/98 REVIE D BY RESOURCE SERVICES 0 2000 4 %749 . i % CJ_°6 -)n1 m 1 � v ;t•- �� e a • aso \Ss c4 / o$iy •4894 66 \ — •6 I --I 0 2 ~ / ),/} cp :. 489r i1. r 829 - -- S.-- Lf �../'iI _ 099 ,` , n F I , ?? gy�pp.. .1$ . y`4kttP� I 4,, \ yp ...8082t V)-3m SCII P r/r6 .. � o 32 0, - \r '� ,, \ �.• 1 '�''D31 lin `A551 E09 o _K- "- f � _ ° �I. I J/ r SEEP �' Ilc u II a "m41: om II -. �,Th ' • • 1.1. ( B ' '"------‘ •4813 e 48/3 / — -- �4823 _ r+n Hce "' e iir7 - - _� ç asc ) / / AAA oi�ii� ,482 .' �/ �• 7-4830,-_, �iTCN ;.)„__z- . , --c u , �_ I�/// _ - f , P FIGURE 2 GOWANDA QUADRANGLE REGISTERED WELL LOCATIONS COLORADO-WELD Co. VARRA COMPANIES 7.5 SERIES PROJECT NO. PREPARED BY CGRS - 1-135-2755 JLA COLORADO GROUNDWATER 00 DATE 07/02/98 REVIEWED BY RESOURCE SERVICES CGWeld Gounry Planning Dept. JAN 0 4 1999 RECEIVED December 29, 1998 Glenn F. Mallory Colorado Department of Public Health and Environment (CDPHE) Hazardous Materials and Waste Management Division 4300 Cherry Creek Drive South Denver, CO 80246-1530 RE: Varra Coal Ash Project Weld County Colorado CGRS No. 1-135-2755 Dear Mr. Mallory: Enclosed please find the draft work plan for the Varra Coal Ash Burial Project. Please note that while the work plan describes in detail the laboratory testing methods and proposed field work, the work plan does not include analytical results or a discussion of analytical results as all of the results have not been received. When all results have been received and tabulated a final work plan will be submitted to all interested parties for review. The work plan is being submitted as a draft in hopes that the time required for review will he lessened once the final draft has been submitted. I have included a summary of analytical results available at this time (Table 2). The results are for water samples obtained form the Sequential Extraction Leaching Procedure (SELP), which is described in detail in the work plan. This test should represent the maximum leaching capability of a material, as it is an agitated extraction test. A review of analytical results shows that none of the samples exceeded hazardous waste characteristic levels. In addition, as a general trend, second extraction results were lower than initial extraction analyses. Aluminum and iron were the analytes most prevalent in exceeding primary or secondary drinking water standards. It is our belief that the non-agitated column leaching test will be most indicitative of field conditions and comparisons of pore volume flow through verses concentration will be made to access possible adverse impacts to waters of the State. P.O. Box 14£39 Sri ,, 71,-/ �: WORK PLAN VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COLORADO CGRS NO. 1-135-2755 by CGRS, INC. COLORADO STATE UNIVERSITY GROUNDWATER PROGRAM April 1, 1999 CGRS,Inc. Table of Contents 1.0 INTRODUCTION 1 1.1 Objectives 1 1.2 Background Information 1 1.2.1 Local Geology/Hydrology 1 1.2.2 Coal Ash Source 2 2.0 INITIAL LABORATORY TESTING 3 2.1 Hydraulic Conductivity 3 2.2 Porosity 3 2.3 Analytical Data 4 2.3.1 SELP 4 2.3.2 SGCLP 5 2.3.3 TCLP 5 2.3.4 SGLP 6 3.0 ANALYTICAL RESULTS 7 3.1 SELP 7 3.2 TCLP 7 3.3 SGLP 8 3.4 SGCLP 8 3.5 Overview of Laboratory Data 8 4.0 PILOT STUDY 9 4.1 Project Start-up 9 4.2 Hydrogeology Determinations 9 4.3 Background Water Quality 10 4.4 Water Quality and Hydrogeologic Monitoring 10 4.5 Contingency Plan and Abatement 11 5.0 PROJECT SCHEDULE 11 6.0 ORGANIZATION AND STAFF ASSIGNMENTS 11 6.1 Project Personnel 11 6.2 Subcontractors 12 7.0 OVERVIEW-QUALITY ASSURANCE/QUALITY CONTROL 12 8.0 REMARKS 13 CGRS,Inc. FIGURES: Figure 1 -Site Location Map Figure 2-Registered Well Location Map Figure 3 -Area Use and Site Condition Map TABLES: Table 1 -Results for Hydraulic Conductivity and Porosity Tests Table 2-Analytical Results—SELP Table 3 -Analytical Results—TCLP Table 4-Analytical Results—SGLP Table 5-Analytical Results-SGCLP Table 6-SELP Analytical Data in Excess of Water Quality Standards APPENDIX: Appendix A—Selected Data—Groundwater Quality and Hydrogeology of the Laramie-Fox Hills Aquifer in the Milton Reservoir Area,Weld County,Colorado Appendix B-Methods and Procedures Appendix C—Quality Assurance Project Plan CGRS,Inc. WORK PLAN _ VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COLORADO CGRS NO. 1-135-2755 1.0 INTRODUCTION This document presents the proposed work scope for the evaluation of coal ash burial in saturated media. The field investigation will be performed in conjunction with a variety of laboratory studies in order to evaluate potential liabilities or benefits associated with coal ash burial. Specifically, this project addresses issues associated with the reclamation of gravel quarries under saturated conditions. A variety of laboratory experiments were conducted in order to evaluate coal ash leaching potentials for different pH ranges relative to effluent pore volume. The information generated by this project will be invaluable to private companies or regulatory agencies insofar as evaluating under what conditions coal ash can be placed without incurring significant liability. This work is performed under the authorization of Varra Companies. The generation of this report was a joint effort between CGRS, Inc. and Colorado State University Groundwater Program(CSU). 1.1 Objectives The purpose of this project is to identify potential liabilities with the reclamation of gravel quarries with coal ash and to determine if coal ash meets the criteria for classification as an inert fill. Specific objectives for the Varra Coal Ash Burial Project are to determine: • Leaching characteristics of coal ash with respect to varying water quality conditions; • Permeabilities of various types of coal ash(bottom and fly ash); • Affects of coal ash burial on local hydrology and water quality; • Hydrogeologic properties of coal ash; and • Physical characteristics of coal ash in saturated media. 1.2 Background Information 1.2.1 Local Geology/Hydrogeology The study area is an active gravel quarry located in the NW 1/4, Section 31, Township 3 North, Range 68 West, 6th P.M., Weld County Colorado (Figure 1). The surficial geology of the area as 1 CGRS,Inc. documented by Colton, 1978, varies between wind blown deposits of clay, silt and sand and sandy to gravelly alluvium, which are Holocene in age. Colluvium consisting of bouldery to pebbly sandy silt and clay may contain and interfmger with alluvium of various ages. The depth to groundwater at the site generally varies between three and ten feet below ground surface(bus). The inferred groundwater flow direction is to the northeast roughly parallel to the St. Vrain River drainage. Water well records obtained from the Colorado Division of Water Resources indicate that one well may be located within one quarter mile of the proposed test plot. The registered well owner is Dakolios Construction and the permitted use of the well is industrial. The location of registered wells within a half-mile radius of the proposed test plot are depicted on Figure 2. Field verification of well locations and construction details, if available will be performed prior to project start-up. Groundwater quality data for the immediate study area are limited. Reeder, 1993, describes in detail the regional hydrogeology near the area of interest. Water quality data for 36 domestic wells completed as bedrock aquifers (Larimie-Fox Hills Formation) in the Milton Reservoir were compiled by Reeder. A review of water quality data indicate that all wells sampled exceeded water quality standards for total suspended solids and a large percentage exceeded standards for pH. Field and analytical data documented by Reeder and other background information are presented in Appendix A. 1.2.2 Coal Ash Source Public Service coal comes from a number of Colorado mines in Routt, Moffat, Delta and Gunnison counties. These mines include West Elk, TwentyMile, Powderhorn, and ColoWyo. This coal is normally purchased under long term contracts, which specify certain analytical parameters. Therefore, the chemical and physical properties of the coal (and resulting ash) do not change significantly from year to year. Analytical information for each of these coal sources is available as is the analytical information on the ash. This information has been provided in our earlier submittal. Comparisons of analytical data completed in the early 1990s with recent data indicate little variation in any of the ash constituents. 2 CGRS,Inc. 2.0 INITIAL LABORATORY TESTING Public Service Company generated analytical data indicating that fly ash is not a characteristic hazardous waste. Numerous analytical methods were used such as toxicity characteristic leaching procedure (TCLP). CGRS in conjunction with Colorado State University Groundwater Program performed a number of tests that included: • Hydraulic Conductivity Testing(Permeameter Test); • Porosity Determination; • Sequential Extraction Leaching Procedure(SELP); • Synthetic Ground Water Column Leaching Procedure(SGCLP); • Toxic Characteristic Leaching Procedure(TCLP); and • Synthetic Ground Water Leaching Procedure(SGLP). A discussion of these tests is provided below. 2.1 Hydraulic Conductivity The hydraulic conductivity of the ash was performed using either a "Constant Head" or "Falling Head" Permeameter. The Constant Head Permeameter works better for high permeability porous materials and the Falling Head Permeameter works best for low permeability porous materials. With either test the flow rate and the potentiometric head loss are measured through a sample of the ash. The hydraulic conductivity was then calculated using Darcy's Law. The hydraulic conductivity of the ash is required to determine the expected rate of groundwater flow through the buried ash and the effects of burial on ground water flow patterns. 2.2 Porosity Porosity is the ratio of the volume of the voids to the bulk volume of the sample. With this test the volume and dry weight of a sample of ash was measured. The ash was then saturated with water under a vacuum pressure and the weight of the saturated sample measured. For saturated conditions the volume of the voids is equal to the volume of the water. The porosity is required to determine the pore volume for the ash. The results of hydraulic conductivity and porosity testing are summarized in Table 1. 3 CGRS,Inc. TABLE 1 -Results for Hydraulic Conductivity and Porosity Tests Sample ID Hydraulic Porosity Conductivity K(ft/day) Cherokee Silo Ash 2/3 0.24 0.51 Cherokee 4 Ash with Sodium 0.23 0.46 Class F Silo Ash with Gypsum 0.09 0.49 Bottom Ash 178. 0.51 Recycled Concrete 111. 0.29 Recycled Asphalt 130. 0.33 The bottom ash, the recycled concrete and the recycled asphalt all had relatively high hydraulic conductivity values in the range of 111 to 178 feet/day. The three fly ash samples had very low hydraulic conductivity values in the range of 0.09 to 0.24 feet/day. The porosity of the fly and bottom ash ranged from 0.46 to 0.51. These values are characteristic of very fine porous materials. The porosity of the recycled concrete and asphalt was 0.29 and 0.33, respectively. 2.3 Analytical Data 2.3.1 "Sequential Extraction Leaching Procedure"(SELP) The purpose of the"Sequential Extraction Leaching Procedure" (SELP) test was to determine the total quantity of the various chemical contaminants that may be potentially leached from the ash. The SELP test used synthetic groundwater with varying pH levels as the leaching fluid(s). With the SELP test, a specified weight(e.g. one kilogram) of the ash was combined with a specified volume of water(e.g. one liter) and agitated by rolling for a specified period of time (e.g. 18 hours). This represented a single extraction. The concentration of the chemical contaminant was then measured in the water. The SELP test was repeated for several sequential extractions until most of the 4 CGRS,Inc. chemical contaminants have been extracted from the ash. This normally requires three or more extractions. Only two extractions were performed due to budgetary constraints. The SELP test was repeated for synthetic groundwater with varying pH values to represent a range of possible site conditions. Synthetic groundwater(s)with pH values of 5, 7 and 8.5 were used. The fast extraction from the SELP test for each pH value was analyzed for the full suite of chemical compounds. These include: • Sulfate • Chloride • Fluoride • Cyanide • Mercury •Nitrate •Nitrite • 20 other metals (Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Lithium, Manganese, Nickel, Selenium, Silver, Thallium, Vanadium and Zinc). Conductivity and pH will of the leachate was measured at C SU prior to sending the sample to the laboratory for chemical analyses. The SELP test was conducted at CSU. The extracted water samples from the test were sent to Analytica Environmental Labs for chemical analyses. Analytical results from the first extraction were used to identify those compounds to be analyzed for in subsequent extractions of the SELP test and in the SGCLP test. Those chemical compounds, which were either non-detect or detected at very low concentrations during the first extraction were not analyzed for in subsequent extractions of the SELP test or in the SGCLP test. 2.3.2 "Toxic Characteristics Leaching Procedure" (TCLP) The "Toxic Characteristic Leaching Procedure" (TCLP) test is designed to determine the mobility of toxicity characteristic constituents and is the EPA method for classifying wastes as hazardous or non hazardous based on toxicity. The full suite of chemical compounds(see list for SELP test) was analyzed during the TCLP test. 2.3.3 "Synthetic Ground Water Leaching Procedure"(SGLP) The"Synthetic Ground Water Leaching Procedure" (SGLP) test is identical to the TCLP test with the exception that synthetic groundwater is used as the leaching fluid. A description of the TCLP test is provided above. The SGLP test was developed to simulate geochemical conditions more 5 CGRS,Inc. closely approximating natural ground water than for the TCLP test. The results of the SGLP are directly comparable to the TCLP test. Groundwater obtained from the study area was used for the test. The full suite of chemical compounds (see list for SELP test) were analyzed during the SGLP test. The groundwater used in the SGLP test as the leaching fluid was analyzed for full suite of chemical compounds. The difference in the before and after chemical concentrations in the ground water used in the SGLP test represents the concentration of the chemical contaminants leached from the ash. 2.3.4 "Synthetic Groundwater Column Leaching Procedure" (SGCLP) The purpose of the "Synthetic Groundwater Column Leaching Procedure" (SGCLP) test was to determine the rate as a function of pore volume at which the chemical contaminant will be leached from the buried ash. The SGCLP test used synthetic groundwater with varying pH levels as the leaching fluid(s). With the SGCLP test, a specified weight (e.g. one kilogram) of the ash was placed in a column. Once the column was saturated, the testing period began. One pore volume of water was passed through the column and the concentration of the various contaminants measured in the outflow water. The SGCLP test was then repeated for several sequential pore volumes of water. The hydraulic head on the column was adjusted so that one pore volume of water was passed through the sample in about 12 hours. Water samples were obtained for analyses at 2, 4 and 8 pore volumes of water flow through. The SGCLP test was repeated for synthetic ground water with varying pH values to represent a range of possible site conditions. Synthetic ground water(s) with pH values of 5, 7 and 8.5 were used as the leaching fluid(s). For the fly ash, which has a very low hydraulic conductivity, the SGCLP test was conducted for 1, 2 and 4 pore volumes. For the bottom ash, the recycled concrete and the recycled asphalt, which have high hydraulic conductivity, water samples were analyzed at 2, 4 and 8 pore volumes. The chemical analyses for the first extraction of the SELP test was used to determine the suite of chemical compounds of interest in the SGCLP test. Chemical compounds, which were either non- detect or detected at very low were eliminated from further testing. The SELP test is a highly 6 CGRS,Inc. agitated test where as the SGCLP test is not. The SGCLP test was conducted at CSU with the collected water samples sent to Analytica Environmental Labs for chemical analyses. • Sulfate • Chloride • Fluoride • Cyanide • Mercury •Nitrite. Nitrate • 10 other metals from the following list of 20 metals (Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Lithium, Manganese, Nickel, Selenium, Silver, Thallium, Vanadium and Zinc). Conductivity and pH will of the leachate was measured at CSU prior to sending the sample to the laboratory for chemical analysis. 3.0 ANALYTICAL RESULTS 3.1 "Sequential Extraction Leaching Procedure" (sELn Analytical results for the SELP are presented in Table 2. As mentioned, the purpose of the SELP testing was to estimate the maximum leaching capability of a material. In general, substantial concentration reductions were observed in second extraction analyses. Of the metals analyzed, at all pHs Aluminum, Boron, Iron and Manganese appeared to be the most leachable. None of these elements are listed in the primary drinking water standards. It appears that variations in pH have some effect in leaching characteristics of the sample set. At a pH of 8.5, there were 14 elements that exceeded standards in samples obtained from Cherokee Silo Ash 2/3. These concentrations were generally much higher than other ash samples as well. Recycled asphalt had the next highest number of elements that were in excess of drinking water standards for metals. At a pH of 7, samples obtained from Class F Silo Ash with Gypsum appeared to be the most leachable and at a pH of 5, samples obtained from the recycled asphalt had the most elements exceeding drinking water standards. Of the nonmetals fluoride appeared to be the most leachable compound, insofar as having the most number of samples exceeding the agricultural water quality standard. 3.2 "Toxic Characteristics Leaching Procedure"(TCLP) The results of TCLP testing are presented in Table 3. A review of Table 3 shows that none of the samples tested exhibited characteristics of a hazardous waste. Overall, analyte concentrations were 7 CGRS,Inc. much less than those resulting from the SELP testing, which was a more aggressive test. Boron, fluoride and manganese appeared to be the most leachable analytes in this test. 3.3"Synthetic Ground Water Leaching Procedure"(SGLP) Analytical results for the SGLP are presented in Table 4. Water was obtained from the gravel quarry pond immediately adjacent from the proposed study area (Figure 3) and was used as the leaching fluid. This water is considered to be representative of local groundwater quality and was analyzed to determine background water quality of the leaching medium. A review of Table 4 shows that the only analytes that were in excess of any standards were boron, manganese, selenium, fluoride, sulfate and nitrite. The water obtained from the quarry had sulfate and fluoride concentrations of 2,900 and 4 mg/L, respectively. These concentrations are considered high enough to inhibit leaching of these analytes to the surrounding groundwater regime. 3.4 "Synthetic Groundwater Column Leaching Procedure" (SGCLP) The results for the SGCLP are presented in Table 5. A review of Table 5 shows that boron is the most leachable element with fluoride and sulfate being the most prevalent nonmetal constituents in excess of applicable standards. With the exception of aluminum and barium all constituents of concern decreased dramatically with respect to increasing pore volumes. It appears that variations in pH may have had a slight affect on leachability of different coal ash samples. 3.5 Overview of Laboratory Data The various testing regimes document hydraulic and leaching characteristics of coal ash. Permeabilities of coal ash varied over three orders of magnitude. The hydraulic conductivity of bottom ash closely approximated recycled concrete and recycled asphalt and is comparable to permeabilities associated with medium and coarse-grained sands. Fly ash samples were three orders of magnitude less permeable than bottom ash and non-ash samples and have permeabilities comparable with silt and clay. In general, the most prevalent elements or compounds detected in the leaching studies coincide with the general composition of coal ash(aluminum, barium, boron, iron and manganese). The intent of SELP study was to determine the maximum leachability of coal ash under different saturated environments — namely different pH values. Fluctuations in pH did seem to have an affect on the 8 CGRS,Inc. leachability of various samples. It appears that under certain conditions, recycled asphalt is more reactive with fluids than coal ash. Recycled concrete had minor reactivity with different leaching fluids. A summary of samples exceeding a water quality standard in the SELP testing is presented in Table 6. The TCLP testing showed dramatically reduced analyte concentrations. Boron, fluoride and manganese were the analytes the exhibited the most leachability above water quality standards in -- this test. The SCLP was identical to the TCLP testing with the exception that the gravel quarry water was used as the leaching medium. A review of Table 4 shows that boron was the most leachable element. Background levels of sulfate and fluoride exceeded water quality standards and were high enough to mask all leaching characteristics of these compounds. The SGCLP showed that boron, fluoride and sulfate were by far the most leachable compounds. Boron and sulfate concentrations decreased dramatically compared to pore volume flow through. 4.0 PILOT STUDY 4.1 Project Start-up The project start-up will consist of developing a work plan and a site specific Health and Safety plan. All required permits will be obtained prior to conducting the investigation. Utility companies will be contacted for the location of all underground utilities prior to commencing investigative activities (telephone, sewer, electrical, cable television, natural gas lines, oil and gas pipelines, buried tanks and wells). 4.2 Hydrology Determinations Prior to initiating coal ash placement, the local groundwater flow direction will be estimated from groundwater monitoring wells installed to determine hydraulic characteristics of the local aquifer and local groundwater quality. It is anticipated that ten wells will be installed to monitor variations in local aquifer characteristics as a result of coal ash burial. The hydraulic conductivity will be estimated by performing slug and/or aquifer testing. Prior to initiating the pilot project groundwater 9 CGRS,Inc. quality samples will be obtained and analyzed for pH, TSS, TDS, and other relevant parameters identified in the laboratory leaching tests. Samples will be obtained from no less than one up- gradient and two down gradient wells. The anticipated locations of the monitoring wells are depicted on Figure 3. Typical monitoring well construction details are presented in Appendix B. 4.3 Background Water Quality In addition to the laboratory testing presented herein, background groundwater quality samples will be obtained from site monitoring wells immediately subsequent to their placement and immediately prior to coal ash placement. The gravel quarry water obtained for the laboratory testing should be chemically consistent with local groundwater as it is in hydraulic connection with proposed testing site. The three sampling events should establish baseline levels of the constituents of concern. 4.4 Water Quality &Hydrogeologic Monitoring The effects on groundwater quality and hydrology as a result of coal ash burial will be evaluated by placing roughly 400 tons of coal ash within a trench at the location shown on Figure 3.The coal ash will be placed so that the water table intersects the coal ash and that any fluctuation of the water table will be within the coal ash bed. The coal ash will be buried in a trench measuring 10 feet in width, 100 feet in length and roughly 10 feet in depth. In order to evaluate hydraulic characteristics of bottom ash and fly ash, one-half of the trench will be filled with fly ash. A native soil divider will be left and the other half of the trench will be filled with bottom ash and fly ash. Bottom ash will be placed in the lower one-half of the saturated portion of the trench and fly ash will be placed to one foot below ground surface. Approximately one foot of native soil will be place over the entire trench. Variations in water quality will be verified through quarterly water quality monitoring for analytical parameters identified in the laboratory quality assurance plan (Appendix C). The results of the analyses will be submitted to the Colorado Department of Public Health and Environment, Division of Minerals and Geology and Weld County Health Department. Within one week of coal ash burial water quality samples will be obtained from all monitoring wells. Water quality samples will be obtained on a weekly basis for one month and then on a monthly basis. The length of 10 CGRS,Inc sampling will be determined after reviewing the initial analytical results; it is not anticipated that more than three months will be required before water quality parameters equilibrate. Surface water quality will be monitored by obtaining samples from the Saint Vrain river downstream of the study area. Surface water samples will be obtained at the same frequency as groundwater samples. 4.5 Contingency Plan and Abatement If adverse changes to water quality as predetermined by all interested parties are observed during testing, the coal ash will be immediately excavated and stored in a dry impoundment within the Varra property boundary. Native soils will be placed in the trench and water quality will be monitored on a monthly basis for the constituents of concern. Additional remedial activities, if needed, will be commensurate with the extent and degree of water quality degradation. 5.0 PROJECT SCHEDULE Upon authorization to initiate field testing, two weeks will be required to contract subcontractors and initiate field activities. Based on laboratory experiments it is anticipated that approximately three months will be required to perform field activities. The project length is based partially on pore volume flow through calculations and the observed leachability of coal ash samples. It is anticipated that a summary report will be submitted within four months of coal ash placement. The report will detail analytical results, hydraulic characteristics of the ash bed, observed variations in hydrogeology and water quality. 6.0 ORGANIZATION AND STAFF ASSIGNMENTS 6.1 Project Personnel Mr. Joby Adams of CGRS will serve as project coordinator and contact to Varra Companies. Dr. James Warner (CSU Groundwater Program Leader) of Colorado State University will provide senior technical review. Mr. Chester Hitchens of CGRS will serve as field coordinator and will be responsible for supervising drilling activities and will perform or supervise water quality sampling. CGRS,Inc. 6.2 Subcontractors Subcontracted services for this project will include Drilling Engineers of Fort Collins, Colorado, and Analytica Environmental Laboratories, Inc., of Broomfield, Colorado. Drilling Engineers will be responsible for drilling soil borings and completing the borings as groundwater monitoring wells. Analytica will analyze groundwater samples for the analytes of concern. 7.0 OVERVIEW - QUALITY ASSURANCE/QUALITY CONTROL Quality assurance (QA) is a management system for ensuring that all information, data, and decisions resulting from the project are technically sound and properly documented. Quality Control (QC) is the functional mechanism through which quality assurance achieves its goals. Quality control programs, for example, define the frequency and methods of checks, audits, and reviews necessary to identify problems and dictate corrective action to resolve these problems, thus ensuring data of high quality. Thus, a QA/QC program pertains to all data collection, evaluation, and review activities that are part of the project. The use of qualified personnel for conducting various portions of the project is of paramount importance to an effective QA/QC program. This pertains not only to qualified QA/QC specialists, but also to specialists in other fields, including hydrogeologists, air quality specialists, soil scientists, analytical chemists and other scientific and technical disciplines. The project manager should ensure that qualified specialists, primarily individuals with the proper education, training, and experience, including licensed or certified professionals, are directing and performing the various project activities. The same general principles apply to selection of contractors and/or outside laboratories. 12 CGRS,Inc. Another important aspect of the QA/QC program is the communication between the QA/QC organization and the project manager. Regular appraisal by the project manager of the quality aspects related to the ongoing project data-gathering efforts provides the mechanism whereby the established objectives may be met. QA/QC procedures should provide details relating to the schedule, information to be provided, and the mechanism for reporting to the project manager. Reports to the project manager should include: • Periodic assessment of measurement data accuracy, precision, and completeness; • results of performance audits; • Results of system audits; • Significant QA/QC problems and recommended solutions; and • Resolutions of previously stated problems. The individual responsible for preparing the periodic reports should be identified. These reports should contain a separate QA/QC section that summarizes data quality information. The Quality Assurance Project Plan is presented as Attachment C. 8.0 REMARKS The scope of work is based upon current available information and our understanding of this project. As the project develops, changes to the project scope of work may be required. If changes in the scope of work are dictated by the needs of the project, these changes will be presented prior to implementation. 13 CGRS,Inc. This report was prepared by CGRS, INC. Date 1-////77 Joby L. da , P.G. i ydrogeologist CGRS,Inc Reviewed by: /_/• N/_.. Date f{//97 r. James W. Warner, P.E. Groundwater Program Leader Colorado State University ,,,,,,,,,,,,,, pp REg/ ''•, �0• '�SW wq?'tye0' pe Z^S `4 16492 '°: '',41/011A1. ,6,,, 14 REFERENCES Dragun, J., 1988. The Soil Chemistry of Hazardous Materials. Hazardous Materials Control Research Institute. Silver Spring, Maryland, pp 76-80 Hassett, D.J. "A Generic Test of Leachability: The Synthetic Groundwater Leaching Procedure" In Proceedings for the Waste Management for the Energy Industries Conference; University of North Dakota, April 29-May 1, 1987. Hem, J. D., 1992. Study and Interpretation of the Chemical Characteristics of Natural Water. U.S. Geological Survey Water-Supply Paper: 2254 Reeder, D.C., 1993. Groundwater Quality and Hydrogeology of the Laramie-Fox Hills Aquifer in the Milton Reservoir Area, Weld County, Colorado: Colorado State University Unpublished Master's Thesis. Sorini, S. 1997. "A Summary of Leaching Methods" American Coal Ash Association, Inc. Alexandria, Virginia. 1 i °) " . \\\____ _ _ + __ .... 4 100-±7 o 4906 _-, — .1 4 19 i — 1 e et • 40 ' / \---//- ^05011� / I J94444 co _�_ O` il I ///// i ii: —_ ---,4,\ i I a ii iI II-. Vn n / it % 3 a/ O I_I / _ Ditch �' • n O //�— II ` ii I 29 :oil__ I: II 0 \ 4850 ..'a /-- -/ k p`A/, 800 , 1 �0 J� \ im / �� 0 SITE I- e '°. 1LOCATION �. Wes.• - II •1: 3 F-! 7- / 4799 1 �I 5,0 ; y.. Y�^O"`7 R'�..:. - _i / 4g5� V,� p�y �'4Wt / p51 a 4809 / 0 55Q/ - BM ' 46Uv � 4813 '462] 4813 a • CHANCE — - II (7-7------__ °65C • ) a II Q / • o / J N FIGURE 1 J .;OWANDA QUADRANGLE VARRA COMPANIES COLORADO-WELD Co SITE LOCATION MAP -COAL ASH STUDY AREA I 7 5 SERIES PROJECT NO PREPA ED BY CG RS 1-135-2755 JLA COLORADO GROUNDWATER J DATE 07/02/98 REVIE D BY RESOURCE SERVICES i 0 2000 \ 1 4906 - —�� J' I �' �' \ / 19 (7, /> ( �J` o -1 v 485° JJJa �°a _ I Y ,478 479 0950 c 66 \ , ! it I dE p __ -_-/lam/ /� 9Ad it e / e• Ditch \-•%-",„ 5, cy.„± } __/--- '-'- ---- ___y :r v °p 9 0 II i o 489] •it 828 -- r II.o ^� is Y i— 4799 rj 'w ae5° ' �" �' �q�St Vrain Sch y \, 1._... ,:.5" to //) a oo •I e / 32 5,55 o �I`31 V �� As7 °'''1 1 4 4809 ...... , -4-_ 'wry ! . i yE, /. ffII BM ' e` / • 4 - 9 4813 • _ 4813 c `� 48T3 � u CI\-- oscCMANOE� - -' III 0 /_61 aII _.40N ^ II ,- 4630��`� O re ,y I/� �\ 4 / - > V V FIGURE 2 GOWANDA QUADRANGLE REGISTERED WELL LOCATIONS VARRA COMPANIES COLORADO-WELD CO. 7.5 SERIES PROJECT NO. PREPARED BY CGRS 1-135-2755 JLA COLORADO GROUNDWATER Impuil DATE 07/02/98 REVIEWED BY RESOURCE SERVICES I0 2000 Ta Analytical Results Fly Ash Disposal Project Weld County,Colorado CGRS Project No. 1-135-2755 Total Metals Analytical Results (mg/L) Sample pH Ex Al Sb As Ba Be B Cd Cr Co Cu Fe Pb Mn Ni Se Ag TI V Zn LI Hg Class F Silo Ash with 8.5 1 27.00 ND ND 3.80 0.003 5.70 ND 0.13 ND 0.03 7.40 ND 0.07 ND ND ND ND 0.05 0.05 0.24 ND Gypsum (C Silo) 2 970 ND ND 8.40 ND 0.69 ND 0.07 ND 0.01 2.20 ND 0.02 ND ND ND ND 0.02 0.02 0.12 ND Bottom Ash 8.5 1 29.00 ND ND 1.30 0.002 1.70 ND ND ND 0.09 15.00 ND 0.14 0.02 ND ND ND 0.05 0.15 0.05 ND 2 37.00 ND ND 1.60 0.003 1.20 ND ND ND 0.12 21.00 ND 0.21 0.01 ND ND ND 0.06 0.22 0.04 ND Cherokee Silo Ash 2/3 8.5 1 780.00 ND 0.40 5.20 0.082 120 0.05 0.52 Oil 0.80 210.00 0.62 1.40 0.18 0.64 ND ND 1.70 1.10 1.50 NA 2 Cherokee 4 Fly Ash 8.5 1 1.50 ND ND 0.98 ND 48 ND 0.19 ND ND 0.31 ND ND ND 0.23 ND ND ND ND 0.76 ND with Sodium 2 3.70 NA NA 2.10 NA 17 NA 0.63 NA NA 0.26 ND NA NA 0.10 NA NA NA NA 0.26 NA Recycled Concrete 8.5 1 1.90 ND ND 0.32 ND ND ND 0.07 ND 0.05 0.56 ND 0.02 0.02 ND ND ND ND 0.01 0.02 ND 2 47.00 NA NA 0.71 NA NA NA 0.05 NA 0.15 56.00 NA 170 0.04 NA NA NA NA 0.57 0.05 NA Recycled Asphalt $.5 1 150.00 ND ND 1.90 0.009 0.09 ND 0.17 0.06 0.41 160.00 0.41 4.30 0.12 ND ND ND 0.31 1.50 0.15 ND 2 2.50 NA NA 0.25 ND ND NA 0.06 ND 0.02 0.27 ND ND ND NA NA NA ND ND 0.02 NA Class F Silo Ash with 7 1 750.00 ND ND 1.90 0.073 21.00 0.01 0.50 0.11 0.59 200.00 0.10 2.00 0.22 ND ND ND 1.30 0.61 0.56 0.002 Gypsum(C Silo) 2 12.00 NA NA 13.00 ND 0.30 ND 0.04 ND 0.01 3.30 ND 0.03 ND NA NA NA 0.02 0.01 0.14 ND Bottom Ash ] 1 0.45 ND ND 0.08 ND 1.00 ND ND ND ND 0.24 ND ND ND ND ND ND ND ND 0.03 ND 2 6.10 ND ND 0.27 ND 0.62 ND ND ND 0.02 3.40 ND 0.04 ND ND ND ND 0.02 0.08 0.01 ND Cherokee Silo Ash 2/3 7 1 0.54 ND ND 0.79 ND 45 ND 0.11 ND ND 0.06 ND ND ND 0.19 ND ND 0.01 ND 0.73 ND 2 110.00 ND ND 6.70 0.008 22 ND 0.05 ND 0.09 32.00 0.11 0.13 0.02 0.13 ND ND 0.17 0.13 0.33 0.001 Cherokee 4 Fly Ash 7 1 0.21 ND ND 0.88 ND 45 ND 0.18 ND ND 0.06 ND ND ND 0.20 ND ND ND ND 0.76 ND with Sodium 2 84.00 NA NA 5.30 NA 24 NA 0.11 NA NA 22.00 NA NA NA 0.14 NA NA NA NA 0.31 NA Recycled Concrete 7 1 2.60 ND ND 0.15 ND ND ND 0.13 ND 0.06 0.64 ND 0.02 ND ND ND ND ND 0.01 0.02 ND 2 State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050 .20/1.0 0.30/5.0 0.050 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards A P P P P A P P A NS S/A P S P P P P A A A P Notes: ND=Not Detected NA=Not Analyzed EX=Extraction mg/L=milligrams per liter A-Agricultural Standard P-Primary Drinking Water Standard 5-Secondary Drinking Water Standard Page 1 of 4 Ta 2 Analytical Results Fly Ash Disposal Project Weld County,Colorado CGRS Project No.1-135-2755 Total Metals Analytical Results (mg/L) Sample pH Ex Al Sb As Ba Be B Cd Cr Co _ Cu Fe Pb Mn Ni Se Ag Ti V Zn Li Hg Recycled Asphalt 7 1 1.2 ND ND 0.089 ND ND ND ND ND ND 0.88 ND 0.026 ND ND ND ND 0.01 0.011 0.009 ND 2 26 NA NA 0.39 ND 0.18 NA NA ND NA 28 NA 0.076 NA NA NA NA 0.062 0.36 0.03 NA Class F Silo Ash with 5 1 0.10 ND ND 0.98 ND 6.10 ND 0.10 ND ND ND ND ND ND ND ND ND ND ND 0.19 ND Gypsum (C Silo) 2 0.13 NA NA 0.94 NA ND NA 0.06 NA NA NA _ NA NA NA NA NA NA NA NA 0.13 NA Bottom Ash 5 1 6.40 ND ND 0.36 ND 1.20 ND ND ND 0.03 4.20 ND 0.05 ND ND ND ND 0.02 0.06 0.03 ND 2 0.37 NA NA 0.06 NA 0.56 NA NA NA ND 0.20 _ ND ND NA NA NA NA ND ND 0.01 ND Cherokee Silo Ash 213 5 1 44.00 ND ND 2.90 0.0036 51.00 ND 0.13 ND 0.04 12.00 ND 0.05 ND 0.27 ND ND 0.06 0.06 0.77 0.0001 2 5.10 NA NA 1.70 NA 15.00 NA ND NA ND ND NA ND NA ND NA NA 0.03 ND 0.22 ND Cherokee 4 Fly Ash 5 1 0.61 ND ND 0.77 ND 51.00 ND 0.21 ND ND 0.11 ND ND ND 0.21 ND ND ND ND 0.77 ND with Sodium 2 4.10 NA NA 1.10 NA 22.00 NA 0.05 NA NA 0.28 NA NA NA 0.13 NA NA NA NA 0.24 NA Recycled Concrete 5 1 1.30 ND ND 0.45 ND 0.08 ND 0.06 ND 0.04 0.56 ND 0.01 ND ND ND ND ND ND 0.02 ND 2 2.30 NA NA 0.23 NA ND NA 0.08 NA 0.02 0.09 NA ND NA NA NA NA NA NA 0.02 NA Recycled Asphalt 5 1 120.00 ND ND 1.60 0.01 0.09 ND 0.13 0.05 0.33 140.00 0.33 3.90 0.10 ND ND ND 0.26 1.30 0.12 ND 2 87.00 NA NA 1.00 0.01 0.08 NA 0.07 0.03 0.22 90.00 0.19 2.30 0.62 NA NA NA 0.17 0.86 0.08 NA State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050 .20/1.0 0.30/5.0 0.050 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards A P P P P A P P A A/S S/A P S P P P P A A A P Notes: ND=Not Detected NA=Not Analyzed EX=Extraction mglL=milligrams per liter A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 2 of 4 1 I Table 2 Analytical Results Continued Sample pH Ext Other Analytical Results (mg/L) Total Cyanide Free Cyanide Chloride Fluoride Sulfate Nitrate Nitrite Class F Silo Ash with Gypsum (C Silo) 8.5 1 ND NA 130 8.4 23 7.9 4.6 2 ND NA 20 5.8 65 3.3 1 Bottom Ash 8.5 1 ND NA 29 0.95 170 1.1 0.031 2 ND NA 6.5 0.35 45 0.31 0.067 Cherokee Silo Ash 2/3 8.5 1 NA 0.021 5.1 3.1 ND 0.35 0.013 - 2 NA 0.016 5.7 1.3 69 ND 0.0058 Cherokee 4 Fly Ash with Sodium 8.5 1 0.021 4.9 5.8 1100 0.14 ND 2 NA 0.012 1.2 3.1 59 0.15 0.0082 Recycled Concrete 8.5 1 HA. 0.047 26 5.3 10 1.4 0.096 2 NA 0.027 1.5 1.2 8.3 0.4 0.034 Recycled Asphalt 8.5 1 NA 0.012 10 0.98 44 ND 0.0078 2 NA ND 1.6 1.2 8.2 0.2 0.0055 Trip Blank 1 8.5 NA NA 31 1.5 2.6 NA NA Class F Silo Ash with Gypsum (C Silo) 7 1 ND 120 11 840 7.4 1.3 2 N A ND 31 7.4 19 2.1 1 Bottom Ash 1 NA ND 23 0.89 140 0.87 0.048 2 NA ND 5.1 0.46 33 0.16 ND Cherokee Silo Ash 2/3 7 1 NA ND 4.1 4.7 430 0.23 0.014 2 NA ND 1.8 2.3 60 0.17 0.32 Cherokee 4 Fly Ash with Sodium 7 1 0.011 3.4 5.1 430 0.2 0.017 2 NA ND 1.8 3.1 49 0.12 0.036 Recycled Concrete 7 1 NA 0.11 26 4.1 31 0.92 ND 2 State Water Quality Standards 0.2 250 2.0 250 10 1 P S A P P P Note: NA-Not Analyzed ND=Not Detected A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Other Analytical Page 3 of 4 \\CGRS_HQ_SERVER\JOBY\EXCEL\Varra Chem List2.zls Analytical Results in Excess of Water Quality Standards Fly Ash Disposal Project Weld County, Colorado CGRS Project No. 1-135-2755 TOTAL METALS Ex Total Class F Silo Ash with 1 6 11 1 18 Gypsum (C Silo) 2 3 3 0 6 Bottom Ash 1 4 1 3 8 2 4 2 0 6 Cherokee Silo Ash 2/3 1 11 4 6 21 2 NR 8 2 10 Cherokee 4 Fly Ash 1 4 3 3 10 with Sodium 2 4 5 2 11 1 2 1 4 Recycled Concrete 1 2 3 NR 0 3 1 9 1 8 18 Recycled Asphalt 2 0 3 7 10 pH 8.5 7 5 OTHER ANALYTICAL Class F Silo Ash with 1 2 2 3 7 Gypsum (C Silo) 2 1 1 2 4 1 0 0 1 1 Bottom Ash — 2 0 0 0 0 1 1 2 2 5 Cherokee Silo Ash 2/3 2 0 1 1 2 Cherokee 4 Fly Ash 1 2 2 2 6 with Sodium 2 1 1 1 3 1 1 1 2 4 Recycled Concrete 2 0 0 1 1 1 0 2 0 2 Recycled Asphalt 2 0 0 0 0 pH 8.5 7 5 Ex-Extraction# NR-Results not received at this time Page 1 of 4 ATTACHMENT A METHODS AND PROCEDURES CGRS, Inc. METHODS AND PROCEDURES Soil Borings Soil sampling will be conducted in accordance with ASTM:D 1586-87. Using this procedure, a 2-inch O.D. split-spoon sampler will be driven into the soil by a 140 pound weight falling 30 inches. After an initial set of 6 inches, the number of blows required to drive the sample an additional 12 inches, known as the penetration resistance (N value), will be recorded. The N value is an index of the relative density of cohesionless soils and the consistency of cohesive soils. Soil Classification/Characterization As samples are obtained in the field, they will be visually inspected and classified in accordance with ASTM:D 1488-84. Representative portions of the samples will then be retained for further examination and for verification of the various strata, the N value, water level data, and pertinent information regarding the method of maintaining and advancing the boring will be provided. Charts illustrating the soil classification procedure,descriptive terminology and symbols used on the logs will be provided. Decontamination _ — To avoid potential transport of contaminated materials to the project site, all drilling equipment and down- hole tools will be steam cleaned prior to mobilization. Monitoring Well Construction Monitoring wells will be installed utilizing the following general construction criteria: • borehole diameter: minimum 6.25inches; • well diameter: 2 inches; • estimated depth: 15 —30 feet below ground surface; • casing material: schedule 40, flush thread PVC; • well screen: 2 inch I.D., 10 feet in length, #0.01 slot PVC; • estimated screened interval: 5 feet above and 10- 25 feet below the groundwater table; • annular pack: 10-20 silica sand; • protective casing: minimum 12 inch I.D., steel flush or above grade, locking cap; and • annular seal: cement grout and bentonite pellets. Groundwater Sampling All borings where groundwater is encountered will be sampled from the suspected cleanest to the most contaminated according to the protocols listed below. All pertinent information will be recorded on a sampling information form. CGRS, Inc. Field Protocol Step 1 -Measure water level. Step 2-A dedicated polyethylene bailer will be used to develop each boring. Three bore volumes will be evacuated from each boring prior to sampling. Step 3-Collect water samples. Water samples will be collected using a polyethylene bailer. A field blank will be collected during the sampling program to ensure quality control. Step 4-Store samples in a cooler on ice for transport to the laboratory. Follow all documentation and chain-of-custody procedures. Step 5-Clean equipment. Water level measurement equipment will be cleaned with ethanol followed by a deionized water rinse. Upon completion of soil or groundwater sampling, a chain of custody log will be initiated. A copy of the chain of custody will be returned to the project manager. Chemical Analysis All analytical parameters are described in the Laboratory Quality assurance plan presented as Appendix C. Groundwater Elevation Measurements The following outlines our standard groundwater quality sampling methodology. Before purging any of the soil test borings or monitoring wells,water level measurements must be taken. Measuring Point Establish the measuring point for the well. The measuring point is marked on the north side of the top of the temporary monitoring well riser. The top of the riser is normally a 2 inch casing inside a locked protective casing. The riser will be PVC pipe, galvanized pipe or stainless steel pipe. The measuring point should be described on the groundwater sample collection record. Access After unlocking or opening a monitoring well, the first task will be to obtain a water level measurement. Water level measurements will be made using an electronic water level indicator. Depth to water and total depth of the well will be measured for calculation of purge volume. CGRS, Inc. Measurement To obtain a water level measurement, lower a decontaminated electronic water level probe into the monitoring well. Care must be taken to assure that the electronic probe hangs freely in the monitoring well and is not adhering to the well casing. The electronic probe will be lowered into the well until the audible sound of the unit is detected and the light on the electronic sounder illuminates. At this time, the precise measurement should be determined by repeatedly raising and lowering the probe to obtain an exact measurement. The water level measurement is then entered on the groundwater sampling collection record sheet or groundwater level data sheet to the nearest 0.01 feet. Decontamination The electronic probe shall be decontaminated immediately after use by wiping with isopropyl alcohol- - soaked paper towels. Always proceed in order from the suspected cleanest well or soil test boring to the suspected most contaminated one. Purge Volume Computation All soil test borings and temporary monitoring wells will be purged prior to sample collection. Depending upon the rate of recovery, three to five volumes of groundwater present in a well or bore hole shall be withdrawn prior to sample collection. If a well or bore hole bails dry, the well or bore hole should be allowed to recharge and a sample taken as soon as there is sufficient volume for the intended analysis. The volume of water present in each well or bore hole shall be computed using the two measurable variables, length of water column in soil boring or monitoring well and diameter. Purging and Sample Collection Procedures Bailing • Obtain a laboratory decontaminated disposable bailer and a spool of nylon rope or equivalent bailer cord. Tie a bowline knot or equivalent through the bailer loop. Test the knot for adequacy by creating tension between the line and the bailer. Tie again if needed. New rope will be used for every sample or purge. New clean latex gloves will be used when touching the rope or bailer. • Spread a clean plastic sheet near the base of the well. The plastic sheet should be of sufficient size to prevent bailer or bailer rope from contacting the ground surface. • Place the bailer inside the well to verify that an adequate annulus is present between the bailer and the well casing to allow free movement of the bailer. • Lower the bailer carefully into the well casing to remove the sample from the top of the water column, taking care not to agitate the water in the well. CGRS, Inc. • Pour the bailed groundwater into a bucket. Once the bucket is full, transfer the water to a barrel and contain on-site. • Raise the bailer by grasping a section of cord, using each hand alternately. This bailer lift method will assure that the bailer cord will not come into contact with the ground or other potentially contaminated surfaces. Sampling Instructions for obtaining samples for parameters are reviewed with the laboratory coordinator to insure that proper preservation and filtering requirements are met. • Appropriate sample containers will be obtained from the contract laboratory. After samples are collected, they will be put on ice in coolers (4°C). Care will be taken to prevent breakage during transportation or shipment. • Samples collected by bailing will be poured directly into sample containers from bailers. The sample should be poured slowly to minimize air entrapment into the sample bottle. During collection,bailers will not be allowed to contact the sample containers. • Upon completion of sampling a chain-of-custody log will be initiated. Chain-of-custody records will include the following information: project name and number, shipped by, shipped sampling point, location, field ID number, date, time, sample type, number of containers, analysis required and sampler's signature. The samples and chain-of-custody will be delivered to the laboratory. Upon arrival at the laboratory the samples will be checked in by the appropriate laboratory personnel. Laboratory identification numbers will be noted on the chain-of-custody record. Upon completion of the laboratory analysis, the completed chain-of-custody record will be returned to the project manager. Field Cleaning Procedures For all equipment to be reused in the field,the following cleaning procedures must be followed: • Disassemble the equipment to the extent practical. • Wash the equipment with distilled water and laboratory-grade detergent. • Rinse with distilled water until all detergent is removed. • Rinse the equipment with isopropyl or methanol, making sure all surfaces, inside and out, are rinsed. • Triple rinse the equipment with distilled water. Laboratory Selection The project manager should consider the following factors when selecting a laboratory: • Capabilities (facilities, personnel, instrumentation), including: • Participation in interlaboratory studies (e.g., EPA or other Federal or State agency sponsored • analytical programs); • Certifications (e.g., Federal or State); CGRS, Inc. • References (e.g. other clients); and • Experience (UST, RCRA and other environmentally related projects). • Service; • Turnaround time; and • Technical input(e.g., recommendations on analytical procedures). The project manager is encouraged to gather pertinent laboratory-selection information prior to extensively defining analytical requirements under the project. A request may be made to a laboratory to provide a qualifications package that should address the points listed above. Once the project manager has reviewed the various laboratory qualifications, further specific discussions with the laboratory or laboratories should take place. In addition, more than one laboratory should be considered. For large-scale investigations, selection of one laboratory as a primary candidate and one or two laboratories as fall-back candidates should be considered. The quality of the laboratory service provided is dependent on various factors. The project manager should be able to control the quality of the information (e.g., samples) provided to the laboratory. It is extremely important that the project manager communicate to the laboratory all the requirements relevant to the _ — project. This includes the number of samples and their matrices, sampling schedule, parameters and constituents of interest, required analytical methodologies, detection limits, holding times, deliverables, level of QA/QC, and required turnaround of analytical results. Field and Laboratory Ouality Control General Quality control checks are performed to ensure that the data collected is representative and valid data. Quality control checks are the mechanisms whereby the components of QA objectives ore monitored. Examples of items to be considered are as follows: I. Field Activities: • Use of standardized checklists and field notebooks; • Verification of checklist information by an independent person; • Strict adherence to chain-of-custody procedures; • Calibration of field devices; • Collection of replicate samples; and • Submission of field blanks, where appropriate. 2. Analytical Activities: CGRS, Inc. • Method blanks; • Laboratory control samples: • Calibration check samples; • replicate samples; • Matrix-spiked samples; • "Blind"quality control samplers; • Control charts; • Surrogate samples; • Zero and span gases; and • Reagent quality control checks. Blind Duplicates Blind duplicate samples will be collected for 10% of the samples collected or once per site, whichever is greater. These blind duplicate samples will be forwarded to the laboratory as a check of laboratory reproducibility. Equipment(Rinseate)Blank The equipment (rinseate) blank is designed to identify potential cross-contamination in the field between sample sources due to deficient field cleaning procedures. This blank also addresses field preservation procedures, environmental site interference, integrity of the source blank water for field cleaning and those concerns singularly addressed by the travel blank. Equipment blanks are taken once per site, when equipment is cleaned in the field. This provides a quality control check on field cleaning procedures. Field Blank Field blanks are used to evaluate the sample container filling procedure, the effects of environmental contaminants at the site, purity of preservatives or additives and those concerns uniquely addressed by the travel blank. Field blanks are taken downwind of the most contaminated area of the site by filling laboratory cleaned and prepared sample containers (appropriate for the parameters group) with deionized or organic-free water supplied by the laboratory. The blank sample container is then sealed, grouped,transported and stored with the real samples collected for the same parameters group. CGRS, Inc. Travel(Trip)Blanks The travel blank is designed to address interferences derived from improper sample container cleaning preparation, contaminated source blank water, sample cross-contamination during storage/transport and extraneous environmental conditions affecting the sampling event to and from the site, including delivery to the laboratory. Travel blanks are composed in the appropriate sample container using source blank water. Preservatives or additives are added if required for the parameters group. Travel blanks are then sealed and stored in the ice chest where real samples will be stored and transported. Travel blanks are to originate at the laboratory providing the blank water for the equipment and field blanks. Protocol for Analyzing Blank Samples If used, the equipment blank will be analyzed first. If contamination is found to be present, the field blank will then be analyzed. If the equipment blank is not used, the first blank analyzed will be the field blank. If any blank is found to be contaminant-free, the sequence of analyses will be terminated. ATTACHMENT B QUALITY ASSURANCE PROJECT PLAN Table of Contents 1.0 Project Management 1 1.1 Introduction 1 1.2 QAPP Distribution List 1 1.3 Project Organization 1 1.4 Problem Definition/Background 2 1.5 Intended Usage of Data 2 1.6 Project Task/Description 2 1.7 Measurement Quality Objectives 3 1.8 Data Quality Objectives 3 1.8.1 Data Precision and Accuracy 4 1.8.2 Data Representativeness 4 1.8.3 Data Comparability 4 1.8.4 Data Completeness 5 1.9 Special Training Requirements 5 1.10 Documentation and Records 5 2.0 Measurement/Data Aquisition 6 2.1 Sampling Process Design 6 2.2 Sampling Method Requirements 7 2.3 Sample Handling and Custody Procedures 7 2.3.1 Sample Identification 7 2.3.2 Sample Method Requirements 7 2.3.3 Sample Custody 7 2.3.4 Chain of Custody Records 8 2.3.5 Transfer of Custody and Shipment 8 2.3.6 Laboratory Custody Procedures 9 2.4 Laboratory Deliverables 9 2.5 Field and Laboratory QA/QC Procedures 10 2.6 Instrument/Equipment Testing, Inspection and Maintenance Requirements 10 2.7 Instrument Calibration and Frequency 10 2.8 Inspection/Acceptance Requirements 11 2.9 Data Acquisition Requirements 1 1 2.10 Data Management 11 3.0 Assessment/Oversight 12 3.1 Assessment and Response Actions 12 3.2 Reports 13 4.0 Data Validation and Usability 14 4.lData Review Validations and Verification 14 4.2 Validation and Verification Methods 14 4.3 Reconciliation with DQO's 14 Table of Contents - Continued Figures Figure 1 -Area Use and Site Condition Map Figure 2—Monitoring Well Placement Map Figure 3 —Monitoring Well Construction Detail Table Table 1 —Summary of Parameters, Sample Containers, Holding Times and Analytical Methods Table 2—Contents of Digital Analytical Deliverables Appendix Appendix A—Resumes QUALITY ASSURANCE PROJECT PLAN (QAPP) FOR THE VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COLORADO 1.0 Project Management 1.1 Introduction This Quality Assurance Project Plan (QAPP) presents the organization, objectives, planned activities and specific Quality Assurance (QA)/Quality Control (QC) procedures associated the Varra Coal Ash Project. Specifically it is being prepared as part of a column leaching study. All QA/QC procedures will be structured in accordance with applicable technical standards. This abbreviated QAPP bas been prepared in accordance with the U.S. EPA RCRA QAPP Instructions, and other relevant guidance documents. 1.2 QAPP Distribution List The following have been provided copies of the work plan and this QAPP. a) Brad Janes—Varra Companies b) Chris Varra—Varra Companies c) Christina Kamnikar—DMG d) George Moravec—CDPH&E e) Harry Posey—DMG f) Jerald Ritenour—Barringer Laboratories g) Ken Niswonger—CDPH&E h) Roger Doak—CDPH&E i) Trevor Jiricek—Weld County Health 1.3 Project Organization Name/Affiliation Title/Responsibility Chris Varra—Varra Companies Petitioner Christina Kamnikar—DMG MLR Permit Review George Moravec—CDPH&E Water Quality Overview Glen Mallory —CDPH&E Certificate of Designation Review Jerald Ritenour—Barringer Laboratories Laboratory Project Manager Joby Adams—CGRS, Inc. Project Manager Ken Niswonger—CDPH&E Technical Oversight Robert Zielinski—USGS Column Leaching Method Oversight Roger Doak—CDPH&E Certificate of Designation Review Trevor Jiricek—Weld County Health USR/Certificate of Designation Review Varra Companies Quality Assurance Project Plan Page I 1.4 Problem Definition/Background Varra Companies has submitted a proposal to reclaim approximately 11 acres of a mined out, flooded gravel quarry using coal ash as fill material. Numerous permits have been submitted proposing bench scale testing followed by a small scale field study to evaluate the economic and technical feasibility of using coal ash as fill material in saturated conditions. The proposed field study consists of placing 400 tons of coal ash below the water table at the Varra gravel quarry in Weld County,Colorado Five different leaching experiments were conducted in order to evaluate coal ash leaching potentials. Two of the leaching experiments compared element and compound water quality for different pH ranges relative to effluent pore volume. However, the data generated from the different leaching tests were not comparable to each other or to water quality standards. It was recommended by various member of the Colorado Department of Public Health and Environment (CDPH&E) that additional leaching tests be performed that would simulate, to the extent possible, conditions that would be encountered at the Varra property. A modified form of ASTM D 4874-95 Standard Test Method for Leaching Solid Material in Column Apparatus was used to simulate field conditions. Testing results have been submitted as part of a permit application to conduct the pilot study. 1.5 Intended Usage of Data CGRS will use the data obtained in a variety of ways. The major applications of data are: Health and Safety—Data are used to determine concentration of chemicals to which workers will be or are being exposed. Site Characterization—Data are used to determine local physical and chemical properties of soil and water at the Varra property. Samples of soils, surface and ground water will be analyzed in the field using portable or transportable instruments or sent to the laboratory for certified chemical analyses. Project Feasibility—Data obtained from the pilot study will be used to assess the feasibility of large scale reclamation using coal ash. Risk Assessment—Data are used to calculate the effects of target analytes upon human health and other environmental receptors. Column study data will be compared to field data to assess the validity of column leaching studies and analytical solute transport and groundwater flow solutions. 1.6 Project Task/Description The purpose of the pilot project is to determine the feasibility of using coal ash as fill material in saturated conditions. This project will be accomplished by submitting required permits in combination with conducting bench scale leaching tests and a small scale ash burial and water quality monitoring program. The permit submittals are required as coal ash is classified as a solid waste and as such is subject to regulation under RCRA. The laboratory testing and proposed field tests are being conducted to fulfill permit requirements as well as provide assurance to all parties involved the placement of coal ash below the water table at this specific site will not cause adverse environmental impacts. The scope of work for this project involves, development of Health and Safety and site-specific work plans, field investigations, laboratory analysis of water samples, analysis of hydraulic and hydrogeologic properties, and the preparation of a report detailing the results of the investigation. Varna Companies Quality Assurance Project Plan Page 2 Project Timetable Activity Projected Start Date Anticipated Completion Date Submit supplemental information 03/2000 07/2000 and finalize permits to regulatory agencies Install pre-project monitoring wells Upon receipt that project Two week after notice is technically feasible from CDPHE Finalize CD and USR submittals 09/2000 10/2000 Construct pilot trench/monitoring 10/2000 11/2000 network Conduct monitoring 11/2000 11/2001 Submit monitoring information to 11/2000 12/2001 — -- regulatory agencies 1.7 Measurement Quality Objectives Quality assurance (QA) is a management system for ensuring that all information, data, and decisions based upon the interpretation of the analytical data are technically sound and properly documented. Quality control (QC) is the mechanism whereby the QA system is ensured. The QA system is presented in this QAPP. The goal of the environmental data collection is to produce data capable of withstanding scientific scrutiny and of a quality appropriate for a specific task. This will allow CGRS, Inc. to fully assess the impact of past activities and target analytes, i.e., identification, quantification,and delineation of the extent. Data quality refers to the level of uncertainty associated with a data set. Data quality objectives (DQOs) for each task will reflect the amount of uncertainty in the data that will be acceptable to meet the goals of the program and the objectives of the task. Project and task DQOs are discussed in Section 1.8. Techniques to validate and verify the quality of the data are presented in Section 4.2. Quality assurance objectives differ for individual sample matrix groups and parameters by site. The QA objectives will be based on a common understanding of the intended use of the resulting data, available laboratory procedures, and available resources. Special attention must be paid to the detection limits and holding times. These limits are sometimes insufficient for the analysis of drinking water,groundwater,and/or soils. 1.8 Data Quality Objectives DQOs are qualitative and quantitative statements that specify the quality of the data required to support decisions made during the project. DQOs are applicable to collection activities and are Varm Companies _ Quality Assurance Project Plan Page 3 based on the end use of the data being collected. DQOs will be described in detail within individual sampling and analyses plans(SAPs). Precision, Accuracy, Representativeness, Completeness and Comparability (PARCC) parameters are indicators of data quality. The end use of the measurement data should define the necessary PARCC parameters. Numerical precision, accuracy, and completeness goals must be established in each site SAP and will aid in selecting the measurement methods. 1.8.1 Data Precision and Accuracy Precision is a measurement of the reproducibility of a measurement under a given set of conditions. The closer the numerical values of the measurements, the more precise is the overall measurement. Precision will be stated in terms of the standard deviation for three or more measurements of the percent difference for two measurements, depending on the necessary precision of a particular study. Laboratory precision will be within established control limits for a particular analytical method, if known. For chemical analyses, laboratory precision will be assessed using laboratory- spiked samples Accuracy is defined as the degree of agreement between the measurement and average of measurements of measurements for a parameter and the accepted reference or true value. It will be expressed as the difference between the measured value (X) and the reference or true value (T), the difference in percent between two values, 100(X-T)/T, or a ratio of the two values, X/T,depending upon the study. Laboratory accuracy will be within established control limits for a particular method when known. For chemical analyses, laboratory accuracy will be assessed using laboratory-spiked samples. 1.8.2 Data Representativeness Representativeness expresses the degree to which data accurately and precisely represent a characteristic of a population, parameter variations at a sampling point, a process condition or an environmental condition. Accurate sample collection requires that samples be undisturbed and representative of the native substance being sampled. All measurements will be made so that the results are accurately representative of the media (air, biota, soil or water) and specific time, place and conditions being measured. Representativeness of a sample will be ensured by systematic,documented and (whenever possible) random sampling designs. Project Managers designing SAPs will ensure that, whenever possible, probabilistic sampling designs are used and that a sufficient number of samples are collected to meet the DQOs of the project. To minimize the introduction of error during the field program, general requirements for sample collection and handling have been devised and are described in the QAPP. Specific procedures will be presented in respective SAPs. 1.8.3 Data Comparability Data comparability expresses the confidence factor by which one data set can be compared to another. All data will be calculated and reported in units consistent with all the sites involved and the regulatory standards allowing for comparability of databases within the project. Data comparability will be achieved using standard field and analytical methods or written procedures. Data with different quality objectives will be compared in a statistically defensible manner outlined when the data are presented. Factors that will ensure data comparability are summarized as follows: • Standard procedures for sample collections; • Standard sample handling and transport; Varra Companies _ Quality Assurance Project Plat Page 4 • Uniform sampling containers (i.e. containers that are supplied, constructed, cleaned and prepared identically); • Standardized forms and/or electronic data storage devices for recording field and analytical data, prepared sample identification tags, and Chain-of-Custody (COC) records; • Field team performance observations; • Field and laboratory instrument performance; • Standardized protocols for field and laboratory instrument calibrations using certified standard solutions; • Data documentation audits to determine data adequacy; and • Known and validated uncertainties for field and analytical data. 1.8.4 Data Completeness Completeness is defined as a measure of the amount of valid data obtained from a measurement system compared to the amount that was expected under correct normal conditions. Field sampling conditions are unpredictable and non-uniform. Other problems affecting field completeness will be equipment/instrument malfunctions and problems with sample recovery. These problems will be reduced by training field team members to perform basic repairs and by supplying spare parts and equipment at the field site. Analytical completeness is affected by a sample not analyzed before its holding time is expired; if it is damaged during handling, shipping, unpacking, or storage; or if the laboratory data cannot be validated and the sample cannot be reanalyzed. Critical samples are those samples that are essential to the successful completion of the project. The completeness goal for crucial samples is 100%. The project team will present any deviation from the sampling plan. 1.9 Special Training Requirements No special training requirements or certifications are required for this project except for the 40-hour HAZWOPER class and annual refreshers. Resumes of CGRS personnel who may be involved with this project are presented in Attachment A. 1.10 Documentation and Records Activities that affect data and data quality and that potentially will be used as evidence will be documented. The project manager will maintain a supply of and will control these documents. The following documents will be used if appropriate: ➢ Sample labels; ➢ Chain-of-Custody records; ➢ Sample analysis request sheets; ➢ Electronic data storage devices and/or field logbooks; ➢ Calibration logbooks; ➢ Shipping logbooks; ➢ SAPs; ➢ QAPP: ➢ Progress and interim reports; V arra Companies �. � . Quality Assurance Project Plan Page 5 ➢ Information written on photos, maps and drawings; ➢ Laboratory data packages; and ➢ Data qualification packages. All information pertinent to field sampling operations will be recorded including all field observations and in situ measurements necessary to explain and reconstruct sampling operations. The primary repository for the information will be a Dell computer backed up with a field logbook. Each sample will be identified with a label.Labels will be placed on the containers prior to or at the time of sampling. Samples requiring refrigeration will be placed in a chest immediately after collection. A description of sampling locations, sample containers, time of collection, preservations if any used and various other pertinent facts relative to sample collection and preservation will be recorded in the field logbook. Sample/data collection activities will be documented fully and accurately. Log books will be used to record mapping locations and specific considerations associated with sample acquisition, preparation, transportation, receipt by a certified laboratory and analysis to be performed on the sample. Sample locations will be surveyed so the exact sample locations will be known. In addition, logbooks will be used to record when and where photographs, temperatures, pressures, etc. are taken. Field sampling team will have at least one person designated as the Site Supervisor who will be thoroughly familiar with documentation procedures. The site supervisor will personally perform, or at least oversee, the completion of documents that accompany the samples. For consistency in data recording, whenever possible, one person on each field sampling team will record data. Using one person to record data will permit timely recording of observations, enable more data to be recorded,and minimize any chances of contaminating field records. Documentation in logbooks, sample tags, labels, custody seals and other accountable serialized documents will be completed with permanent reproducible ink. None of these documents will be destroyed or thrown away, even if the comments are illegible or if inaccuracies are recorded that must be replaced. The documents will be marked "VOID" and maintained by CGRS. CGRS will hold all documentation for 5 years subject to the availability of any other authorized person. Document control means that controlled documents will receive review and concurrence as appropriate, the distribution of the documents will be recorded and revisions will be made in all distributed copies. The preparation, issuance and revisions of documents that specify quality requirements or prescribed activities affecting quality will be controlled to ensure that correct documents are used. Control will consist of item identification, secure storage and documented distribution. 2.0 Measurement/Data Acquisition 2.1 Sampling Process Design The pilot trench will be constructed downgradient of the proposed large scale reclamation as shown on Figure 1. The trench will consist of two coal ash cells with a native soil divider as shown on Figure 2. The ash will be obtained from Public Service Company's Cherokee power plant and will consist of a combination of Class F silo ash with gypsum and Cherokee 4 fly ash with sodium. Monitoring wells will be installed within the ash deposit(s) and compliance points or sentinel wells will be installed no less than 50 feet downgradient of the trench. It is anticipated that a minimum of eight wells will be installed up, down and cross gradient to the trench; however, additional wells Varra Companies Quality Assurance Project Plan Page 6 will be installed as necessary to adequately monitor variations in water quality and groundwater flow direction. Water quality samples from site monitoring wells on a periodic basis in order to evaluate possible changes in water quality. The sampling frequency will be weekly for the first month, biweekly for the second month, monthly for the third month and then quarterly until project termination. 2.2 Sampling Method Requirements All groundwater samples will be obtained using protocol presented in the Work Plan. All samples will be analyzed after the 0.45 µm filtration with the exception of field parameters. The samples will be collected in appropriate sample containers and will be transported to the laboratory under strict chain-of-custody procedures and holding times. Samples will be analyzed for alkalinity as bicarbonate and carbonate, chloride, fluoride, phosphorus, nitrate, nitrite, and sulfate along with other metals aluminum,antimony,arsenic, barium,beryllium,boron,calcium,cadmium,chromium, cobalt, copper, iron, lead, lithium, manganese, mercury, molybdenum, nickel, phosphorous, potassium, selenium, silver, thallium, titanium, uranium, vanadium and zinc. Field parameters such as pH, conductivity and temperature will be measured with a HyDAC digital conductivity, pH and temperature meter. 2.3 Sample Handling and Custody Procedures 2.3.1 Sample Identification A sample identification scheme will be used that maintains consistency for the names of water quality samples, as well labels affixed to each sample container, and entered on to the Chain-of- Custody(COC)forms. The following scheme will be followed: 1. Samples from the field study will be identified by the monitoring well it was obtained from. For example water obtained from monitoring well MW-1 would be identified as PT-MW-1. 2. Water samples obtained from the gravel quarry will be identified as Pond. 2.3.2 Sample Method Requirements Analytical procedures for water and soil samples will conform to the USEPA guidelines described in SW 846 (Test Methods for Evaluating Solid Waste/PhysicaUChemical Methods, 3rd ed.). Table 1, presents the analyses that are anticipated on the project. 2.3.3 Sample Custody Strict chain-of-custody (COC) protocol will be maintained throughout the life of the field program and will be controlled through the use of a COC Record supplied by the laboratory. The following procedures will be used to document,establish,and maintain custody of field samples: • Sample labels will be completed for each sample using waterproof ink; making sure that the labels are legible and affixed firmly on the sample container; • All Sample-related information will be recorded in the project log book; • The field sampling technician will retain custody of the samples until they are transferred or properly dispatched to a laboratory; and, • As fieldwork is conducted the on-site CGRS technical lead will determine whether these procedures are being followed, if corrections need to be made, and if additional samples are required. Varna Companies Quality Assurance Project Plan Page 7 2.3.4 Chain of Custody Records A Chain of Custody Record will be maintained in the field for all samples to be shipped to the laboratory for analysis. The three lines of information to be entered into the COC box titled "Project or P.O.#" are: Line 1. Client Name, i.e. "Varra Companies" Line 2. Project Name, i.e. "Varra Coal Ash Project" Line 3. Site Number, i.e. "2755aa" The three lines of information will be provided on the laboratory paper(hard copy)reports as a page header, and on the electronic deliverables as three individual fields in each analytical record. The "Sample Identification" entries to the COC will be completed as described in Section 2.3.1 of this QAPP. 2.3.5 Transfer of Custody and Shipment Due to the evidentiary nature of field sample collection,the possession of samples must be traceable from the time the samples are collected until they are introduced as evidence in legal proceedings. A sample is defined as being under a person's custody if any of the following conditions exist: (1) it is in their possession, (2) it is in their view after being in their possession, (3) it is in a secure locked location after having been in their possession, and (4) it is in a designated secure area. The following procedures will be used in transferring and shipping samples: • Field personnel will maintain detailed notes in field logbooks documenting the collection and identification of the required samples. The logbooks will be checked against the COC records for completeness and traceability. • A COC record will accompany all sample shipments. When transferring samples, the individuals relinquishing and receiving will sign, date, and note time on the record. The COC documents transfer of sample custody from the field-sampling technician to another person or to the laboratory. • Each cooler is to contain samples from one site. No mixing of samples from multiple sites will be allowed in a given cooler. • Samples will be properly packaged for shipment and shipped to the laboratory for analysis with a separate signed COC record enclosed in each sample box or cooler. Two copies of this record will accompany the samples to the laboratory. The laboratory maintains one file copy, and the completed original will be returned to the project manager as part of the final analytical report. This record will be used to document sample custody transfer from the field-sampling technician to the laboratory or to the CGRS offices. Just prior to shipment to the laboratory, coolers will be secured with custody seals. • Whenever samples are split with a facility operator or government agency, a separate COC record will be prepared for those samples and so marked to indicate with whom the samples are being split. • The COC record showing identification of the contents will accompany all packages. The original record will accompany the shipment and the field team leader will retain a copy. • A bill of lading will be used for all samples sent by common carrier. Receipt of bills of lading will be retained as part of the COC permanent documentation. Varra Companies Quality Assurance Project Plan Page 8 2.3.6 Laboratory Custody Procedures The laboratory, at a minimum, will check all incoming samples for integrity and note any observations of the original COC record. Each sample will be logged into the laboratory system by assigning it a unique laboratory identification number. This number and the field sample identification number will be recorded on the laboratory report. The original COC record will be returned to the CGRS project manager for filing. The laboratory sample custodian will use the following procedures to maintain the COC records once the samples arrive at the laboratory. • The samples received by the laboratory will be cross-checked to verify that the information on the sample label matches that on the COC record included with the sample shipment. • The "Received by Laboratory" box on the COC record will be signed on receipt. Any discrepancies between the COC record and the shipment contents will be resolved as soon as possible through communication with CGRS personnel. • The status of the sample receipt and analysis will be tracked within the analytical laboratory by a laboratory information management system (LIMS) or equivalent computerized management system. For data that are input by an analyst and processed using a computer, a copy of the input data will be kept and identified with the project number and any other needed information. The samples analyzed will be clearly noted and the input data signed and dated by the analyst. 2.4 Laboratory Deliverables The laboratory is required to submit EPA QC Level III data packages (CLP-equivalent) to CGRS, Inc. within 21 days from the date of acceptance on the Sample Receipt Form. Details of the deliverables are presented below. • Sample Receipt - The laboratory will complete and submit a "Sample Receipt" form for all sample shipments received. The purpose of the form is to note problems with sample packaging, COCs, and sample preservation. Problems noted on the form will be communicated to CGRS, Inc. as soon as possible. • Reporting of Analytical Results — For each analytical method performed, the laboratory will report all analytes as detected concentrations or as less than the specific limits or quantification. All samples with out-of-control spike recoveries being attributed to matrix interferences should be designated as such. All soil/sediment and solid waste samples should be reported on a dry-weight basis with percent moisture also reported. Also, report dates of extraction/preparation, dates of analysis, and dilution factors when applicable. An electronic deliverable (LIMS) will be provided that conforms to the CGRS project data requirements. An example of the data deliverable is provided as Table 2. • Internal Quality Control Reporting — Internal QC samples should be analyzed at rates specified in the method (SW-846). At a minimum, QC deliverables will consist of laboratory blank results, surrogate spike percent recoveries, results of IC/ICP analyses, laboratory control sample data, laboratory duplicate results, and if requested, calibration and tuning data. The internal QC data will not be delivered unless requested by Varra or CGRS personnel. Varna Cuinparnec Quality Assurance Project Plan Page 9 2.5 Field and Laboratory QA/QC Procedures Quality control checks are performed to ensure that the data collected are representative and valid. Quality control checks are the mechanisms whereby the data quality objectives are monitored. The quality control samples to be collected on the project are described below. • Duplicate Samples — As a check for laboratory reproducibility, blind duplicate samples (unknown by the laboratory to be duplicates) will be collected and submitted to the laboratory at a rate of one for every 10 water samples collected, or once per site, whichever is greater. • Field Blank Samples —To evaluate sample bottle filling procedures and the effects of environmental contaminants at the site, one VOA water sample per site is collected in laboratory-cleaned and prepared containers of deionized or organic-free water supplied by the laboratory. Field blanks are collected downwind of the most contaminated area within a site. The sample is sealed, labeled and shipped with the real samples collected for the same parameter group. • Travel (Trip) Blanks — Trip blanks are intended to address interferences derived from improper sample container cleaning, preparation, contaminated source blank water, sample cross-contamination during storage and shipment, and environmental conditions affecting the sampling event to and from the site, including delivery to the laboratory. Trip blanks will originate at the laboratory and will consist of VOA vials filled with source blank water, and will be sealed and stored in the cooler where real samples will be stored and shipped. • Equipment Blanks — Rinseate blanks, intended to provide quality control on field cleaning procedures, will be collected once per site. 2.6 Instrument/Equipment Testing,Inspection and Maintenance Requirements SOPs or manufacturer instructions for calibration of equipment will be referenced or included in each site SAP. These procedures for calibration will conform to manufacturer's recommended procedures or explain the deviation from said procedures. A copy of the procedure should be kept with the instrumentation. Calibration standards will be traceable to the National Institute of Standards and Technology (NIST) or other nationally recognized sources. The information will be recorded in the equipment calibration logbook. The date of calibration, an identification of standards used, the names of personnel performing calibration, the results of any calibration, and a list of any corrective actions taken will be recorded in the calibration logbook. One logbook will be maintained for each piece of equipment or device. A list of field equipment used in a sampling task will be included in each site SAP. A review of each site SAP by the Project Manager will ensure that measuring and test devices are of the proper type,range,and accuracy for the test to be performed within the established DQOs of a task. All measuring and test devices requiring calibration will be marked with calibration due dates. Documented and approved laboratory procedures will be used to calibrate analytical instruments. If necessary, at the discretion of the Program Manager, audits of instrument calibration laboratories will be performed to ensure proper calibration of instruments. Audits conducted by the Project Manager may be used to satisfy the audit requirements. 2.7 Instrument Calibration and Frequency This section provides guidance for control, calibration, and adjustment of field and laboratory measuring and testing instruments. Once calibrated, these devices must then be transported and handled to prevent the device from becoming out of calibration. Varna Companies Quality Assurance Project Plan Page 10 A calibration program will control measuring and test equipment used in the field and laboratory. Equipment of the proper type, range, accuracy and precision will provide data compatible with project requirements and desired results. Calibration of measuring and test equipment may be performed internally using reference standards or externally by agencies or manufacturers. Data generated from equipment that has failed calibration shall be evaluated and qualified for use on the project. The evaluation/qualification process is the responsibility of the Project Manager. The method of qualification and the results of the data evaluation will be documented. 2.8 Inspection/Acceptance Requirements for Supplies and Consumables No special requirements are needed. 2.9 Data Acquisition Requirements Paper and electronic transfer of data will be conducted with multiple levels of redundancy. Data will be verified manually and at time electronically at each stage of transfer to ensure accuracy. The flow data from collection through storage is described in the CGRS data management system. Data validation is the process by which a sample measurement, method, or piece of data is deemed useful for a specified purpose. Data validation methods will depend on the type of study that generated the data,the type of sampling,the test method,and the end use (DQOs)of the data. The Project Manager is responsible for specifying (in the site-specific SAP) the systematic process to be used to review the body of data against a set of criteria to assure that the data are adequate for their intended use. The process shall consist of data editing, screening, checking, auditing, verification, certification, and review. Criteria for accepting or rejecting data are dependent on the DQOs for a particular task. Data qualified for use in one task may not be acceptable for use in another task. 2.10 Data Management The data management system provides control and retention for project-related information. Data control includes receipt from external sources, transmittal, transfer to storage and indication of record status. Retention includes receipt at storage areas, indexing, and filing, storage and maintenance and retrieval. The control of records provides for the flow of information both internal and external to CGRS. Typical controls applied by CGRS for the various record systems are described in the following sections. Project related materials which are incoming to CGRS in the form of correspondence, drawings, sketches, logs, authorizations, or other information shall be routed to the project manager after the original is marked with the date received by a secretary assigned this duty. The manager shall then mark the original with the project number and determine which personnel shall review the incoming materials and shall route the materials accordingly. As soon as practical, correspondence originals shall be placed in the project file. If the correspondence is required by CGRS personnel for reference, a copy should be made rather than holding the original. Client drawings should be placed in the project file when they are received. The file index shall indicate the date received, drawing number and revision number. If revised issues of drawings pertinent to a project are received, superseded drawings shall be marked "void," "see revision," or with a similar notation. Varra Companies _ Quality Assurance Project Plan Page I I Project-related materials transmitted external to CGRS including correspondence, reports, drawings and sketches shall be appropriately reviewed, approved and, as required, signed prior to transmittal. Project correspondence shall, as a minimum, be signed by the project manager or an individual assigned this responsibility by the project manager. If joint signatures are desirable, the originator of the correspondence, when different than management, may also sign. Outgoing project correspondence and reports should be read, as appropriate, by the project manager prior to mailing. If, because of scheduling difficulties, it is necessary to mail correspondence prior to the project manager reading the final copy, the department manager or office manager shall read the correspondence. A copy shall then be routed to the project manager. Drawings issued in final form shall be approached prior to issuance by the project manager or a member of the project team delegated this responsibility by the project manager. Drawings which are issued "preliminary" do not require approval prior to issue; however, they shall be clearly marked to indicate preliminary status. Drawings issued as a separate transmittal shall be accompanied by a transmittal letter listing each drawing by number. If a drawing is "preliminary," it shall be stated in the letter. A copy of the drawing may be maintained by CGRS with the letter of transmittal, if deemed necessary by the project manager. If an original drawing is transmitted to the client at their request, a good quality reproducible of that drawing shall be prepared prior to transmittal and filed in the CGRS original drawing file maintained by Drafting personnel. The transmittal letter shall explicitly state that the original drawing has been transmitted to the client. Records submitted to the project file, with the exception of correspondence, should be bound, placed in folders or binders, or otherwise secured for filing. Folders or binders containing calculations and their checkpoints shall be marked with the title of the calculations. 3.0 Assessment/Oversight 3.1 Assessment and Response Actions The project manager will conduct an audit of the field activities for this project as requested by authorized review personnel. An audit will be conducted on field activities as field data are generated, reduced, and analyzed. Items will include, but are not limited to, calibration records of field equipment, daily entries in logbooks, decontamination procedures, photographs, video logs, data logs, drilling, well installation,and sampling. The primary objective of the field audit is to determine the status of sampling operations. Emphasis is placed on: • Verifying that operational aspects and procedures are in accordance with the protocols and QA/QC plan; • Verify the collection of all samples, including duplicates and field blanks; • Verifying that documentation is in order and sufficient to establish the collection location of any sample collected; Varra Companies Quality Assurance Project Plan Page 12 • Determining discrepancies that exist and initiating corrective action, as appropriate; and • Collecting independent samples. Records inspected include: • COC forms; • Sample logs; • Sample shipping logbooks; • Sample collection logbooks; • SAPs; and • SOPs and sampling procedures. After completion of the surveillance, any deficiencies will be discussed with the field staff and corrections will be identified. If any of these deficiencies could affect the integrity of the samples being collected, the audit team will inform the field staff immediately so that corrective action can be implemented immediately. The project manager will submit a surveillance report to the manager of the task and to the organization or subcontractor that was observed. 3.2 Reports Periodic reports on the performance of the QA program may be prepared by the project manager. When appropriate, analytical laboratory QA/QC reports will be included. At the completion of a task and after data verification and validation,all QC data will be sent to the files. Results from a data collection activity will be reported in units consistent throughout a task. Data from each different task will be compared using referenced statistical methods when data are presented. When applicable, for example, presenting data on chemical concentrations, the method detection limit, the environmental background concentration, and any applicable State or Federal regulatory limits will be presented with the analytical data. At minimum, laboratory reports will contain the following information for sample analysis: • Title of project and project identification number; • Name of report; • Date report was prepared; • Name, address, and telephone number of the laboratory; • Sample identification number(s); • Matrix of samples; • Level III—Method blanks, blank/spikes, surrogates, matrix spikes, control charts, matrix spike duplicates, duplicates, GC/MS tuning information, raw data, internal standard area summaries, and initial and continuing calibration data; • Level IV — When requested a data package as thorough as those required by the CLP shall be delivered. The package shall include a summary and the remainder of the package, including initial and continuing calibration, matrix spikes, matrix spike duplicates, as applicable, blanks, duplicates, surrogate recoveries, chromatograms, mass spectra, laboratory control samples, and absorbance data. For methods that are not defined by the CLP, the calibration information, method blanks, blank/spikes, Varra Companies Quality Assurance Project Plan Page 13 chromatograms, absorbance, matrix spikes, and matrix spike duplicated should be included; • Level V—Method blank data and the control chart from the blank/spike; • Date of analysis was performed; • Signature of laboratory manager; • Method precision, accuracy, and completeness attainable; • QA checks to be run as part of the method; and • Limitations of the method. 4.0 Data Validation and Usability 4.1Data Review Validations and Verification Data reduction refers to computations and calculations performed on data. This includes, but is not limited to, summary statistics, standard errors, confidence limits, test of hypothesis relative to the parameters, and model validation. Paper and electronic transfer of data will be conducted with multiple levels of redundancy. Data will be verified manually and at times electronically at each stage of transfer to ensure accuracy. The flow data from collection through storage is described in the CGRS data management system. Data validation is the process by which a sample measurement, method, or piece of data is deemed useful for a specified purpose. Data validation methods will depend on the type of study that — generated the data, the type of sampling, the test method, and the end use(DQOs) of the data. The project manager is responsible for specifying the systematic process to be used to review the body of data against a set of criteria to assure that the data are adequate for their intended use. The process shall consist of data editing, screening, checking, auditing, verification, certification, and review. 4.2 Validation and Verification Methods The project manager will perform the final review and approval of the data prior to it being entered into the last system as valid. The project manager will look at field duplicates, matrix spike/matrix duplicates, lab blanks and lab duplicates to ensure they are acceptable. The project manager will also compare the sample descriptions to the field sheets for consistency and will ensure that any anomalies in the data are appropriately documented. 4.3 Reconciliation with DQOs Once the data results are compiled, the project manager will review the field duplicates to determine if they fall within the acceptance limits as defined in the QAPP. Completeness will also be evaluated to determine if the completeness goal for this project's requirements as outlined in the QAPP (including the accuracy for lab spikes) the data may be discarded and re-sampling may occur. The project manager will be responsible for determining the cause of failure and make the decision to discard the data and re-sample. If the failure is tied to the analysis calibration and maintenance techniques will be reassessed as identified by the appropriate lab personnel. If the failure is associated with the sample collection and re-sampling is needed the samplers will be retrained. Varra Companies Quality Assurance Project Plan Page 14 xi/ / --2531.23 f 0 ; '`ems- N sr, ea? � _ 00,,0 _ � - 1 ,is 0 i- _—_—,-2.1Y-; �y T 11 ` 'A 1 �1 \ \ \ S11ui N ' 2111 ,.r,«e,no,0.M ro,..Lrre.-....a, X4789.2 1 111 \ CYK4NWY 66 I lh / 11 I S I. ,1 11` q, 1'', o X4789.5 1 I ..',. IW WLLO CO 4 - 2- / LMJ CG EXHIBIT D COAL ASH TRENCH AND MONITORING �i.vr2}aCCS# WELL LOCATION PLAN =RL"z/ z.nr2: aft co, 901140 d COO CevairrRrE124 —Yre'i r..E✓Xwn/ / EXHIBIT B 1DEX MAP FIGURE 1 AREA USE AND SITE CONDITION MAP VARRA COAL ASH PROJECT WELD COUNTY, COLORADO LEGEND: ... _ ,..y,.. ° ..... OPROPOSED MONITORING WELL LOCATION INFERRED GROUNDWATER APPLICANT: FLOW DIRECTION 1" =APPR( 4 VARRA COMPANIES 12910 WELD COUNTY ROAD 13 O SOIL SAMPLE LOCATION LONGMONT, COLORADO 80504 _ * POND SAMPLE LOCATION AFTER: NELSON ENGINEERS 640 GREELEY NATIONAL PLAZA GREELEY, COLORADO 80631 PHONE 356-6362 I i NESTED WELL SET NE SW T T - TRENCH DEPTH ESTIMATED AT 10'BGS / 7/ _ _ _ _ _ , _ S _ /// \\\ /// /// \\\ /// \\\ /// \\\ /// \\\ A A (PIERRE SHALE) A 100' NOT TO SCALE LEGEND rra NATIVE SOIL FIGURE 2 k:-:-:- FLY ASH MONITORING WELL PLACEMENT VARRA COAL ASH PROJECT WATER TABLE SURFACE WELD COUNTY, COLORADO 7- _ MONITORING WELL IS SCREENED PROJECT NO. PREPARED BY (DASHED AREA REPRESENTS SCREENED INTERVAL) 2755aa RACAD CG RS DATE REVIEWED BY COLORADO GROUNDWATER 6/19/00 -} RESOURCE SERVICES v ; TYPICAL MONITORING WELL r VENTED CAP LOCKING STEEL CASING (4"DIAMETER) 2"ID SCH 40 PVC RISERWiliZ tit GROUT ,: ' ,, ,,,, #10-20 SILICON SAND „ --_ - "„ 2"ID SCH 40 PVC FACTORY SLOTTED SCREEN (0.1 SLOT) -- '1 /// \\\ /// \\\ /// \\\ /// \\\ /// \\\ /// \N\ 6-1/4" FIGURE 3 MONITORING WELL CONSTRUCTION DETAILS VARRA COAL ASH PROJECT WELD COUNTY, COLORADO PROJECT NO. PREPARED BY 2755aa RACAD CGRS DATE REVJEWED BY COLORADO GROUNDWATER 6/19/00 -r0 RESOURCE SERVICES Table 1 Summary of Parameters, Sample Containers, Holding Times, and Analytical Methods and No. a of Holding Time(I) Parameter Matrix "Typ Analytical Containers' Method(Z) Alkalinity Water 1-100 ml P,G 14 days cool to 4C SM 2320B Chloride Water 1-200 ml,P,G 28 days no preservative required EPA 300.0 Fluoride Water 1-500 ml,P 28 days no preservative required EPA 300.0 Sulfate Water 1 -200 ml,P 28 days cool to 4C EPA 300.0 Nitrate/Nitrite Water 1 -l00 ml,P,G 48 hours cool to 4C EPA 300.0 _ I-500 ml P,G Mercury Water 28 days,HNO3 to pH<2 245.1/7170 Total Metals(RCRA) Water 125-500 ml nalgene 6 months except Mercury at 28 days. For (Red dot) water,preserved with HNO3,not filtered. 6010/7000 Dissolved Metals(RCRA) Water 125-500 ml nalgene 6 months except Mercury at 28 days. Filtered 6010/7000 and preserved in Lab. Anions/General Chemistry Water 250 ml nalgene 28 days 200 Series Notes: (1)All collected samples to he kept cool(4 degrees C) (2)USEPA Method,SW-846(Revised),1986 Table 2 Contents for Digital Analytical Deliverables Origin of Data Laboratory Name of Example of Delivered Generated by Generated in _ CGRS and Lab by Tech Data Field Digital Data Entered on COC Lab COMPANY NA Vara Companies X SITE_NAME Coal Ash Project X SITE_NO 2755aa X SAMPLE_ID1 MW-1 X SAMPLE_DAT 08/27/97 X LAB_ID L15316-01 X MATRIX Water X X METHOD M6010 ICP X DATE_ANALY 09/04/97 X ANALYTE Silver,total (3051) X TEXT_RESUL (blank if ND) X NUMBER_RES (blank if ND) X QUALIFIER U X DILUTION 106 X MDL 0.50000 X PQL 3.00000 X UNITS mg/L X DATE_RECEI 09/03/97 X DATE_EXTRA 09/04/97 X CAS_ 007440-22-4 X BATCH_ID WG47359 X APPENDIX A RESUMES JOBY L. ADAMS, P.G. CG Joby Adams is co-owner and principal hydrogeologist in the CGRS Fort Collins office. He has experience in both the mining and environmental fields, with background as follows: Specialization • Pipeline facility assessment and remediation design • Finite element and finite difference groundwater flow and solute transport modeling • Air dispersion modeling • Compressible gas flow modeling • Well hydraulics • Water well design and installation • UST investigation and remediation • Groundwater quality monitoring, sampling, and chemical analysis • Soil vapor surveys (design, investigation and analysis) • Precision tank and line testing (volumetric and nonvolumetric) Education • M.S. in Hydrogeology-Colorado State University • B.S. in Geology-Colorado State University • National Water Well Association Portable Gas Chromatography Symposium • EPA State UST Programs Symposium • American Society for Testing and Materials Seminar for Phase I Environmental Assessments • OSHA Health and Safety training and certification • ASTM RBCA Training Affiliations • American Institute of Mining Engineers • Colorado Groundwater Association • Colorado Petroleum Storage Tank Committee Registered Professional Environmental Scientist • Hazardous Materials Control Research Institute • Missouri Professional Geologist • National Water Well Association • Oklahoma Corporation Commission, Petroleum Storage Tank Division, Certification of UST Consultant, ID#496 • Utah Certified Consultant • Wyoming Professional Geologist Representative Experience ➢ Conducted research related to elemental leachability of coal combustion by- products and applicable testing methods. Received Department of Energy grant (ECBC) for research related to elemental leachability of coal combustion by- products in saturated conditions. ➢ Provided Expert Testimony services regarding the elemental leachability of slag • deposits near Leadville, Colorado. Page 1 JOBY L. ADAMS, P.G. CG Representative Experience (Continued) > Project Manager for a multi-million dollar environmental due diligence for the purchase of eight natural gas plants and 18 associated compressor stations throughout Oklahoma. > Supervised personnel and subcontractors for activities consisting of excavating and logging over 30 trenches and drilling 836 soil borings of which 239 were completed as groundwater monitoring wells. Aquifer tests and periodic groundwater monitoring were performed as well. > Generated corrective action plans and cost estimates for two gas plants with corrective action costs exceeding 25 million dollars. > Project geologist - on-site investigations for subsurface contamination by hydrocarbons > Coordinated drilling and sampling to determine extent of subsurface herbicide contamination > Logging geologist > Tanker rollover emergency response > Remedial system design and evaluation ➢ Expert witness testimony > Precision tank and line testing > Generated process safety management plans for companies using ammonia > Experienced with gas chromatography(using photoionization, flame ionization and thermal conductivity detectors) > Designed and performed soil vapor surveys in regard to litigation preparation > Designed, permitted, installed and monitored remedial systems to remove subsurface hydrocarbons in the states of Arizona, Colorado, Nebraska, New Mexico, Utah, Washington and Wyoming Publications/Papers • "A Feasibility Study for the Beneficial Use of Coal Ash as Fill Material in Saturated Conditions" - Under peer review for publication. • "Soil Vapor Surveys with Soil Venting as an Aquifer Restoration Technique -A Case History", Delta Environmental Technical Review, March 1990, Vol. 2, No. 1, pages 6-9(with J.M. Kerr and B.S. Steadman) • "Subsurface Contamination by the Herbicide Atrazine" Colorado State University Unpublished Master's Thesis, 1994. Page 2 JOBY L. ADAMS, P.G. CGS Professional Speaking Engagements ➢ "Case History of the Varra Coal Ash Project"— Invited Speaker to the Seventeenth Annual International Pittsburgh Coal Conference, University of Pittsburgh, September 2000. ➢ "Investigation and Remediation Techniques and Theories in regard to Subsurface Contamination by Petroleum Hydrocarbons" - Colorado School of Mines UST Program (ongoing) S. "Case Histories of Investigation and Remediation Projects in Regard to Petroleum Hydrocarbon Contamination Assessment and Abatement" - Colorado State University(Advanced Topics in Hydrogeology Guest Lecture Series, 1992) ➢ "Case Histories of Investigation and Remediation Projects and Theories and Applications of Field Tracer Studies" - Colorado State University, Department of Civil Engineering, Groundwater Program (ongoing) Page 3 CHESTER HITCHENS CG Chester Hitchens is a hydrogeologist with CGRS, Inc. with twelve years of professional experience at providing services specializing in design and implementation of site investigations involving petroleum and petrochemical products. Mr. Hitchen's background includes: Specialization • Contaminant recovery system design, including soil vapor extraction, air sparging and hydraulic containment/recovery • Management of petroleum cleanups • Air rotary, mud rotary, reverse rotary and auger drilling • Groundwater sampling techniques for both organic and inorganic contaminants, organic and biomonitoring analyses • Communication with state and other regulatory agencies • Prepurchase environmental investigations • RBCA and expert witness Education • M.S. (in progress) Geology—Colorado State University • B.A. Geology—University of Northern Colorado • ASTM RBCA Training Affiliations • Wyoming Professional Geologist#817 • New Mexico Environment department Certified Scientist#087 • Colorado Petroleum Storage Tank Fund Registered Professional Environmental Scientist#5148 • Certified Washington State Site Association • Association of Ground Water Scientists and Engineers • South Dakota Certified Petroleum Release Remediator#R-141 • Instructor Hydrogeology—University of Northern Colorado Representative Experience • Managed over 75 investigation and remediation projects at service stations, bulk plants, industrial facilities and automobile dealerships. • Negotiated closure and clean up stipulations with various regulatory agencies, both with and without performing remedial activities. • Served as an expert witness regarding various technical aspects of an alleged -- gasoline loss in a residential subdivision, including date of release, volume of release and hydraulic characteristics of the aquifer. • Served as technical advisor for a responsible party(RP) associated with a gasoline release to a surface water body. The RP was issued a Notice of Violation from the United States Environmental Protection Agency. Mr. Hitchens provide technical assistance to the RP's attorney and negotiated with the state of Idaho attorney general to prepare a Content Decree for the proposed clean up activities at the facility. Page 1 CHESTER HITCHENS CG Representative Experience (Continued) • Served as a Project Hydrogeologist on site investigations involving soil and groundwater contamination in Colorado, Idaho, Nebraska, New Mexico, Washington and Wyoming. Projects involve initial site investigation, evaluation of hydraulic characteristics of the aquifer, contaminant transport and preparation and implementation of remedial action plans for soil and groundwater clean up. • Conducted water rights adjudication for municipalities. Projects involved reviewing of court records, establishing baseline data for groundwater usage, and development of a data for the municipalities for the management of their ground water usage. • Evaluated potential for groundwater recharge and hydrogeology of an alluvial basin in southwestern Arizona. Project involved defining the saturated and unsaturated hydraulic characteristics of the basin, conducting long-term aquifer tests on large diameter irrigation wells, developing a groundwater flow model to predict the impacts of future groundwater usage an examining geochemical data for the groundwater and surface water proposal to be used for recharge. • Conducted groundwater contamination investigation associated with a dynamite plant. Project involved review of the facility records to determine past operations and disposal practices, examination of fate and transport of contaminants leached from unlined disposal ponds and evaluation of steam and groundwater interaction relating to contaminant transport. Page 2 RANDY S. PRICE, C.P.G. Randy Price is a co-owner and our Environmental Services Field Manager. He has over 9 years of environmental consulting experience and specializes in site investigations utilizing various drilling and sampling methodologies. Mr. Price's background is as follows: Specialization • Project management of a variety of projects including Phase I and II ESAs, fuel tank decommissioning at both singular and multiple sites. • Site investigations utilizing groundwater, soil and soil vapor sampling for organic and inorganic analyses • Groundwater monitoring well installation and design • Phase I and II environmental site assessments • UST removal and closure • Designing and installation of remediation systems (i.e., groundwater recovery, SVE and AS remedial systems) • UST regulatory interpretation, consultation and representation Education • B.S. in Geology- Fort Lewis College • Graduate level courses in Hydrogeology-Colorado State University • Professional Seminars • "Groundwater Investigations Using Portable Gas Chromatography and Other Field Instrumentation" • "Soil Gas: The State of the Art and Beyond" • "Site Assessments and Remedial Action for Petroleum Contaminated Soils" • EPG Service School -"Operation & Maintenance of Remediation Equipment" • OSHA Health and Safety training and certification • OSHA Hazardous Waste Supervisor training • Cathodic protection training • ASTM RBCA Training Affiliations • Utah Certified Consultant#CC0092 • American Institute of Professional Geologists, CPG-8890 • Association of Groundwater Scientists and Engineers, National Groundwater Association • Colorado Hazardous Waste Management Society • Colorado Petroleum Storage Tank Committee Registered Professional Environmental Scientist, #503 • Wyoming Professional Geologist, PG-537 Representative Experience • Wellsite geologist - extensive experience with geophysical well logs, sample descriptions, coring and drilling procedures • Supervised and managed the removal of numerous USTs • Project geologist - on-site investigations for subsurface contamination by hydrocarbons and chlorinated solvents Page 1 RANDY S. PRICE, C.P.G. CG Representative Experience (continued) • Design and implement sampling strategies for site characterization related to surface and subsurface chemical releases • Aerial photograph interpretation, regulatory review, site assessments, owner/employee interviews and media sampling performed for Phase I and II real estate assessments for due dilignece projects throughout Texas, Lousiana, Nebraska,Wyoming, Utah, Maryland, Iowa and Colorado. • Gas chromatography using photoionization, flame ionization, thermal conductivity and electron capture detectors • Project manager of an 8,300 gallon release into a monitoring well. Obtained site closure in 2.5 years at a cost of less than $250,000. • Field team leader for subsurface investigation to evauate 15 miles of natural gas pipeline in southwestern Colorado. Sampling activities were performed utilizing an ATV Geoprobe. Sample analysis was performed on site in a mobile laboratory. Page 2 JAMES W. WARNER, Ph.D., P.E. CG Dr. Jim Warner is a senior engineering consultant for CGRS. He is also an associate professor and groundwater/environmental hydrogeology program leader in the Department of Civil Engineering at Colorado State University. Dr. Warner has over twenty years of experience as a practicing groundwater engineer and is the author of over eighty technical publications and reports on groundwater. Dr. Warner has worked internationally and is currently involved with the Egypt Water Use and Management Project. He is also on the peer review committee for the United States Department of Energy. Specialization • Groundwater flow and contaminant transport modeling • Aquifer remediation • Code development • Feasibility studies and remedial investigations • Geostatistics Education • Ph.D. in Civil Engineering - Colorado State University Major Field of Study-Groundwater Hydrology/Water Resources Systems Engineering • Graduate level courses in Civil Engineering- California State University at Long Beach Major Field of Study-Hydraulics and Surface Water Hydrology(total of seven courses) • M.S. in Systems Engineering -California State University at Fullerton - Major Field of Study-Statistics and Optimization • M.B.A. in Business Administration- California State University at Fullerton Major Field of Study-Operation Research and Statistical Decision Theory • B.S. in Civil Engineering- California State University at Fresno • OSHA Health and Safety training and certification Affiliations and Honors • American Geophysical Union (AGU) • American Institute of Hydrogeology(AIR) • American Society of Engineering Education (ASEE) • American Water Resources Association (AWRA) • Dean's Council Award for Outstanding Civil Engineering Faculty- 1993 • Geological Society of America (GSA) • International Association of Hydrogeologists (IAH) • International Water Resources Association (IWRA) • National Water Well Association (NWWA) • Professional Engineer(#16492) - State of Colorado • Professional Engineer- State of Wyoming • Professional Hydrogeologist-American Institute of Hydrogeologist Page 1 CG � JAMES W. WARNER, Ph.D., P.E. Representative Experience • Associate Professor of Civil Engineering, Groundwater/Environmental Hydrogeology program -Colorado State University(1981 to present): ♦ Conduct research and advise graduate students in groundwater • Develop and teach graduate courses in groundwater contaminant transport modeling, quantitative hydrogeology, solutions to groundwater problems, groundwater engineering, geostatistics and conjunctive use of groundwater and surface waters • Graduated 15 Ph.D. students and 32 M.S. students • Civil Engineering Groundwater Program Leader- Colorado State University • Groundwater hydrologist - US Geological Survey, Water Resources Division (1968-1981): ♦ Seven years in the Denver, Colorado office ♦ Six years in the Laguna Nigel, California office (Southern California District Office • Project chief/member on complex hydrologic studies • Office consultant on technical matters related to groundwater hydrology • Groundwater technical adviser - Egypt Groundwater Research Institute in Cairo, Egypt - . • assist in developing research plans • train Egyptian engineers in groundwater • assist in formulating plans of action to control groundwater contamination • assist in implementation of conjunctive use of groundwater with surface water for irrigation use in Egypt • Groundwater modeling projects • Groundwater author- over 80 technical publications and reports • Associate editor-Journal of Engineering Geology • Research funding - has received over$1.6 million in external funding over the past six years • Research areas - computer code development, groundwater flow and contaminant transport modeling, stochastic modeling, fracture-flow modeling, monitoring criteria, conjunctive use of groundwater and surface water, toxic wastes in groundwater systems, multi-phase multi-species contaminant transport, water resources systems analysis, microbial growth in aquifer systems and aquifer remediation • Computer code development for the Colorado State University finite element groundwater modeling package, also used by consulting firms, the US Army Corps of Engineers, Waterways Experiment Station (i.e., Rocky Mountain Arsenal) - GWFLOW (2-dimensional flow model), GWTRAN (2-D/quasi 3-D contaminant transport model), GWFRAC (double porosity flow model), GWCH2O (vertically integrated density dependent flow model), GWBIO (2-D model for solving biologically active contaminant transport), GW3D-REACT (full 3-D multi-species contaminant transport model) Page 2 Mr. Glenn Mallory Varra Coal Ash Project December 29, 1998 Page 2 If you have any questions regarding this letter or require further information, please contact me at (800) 288-2657. Sincerely, CGRS, C. Nio,- , ' , Joby Adams, P.G. r crpal/Hydrogeologist Attachments cc: Mr. Chris Varra — Varra Companies Mr. Dave Goss — PSC Mr. Terry Staley - PSC Mr. Trevor Jiricek -Weld County Health Department Mr. Harry Pose - Colorado Division of Minerals and Geology Mr. Ben Patton-Weld County Planning \\CGRS HQ SERVERWoby\WINWORD\LETTERS\statecoverltr.doc l l 1 I I I I I ) I I I I I TAbu 2 Analytical Results-SELP Varra Coal Ash Project Weld County,Colorado CGRS Project No.1435-2755 Total Metals Analytical Results (mg/L) Sample pH Ex Al Sb As Ba Be B Cd Cr Co Cu Fe Pb Mn Ni Se Ag Ti V Zn Li Hg Class F Silo Ash with 85 1 27.00 ND ND 3.80 0.003 5.70 ND 0.13 ND 0.03 7.40 ND 0.07 ND ND ND ND 0.05 0.05 0.24 NO Gypsum (C Silo) 2 9.70 ND ND 8.40 ND 0.69 ND 0.07 ND 0.01 2.20 ND 0.02 ND ND ND ND 0.02 0.02 0.12 ND 1 29.00 ND ND 1.30 0.002 1.70 ND ND ND 0.09 15.0 ND 0.14 0.02 ND ND ND 0.05 0.15 0.05 ND Bottom Ash 85 2 37.00 ND _ ND 1.60 0.003 1,20 ND ND ND 0.12 21.0 ND 0.21 0.01 ND _ ND ND 0.06 0.22 0.04 ND 1 780.00 ND 0.40 5.20 0.082 120 0.05 0.52 0.11 0.80 210.0 0.62 1.40 0.18 0.64 ND ND 1.70 1.10 1.50 NA Cherokee Silo Ash 2/3 8.5 2 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR Cherokee 4 Fly Ash with a5 1 1.50 ND ND 0.98 ND 48 ND 0.19 ND ND 0.31 _ ND ND ND 0.23 ND ND ND ND 0.76 ND Sodium 2 3.70 NA NA 2.10 NA 17 NA 0.63 NA NA _ 0.26 ND NA NA 0.10 NA NA NA NA 0.26 NA 1 1.90 ND ND 0.32 ND ND ND 0.07 ND 0.05 0.56 ND 0.02 0.02 ND ND ND ND 0.01 0.02 ND Recycled Concrete 8.5 2 47.0 NA NA 0.71 NA NA NA 0.05 NA 0.15 _ 56 NA 1.70 0.04 NA NA NA NA 0.57 0.05 NA 1 150.0 ND ND 1.90 0.009 0.09 ND 0.17 0.06 0.41 160 0.41 4.30 0.12 ND ND ND 0.31 1.50 0.15 ND Recycled Asphalt 8.5 2 2.50 NA NA 0.25 ND ND NA 0.06 ND 0.02 0.27 ND ND ND NA NA NA ND ND 0.02 NA Class F Silo Ash with 7 1 750.0 ND ND 1.90 0.073 21.0 0.01 0.50 0.11 0.59 200.0 0.10 2.0 0.22 ND ND ND 1.30 0.61 0.56 0.002 Gypsum(C Silo) 2 12.0 NA NA 13.0 ND 0.30_ ND 0.04 ND 0.01 3.30 ND 0.03 ND NA NA NA 0.02 0.01 0.14 ND `1 0.45 ND ND 0.08 ND 1.00 ND ND ND ND 0.24 ND ND ND ND ND ND ND ND 0.03 ND Bottom Ash 7 2 6.10 ND ND 0.27 ND 0.62 ND ND ND 0.02 3.40 ND 0.04 ND ND ND ND 0.02 0.08 0.01 ND 1 0.54 ND ND 0.79 ND 45 ND 0.11 ND ND 0.06 ND ND ND 0.19 ND ND 0.01 ND 0.73 ND Cherokee Silo Ash 2/3 7 2 110.0 ND _ ND 6.70 0.008 22 ND 0.05 ND 0.09 32.0 0.11 0.13 0.02 0.13 ND ND 0.17 0.13 0.33 0.001 Cherokee 4 Fly Ash 1 0.21 ND ND 0.88 ND 45 ND 0.18 ND ND 0.06 ND ND ND 0.20 ND ND ND ND 0.76 ND with Sodium 7 2 84.0 NA NA 5.30 NA 24 NA 0.11 NA NA 22.0 NA NA NA 0.14 NA NA NA NA 0.31 NA 1 2.60 ND ND 0.15 ND ND ND 0.13 ND 0.06 0.64 ND 0.02 ND ND ND ND ND 0.01 0.02 ND Recycled Concrete 7 2 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050 .20/1.0 0.30/5.0 0.050, 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards A PPPP A P P A NS S/A P S P P P P A A A P Notes: ND=Not Detected NA=Not Analyzed EX=Extraction mg/L=milligrams per liter A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard NR-Samples Not Analyzed Page 1 of 4 I I I i i I I I I I I I I I I ) TABLE 2 Analytical Results-SELF Varra Coal Ash Project Weld County,Colorado CGRS Project No.1-135-2755 Total Metals Analytical Results (mg/L) Sample pH Fat Al Sb As Ba Be B _ Cd Cr Co Cu Fe Pb Mn Ni Se Ag Ti V Zn Li Hg 1 1.2 ND ND 0.089 ND ND NO ND ND ND 0.88 ND 0.026 ND ND ND ND 0.01 0.011 0.009 ND Recycled Asphalt 7 2 26 NA NA 0.39 ND 0.18 NA NA ND NA 28 NA 0.076 NA NA NA NA 0.062 0.36 0.03 _ NA Class F Sib Ash with 5 1 0.10 ND ND 0.98 ND 6.10 ND 0.10 ND ND ND ND ND ND ND ND ND ND ND 0.19 ND Gypsum (C Sib) 2 0.13 NA NA 0.94 NA ND_ NA 0.06 NA NA NA NA NA NA NA NA NA NA NA 0.13 NA 1 640 ND ND 0.36 ND 1.20 ND ND ND 0.03 4.20 ND 0.05 ND ND ND ND 0.02 0.06 0.03 ND Bottom Ash 5 2 0.37 NA NA 0.06 NA 0.56 NA NA NA ND 0.20 ND ND NA NA NA NA ND ND 0.01 ND Cherokee Silo Ash 2/3 5 1 44.0 ND ND 2.90 0.0036 51.00 ND _0.13 ND - 0.04 12.00 ND 0.05 ND 0.27 ND ND 0.06 0.06 0.77 0.0001 2 5.10 NA NA 1.70 NA 15.00 NA ND NA ND ND NA ND NA ND NA NA 0.03 ND 0.22 ND Cherokee 4 Fly Ash with 5 1 0.61 ND ND 0.77 ND 51.00_ ND 0.21 ND ND 0.11 ND ND NO 0.21 ND ND ND ND 0.77 ND Sodium 2 4.10 NA NA 1.10 NA 22.00 NA 0.05 NA NA 0.28 NA NA NA 0.13 NA NA NA _ NA 0.24 NA 1 1.30 ND ND 0.45 ND 0.08 ND 0.06 ND 0.04 0.56 ND . 0.01 ND ND ND ND ND ND 0.02 ND Recycled Concrete 5 2 230 NA NA 0.23 NA ND NA 0.08 NA 0.02 0.09 NA ND NA NA NA NA NA NA 0.02 NA Recycled Asphalt 5 1 120.0 ND ND 1.80 0.01 0.09 ND 0.13 0.05 0.33 140.0 0.33 3.90 0.10 ND ND ND 0.26 1.30 0.12 ND 2 87.0 NA NA 1.00 0.01 0.08 NA 0.07 0.03 0.22 90.0 0.19 2.30 0.62 NA NA NA 0.17 0.86 0.08 NA State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050 .20/1.0 0.30/5.0 0.050 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards A PPPP A P P A AIS S/A P S PPPP A A A P Notes: ND=Not Detected NA=Not Analyzed EX=Extraction mg/L=milligrams per liter A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard NR-Samples Not Analyzed Page 2 of 4 I TABLE 2 Analytical Results- SELP Varra Coal Ash Project Weld County, Colorado CGRS No. 1-135-2755 Sample pH Ext Other Analytical Results(mg/L) Total Cyanide Free Cyanide Chloride Fluoride Sulfate Nitrate Nitrite Class F Silo Ash with Gypsum (C Silo) 8.5 1 ND NA 130 8.4 23 7.9 4.6 2 ND NA 20 5.8 65 3.3 1 Bottom Ash 8.5 1 ND NA 29 0.95 170 1.1 0.031 2 ND NA 6.5 0.35 45 0.31 0.067 Cherokee Silo Ash 2/3 8.5 1 NA 0.021 5.1 3.1 ND 0.35 0.013 2 NA 0.016 5.7 1.3 69 ND 0.0058 Cherokee 4 Fly Ash with Sodium 8.5 1 NA 0.021 4.9 5.8 1100 0.14 ND 2 NA 0.012 1.2 3.1 59 0.15 0.0082 Recycled Concrete 8.5 1 NA 0.047 26 5.3 10 1.4 0.096 2 NA 0.027 1.5 1.2 8.3 0.4 0.034 Recycled Asphalt 8.5 1 NA 0.012 10 0.98 44 ND 0.0078 2 NA ND 1.6 1.2 8.2 0.2 0.0055 Trip Blank 1 8.5 NA NA 31 1.5 2.6 NA NA Class F Silo Ash with Gypsum (C Silo) 7 1 NA ND 120 11 840 7.4 1.3 2 NA ND 31 7.4 19 2.1 1 Bottom Ash 1 NA ND 23 0.89 140 0.87 0.048 2 NA ND 5.1 0.46 33 0.16 ND Cherokee Silo Ash 2/3 7 1 NA ND 4.1 4.7 430 0.23 0.014 2 NA ND 1.8 2.3 60 0.17 0.32 Cherokee 4 Fly Ash with Sodium 7 1 NA 0.011 3.4 5.1 430 0.2 0.017 - 2 NA ND 1.8 3.1 49 0.12 0.036 Recycled Concrete 7 1 NA 0.11 26 4.1 31 0.92 ND - 2 - State Water Quality Standards 0.2 250 2.0 250 10 1 P S A P P P Page 3 of 4 I I TABLE 2 Analytical Results - SELP Varra Coal Ash Project Weld County, Colorado CGRS No. 1-135-2755 Sample pH En Other Analytical Results(mg/L) Total Cyanide Free Cyanide Chloride Fluoride Sulfate Nitrate Nitrite Recycled Asphalt 7 1 NA ND 8.1 2.1 ND ND 44 2 NA 0.011 1.9 0.52 11 ND ND Trip Blank 2 7 NA NA ND 1.6 ND 0.14 ND Class F Silo Ash with Gypsum (C Silo) 5 1 NA ND 120 14 760 7.9 8.40 2 NA ND 29 11 16 2 3.60 Bottom Ash 5 1 NA ND 23 2.8 120 0.78 0.031 2 NA ND 7.9 1.6 37 0.24 ND Cherokee Silo Ash 2/3 5 1 NA 0.013 4.8 7.3 640 0.2 0.012 2 NA ND 2.4 5.6 28 0.31 ND Cherokee 4 Fly Ash with Sodium 5 1 NA 0.016 4.5 7.4 550 0.75 0.019 2 NA ND 2.4 8.1 61 0.31 0.028 Recycled Concrete 5 1 NA 0.015 24 5.5 8.1 1.1 4.70 2 NA 0.056 15 6.7 20 0.63 0.047 Recycled Asphalt 5 1 NA ND 13 2.4 45 0.20 ND 2 NA ND 5.3 1.4 14 0.33 ND State Water Quality Standards 0.2 250 2.0 250 10 1 Note: P S A S P P NA-Not Analyzed ND=Not Detected A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 4 of 4 TABLE 3 TCLP Analytical Results Varra Coal Ash Project Weld County Colorado CGRS NO.1-135-2755 Sample Ex Al Sb As Ba Be B Cd Cr Co Cu Fe Pb Mn Ni Se Ag Ti V Zn Li Hg Class F Silo Ash with Gypsum (C Silo) 0.32 ND ND 3.10 ND 2.20 ND 0.031 ND ND ND ND ND ND ND ND NA ND ND 0.05 NA Bottom Ash 0.96 ND ND 0.62 ND 0.96 ND ND ND 0.0083 0.063 ND 0.12 0.02 ND ND NA ND 0.10 ND NA Cherokee Silo Ash 2/3 ND ND 0.16 0.35 ND 24 ND ND ND ND ND ND 0.11 ND 0.41 ND NA 0.18 ND 0.21 NA Cherokee 4 Fly Ash with Sodium ND ND 0.23 0.37 ND 25 0.0057 ND ND ND ND ND 0.08 0.011 0.390 ND NA 0.34 0.0082 0.19 NA Recycled Concrete ND ND ND 0.36 ND 0.17 ND 0.061 ND 0.012 ND ND ND ND ND ND NA 0.041 ND 0.019 NA Recycled Asphalt 0.37 ND ND 0.52 ND 0.24 ND ND 0.015 0.015 0.25 ND ND 0.02 ND ND NA ND 0.26 ND NA State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050_.20/1.0 0.30/5.0 0.050 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards A P P P P A P P A NS S/A P SP P P P A A A P Notes: ND=Not Detected NA=Not Analyzed EX=Extraction mg/L=milligrams per liter A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 1 of 2 I I I I I 1 I 1 I I � I I I I I I I I I TABLE 3 TCLP Analytical Results Varra Coal Ash Project Weld County, Colorado CGRS NO. 1-135-2755 Sample - Other Analytical Results(mg/L) Total Cyanide Free Cyanide Chloride Fluoride Sulfate Nitrate Nitrite Class F Silo Ash with Gypsum (C Silo) ND NA 98 8.4 220 3.4 46 Bottom Ash ND NA 32 0.013 140 0.81 ND Cherokee Silo Ash 2/3 ND NA 0.61 5.8 240 ND ND Cherokee 4 Fly Ash with Sodium ND NA ND 41 140 ND ND Recycled Concrete ND NA 7.2 ND 41 0.29 ND Recycled Asphalt ND NA 5.9 0.27 29 ND ND State Water Quality Standards 0.2 250 2.0 250 10 1 P S A P P P Note: NA-Not Analyzed ND=Not Detected A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 2 oft TABLE 4 SGLP Analytical Results Varra Coal Ash Project Weld County, Colorado CGRS No. 1-135-2755 Sample Ex Al Sb As Ba Be B Cd Cr Co Cu Fe Pb Mn Ni Se Ag Ti V Zn Li Hg Ash with Gypsum (C Silo) 1 0.28 ND ND 0.71 ND 3.40 ND 0.033 ND ND ND ND ND ND ND ND NA ND 0.010 0.094 NA Bottom Ash 1 0.073 ND ND 0.12 ND 0.80 ND ND ND ND ND ND 0.010 ND ND ND NA ND ND 0.057 NA Cherokee Silo Ash 2/3 1 ND ND ND 1.10 ND 16 ND 0.033 ND ND ND ND ND ND 0.31 ND NA 0.04 ND 0.26 NA Cherokee 4 Fly Ash with Sodium 1 ND ND ND 1.10 ND 16 ND 0.06 ND ND ND ND ND ND 0.340 ND NA 0.07 0.005 0.23 NA Recycled Concrete 1 0.32 ND ND 0.11 ND 0.13 ND 0.068 ND 0.012 0.22 ND ND ND ND ND NA 0.01 0.011 0.054 NA Recycled Asphalt 1 0.12 ND ND 0.067 ND 0.58 ND ND ND ND 0.074 ND 0.071 ND ND ND NA ND ND 0.051 NA Gravel Quarry Water ND ND ND 0.010 ND 0.30 ND 0.06 ND ND 0.056 ND 0.028 ND ND ND ND ND ND 0.027 NA State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050 .20/1.0 0.30/5.0 0.050 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards APPP P A P P A AB S/A PSPP PP A A A P Notes: ND=Not Detected NA=Not Analyzed EX=Extraction mglL=milligrams per liter A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 1 of 2 I I 1 I I I I 1 i 1 I 1 j 1 TABLE 4 SGLP Analytical Results Varra Coal Ash Project Weld County,Colorado CGRS No. 1-135-2755 Sample Other Analytical Results(mg/L) Total Cyanide Free Cyanide Chloride Fluoride Sulfate Nitrate Nitrite Class F Silo Ash with Gypsum (C Silo) ND NA 150 4.5 2700 4.1 4.63 Bottom Ash ND NA 110 0.9 3000 1.9 ND Cherokee Silo Ash 2/3 ND NA 83 5.3 3400 0.083 ND _ Cherokee 4 Fly Ash with Sodium ND NA 84 _ 4.4 3300 0.86 ND Recycled Concrete ND NA 110 0.19 2500 1.3 0.12 - Recycled Asphalt ND NA 97 _ 0.95 2800 1 ND Gravel Quarry Water ND NA 76 4.0 2900 1 ND State Water Quality Standards 0.2 250 2.0 250 10 1 P S A P P P Note: NA-Not Analyzed ND=Not Detected A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 2 of 2 I I TA.,LE 5 Analytical Results-SGCLP Varra Coal Ash Project Weld County,Colorado CGRS Project No.1-135-2755 Total Metals Analytical Results (mg/L) Sample pH PV Al Sb As Ba Be B Cd Cr Co Cu Fe Pb Mn NI Se Ag Ti V Zn Li Hg 1 ND NA NA 0.29 NA 290 NA 0.31 NA NA ND NA NA NA NA NA NA ND 0.023 1.20 NA Class F Silo Ash with 8.5 2 ND NA NA 1.80 NA 9.50 NA 0.20 NA NA ND NA ND NA NA NA NA ND 0.0073 0.31 NA Gypsum (C Silo) 4 ND NA NA 2.50 NA 2.0 NA 0.09 NA NA ND NA ND NA NA NA NA ND ND 0.22 NA 1 0.24 NA NA 0.059 ND 2.10 NA NA NA 0.0087 ND ND ND NA NA NA NA ND NA NA NA Bottom Ash 8.5 4 0.23 NA NA 0.022 ND 0.52 NA NA NA ND ND ND ND NA NA NA NA ND NA NA NA 8 0.29 NA NA 0.033 NA 0.30 NA NA NA ND ND NA ND NA NA NA NA NA NA NA NA l 1 0.98 NA NA 0.53 ND 130 NA 0.076 ND NA 0.11 ND ND ND NA NA NA 0.026 NA NA NA Cherokee Silo Ash 2/3 8.5 2 0.94 NA NA 1.10 ND 40 NA ND ND NA 0.19 NO ND ND NA NA NA ND NA NA NA 4 5.80 NA NA 7.20 ND 22 NA ND ND NA ND ND ND ND NA NA NA ND NA NA NA 1 6.60 NA NA 0.72 NA 140 NA 0.46 NA NA 0.82 NA NA NA 1.10 NA NA NA NA 2.80 NA Cherokee 4 Fly Ash with 8.5 2 0.91 NA NA 0.69 NA 47 NA 0.016 NA NA 0.25 NA NA NA 0.19 NA NA NA NA 0.53 NA Sodium 4 5.90 NA NA 9.30 NA 19 NA ND _ NA NA 0.17 NA NA NA ND NA NA NA NA 0.21 NA 1 ND NA NA 1.30 ND 25.00 NA 0.33 ND 0.048 ND 0.27 ND ND NA NA NA ND NA 0.79 NA Class F Silo Ash with 7 2 ND NA NA 1.50 ND 4.40 NA 0.22 ND 0.026 ND 0.09 ND ND NA NA NA NO NA 0.29 NA Gypsum(C Silo) 4 ND NA NA 6.50 ND 0.81 NA 0.017 ND ND ND ND ND ND NA NA NA ND NA 0.27 NA 1 0.30 NA NA 0.04 ND 2.20 NA NA NA NA ND NA ND NA NA NA NA NA NA NA NA Bottom Ash 7 4 0.18 NA NA 0.023 ND 0.65 NA NA NA NA ND NA ND NA NA NA NA NA NA NA NA 8 0.39 NA NA 0.058 ND 0.39 NA NA NA NA 0.071 NA ND NA NA NA NA NA NA NA NA 1 1.40 NA NA 0.41 ND 190 NA 0.21 ND 0.0086 ND ND ND NA 1.30 NA NA 0.013 NA 4.30 NA Cherokee Silo Ash 2/3 7 2 0.46 NA NA 0.77 ND 54 NA 0.015 ND ND 0.076 ND ND NA 0.22 NA NA ND NA 0.47 NA 4 5.40 NA NA 5.30 ND 21 NA ND ND ND 0.17 ND ND NA ND NA NA ND NA 0.16 NA 1 1.00 NA NA 0.58 NA 210 NA 0A7 NA NA ND NA NA NA 1.40 NA NA NA NA 5.10 NA Cherokee 4 Fly Ash 7 2 0.30 NA NA 0.63 NA 64 NA 0.018 NA NA 0.051 NA NA NA 0.21 NA NA NA NA 0.52 NA with Sodium 4 5.60 NA NA 6.70 NA 22 NA ND NA NA ND NA NA NA ND NA NA NA NA 0.35 NA State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050 .20/1.0 0.30/5.0 0.050 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards A P P P P A P P A A/S S/A P S P P P P A A A P Page 1 of 4 / ) 1. LE 5 Analytical Results-SGCLP Varra Coal Ash Project Weld County,Colorado CGRS Project No.1-135-2755 Sample pH pv Al Sb As Ba Be B Cd Cr Co Cu Fe Pb Mn Ni Se Ag Ti V Zn Li Hg 1 0.091 NA NA 15 NA 20 NA 0.34 NA NA NA NA NA NA NA NA NA NA NA 1.10 NA Class F Silo Ash With 5 2 0.710 NA NA 14 NA 0.11 NA ND NA NA NA NA NA NA NA NA NA NA NA 0.82 NA Gypsum (C Sib) _4 0.24 NA NA 29 NA ND _ NA ND NA NA NA NA NA NA NA NA NA NA NA 0.11 NA 1 0.087 NA NA 0.11 NA 3.10 NA ND NA ND ND NA ND NA NO NA NA ND 0.0068 0.12 NA Bottom Ash 5 4 0.130 NA NA 0.018 NA 0.47 NA ND NA NA ND NA NA NA ND NA NA NO ND ND NA 8 0.26 NA NA 0.02 NA 0.23 NA NA NA ND ND NA NO NA NA NA NA ND ND ND NA 1 0.42 NA NA 0.42 NA 170 NA 0.087 NA NA 0.062 NA NA NA 1.10 NA NA 0.02 0.036 5.50 NA Cherokee Silo Ash 2/3 5 2 0.25 NA NA 0.68 NA 41 NA 0.014 NA NA 0.089 NA NA NA 0.19 NA NA ND 0.025 0.61 NA 4 4.80 NA NA 5.10 NA 22 NA ND NA NA ND NA NA NA 013 NA NA ND ND 0.19 NA 1 9.20 NA NA 7.30 NA 49 NA 0.081 NA NA 2.0 NA NA NA 0.31 NA NA NA NA 1.70 NA Cherokee Fly Ash With 5 2 10.00 NA NA 25.00 NA 14 — NA ND NA NA 1,30 NA NA NA ND NA NA NA NA 0.26 NA Sodium 4 12.00 NA NA 12.00 NA 10.00 NA ND NA NA 0.16 NA NA NA ND NA NA NA NA 0.009 NA State Water Quality 5.0 0.006 0.050 2.0 0.004 0.750 0.005 0.100 0.050 .20/1.0 0.30/5.0 0.050 0.050 0.200 0.050 0.050 0.002 0.100 2.0 2.50 0.002 Standards A P P P _ P A P P A A/S S/A _ P S P P P P A A A P Notes: ND=Not Detected NA=Not Analyzed pv=Extraction mg/L=milligrams per liter A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 2 of 4 • i I I I I I I I I I I I I I I I TABLE 5 Analytical Results - SGCLP Varra Coal Ash Project Weld County, Colorado CGRS No. 1-135-2755 Sample pH PV Other Analytical Results(mg/L) Total Cyanide Free Cyanide Chloride Fluoride Sulfate Nitrate Nitrite 1 ND NA 290 7.7 1400 17.0 22.0 Class F Silo Ash with Gypsum (C Silo) 8.5 2 ND NA 59 6.8 1100 4.0 5.1 4 ND NA 30 T2 860 2.7 3.2 1 ND NA 74 1.5 350 1.4 0.379 Bottom Ash 8.5 4 ND NA 8.2 0.57 46 0.22 ND 8 r 0.015 NA 2.2 0.98 16 ND ND 1 ND NA 12 11 1700 0.034 0.022 Cherokee Silo Ash 2/3 8.5 2 ND NA 9.5 7 930 ND 0.006 4 ND NA 3.5 3.9 7 ND ND 1 ND NA 12 19 3080 1.2 0.093 Cherokee 4 Fly Ash with Sodium 8.5 2 ND NA 6.64 10.2 1100 ND 0.013 4 ND NA 1.69 3.72 5.9 0.18 ND 1 ND NA 557 17 1700 30 47 Class F Silo Ash with Gypsum (C Silo) 7 2 ND NA 52 14 1400 4.3 5.6 4 ND NA 29 9.3 300 3.9 4 1 ND NA 86.1 2.25 449 0.703 1.25 Bottom Ash 7 4 ND NA 4.96 1.5 36.4 ND ND 8 ND NA 1.9 4.6 10 ND ND 1 ND NA 6.9 11.1 1600 0.44 0.019 Cherokee Silo Ash 2/3 7 2 ND NA ND 12,4 777 ND 0.007 4 ND NA ND 5.04 8.2 0.166 ND 1 0.02 NA 5.7 11 1300 0.3 0.03 Cherokee 4 Fly Ash with Sodium 7 2 ND NA ND 8.9 870 ND 0.0086 4 ND NA ND 7.1 10 0.17 ND State Water Quality Standards 0.2 250 2.0 250 10 1 P S A P P P Page 3 of 4 I 1 I I I I I I I I I I I I I I I I l TABLE 5 Analytical Results- SGCLP Varra Coal Ash Project Weld County, Colorado CGRS No. 1-135-2755 Sample pH PV Other Analytical Results (mg/L) Total Cyanide I Free Cyanide I Chloride I Fluoride I Sulfate I Nitrate I Nitrite Sample pH PV Other Analytical Results (mg/L) Total Cyanide Free Cyanide Chloride Fluoride Sulfate Nitrate Nitrite 1 0.014 NA 1300 7 2100 74 120.00 Class F Silo Ash with Gypsum (C Silo) 5 2 ND NA 110 4.2 13 8.1 13.00 4 ND NA 3.5 4 5.2 1.7 0.62 1 ND NA 170 2.5 890 0.17 0.0064 Bottom Ash 5 4 ND NA 1.6 0.57 13 ND ND 8 ND NA 0.94 0.42 6.2 ND ND 1 ND NA 2.2 7.9 1500 ND 0.013 Cherokee Silo Ash 2/3 5 2 NA NA 1.2 5.2 760 ND 0.0067 4 ND NA 1.5 3.7 7.9 0.18 ND 1 ND NA 6 11 3100 0.4 0.09 Cherokee 4 Fly Ash with Sodium 5 2 ND NA 0.6 2.3 3.5 ND 0.03 4 ND NA 1 1.7 0.64 ND ND State Water Quality Standards 0.2 250 2.0 250 10 1 Note: P S A S P P NA-Not Analyzed ND=Not Detected pv=Pore Volume A-Agricultural Standard P-Primary Drinking Water Standard S-Secondary Drinking Water Standard Page 4 of 4 TABLE 6 SELP Analytical Results in Excess of Water Quality Standards Fly Ash Disposal Project Weld County,Colorado CGRS Project No.1-135-2755 ELEMENTS Ex Total Class F Silo Ash with 1 6 12 1 19 Gypsum (C Silo) 2 3 3 0 6 1 4 1 3 8 — Bottom Ash 2 4 2 0 6 1 14 4 6 24 Cherokee Silo Ash 2/3 2 NR 8 2 10 -- Cherokee 4 Fly Ash 1 4 3 3 10 with Sodium 2 4 5 2 11 1 1 2 1 4 Recycled Concrete 2 3 NR 0 3 1 9 1 8 18 Recycled Asphalt 2 0 3 7 10 pH 8.5 7 5 OTHER ANALYTICAL Class F Silo Ash with 1 2 2 3 7 Gypsum (C Silo) 2 1 1 2 4 1 0 0 1 1 Bottom Ash 2 0 0 0 0 1 1 2 2 5 Cherokee Silo Ash 2/3 2 0 1 1 2 Cherokee 4 Fly Ash 1 2 2 2 6 with Sodium 2 1 1 1 3 1 1 1 2 4 Recycled Concrete 2 0 0 1 1 1 0 2 0 2 Recycled Asphalt 2 0 0 0 0 pH 8.5 7 5 NR-Samples not ran by laboratory varracompare APPENDIX - A Selected Data—Groundwater Quality and Hydrogeology of the Laramie-Fox Hills Aquifer in the Milton Reservoir Area, Weld County,Colorado I p I • Fort Collins I Larimer Greeley County Study Area RWIT Boulder . County Weld ' Longmont County r • Boulder Adams County Jefferenn County -------urd: Golden Denver - Arapahoe County 0 feet 52300 105600 SCALE: 1:633,600 Figure 1 - Location of the study area. 1. 2 i I — ' .I s _ __r ' v A...1 I I \. 1L , --7 J�urArt AIRA � y'• r' /1 .` . `ll . r- 7 iU 'E4 . flfl7 ...A. F .�•ii— eta ' I I a1..._ _ - • --i rte'— -3 I s s,,it \ h O I I • � ` P ,L? ;�` �.. ; A%L 7' �`�� 'L e = R T t ).O. La it; i �'� '.� ' �� _ I• J '� > _ -sra---- I _ I'� _ I - d lie . I r . ��•.. 10 L .OAMCMETFAS EXPLANATION I OUTCROP GC PRF,'.MAAV.M ROOKS .— -APPRO%ANTE 1D41 OF THE 3.1RMA N FOX HILLS AOUFE% MfA UtOOLLA0 OY ME 1 flMS' DATA PCOETS FOX 1!015 MUAFA • Mood mowed n 1961 FAULT-0.r..1 dr.nMr.E • NsE I -BOO POTENT101QTNC COIFTOUR-9oIn anrd Yvm...la11.010.1111110011m Smutted nMgwm Y.J n.f. It.calmly P�r�rn9.d merited n M Lan..rFo M4 ma*.[MindComm dr.N+fir'brad .butyl YA Inn Daum.w1...y I - Figure 9 - Potentiometric Hap of the R1-f Aquifer in the Denver Basin (Robson and Banta, 1987) . Iii I 34 I GROUNDWATER QUALITY OF THE AREA The compiled groundwater quality data were compared with Federal and State Applicable or Relevant and Appropriate Requirements (ARAR's) . The ARAR's were obtained from the Colorado Department of Health (1985) water quality numeric recommendations and standards. Table IX summarizes the ARAR's and water quality parameters which exceed applicable standards. Sulfate, iron, fluoride, pH, ROE and, manganese _ - parameters were found to exceed applicable standards. Figure 19 shows the distribution of samples exceeding ARAB concentrations. With the exception of pH and ROE, the highest percentage of samples that exceed ARAR's are from Data Groups "B" and "C" . Over 60% of Data Group "C" samples and, 45°- Data Group "B" samples exceed the ARAR' s for sulfate concentrations. Additionally, the ARAB concentration for dissolved iron is exceeded by 36% of the samples from Data Group "B" . Thirteen percent of the Group "C" samples exceed the ARAB for fluoride. Over 82% of the samples from Data Group "A" exceed the applicable water quality standard for pH. All of the samples (groups "A" "B" - and "C") exceed the ARAR value (500mg/1) for ROE (TDS) . 67 I. Table IX - ARAR's and Summary of Exceedances I. PARAMETER APPLICABLE STANDARDS PERCENTAGE OF SAMPLING STATIONS ag/L EXCEEDING STANDAkuS GROUP A GRWP B GRWP C L Na NS SO4 250 - CDH 6W DWSTD OX 45% 63% r Ca MS L Mg NS Fe 0.3 - COH GW GUSTO 8% 36% 13% Fl 2.0 - CDR GW DWSTD 0% 0% 13% L Cl 250 - CON GW DUST() 0% 0% O% pH 6.5-8.5 - COX GU DWSTD 82% 36% 25% CO3 NS LROE (TDS) 500 - CDH GW DWSTD 100% 100% 100X EC NS NO3-N 10.0 - CDH GW DWSTD OX OX 0% L K NS Ba 1.0 CDN GW DWSTD O% 0% 0% Co NS I Pb 0.05 - CDH GW DWSTD 0% DX OX Mn 0.05 - CDH GW DWSTD 0% 18% 38% Mo 0.1 - CON AG O% 0% 0% Sr NS IV 0.1 - CDH AG 0% 0% 0% Be 0.1 - CDH AG OX 0% 0% Cu 1.0 - CDH 6W DWSTD 0% 0% 0% I Li 2.5 - CON AG 0% 0% 0% Si MS Zn 2.0 - CGH AG 0% OX L- ' Cd 0.01 - CDH GW DWSTD OX DX 0% Ag 0.05 CDH CV DWSTD 0% 0% OX Cr 0.05 - CDH GW DWSTD 0% 0% OX ' Ni 0.2 - CDH kG OX 0X OX I I CDH - Colorado Department of Health SW - Surface Water _ GW - Groundwater I.. DWSTD - Drinking Water Standard NS - No Standard NA - Not Available I i 68 DISTRIBUTION OF SAMPLES EXCEEDING WATER QUALITY STANDARDS I i 70— b1 U CCUJ ,01 fl ao I to— I - FO4 Fe F PH ROE Mn PARAMETERS ISM GROUP A _GROUP B GROUP C ' WATER QUALITY STANDARDS: 5Oe 250 Fe 03 I F 2.0 pH 63-83 ROE 500 Mn 0.05 I •UNITS IN mg/L except for pH I Figure 19 - Graph represents the distribution of parameters exceeding ARAR concentrations. 69 Eighteen percent of Data Group "B" samples and 38% of Data Group "C" samples exceed the ARAR concentration (0. 05 mg/1) for manganese. Despite having iron, pH, and ROE parameters exceeding ARAR concentrations (Table IX) , the Data Group "A" samples, representing the groundwater from the Kl-f Aquifer, is of better quality for human consumption and domestic purposes than the groundwater of Data Groups "B" and "C" . However, the NA-CO3+HCO3 groundwater in the K1-f Aquifer may not be suitable as drinking water for persons on low sodium diets. The mean ROE value of 592 mg/L exceeds the ARAR concentration of 500 mg/L due to the high mean concentrations of sodium (242 mg/L) and carbonate + bicarbonate (461 mg/L) ions. The groundwater collected from wells in Data Group "B" was of a lesser quality than the groundwater from Data Group "'." . The mean sulfate, ROE and dissolved iron concentrations within Data Group "B" exceed ARAR' s. The high sulfate concentrations in the drinking water obtained from wells in Group "B" may act as a laxative if consumed and the high iron concentrations may cause staining of plumbing and bathroom fixtures (Driscoll, 1986) . In addition, the high soodium-sulfate concentration may not have an aestically pleasent taste or smell. The groundwater quality from wells in Data Group "B" is not suitable for 70 human consumption and most domestic purposes. The water quality of the groundwater sampled from wells comprising Data Group "C" is unfit for human consumption. The mean sulfate concentration of 647 mg/L and the mean ROE value of 1390 mg/L exceeds the ARAR concentrations summarized in Table IX, with the mean ROE value exceeding 1, 000 mg/L the groundwater is classified as brackish (Freeze and Cherry, 1979) . Water which has a dissolved solids concentration greater than 1000 mg/L is a high salinity hazard and is unsuitable for most types of irrigation due to the potential salt buildup in the soil (Robson, 1989) . II - 71 JUN-16-1998 10:28 ..._ REPORT DATE 04/29/98 COLORADO WELLS, APPLICATIONS. AND PERMITS PACE 1 COLORADO DIVISION OP WATER RESOURCES E D CO OWNER INFORMATION - ACTIVITY STATUS 1ST 11S6D ANNUAL ACRES GEOL WKLL WELL WATER SEC LOCAT'N TOWN P CD DATE CD DATE WD MD DB USE DATE APROP IRR AQFR YIELD DEPTH LEVEL COORDINATES QTRS SC SHIP RANGE M 1 62 6IEGRISI CONST 6999 YORK St DENVER, CO 90729 GRAVEL PIT _ AP 02/20/90 AU 03/20/90 5 0 G r,'w 11 3 N 67 H S 1 62 OAKOLIOS ERNEST R. COI.UNN, CO 80401 AP OS/n3/85 AU 05/07/45 2 A Ow SW 31. 3 N 67 W S 169F 1 62 VARRA COMPANIES 2130 S 96TH ST BROOMFIELD, CO 60020 _ EP 01/02/67 EP 02/06/98 5 4 GW r O100N.0200E NENE 31 3 N 67 W S 1 62 VARRA COMPANIES 2110 S 46111 BROOMFIELD. CO 80020 GRAVEL PIT /^� __ AP 07/16/90 AU 05/21/90 5 0 G Gw 4tbr; SWNE 31 3 N 67 W S 426AD 1 62 DAKOLIOS CNSTR CO DENVER, CO 80221 / AD A 4 NENW 11 3 N 67 W 5 1 62 VAµkA COMPANIES 2130 5 96TH BROOMFIELD. CO 80020 GRAVEL PIT _ AP 07/16/90 AU 09/20/90 S 0 G CW SWNW 31 1 N 67 w S 1 936 1 62 ST VRAIN SAN DIST 600 KIMMAR% ST STE B LONGMONT, CO 80502 n,.,wt'°.✓ RP 09/19/87 SA 12/12/88 5 3 12/15/87 0.13 KLF 2.50 150 12 22155,2405E NWSE 31 3 N 6; w S -=796M 1 62 ST. VRAIN SAN. 600 KI'MBARK ST STE B LONGMONT, CO 00502 OWLFt _ NP 12/01/67 SA 5 0 OT/06/BB OW 18 19135,2910E NWSE 31 3 N 67 W S 32796M 1 62 ST. VRAIN SAN. 600 KIMBARK ST STE ➢ LONGMONT. CO 60502 c,{1.2 r NP 12/01/97 SA 5 0 07/08/88 OW 18 19+aS,2410E NWSE 11 3 N 67 W S 795M 1 62 ST VRAIN SANITATION DIST GOO KIMBARK ST STE 8 LONGMONT. CO 60502 5 0 12/15/87 18 1933.5,2925E NWSE 31 N F7 W S 1 62 VARRA COMPANIES 2130 S 96TH BkOOMFILLD. CO 00020 AP 12/23/96 5 C 5'(fi4.(( ?It Ow NESW 31 3 N 4'r w S 1 a5 1 62 GOULD L LONGM0N1', CO 80501 NP n4/06/02 AR 04/27/63 5 R SWSW 11 1 N a7 W 5 154183 1 62 GOULD LEE 12146 WELD CNTY RD 13 LONGMONT. CO 90501 _ NP 04/26/89 AR 05/16/89 5 89 GB 75.00 32 10 03905,O100w SWSW 11 3 N 67 W S 1_.183 A 1 62 GOULD LEE 12148 WELD CNTY RD 11 LONGMONT, CO 90501 NP 04/26/69 AR 05/19/89 5 89 Ow 03905,OtO0W Sw5W 31 3 N 47 w 5 569 1 62 GOULD LEE RT 4 LONGMONT. CO 90501 S 9 05/03/66 25.00 25 6 SWSW 31 3 N 67 W S JUN-16-1998 10:27 c.ep+ REPORT DATE 04/29/99 COLORADO WELLS, APPLICATIONS, AND PERMITS ONCE 1 COGOWADO DIVISION OF BAYER RESOURCES F MIT D CO ONNER INFORMATION ACTIVITY STATUS 1ST USED ANNUAL ACRES GEOL WELL NELL WATER $6C LOCAT'N CD DATE CD DATE WD MU DD USE DATE APROP IRE AQFR YIELD DEPTH LEVEE COORDINATES Q1R5 SC SHIP RANGE M 9705E 1 G2 WALpH Nlx PRODUCE. 1NC 19460 Us Hwy 05 OLLCREST. CO 90622 -- RC 12/02/92 5 t 02/28/40 1000.00 16 �. 2 374 1 62 RALPH NIX PRODUCE 16759 WCR 44 GILCRESI, CO 80623 SENT 26 3 N 6% u 5 NP 10/10/76 RC 04/24/97 2 A L CH 15.0R 70 )I. /[40N,ON%5G SEND 28 A N 6/ w ≤ 2409F R 1 G2 KURTZ CATTLE CO ; AGRICOLA REALTY 6 MGMT FT NONCAN. CO 80701 NP 11/10/94 2 1 CW ON 2592N,2gG5E SENW 26 3 N 67 N ti 124F 1 62 KURT'/, HELENE 0 6 MAX 5676 E 17111 AVE DENVER 20, CO 50220 - 5 1 05/20/63 1000.00 18 5 NWSN 28 ] N 67 N 5 %"'1]7 1 62 RALPH NIX PRODUCE. INC 19480 VS Huy 85 GILCREST, CO ROfi2J KC 12102/92 5 8 05/10/09 15.00 24 a lU\N 20 1 N 6'I N S 136175 1 62 LEER 6 AULT. CO 00521 NP 04/27/54 5 0 01/70/85 1 12 1 62 KURTZ ALBERT R F D I'LATTEVILLE. CO 80651 NE 29 3 N 67 W S 5 9 loon 18 4 N ENE 39 7 N v7 w 5 1 6; LE511 B AULT. CO 50610 TN 04/16/34 5 1 40MH 1 62 CO DAIRY FARMS NENw 29 1 N 67 w 5 C/0 LEER DRILLING AULT, CO 80610 mil 02/05/52 E D Ow e N27N,249vw NE NH 29 I N 67 W 5 97A29VE 1 62 AURORA DAIRY CORP 7386 HWY 66 LONGMONT. CO 00000 AV 02/07/92 5 39 OW 062%N,2497W Nrivw 29 3 N 6% u II 144175 1 62 PSI, ASSOCIATES LONOMONT, CO 80501 '- NP 10/12/82 RC 01/20/84 5 a NCNH 29 3 N 67 N S 2 R 1 62 COLORADO DAIRY FARMS 7388 HWY 66 LONGMONT', CO 80501 NP oz/06/9a SA 07/15/92 5 9 n2/26/92 150.80 GW 290 .00 25 2 2a2741,21 02W NFNW 29 3N 6iWS 25867F 1 62 PSF ASSOCIATES %708 STATE HWY 66 LONGMONT. CO 80501 AB 02/14/92 S 9 09/09/82 205.00 70 2 a''27N,2797w NENW 29 3 N 67 W S JUN-16-1 VO JUN-16-11 1 : F.GJ REPORT DATE 04/29/90 COLORADO WELLS, APPLICATIONS, AND PERMITS VAQE 1 COLORADO DIVISION OF WATER RESOURCES t "T D CO OWNER INFORMATION ACTIVITY STATUS 1ST USED ANNUAL ACRES GEOL WELL WELL WATER SEC LOCAT'N TOWN P CU DATE CD DATE WU MD DB USE DATE APHOP IRA AQPR YIELD DEPTH LEVEL COORDINATES QTRS SC SHIP RANGE M 19074MH 1 62 AT&T COMMUNICATIONS a CERTIFIED ENV CONSULT SALT LAKE CITY. UT 04115 NH 10/19/92 5 0 M OW 0.E0 10 6 NR 30 3 N 67 W S _ .462 1 62 HESS LANCE - CEC 2757 S 300 WEST MD SALT LAKE. UT 84115 NP 11/01/93 5 0 M UNC O114N,7c93E NWNE 30 3 N 67 w S '-"5467 1 62 HESS LANCE - CEC 2757 S 300 WEST MR SALT LAKE. UT 84115 _ NP 11/01/91 5 0 M UNC 0177N,2444E NWNE 30 3 N 67 w 5 175464 1 62 HESS LANCE -- CSC 2757 S 300 WEST MR SALT LAKE. UT 04115 NP 11/01/91 5 0 M UNC 0094N,2498E NWNW 30 3 N 6' W S ;465 1 62 HESS LANCE - CEC 2757 5 300 WEST ID SALT LAKE, UT 81115 NP 11/01/93 5 0 M INC 0177N,2491E NWNE 30 3 N 67 W 5 Colorado eamflow I i Page i 1 r Streamflow Colorado Streamflow Information Here's the streamflow information you requested: ST. VRAIN CREEK NEAR PLATTEVILLE, AT THE MOUTH 400 7 350 m 300 ` 250 a 200 2 150 100 u 50 0 20-Jun 21-Jun 22-Jun 23-Jun 24-Jun 25-Jun 26-Jun 27-Jun 28-Jun 29-Jun 30-Jun Chart prepared on 6/30/98 10:07:28 AM - Days go from Midnight to Midnight Estimated Channel Capacity 1650 CFS WaterTalk (303) 831-7135 Division 1, Station 59 [Another Stream] Nat ii al Resource, I Parks I \\'ildlite Wale) p Geology Oil & Gas I Mining I l And I Overview http L'www dnr state co us/scripts/gage/gage.idc 6/30/98 I I I I I I I I I I I i I I Coloradc trent Streamflow Conditions - Wate... ! Page 1 :3 GS . . . science'agnanglngwnrld Colorado Current Streamflow Conditions - Water Quality Updated TUESDAY JUN 30, 1998 13:08:11 Streamflow conditions are monitored by the U.S. Geological Survey with support from Federal, State, and local cooperators. PROVISIONAL DATA SUBJECT TO REVISION--Select a station number from the table to view graph(s) and other data for a station. Water Specific Dissolved pH Station Station Temp Rainfall Flow Stage Conductanc Oxygen Standard Number Name °C Inches ft3/s ft µS/cm mg/L Units Date/Time a SOUTH PLATTE RIVER BASIN 06 97100 Tarryal Creek below Park Gulch near __ __ 20 3.85 -- -- -- 06/30 Como, Co 08:00 06701970 Spring Cr above mouth nr South Platte 06/30 0 41 3.76 Co. 12:50 06706800 Buffalo Creek at mouth at Buffalo 06/30 0 31 3.75 Creek 11:00 06709000 Plum Creek near Sedalia, Co. -- 0 29 1.85 -- -- -- 06/30 10:45 06709530 Plum Creek at Titan Rd nr Louviers, 06/30 3.4 6.27 Co 11:30 0671024? South Platte River below Union Ave, 06/30 87 10 91 at Englewood 09:30 06/30 0671 1565 South Platte River at Englewood, Co. 0 -- 112 1.73 389 1.6 7.8 10:30 06/30 06712000 Cherry Creek near Franktown, Co. -- 0 2.6 2.16 -- -- -_ 09:45 (lbw l � 1 South Platte R at 64th Ave. Commerce __ 146 2.65 -- -- __ 06/30 City, Co. 09:00 http //nwis-colo crusgs.gov/rt-cgi/gen_thl_pg_ex 6/30/98 I I Coloraac rreiit Streamlflow Londitions - Wate..' Page 2 3 Leavenworth Creek @ mouth nr 06/30 06714800 Georgetown, Co 0 48 4.33 0 - 12:30 06716500 Clear Creek near Lawson, Co. -- 0 488 4.52 -- -- __ 06/30 12:30 06719505 Clear Creek at Golden, Co. -- -- 676 6.51 -- __ __ 06/30 10:00 06720255 Uvalda Intercept bl 56th Av at Rocky 06/30 0 .35 -665.7 Mtn Ars, Co 12:15 06720285 Havana Intercept bl 56th Av, at Rocky 06/30 0 1.3 10.63 Mtn Ars, Co 07:45 06720460 First Cr bel Buckley Rd, at Rocky Mtn 06/30 0 0 .81 Arsenal, C 07:45 06720490 First Cr at Hwy 2, near Rocky Mtn -- -- 0 72 06/30 Arsenal, Co 07:00 06730200 Boulder Cr at North 75th St nr Boulder -- -- 300 5.86 -- -- -- 06/30 12:00 06741510 Big Thompson River at Loveland, Co. -- -- 159 2.62 -- -- -- 06/30 11:00 0675 150 North Fork Cache La Poudre River 06/30 100 2.98 below Halligan Reservoir near V Dal 10:45 06752260 Cache La Poudre River at Fort Collins, 06/30 14.9 409 3.51 48 8.3 Co. 12:15 06752280 Cache La Poudre R ab Boxelder C, nr 06/30 273 5.16 Timnath, Co. 10:45 06754000 South Platte River near Kersey, Co. -- -- 509 3.65 -- -- _- 06/30 10:30 393109104464500 Cherry Creek near Parker, Co -- -- 1.9 2.66 -- -- __ 06/30 01:45 3936471054?5317 South Clear Creek abv Naylor Creek 7 6 -- 3.3 7.41 68 -- -- 06/30 nr Georgetown 02:00 394839104570300 Sand Creek at mouth nr Commerce -- -- 310 5.74 06/30 City,co 04:30 UPPER ARKANSAS RIVER BASIN http //nwis-colo.cr usgs gov/rt-cgi/gen_tbl_pg_ex 6/30/98 APPENDIX —B Methods and Procedures CGRS,Inc. METHODS AND PROCEDURES Soil Borings Soil sampling will be conducted in accordance with ASTM:D 1586-87. Using this procedure, a 2- inch O.D. split-spoon sampler will be driven into the soil by a 140 pound weight falling 30 inches. After an initial set of 6 inches, the number of blows required to drive the sample an additional 12 inches, known as the penetration resistance(N value), will be recorded. The N value is an index of the relative density of cohesionless soils and the consistency of cohesive soils. — Soil Classification/Characterization As samples are obtained in the field, they will be visually inspected and classified in accordance with ASTM:D 1488-84. Representative portions of the samples will then be retained for further examination and for verification of the various strata, the N value, water level data, and pertinent information regarding the method of maintaining and advancing the boring will be provided. Charts illustrating the soil classification procedure, descriptive terminology and symbols used on the logs will be provided. Decontamination To avoid potential transport of contaminated materials to the project site, all drilling equipment and down-hole tools will be steam cleaned prior to mobilization. To prevent cross contamination between soil borings or monitoring wells all down-hole equipment will also be steam cleaned and rinsed with water between soil borings. Monitoring Well Construction Monitoring wells will be installed utilizing the following general construction criteria: • borehole diameter: minimum 6.25 inches; • well diameter: 2 inches; • estimated depth: 15 feet below ground surface; • casing material: schedule 40, flush thread PVC; CGRS,Inc. • well screen: 2 inch I.D., 10 feet in length, #0.01 slot PVC; • estimated screened interval: 5 feet above and 5 feet below the groundwater table; • annular pack: 10-20 silica sand; • protective casing: minimum 12 inch I.D., steel flush or above grade, locking cap; and • annular seal:cement grout and bentonite pellets. Groundwater Sampling All borings where groundwater is encountered will be sampled from the suspected cleanest to the most contaminated according to the protocols listed below. All pertinent information will be recorded on a sampling information form. Field Protocol Step 1 -Measure water level. Step 2 -A dedicated polyethylene bailer will be used to develop each boring. Three bore volumes will be evacuated from each boring prior to sampling. Step 3 -Collect water samples. Water samples will be collected using a polyethylene bailer. A field blank will be collected during the sampling program to ensure quality control. Step 4-Store samples in a cooler on ice for transport to the laboratory. Follow all documentation and chain-of-custody procedures. Step 5 -Clean equipment. Water level measurement equipment will be cleaned with ethanol followed by a deionized water rinse. Upon completion of soil or groundwater sampling, a chain of custody log will be initiated. A copy of the chain of custody will be returned to the project manager. CGRS,Inc. Chemical Analysis All analytical parameters are described in the Laboratory Quality assurance plan presented as Appendix C. Groundwater Elevation Measurements The following outlines our standard groundwater quality sampling methodology. Before purging any of the soil test borings or monitoring wells, water level measurements must be taken. Measuring Point Establish the measuring point for the well. The measuring point is marked on the north side of the top of the temporary monitoring well riser. The top of the riser is normally a 2 inch casing inside a locked protective casing. The riser will be PVC pipe, galvanized pipe or stainless steel pipe. The measuring point should be described on the groundwater sample collection record. Access After unlocking or opening a monitoring well, the first task will be to obtain a water level measurement. Water level measurements will be made using an electronic water level indicator. Depth to water and total depth of the well will be measured for calculation of purge volume. Measurement To obtain a water level measurement, lower a decontaminated electronic water level probe into the monitoring well. Care must be taken to assure that the electronic probe hangs freely in the monitoring well and is not adhering to the well casing. The electronic probe will be lowered into the well until the audible sound of the unit is detected and the light on the electronic sounder illuminates. At this time, the precise measurement should be determined by repeatedly raising and lowering the probe to obtain an exact measurement. The water level measurement is then entered on the groundwater sampling collection record sheet or groundwater level data sheet to the nearest 0.01 feet. CGRS,Inc. Decontamination The electronic probe shall be decontaminated immediately after use by wiping with isopropyl alcohol-soaked paper towels. Always proceed in order from the suspected cleanest well or soil test boring to the suspected most contaminated one. Purge Volume Computation All soil test borings and temporary monitoring wells will be purged prior to sample collection. Depending upon the rate of recovery, three to five volumes of groundwater present in a well or bore hole shall be withdrawn prior to sample collection. If a well or bore hole bails dry, the well or bore hole should be allowed to recharge and a sample taken as soon as there is sufficient volume for the intended analysis. The volume of water present in each well or bore hole shall be computed using the two measurable variables, length of water column in soil boring or monitoring well and diameter. Purging and Sample Collection Procedures Bailin • Obtain a laboratory decontaminated disposable bailer and a spool of nylon rope or equivalent bailer cord. Tie a bowline knot or equivalent through the bailer loop. Test the knot for adequacy by creating tension between the line and the bailer. Tie again if needed. New rope -- will be used for every sample or purge. New clean latex gloves will be used when touching the rope or bailer. • Spread a clean plastic sheet near the base of the well. The plastic sheet should be of sufficient size to prevent bailer or bailer rope from contacting the ground surface. • Place the bailer inside the well to verify that an adequate annulus is present between the bailer and the well casing to allow free movement of the bailer. • Lower the bailer carefully into the well casing to remove the sample from the top of the water column, taking care not to agitate the water in the well. CGRS,Inc. • Pour the bailed groundwater into a bucket. Once the bucket is full, transfer the water to a barrel and contain on-site. • Raise the bailer by grasping a section of cord, using each hand alternately. This bailer lift method will assure that the bailer cord will not come into contact with the ground or other potentially contaminated surfaces. Sampling • Instructions for obtaining samples for parameters are reviewed with the laboratory coordinator to insure that proper preservation and filtering requirements are met. • Appropriate sample containers will be obtained from the contract laboratory. After samples are collected, they will be put on ice in coolers (4°C). Care will be taken to prevent breakage during transportation or shipment. • Samples collected by bailing will be poured directly into sample containers from bailers. The sample should be poured slowly to minimize air entrapment into the sample bottle. During collection, bailers will not be allowed to contact the sample containers. • Upon completion of sampling a chain-of-custody log will be initiated. Chain-of-custody records will include the following information: project name and number, shipped by, shipped sampling point, location, field ID number, date, time, sample type, number of containers, analysis required and sampler's signature. The samples and chain-of-custody will be delivered to the laboratory. Upon arrival at the laboratory the samples will be checked in by the appropriate laboratory personnel. Laboratory identification numbers will be noted on the chain-of-custody record. Upon completion of the laboratory analysis,the completed chain-of-custody record will be returned to the project manager. Field Cleaning Procedures For all equipment to be reused in the field, the following cleaning procedures must be followed: • Disassemble the equipment to the extent practical. • Wash the equipment with distilled water and laboratory-grade detergent. CGRS, Inc. • Rinse with distilled water until all detergent is removed. • Rinse the equipment with isopropyl or methanol, making sure all surfaces, inside and out, are rinsed. • Triple rinse the equipment with distilled water. Laboratory Selection The project manager should consider the following factors when selecting a laboratory: • Capabilities (facilities, personnel, instrumentation), including: • Participation in interlaboratory studies(e.g., EPA or other Federal or State agency sponsored analytical programs); • Certifications (e.g., Federal or State); • References (e.g. other clients); and • Experience(UST, RCRA and other environmentally related projects). • Service; • Turnaround time; and • Technical input(e.g., recommendations on analytical procedures). The project manager is encouraged to gather pertinent laboratory-selection information prior to extensively defining analytical requirements under the project. A request may be made to a laboratory to provide a qualifications package that should address the points listed above. Once the project manager has reviewed the various laboratory qualifications, further specific discussions with the laboratory or laboratories should take place. In addition, more than one laboratory should be considered. For large-scale investigations, selection of one laboratory as a primary candidate and one or two laboratories as fall-back candidates should be considered. The quality of the laboratory service provided is dependent on various factors. The project manager should be able to control the quality of the information (e.g., samples) provided to the laboratory. It is extremely important that the project manager communicate to the laboratory all the requirements relevant to the project. This includes the number of samples and their matrices, sampling schedule, parameters and constituents of interest, required analytical methodologies, detection limits, holding times, deliverables, level of QA/QC, and required turnaround of analytical results. CGRS,Inc. Field and Laboratory Quality Control General Quality control checks are performed to ensure that the data collected is representative and valid data. Quality control checks are the mechanisms whereby the components of QA objectives ore monitored. Examples of items to be considered are as follows: 1. Field Activities: • Use of standardized checklists and field notebooks; • Verification of checklist information by an independent person; • Strict adherence to chain-of-custody procedures; • Calibration of field devices; • Collection of replicate samples; and • Submission of field blanks, where appropriate. 2. Analytical Activities: • Method blanks; • Laboratory control samples: • Calibration check samples; • replicate samples; • Matrix-spiked samples; • "Blind"quality control samplers; • Control charts; • Surrogate samples; • Zero and span gases; and • Reagent quality control checks. Blind Duplicates Blind duplicate samples will be collected for 10% of the samples collected or once per site, whichever is greater. These blind duplicate samples will be forwarded to the laboratory as a check of laboratory reproducibility. CGRS,Inc. Equipment(Rinseate)Blank The equipment (rinseate) blank is designed to identify potential cross-contamination in the field between sample sources due to deficient field cleaning procedures. This blank also addresses field preservation procedures, environmental site interference, integrity of the source blank water for field cleaning and those concerns singularly addressed by the travel blank. Equipment blanks are taken once per site, when equipment is cleaned in the field. This provides a quality control check on field cleaning procedures. Field Blank Field blanks are used to evaluate the sample container filling procedure, the effects of environmental contaminants at the site, purity of preservatives or additives and those concerns uniquely addressed by the travel blank. Field blanks are taken downwind of the most contaminated area of the site by filling laboratory cleaned and prepared sample containers (appropriate for the parameters group) with deionized or organic-free water supplied by the laboratory. The blank sample container is then sealed, grouped, transported and stored with the real samples collected for the same parameters group. Travel(Trip)Blanks The travel blank is designed to address interferences derived from improper sample container cleaning preparation, contaminated source blank water, sample cross-contamination during storage/transport and extraneous environmental conditions affecting the sampling event to and from the site, including delivery to the laboratory. Travel blanks are composed in the appropriate sample container using source blank water. Preservatives or additives are added if required for the parameters group. Travel blanks are then sealed and stored in the ice chest where real samples will be stored and transported. Travel blanks are to originate at the laboratory providing the blank water for the equipment and field blanks. CGRS,Inc. Protocol(or Analyzing Blank Samples If used, the equipment blank will be analyzed first. If contamination is found to be present, the field blank will then be analyzed. If the equipment blank is not used, the first blank analyzed will be the field blank. If any blank is found to be contaminant-free, the sequence of analyses will be terminated. APPENDIX C Quality Assurance Project Plan QUALITY ASSURANCE PROJECT PLAN FOR THE VARRA COAL ASH BURIAL PROJECT WELD COUNTY,COLORADO 1.0 Introduction This Quality Assurance Project Plan (QAPP) briefly describes the field data collection activities and laboratory analyses being conducted as part of the Varra Coal Ash Burial Project in Weld County, Colorado. The work described in this QAPP is being conducted to address possible concerns related to coal ash burial in saturated mediums. Described in the sections below are the project objectives, scope of work, sample handling and Chain-of-Custody procedures, data quality assurance, and laboratory deliverables. 2.0 Objectives The data being collected are intended to support the following objectives: • Identify potential on-site and off-site contamination to soils, groundwater, and surface water that have occurred from past operations at the various sites; • Determine the extent of contamination(if any); • Characterize hydrogeologic and surface water conditions in sufficient detail to describe hydrostratigraphy, direction and velocity of groundwater flow, and the relationship between groundwater and surface water; • Develop and implement monitoring programs for the various media; and, • Employ industry standard field and laboratory methods suitable to meet CLP or equivalent(such as EPA QC Level III)Data Quality Objectives. 3.0 Scope of Work The scope of work for this project involves, development of Health and Safety and site-specific Work Plans, field investigations, laboratory analysis of water samples, analysis of hydraulic and hydrogeologic properties, and the preparation of a report detailing the results of the investigation. Field investigative techniques include soil and groundwater sampling using direct push and hollow stem auger techniques. 3.1 Sample Identification A sample identification scheme will be used that maintains consistency for the names of boreholes and monitoring wells, as well labels affixed to each sample container, and entered on to the Chain-of-Custody(COC)forms. The following scheme will be followed: 1. Samples from soil borings that are not converted to monitoring wells are named SB; 2. Samples from soils collected during drilling of monitoring wells are named MW; and 3. Depth of soil sampled indicated by @(depth interval). For example a soil sample might be identified as MW-4 @ 10-11.5. Groundwater, surface water, and sediment samples will be named with no depth interval (i.e. MW-4, SW-4, SED-4, respectively). 3.2 Analytical Suites Analytical procedures for water and soil samples will conform to the USEPA guidelines described in SW 846 (Test Methods for Evaluating Solid Waste/Physical/Chemical Methods, 3'd ed.). Table 1 —C, presents the analyses that are anticipated on the project. The analytical suite at a particular site will be determined on a site by site basis. 3.3 Sample Custody Strict chain of custody (COC)protocol will be maintained throughout the life of the field program and will be controlled through the use of a COC Record supplied by the laboratory. The following procedures will be used to document, establish, and maintain custody of field samples: • Sample labels will be completed for each sample using waterproof ink; making sure that the labels are legible and affixed firmly on the sample container; • All Sample-related information will be recorded in the project log book; • The field sampling technician will retain custody of the samples until they are transferred or properly dispatched to a laboratory; and, • As fieldwork is conducted the on-site CGRS technical lead will determine whether these procedures are being followed, if corrections need to be made, and if additional samples are required. 3.3.1 Chain of Custody Records A Chain of Custody Record will be maintained in the field for all samples to be shipped to the laboratory for analysis. The three lines of information to be entered into the COC box titled "Project or P.O.#"are: Line 1. Client Name, i.e. "Varra Companies" Line 2. Site Name, i.e. "Pit 112" Line 3. Site Number, i.e. "2755" The three lines of information will be provided on the laboratory paper (hard copy) reports as a page header, and on the electronic deliverables as three individual fields in each analytical record. Varra Companies Quality Assurance Project Plan Page 1 The "Sample Identification" entries to the COC will be completed as described in Section 3.1 of this QAPP. 3.3.2 Transfer of Custody and Shipment Due to the evidentiary nature of field sample collection, the possession of samples must be traceable from the time the samples are collected until they are introduced as evidence in legal proceedings. A sample is defined as being under a person's custody if any of the following conditions exist: (1) it is in their possession, (2) it is in their view after being in their possession, (3) it is in a secure locked location after having been in their possession, and (4) it is in a designated secure area. The following procedures will be used in transferring and shipping samples: • Field personnel will maintain detailed notes in field logbooks, documenting the collection and identification of the required samples. The logbooks will be checked against the COC records for completeness and traceability. • A COC record will accompany all sample shipments. When transferring samples, the individuals relinquishing and receiving will sign, date, and note time on the record. The COC documents transfer of sample custody from the field sampling technician to another person or to the laboratory. • Each cooler is to contain samples from one site. No mixing of samples from multiple sites will be allowed in a given cooler. • Samples will be properly packaged for shipment and shipped to the laboratory for analysis with a separate signed COC record enclosed in each sample box or cooler. Two copies of this record will accompany the samples to the laboratory. The laboratory maintains one file copy, and the completed original will be returned to the project manager as part of the final analytical report. This record will be used to document sample custody transfer from the field sampling technician to the laboratory or to the CGRS offices. Just prior to shipment to the laboratory, coolers will be secured with custody seals. • Whenever samples are split with a facility operator or government agency, a separate COC record will be prepared for those samples and so marked to indicate with whom the samples are being split. • The COC record showing identification of the contents will accompany all packages. The original record will accompany the shipment and the field team leader will retain a copy. • A bill of lading will be used for all samples sent by common carrier. Receipt of bills of lading will be retained as part of the COC permanent documentation. Varna Companies Quality Assurance Project Plan Page 2 3.33 Laboratory Custody Procedures The laboratory, at a minimum, will check all incoming samples for integrity and note any observations of the original COC record. Each sample will be logged into the laboratory system by assigning it a unique laboratory identification number. This number and the field sample identification number will be recorded on the laboratory report. Samples will be stored and analyzed according to the methods described in Section 3.1. The original COC record will be returned to the CGRS project manager for filing. The laboratory sample custodian will use the following procedures to maintain the COC records once the samples arrive at the laboratory: • The samples received by the laboratory will be cross-checked to verify that the information on the sample labels matches that on the COC record included with the sample shipment; • The "Received by Laboratory" box on the COC record will be signed on receipt. Any discrepancies between the COC record and the shipment contents will be resolved as soon as possible through communication with CGRS personnel; • The status of the sample receipt and analysis will be tracked within the analytical laboratory by a laboratory information management system (LIMS) or equivalent computerized management system. For data that are input by an analyst and processed using a computer, a copy of the input data will be kept and identified with the project number and any other needed information. The samples analyzed will be clearly noted and the input data signed and dated by the analyst. 3.4 Laboratory Deliverables The laboratory is required to submit EPA QC Level III data packages (CLP-equivalent) to CGRS, Inc. within 21 days from the date of acceptance on the Sample Receipt Form. Details of the deliverables are presented below. • Sample Receipt - The laboratory will complete and submit a "Sample Receipt" form for all sample shipments received. The purpose of the form is to note problems with sample packaging, COCs, and sample preservation. Problems noted on the form will be communicated to CGRS, Inc. as soon as possible. • Reporting of Analytical Results — For each analytical method performed, the laboratory will report all analytes as detected concentrations or as less than the specific limits or quantification. All samples with out-of-control spike recoveries being attributed to matrix interferences should be designated as such. All soil/sediment and solid waste samples should be reported on a dry-weight basis with percent moisture also reported. Also, report dates of extraction/preparation, dates of analysis, and dilution factors when applicable. An electronic deliverable (LIMS) will be provided that conforms to the CGRS project data requirements. An example of the data deliverable is provided as an appendix. • Internal Quality Control Reporting—Internal QC samples should be analyzed at rates specified in the method (SW-846). At a minimum, QC deliverables will consist of laboratory blank results, surrogate spike percent recoveries, results of MS/MSD analyses, laboratory control sample data, laboratory duplicate results, and if requested, calibration and tuning data. The internal QC data will not be delivered unless requested by Varra or CGRS personnel. Vane Companies Quality Assurance Project Plan Page 3 3.5 Field and Laboratory QA/QC Procedures Quality control checks are performed to ensure that the data collected are representative and valid. Quality control checks are the mechanisms whereby the data quality objectives are monitored. The quality control samples to be collected on the project are described below. • Duplicate Samples — As a check for laboratory reproducibility, blind duplicate samples(unknown by the laboratory to be duplicates) will be collected and submitted to the laboratory at a rate of one every 10 water samples collected, or once per site, whichever is greater. No duplicate soil samples will be collected. • Field Blank Samples —To evaluate sample bottle filling procedures and the effects of environmental contaminants at the site, one VOA water sample per site is collected in laboratory-cleaned and prepared containers of deionized or organic-free water supplied by the laboratory. Field blanks are collected downwind of the most contaminated area within a site. The sample is sealed, labeled and shipped with the real samples collected for the same parameter group. • Travel(Trip) Blanks—Trip blanks are intended to address interferences derived from improper sample container cleaning, preparation, contaminated source blank water, sample cross-contamination during storage and shipment, and environmental conditions affecting the sampling event to and from the site, including delivery to the laboratory. Trip blanks will originate at the laboratory and will consist of VOA vials filled with source blank water, and will be sealed and stored in the cooler where real samples will be stored and shipped. • Equipment (Rinseate) Blanks—Rinseate blanks, intended to provide quality control on field cleaning procedures, will be collected once per site. Varra Companies Quality Assurance Project Plan Page 4 Table 1 - C Summary of Parameters, Sample Containers, Holding Times, and Analytical Methods Parameter Matrix ta No.and Type of Holding Time(1) Analytical Coniners-` Method(2) Free Cyanide. Water 1-200 ml P,G 14 days,4C,NaOH to ph>12 EPA 300.0 Chloride Water 1-200 ml,P,G 28 days no preservative required EPA 300.0 -- Fluoride Water 1-500 ml,P 28 days no preservative required EPA 300.0 Sulfate -- Water 1 -200 ml,P 28 days cool to 4C EPA 300.0 Nitrate Water 1 -100 ml,P,G 48 hours cool to 4C EPA 300.0 Mercury Water 1-500 ml P,G 28 days.HNO3 to pH<2 245.1/7170 Total Metals(RCRA) Water 125-500 ml nalgene (Red dot) 6 months except Mercury at 28 days. For 6010/7000 water,preserved with HNO3,not filtered. Dissolved Metals(RCRA) Water 125-500 ml nalgene 6 months except Mercury at 28 days. Filtered 6010/7000 (Green dot) and preserved in Lab. Anions/General Chemistry Water 250 ml nalgene(White 28 days 200 Series Notes: (1)All collected samples to be kept cool(4 degrees C) (2)USEPA Method,SW-846(Revised), 1986 Table 2 - C Content of Digital Analytical Deliverables — (LIMS Download) _ Origin of Data Generated by CGRS Generated in Lab Laboratory Name of Data Example of Delivered and Entered on by Analytica Field Digital Data COC COMPANY_NA Varra Energy X SITE_NAME Coal Ash Project X SITE_NO 2755aa X SAMPLE_ID1 MW-I X SAMPLE_DAT 08/27/97 X LAB_ID L15316-01 X MATRIX Water X X METHOD M6010 ICP X DATE_ANALY 09/04/97 X ANALYTE Silver, total (3051) X TEXT_RESUL (blank it ND) X — NUMBER_RES (blank if ND) X QUALIFIER U X DILUTION 106 X MDL 0.50000 X PQL 3.00000 X UNITS mg/Kg X DATE_RECEI 09/03/97 X DATE_EXTRA 09/04/97 X CAS_ 007440-22-4 X BATCH ID WG47359 X TABLE3 - C Analytical Suites Field Pilot Test Varra Coal Ash Project Weld County, Colorado CGRS No. 1-135-2755 Analvte Standard Units Aluminum 5.000 mg/L Arsenic 0.050 mg/L Barium 2.000 mg/L Boron 0.750 mg/L Cadmium 0.005 mg/L Chromium 0.100 mg/L Colbalt 0.050 mg/L Iron 0.300 mg/L Lead 0.050 mg/L Manganese 0.050 mg/L Mercury 0.002 mg/L Selenium 0.050 mg/L Chloride 250 mg/L Fluoride 2.0 mg/L Free Cyanide 0.20 mg/L pH 6.5-8.5 s.u. Sulfate 250 mg/L Total Dissolved Solids 500 mg/L mg/L-milligram per liter s.u.-standard units NE1D E.N\IAt MO y �p WORK PLAN VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COUNTY COLORADO CGRS NO. 1-135-2755 by CGRS, INC. December 29, 1998 IJi u4 UU CGRS,Inc. Table of Contents 1.0 INTRODUCTION 1 1.1 Objectives 1 1.2 Background Information 2 -- 1.2.1 Local Geology/Hydrology 2 1.2.2 Coal Ash Source 3 2.0 INITIAL LABORATORY TESTING 3 2.1 Hydraulic Conductivity 3 2.2 Porosity 3 2.3 Analytical Data 4 2.3.1 SELP 4 2.3.2 SGCLP 5 2.3.3 TCLP 7 2.3.4 SGLP 7 3.0 PILOT STUDY 7 4.0 PROJECT SCHEDULE 9 5.0 ORGANIZATION AND STAFF ASSIGNMENTS 9 3.1 Project Personnel 9 3.2 Subcontractors 9 6.0 OVERVIEW-QUALITY ASSURANCE/QUALITY CONTROL 9 7.0 REMARKS 10 FIGURES: Figure 1 -Site Location Map Figure 2—Registered Well Location Map Figure 3—Area Use and Site Condition Map APPENDIX: Appendix A—Selected Data—Groundwater Quality and Hydrogeology fo the Laramie-Fox Hills Aquifer in the Milton Reservoir Area, Weld County,Colorado Appendix B-Methods and Procedures Appendix C—Quality Assurance Project Plan CGRS, Inc. WORK PLAN VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COLORADO CGRS NO. 1-135-2755 1.0 INTRODUCTION This document presents the proposed work scope for the evaluation of coal ash burial in saturated media. The field investigation will be performed in conjunction with a variety of laboratory studies in order to evaluate potential liabilities or benefits associated with coal ash burial. Specifically, this project addresses issues associated with the reclamation of gravel quarries under saturated conditions. A variety of laboratory experiments were conducted in order to evaluate coal ash leaching potentials for different pH ranges relative to effluent pore volume. The information generated by this project will be invaluable to private companies or regulatory agencies insofar as evaluating under what conditions coal ash can be placed without incurring significant liability. — 1.1 Objectives The purpose of this project is to identify potential liabilities with the reclamation of gravel quarries with coal ash and to determine if coal ash meets the criteria for classification as an inert fill. Specific objectives for the Varra Coal Ash Burial Project are to determine: • Leaching characteristics of coal ash with respect to varying water quality conditions; • Permeabilities of various types of coal ash (bottom and fly ash); • Affects of coal ash burial on local hydrology and water quality; • Hydrogeologic properties of coal ash; and • Physical characteristics of coal ash in saturated media. 1.2 Background Information 1.2.1 Local Geology/Hydrogeology The study area is an active gravel quarry located in the NW 1/4, Section 31, Township 3 North, Range 68 West, 6th P.M., Weld County Colorado (Figure 1). The surficial geology of the area as documented by Colton, 1978, varies between wind blown deposits of clay, silt and sand and sandy to gravelly alluvium, which are Holocene in age. Colluvium consisting of bouldery to pebbly sandy silt and clay may contain and interfinger with alluvium of various ages. 1 CGRS,Inc. The depth to groundwater at the site generally varies between three and ten feet below ground surface (bgs). The inferred groundwater flow direction is to the northeast roughly parallel to the St. Vrain River drainage. Water well records obtained from the Colorado Division of Water Resources indicate that one well may be located within one quarter mile of the proposed test plot. The registered well owner is Dakolios Construction and the permitted use of the well is industrial. The location of registered wells within a half mile radius of the proposed test plot are depicted on Figure 2. Field verification of well locations and construction details, if available will be performed prior to project start-up. Groundwater quality data for the immediate study area are limited. Reeder, 1993, describes in detail the regional hydrogeology near the area of interest. Water quality data for 36 domestic wells completed as bedrock aquifers (Larimie-Fox Hills Formation) in the Milton Reservoir were compliled by Reeder. A review of water quality data indicate that all wells sampled exceeded water quality standards for total suspended solids and a large percentage exceeded standards for pH. Field and analytical data documented by Reeder and other background information are presented in Appendix A. 1.2.2 Coal Ash Source Public Service coal comes from a number of Colorado mines in Routt, Moffat, Delta and Gunnison counties. These mines include West Elk, TwentyMile, Powderhorn, and ColoWyo. This coal is normally purchased under long term contracts which specify certain analytical parameters. Therefore, the chemical and physical properties of the coal (and resulting ash) do not change significantly from year to year. Analytical information for each of these coal sources is available as is the analytical information on the ash. This information has been provided in our earlier submittal. Comparisons of analytical data completed in the early 1990s with recent data indicate little variation in any of the ash constituents. 2 CGRS, Inc. 2.0 INITIAL LABORATORY TESTING Public Service Company generated analytical data indicating that fly ash is not a characteristic hazardous waste. Numerous analytical methods were used such as toxicity characteristic leaching procedure (TCLP). CGRS in conjunction with Colorado State University Groundwater Program performed a number of tests which included: • Hydraulic Conductivity Testing (Permeameter Test); • Porosity Determination; • Sequential Extraction Leaching Procedure (SELP); • Synthetic Ground Water Column Leaching Procedure (SGCLP); • Toxic Characteristic Leaching Procedure (TCLP); and • Synthetic Ground Water Leaching Procedure (SGLP). A discussion of these tests and the loading calculations to the environment is provided below. 2.1 Hydraulic Conductivity The hydraulic conductivity of the ash was performed using either a "Constant Head" or "Falling Head" Permeameter. The Constant Head Permeameter works better for high permeability porous materials and the Falling Head Permeameter works best for low permeability porous materials. With either test the flow rate and the potentiometric head loss are measured through a sample of the ash. The hydraulic conductivity was then calculated using Darcy's Law. The hydraulic conductivity of the ash is required to determine the expected rate of groundwater flow through the buried ash and the effects of burial on ground water flow patterns. 2.2 Porosity Porosity is the ratio of the volume of the voids to the bulk volume of the sample. With this test the volume and dry weight of a sample of ash was measured. The ash was then saturated with water under a vacuum pressure and the weight of the saturated sample measured. For saturated conditions the volume of the voids is equal to the volume of the water. The porosity is required to determine the pore volume for the ash. The results of hydraulic conductivity and porosity testing are summarized in Table I. 3 CGRS,Inc. TABLE 1 -Results for Hydraulic Conductivity and Porosity Tests Sample ID Hydraulic Porosity Conductivity K (ft/day) Cherokee Silo Ash 2/3 0.24 0.51 Cherokee 4 Ash with Sodium 0.23 0.46 Class F Silo Ash with Gypsum 0.09 0.49 Bottom Ash 178. 0.51 Recycled Concrete 111. 0.29 Recycled Asphalt 130. 0.33 The bottom ash, the recycled concrete and the recycled asphalt all had relatively high hydraulic conductivity values in the range of 111 to 178 feet/day. The three fly ash samples had very low hydraulic conductivity values in the range of 0.09 to 0.24 feet/day. The porosity of the fly and bottom ash ranged from 0.46 to 0.51. These values are characteristic of very fine porous materials. The porosity of the recycled concrete and asphalt was 0.29 and 0.33, respectively. 2.3 Analytical Data 2.3.1 "Sequential Extraction Leaching Procedure" (SELP) The purpose of the "Sequential Extraction Leaching Procedure" (SELP) test was to determine the total quantity of the various chemical contaminants that may be potentially leached from the ash. The SELP test used synthetic groundwater with varying pH levels as the leaching fluid(s). With the SELP test, a specified weight (e.g. one kilogram) of the ash was combined with a 4 CGRS, Inc. specified volume of water (e.g. one liter) and agitated by rolling for a specified period of time (e.g. 18 hours). This represented a single extraction. The concentration of the chemical contaminant was then measured in the water. The SELP test was repeated for several sequential extractions until most of the chemical contaminants have been extracted from the ash. This normally requires three or more extractions. Only two extractions were performed due to budgetary constraints. The SELP test was repeated for synthetic groundwater with varying pH values to represent a range of possible site conditions. Synthetic groundwater(s) with pH values of 5, 7 and 8.5 were used. The first extraction from the SELP test for each pH value was analyzed for the full suite of chemical compounds. These include: • Sulfate • Chloride • Fluoride • Cyanide • Mercury • Nitrate • Nitrite • 20 other metals (Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Lithium, Manganese, Nickel, Selenium, Silver, Thallium, Vanadium and Zinc). Conductivity and pH will of the leachate was measured at CSU prior to sending the sample to the laboratory for chemical analyses. The SELP test was conducted at CSU. The extracted water samples from the test were sent to Analytica Environmental Labs for chemical analyses. Analytical results from the first extraction were used to identify those compounds to be analyzed for in subsequent extractions of the SELP test and in the SGCLP test. Those chemical compounds, which were either non-detect or detected at very low concentrations during the first extraction were not analyzed for in subsequent extractions of the SELP test or in the SGCLP test. 5 CGRS,Inc. 2.3.2 "Synthetic Groundwater Column Leaching Procedure" (SGCLP) The purpose of the "Synthetic Groundwater Column Leaching Procedure" (SGCLP) test was to determine the rate as a function of pore volume at which the chemical contaminant will be leached from the buried ash. The SGCLP test used synthetic groundwater with varying pH levels as the leaching fluid(s). With the SGCLP test, a specified weight (e.g. one kilogram) of the ash was placed in a column. Once the column was saturated, the testing period began. One pore volume of water was passed through the column and the concentration of the various contaminants measured in the outflow water. The SGCLP test was then repeated for several sequential pore volumes of water. The hydraulic head on the column was adjusted so that one pore volume of water was passed through the sample in about 8 hours. Water samples were be obtained for analyses at 2, 4 and 8 pore volumes of water flow through. The SGCLP test was repeated for synthetic ground water with varying pH values to represent a range of possible site conditions. Synthetic ground water(s) with pH values of 5, 7 and 8.5 were used as the leaching fluid(s). For the fly ash, which has a very low hydraulic conductivity, the SGCLP test was conducted for 1,2 and 4 pore volumes. For the bottom ash, the recycled concrete and the recycled asphalt, which have high hydraulic conductivity, water samples were analyzed at 2, 4 and 8 pore volumes. The chemical analyses for the first extraction of the SELP test was used to determine the suite of chemical compounds of interest in the SGCLP test. Chemical compounds, which were either non-detect or detected at very low were eliminated from further testing. The SELP test is a highly agitated test where as the SGCLP test is not. The SGCLP test was conducted at CSU with the collected water samples sent to Analytica Environmental Labs for chemical analyses. • Sulfate • Chloride • Fluoride • Cyanide • Mercury • Nitrite • Nitrate • 10 other metals from the following list of 20 metals (Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Lithium, Manganese, Nickel, Selenium, Silver, Thallium, Vanadium and Zinc). Conductivity and pH will of the leachate was measured at CSU prior to sending the sample to the laboratory for chemical analysis. 6 CGRS, Inc. 2.3.3 "Toxic Characteristics Leaching Procedure" (TCLP) The "Toxic Characteristic Leaching Procedure" (TCLP) test is designed to determine the mobility of toxicity characteristic constituents and is the EPA method for classifying wastes as hazardous or non hazardous based on toxicity. The full suite of chemical compounds (see list for SELP test) was analyzed during the TCLP test. 2.3.4 "Synthetic Ground Water Leaching Procedure" (SGLP) The "Synthetic Ground Water Leaching Procedure" (SGLP) test is identical to the TCLP test with the exception that synthetic groundwater is used as the leaching fluid. A description of the TCLP test is provided above. The SGLP test was developed to simulate geochemical conditions more closely approximating natural ground water than for the TCLP test. The results of the SGLP are directly comparable to the TCLP test. Groundwater obtained from the study area was used for the test. The full suite of chemical compounds (see list for SELP test) were analyzed during the SGLP test. The groundwater used in the SGLP test as the leaching fluid was analyzed for full suite of chemical compounds. The difference in the before and after chemical concentrations in the ground water used in the SGLP test represents the concentration of the chemical contaminants leached from the ash. 3.0 PILOT STUDY The project start-up will consist of developing a work plan and a site specific Health and Safety plan. All required permits will be obtained prior to conducting the investigation. Utility companies will be contacted for the location of all underground utilities prior to commencing investigative activities (telephone, sewer, electrical, cable television, natural gas lines, oil and gas pipelines, buried tanks and wells). Prior to initiating coal ash placement, the local groundwater flow direction will be estimated from groundwater monitoring wells installed to determine hydraulic characteristics of the local aquifer and local groundwater quality. It is anticipated that ten wells will be installed to monitor 7 CGRS,Inc. variations in local aquifer characteristics as a result of coal ash burial. The hydraulic conductivity will be estimated by performing slug and/or aquifer testing. Prior to initiating the pilot project groundwater quality samples will be obtained and analyzed for pH, TSS, TDS, and other relevant parameters identified in the laboratory leaching tests. Samples will be obtained from no less than one up-gradient and two down gradient wells. The anticipated locations of the monitoring wells are depicted on Figure 3. Typical monitoring well construction details are presented in Appendix B. The effects on groundwater quality and hydrology as a result of coal as burial will be evaluated by placing roughly 400 tons of coal ash within a trench at the location shown on Figure 3. The coal ash will be placed so that the water table intersects the coal ash and that the seasonal fluctuation of the water table will be within the coal ash bed. The coal ash will be buried in a trench measuring 10 feet in width, 100 feet in length and roughly 10 feet in depth. In order to evaluate hydraulic — characteristics of bottom ash and fly ash, one-half of the trench will be filled with fly ash. A native soil divider will be left and the other half of the trench will be filled with bottom ash and fly ash. Bottom ash will be placed in the lower one-half of the saturated portion of the trench and fly ash will be placed to one foot below ground surface. Approximately one foot of native soil will be place over the entire trench. Variations in water quality will be verified through quarterly water quality monitoring for analytical parameters identified in the laboratory quality assurance plan Appendix C. The results of the analyses will be submitted to the Colorado Department of Public Health and Environment, Division of Minerals and Geology and Weld County Health Department. Within one week of coal ash burial water quality samples will be obtained from all monitoring wells. Water quality samples will be obtained on a weekly basis for one month and then on a monthly basis. The length of sampling will be determined after reviewing the initial analytical results; it is not anticipated that more than three months will be required before water quality parameters equilibrate. 8 CGRS, Inc. 4.0 PROJECT SCHEDULE Based on laboratory experiments it is anticipated that approximately three months will be required to perform field activities. The project length is based partially on pore volume flow thorugh calculations. It is anticipated that a summary report will be submitted within four months of coal ash placement. 5.0 ORGANIZATION AND STAFF ASSIGNMENTS 5.1 Project Personnel Mr. Joby Adams of CGRS will serve as project coordinator and contact to Varra Companies. Mr. Chester Hitchens will serve as field coordinator and will be responsible for supervising drilling activities and will perform water quality sampling as well. 5.2 Subcontractors Subcontracted services for this project will include Universal Drilling of Brighton, Colorado, and Quanterra Laboratories of Brighton, Colorado. Universal Drilling will be responsible for drilling soil borings and completing the borings as groundwater monitoring wells. Quanterra Laboratory will analyze groundwater samples for inorganic related constituents. 6.0 OVERVIEW- QUALITY ASSURANCE/QUALITY CONTROL Quality assurance (QA) is a management system for ensuring that all information, data, and decisions resulting from the project are technically sound and properly documented. Quality Control (QC) is the functional mechanism through which quality assurance achieves its goals. Quality control programs, for example, define the frequency and methods of checks, audits, and reviews necessary to identify problems and dictate corrective action to resolve these problems, thus ensuring data of high quality. Thus, a QA/QC program pertains to all data collection, evaluation, and review activities that are part of the project. The use of qualified personnel for conducting various portions of the project is of paramount importance to an effective QA/QC program. This pertains not only to qualified QA/QC specialists, but also to specialists in other fields, including hydrogeologists, air quality specialists, soil 9 CGRS, Inc. scientists, analytical chemists and other scientific and technical disciplines. The project manager should ensure that qualified specialists, primarily individuals with the proper education, training, and experience, including licensed or certified professionals, are directing and performing the various project activities. The same general principles apply to selection of contractors and/or outside laboratories. Another important aspect of the QA/QC program is the communication between the QA/QC organization and the project manager. Regular appraisal by the project manager of the quality aspects related to the ongoing project data-gathering efforts provides the mechanism whereby the established objectives may be met. QA/QC procedures should provide details relating to the schedule, information to be provided, and the mechanism for reporting to the project manager. Reports to the project manager should include: • Periodic assessment of measurement data accuracy,precision, and completeness; _ — • results of performance audits; • Results of system audits; • Significant QA/QC problems and recommended solutions; and • Resolutions of previously stated problems. The individual responsible for preparing the periodic reports should be identified. These reports should contain a separate QA/QC section that summarizes data quality information. The Quality Assurance Project Plan is presented as Attachment C. 7.0 REMARKS The scope of work and estimated costs are based upon current available information and our understanding of this project. As the project develops, changes to the project scope of work may be required. If changes in the scope of work are dictated by the needs of the project, these changes will be presented prior to implementation. 10 CGRS,Inc. This report was prepared by CGRS, INC. Date Joby L. Adams Principal/Hydrogeologist Reviewed by: Date Dr. James W. Warner, P.E. Groundwater Program Leader Colorado State University 11 CGRS, Inc. APPENDIX A SELECTED DATA— Groundwater Quality and Hydrogeology of the Laramie-Fox Hills Aquifer in the Milton Reservoir Area,Weld County Colorado 1 r P Fort Collins Larimer Greeley County Study Area ti�1111,�IT�111�1 •1 1,�1 1 it ..n•,alilPl;"!;�1u71�,�;1,�� �1. Boulder County Weld ' Longmont County ' Boulder Adams County Jeffercnn County Golden Denver Arapahoe County 0 feet 52300 105600 SCALE: 1:633,600 Figure 1 - Location of the study area. 2 I • :2I —�� • �� ^r r' L --- n ,,.. _ t j \'Y.r �►., ..� NIL .-1 i '-'5: • ice;_ % ' lli: sf et se k = avT / /iAu▪ fnd --.L.‘":—.1000— -, p 3-- -./ •1 r I �' \ >._d-'�,'�eceCY ' T _ -, „ C.x r� e j e� - 1 ' -, ♦ t _�c 'ice_ p \`_ --1- ...."C°I i tt Y 1_ Si _ E _ ,� R 4. _A I P — a-R . - I 6- � ) - y, o I i I' I ' f t. + I I /rl rt.,. 1 . j . �C . t J _r � ' � 'p I ., �( �_ i , �I� '-�- ' ` I r � 01 E _ �_ , ,-n� _ ' , 1 ,1 ¢ x a w.mi.. 1 HI 1C n ro.�.c..cTtRs D(PLANATION ' OUTCROP Of PRECAMBRIAN ROCIL — 'APPRO%A1ATE QUFIMIT OF THE I..RAM� FOX MA1 AOUFFA MlA u1001LAM.r ME LAAANS DATA POINTS •FO%10.15 A^li 1FER Had.on*n 1%1 ----FAULT-O.MC dr.mired —42W--POTENOOMElltr CONTOUR-9v°+ • Had„mead Smarts'.n..ua...°a .1t4.aI aa.d.. Led n.i. .^m weak Pan""1 I =wised a the La.n..-F..1s vatic 0...d dr.m.nN bud Groot..uar1100 Ion. Daum is r N ` Figure 9 - Potentiometric Map of the R1-f Aquifer in the Denver Basin (Robson and Banta, 1987) . I 34 I GROUNDWATER QUALITY OF THE AREA The compiled groundwater quality data were compared with Federal and State Applicable or Relevant and Appropriate Requirements (ARAR's) . The ARAR's were obtained from the Colorado Department of Health (1985) water quality numeric recommendations and standards. Table IX summarizes the ARAR's and water quality parameters which exceed applicable standards. Sulfate, iron, fluoride, pH, ROE and, manganese - parameters were found to exceed applicable standards. Figure 19 shows the distribution of samples exceeding ARAR concentrations. With the exception of pH and ROE, the highest percentage of samples that exceed ARAR' s are from Data Groups "B" and "C" . Over 60% of Data Group "C" samples and, 45 Data Group "B" samples exceed the ARAR' s for sulfate concentrations. Additionally, the ARAR concentration for dissolved iron is exceeded by 36% of the samples from Data Group "B" . Thirteen percent of the Group "C" samples exceed the ARAR for fluoride. Over 82% ,of the i.' samples from Data Group "A" exceed the applicable water quality standard for pH. All of the samples (groups "A" , "B" and "C") exceed the ARAR value (500mg/1) for ROE (TDS) . 67 II t - a ■ Table IX - ARAR' s and Summary of Exceedances I ill PARAMETER APPLICABLE STANDARDS PERCENTAGE OF SAMPLING STATIONS Rg/L EXCEEDING STANDARDS GROUP A GROUP B GROUP C II Na NS 504 250 - CDH GW DWSTD 0% 45% 63% Ca NS III Mg NS Fe 0.3 - CDH GW DWSTD 8% 36X 13% Ft 2.0 - CDH GW DWSTD 0% 0% 13% NI Cl 250 - CDH GW DWSTD 0% OX 0% pH 6.5-8.5 - CDH GW DWSTD 82% 36% 25% CO3 NS IIROE (TDS) 500 - CDH GW DWSTD 100% 100X 100% EC NS NO3-N 10.0 - COH GW DWSTD 0% OX OX K NS I Ba 1.0 - CDH GW DWSTD 0% 0% 0% Co NS Pb 0.05 - CDH OW DWSTD OX OX 0X Mn 0.05 - CDH GW DWSTD 0% 18% 38% Mo 0.1 - CDH AG 0% DX OX Sr NS . V 0.1 - CDH AG OX OX OX Be 0.1 - CDN AG 0% OX OX Cu 1.0 - CDH GW DVSTD 0% 0% 0% Li 2.5 - CDH AG 0% 0% 0X II Si NS Zn 2.0 - CON AG 0% 0% C_ Cd 0-01 - CDH GW DWSTD 0% 0% 0% II Ag 0-05 - CDH Gil DWSTD OX 0% 0% Cr 0.05 - CDH 6W DWSTD 0% 0% OX Ni 0.2 - CDH AG 0% OX OX il CON - Colorado Department of Health ■ SW - Surface Water GW - Groundwater DVSTD - Drinking Water Standard ▪ -- NS - No Standard NA - Not Available IN 68 I DISTRIBUTION OF SAMPLES EXCEEDING WATER QUALITY STANDARDS 10D- I = L. .o-. ,o- I so- i LU CC LU rI $O4 Fe F PH HOE Mn PARAMETERS { gm GROUP A NM GROUP B IZE;S GROUP C WATER QUALITY STANDARDS: I sa 150 Fe 03 F 20 pH 63-Si ROE 5O3 Mn 0.05 •UNITS IN ms/L accpt for pH I Figure 19 - Graph represents the distribution of parameters exceeding ARAR concentrations. I 69 Eighteen percent of Data Group "B" samples and 38% of Data Group "C" samples exceed the ARAR concentration (0. 05 mg/1) for manganese. Despite having iron, pH, and ROE parameters exceeding ARAR concentrations (Table IX) , the Data Group "A" samples, representing the groundwater from the Kl-f Aquifer, is of better quality for human consumption and domestic purposes than the groundwater of Data Groups "B" and "C" . However, the NA-CO3+HC03 groundwater in the Kl-f Aquifer may not be suitable as drinking water for persons on low sodium diets. The mean ROE value of 592 mg/L exceeds the ARAR - -- concentration of 500 mg/L due to the high mean concentrations of sodium (242 mg/L) and carbonate + bicarbonate (461 mg/L) ions. The groundwater collected from wells in Data Group "B" was of a lesser quality than the groundwater from Data Group "'S . The mean sulfate, ROE and dissolved iron concentrations within Data Group "B" exceed ARAR' s. The high sulfate concentrations in the drinking water obtained from wells in Group "B" may act as a laxative if consumed and the high iron concentrations may cause staining of plumbing and bathroom fixtures (Driscoll, 1986) . ' In addition, the high soodium-sulfate concentration may not have an aestically pleasent taste or smell. The groundwater quality from wells in Data Group "B" is not suitable for 70 human consumption and most domestic purposes. The water quality of the groundwater sampled from wells comprising Data Group "C" is unfit for human consumption. The mean sulfate concentration of 647 mg/L and the mean ROE value of 1390 mg/L exceeds the ARAR concentrations summarized in Table IX, with the mean ROE value exceeding 1, 000 mg/L the groundwater is classified as brackish (Freeze and Cherry, 1979) . Water which has a dissolved solids concentration greater than 1000 mg/L is a high salinity hazard and is unsuitable for most types of irrigation due to the potential salt buildup in the soil (Robson, 1989) . 71 JUN-16-1998 10:28 REPORT OATS 04/29/98 COLORADO WELLS. APPLICATIONS. AND PERMITS FACE t COLORADO DIVISION OP WATER RESOURCE'S D CO OWNER INFORMATION - ACTIVITY STATUS 1ST USED ANNUAL ACRES GEOL WKL.L WELL WATER SEC LOCAT'N TOWN p CD DATE CD DATE WD MD DO USE DATE APROP LER AQFR YIELD DEPTH LEVEL COORDINATES (FIRS SC SHIP RANGE H 1 62 SIEGRIST CONST 6909 YORK ST DENVER. CO 80229 GRAVEL. PIT AP 02/20/90 AU 03/20/90 S 0 G GW 11 3 N 67 H S 1 62 DAKOLIOS ERNEST R. COIbEN, CO 80401 AP 0ti/03/85 AU 05/07/85 2 8 CW SW 31 3 N 67 W S 2169F 1 62 VARRA COMPANIES 2130 S 90TH ST BROOMFIELD, CO 80020 EP 07/02/07 EP 02/06/96 5 5 GW .dc r I 0100N.0200E NFNF. 31 3 N 6] W 5 4I.-- 1 67 VARRA COMPANIES 2130 S 981'FI BROOMFIEJ3, CO 80020 CRAVEL PIT ill _ AP 07/16/90 AU 09/21/90 5 0 G GW �•(1 SWNE 31 3 N 67 N 5 0426AD 1 62 DAKOLIOS CNSTR CO DENVER, CO 80221 / AD A 4 NENW 'n 3 N 67 W S 1 62 VAAkA COMPANIES 2130 S 96TH BROOMFIELD, CO 80020 GRAVEL PIT AP 07/16/90 AU 09/20/90 $ 0 G GW SWNW 31 3 N 67 W S 9938 1 62 ST VRAIN SAN DIST 600 KIMBARK ST STE B LONGMONT, CO 80502 (a„,wtkic..../ NP 09/14/87 SA 12/12/80 5 3 12/15/87 0.33 KLF 2.50 150 12 22155,2405E NWSE 31 3 N 6'1 w S —72796M 1 62 ST. VRAIN SAN. 600 KIMBARK ST STE B LONGMONT. CO 80502 oY\--Xl NP 12/01/87 SA 5 0 07/00/88 CH 18 19335,2410E NWSE 31 '3 N 67 N S 3279GM 1 62 ST. VRAIN SAN. 600 KIMBARK ST STE ❑ LONGMONT. CO 60502 "? NI' 12/01/87 SA S D 07/08/08 OW 10 1Y135,2410E NWSE 31 ) N 67 W 5 2795M 1 62 ST VRAIN SANITATION DIST G00 KIMBARK ST STE B LONGMONI, CO 80502 S 0 12/15(87 10 1.9335,2925E NWSE 31 ) N 67 H S 1 62 VARRA COMPANIES 2130 S 96IH Bk0OMF16LD. CO 80020 - AP 12/21/96 9 G 7r&4.d{9('f GW NESW 31 3 N 6'r w S 6 1 62 GOULD L LONGMONT, CO 80501 NP 04/06/82 AR 04/21/8'3 5 8 SW514 31 1 N F7 w 5 154183 1 62 GOULD LEE 12148 WELD CNTY RD 1; LONGMONT CO 805111 NP 04/26/89 AR 05/18/89 5 89 GW 75.00 32 10 0390S,0100W SWSW 33 3 N 67 W S __4183 A 1 62 GOULD LEE 12148 WELD CNTY RD 13 LONGMONT. CO 90501 NP 04/26/89 AR 05/18/89 5 89 GW 03905,0100W SWSW 31 3 N Al W 5 3569 1 62 GOULD LEE RT 4 LONGMONT. CO 90501 S 9 05/03/68 28.00 25 6 5045W 71 3 N 67 N S TnTnl 0 170 r.u4 JUN-16-1998 10:27 REPORT DATE 04/29/99 COLORADO WELLS, APPLICATIONS, AND PERMIT'S PACE 1 COLORADO DIVISION OF WATER RESOURCES :SNIT D CO OWNER INFORMATION ACTIVITY STATUS 1ST USED ANNUAL ACRES CEOL WELL WELL WATER sCC LOCAT'N TOWN P CD DATE CD DATE ND MO DO USE DATE APROP IRR ACFR YIELD DEPTH LEVEL COORDINATES QTES SC SHIP RANGE M 9705E 1 62 RALPH NLX PRODUCE, INC 19480 US Hwy 05 O(LCREST. CO 50123 RC 12/02/92 5 t 02/28/16 1000.0n 1(. ,. SCNE 20 3 N 7 w S '0371 1 62 RALPH NIX PRODUCE 16959 WCR 44 G.ILCRESI, CO 90623 NP 10/.10/96 RC 04/24/97 2 8 L Ow 15.00 70 2', 2S4DN,0975V 5!:99- 20 3 N 67 w 5 _ 2189P K 1 62 KURTZ CATTLE CV 1 ACKICOLA REALTY 6 MGMT FT MORGAN. CO 80701 NP 11/10/91 2 1 Cw 4n 2572N,2865E SENW 29 1 N 67 N s 4124? 1 62 KURTZ HELENE D 6 MAX 5636 G 1"PIU AVE DENVER 20, CO 50220 5 1 05/20/63 1000.00 40 _ NWSW 28 3 N 67 H 5 -5973 1 62 RALPH NIX PRODUCE, INC 19490 US HWY 05 OILCRESI', CO 00623 Nc 12/02/92 5 6 05/10/09 15.00 21 1 SWMW 20 1 N 667 N s 136175 1 62 LESN B AULT. CO 80521 NP 04/27/81 5 0 01/30/85 NE 29 3 N 67 N S 0512 1 62 KURTZ ALBERT K F D ('LATTEVILLE. CO 80651 5 9 10.00 19 4 NENE 29 3 N 67 w 5 1 62 LESN 8 ADLT, CO 80610 TH 04/16/94 5 NENW 29 3 N 67 H 5 9640MH 1 62 CO DAIRY EARNS C/O LESN DRILLING AUI:1', CO 90610 MH 02/0./92 S 0 Qw 00329,2497w NENW 19 3N 67 2N5 -a2029VE 1 62 AURORA DAIRY CORP 7388 HWY 66 LONGMONT. CO 00000 AV 02/07/92 5 39 GN 092O4,2n97W NENW 29 3 N 6,7 w 5 1!4179 1 62 PSF ASSOCIATES LONOMON'1', CO 90501 __ NP 10/12/82 RC 01/20/94 5 A NENW 29 3 N 67 W S R 1 62 COLORADO DAIRY FARMS 7309 HWY 66 LONGNONT', CO 80501 NP 02/06/92 SA 07/15/92 5 9 n3/79/92 350.0 GW 290.00 25 2 0927N,2402W NENW 29 7N 9) N2 25867E 1 62 PSI' ASSOCIATES 7308 STATE HWY 66 LONGMONT, CO 80501 AB 02/14/92 5 9 09/09/82 205.00 19 2 0747N,2297W NENW 29 3 N 67 w S T.00SUN-16-1`3'3d 1b:Cl REPORT DATE 04/29/98 COLORADO WELLS, AP'PLICATIONS, AND PERMITS 0AOK 1 COLORADO DIVISION OF WATER RESOURCES P"^^' D CO OWNER INFORMATION ACTIVITY STATUS 1ST USED ANNUAL ACRES GEOL WELL WELL WATER SEC LOCAT'N TOWN P CD DATE CD DATE. WD MU DB USE DATE APROP IRR AQPR YIELD DEPTH LEVEL COORDINATES OTRS SC SHIP RANGE M 19874MH 1 62 AT&T COMMUNICATIONS 1 CERTIFIED ENV CONSULT SALT LAKE CITY, WI 04115 MH 10/14/92 S O M OW 0 S 10 6 N2 30 I N G7 W S 5462 1 62 HESS LANCE - CEC 2757 S 300 WEST KR SALT LAKE, UT 84115 NP 11/01/92 5 0 M [WC 0134N,2493E NWNE 30 3 N 57 W S -5463 1 62 HESS LANCE - CEC 2757 S 300 WEST KB SALT LAKE, UT 84115 NP 11/01/93 5 0 M UNC 0177N,2'4'E NINE 30 3 N G7 W S 175464 1 62 HESS LANCE - CEC 2757 5 300 WEST KR SALT LAKE. VT 84115 NP 11/01/91 5 0 M I7NC 0094N,2498E NWNA 30 3 N 67 W S 5465 1 62 HESS LANCE - CEC 2757 S 300 WEST KB SALT LAKE, UT 84115 NP 11/01/93 5 0 M INC 0177N,2491E NWNE 30 3 N G7 W S Colorad ireamflow Page 11 r Streamflow Colorado Streamflow Information Here's the streamflow information you requested: ST. VRAIN CREEK NEAR PLATTEVILLE, AT THE MOUTH 400 = 350 m 300 250 a 200 2 150 E 100 a 50 0 , 20-Jun 21-Jun 22-Jun 23-Jun 24-Jun 25-Jun 26-Jun 27-Jun 28-Jun 29-Jun 30-Jun Chart prepared on 6/30/98 10:07:28 AM - Days go from Midnight to Midnight Estimated Channel Capacity 1650 CFS WaterTalk (303) 831-7135 Division 1, Station 59 [Another Stream] Natural Resources I Parks F Wildlife l Wafer Ceologv Oil & Gas I Mining I Land Overview http://www.dnr.state.co us/scripts/gage/gage.idc 6/30/98 I I I I 1 Colorad ltrrent Streamflow Conditions - Wate... i Page 1 113 �� .. science for achanging worlds ,,..e Colorado Current Streamflow Conditions - Water Quality Updated TUESDAY JUN 30, 1998 13:08:11 Streamflow conditions are monitored by the U.S. Geological Survey with support from Federal, State, and local cooperators. PROVISIONAL DATA SUBJECT TO REV ISION--Select a station number from the table to view graph(s) and other data for a station. Water Specific Dissolved pH Station Station Temp Rainfall Flow Stage Conductance Oxygen Standard Number Name °C Inches fP/s ft µS/cm mg/L Units Date/Time *SOUTH PLATTE RIVER BASIN 06697100 Tarryal Creek below Park Gulch near 06/30 20 3.85 Como, Co 08:00 06701970 Spring Cr above mouth nr South Platte 06/30 0 41 3.76 Co. 12:50 06706800 Buffalo Creek at mouth at Buffalo 06/30 0 31 3.75 Creek 11:00 06709000 Plum Creek near Sedalia, Co. -- 0 29 1.85 -- -- __ 06/30 10:45 06709530 Plum Creek at Titan Rd nr Louviers, -- -- 3.4 6.27 06/30 Co , 11:30 South Platte River below Union Ave, 06/30 06710247 at Englewood -- -- 87 10.91 -- -- 09:30 0671 1565 South Platte River at Englewood, Co. 0 -- 112 1.73 389 1.6 7 8 06/30 10:30 06/30 06712000 Cherry Creek near Franktown, Co. -- 0 2.6 2.16 -- -- __ 09:45 06714? 15 South Platte R at 64th Ave. Commerce 06/30 146 2.65 City, Co. 09.00 http://nwis-colo.cr.usgs.gov/rt-cgi/gen_tbl_pg_ex 6/30/98 i Coloradr lrrent Streamflow Conditions - Wate.. } Page 2 t3 Leavenworth Creek @ mouth nr 06/30 06714800 Georgetown, Co 0 48 4.33 0 12:30 06/30 06716500 Clear Creek near Lawson, Co. -- 0 488 4.52 -- -- __ 12:30 06/30 06719505 Clear Creek at Golden, Co. -- -- 676 6.51 -- -- __ 10:00 06720255 Uvalda Intercept bl 56th Av at Rocky 06/30 0 .35 -665.7 Mtn Ars, Co 12:15 06720285 Havana Intercept bl 56th Av, at Rocky 06/30 0 1.3 10.63 Mtn Ars, Co 07:45 06720460 First Cr bel Buckley Rd, at Rocky Mtn 06/30 0 0 .81 Arsenal, C 07:45 06720490 First Cr at Hwy 2, near Rocky Mtn 0 72 06/30 Arsenal, Co 07:00 06/30 06730200 Boulder Cr at North 75th St nr Boulder -- -- 300 5.86 -- -- __ 12:00 06/30 06741510 Big Thompson River at Loveland, Co. -- -- 159 2.62 -- -- __ 11:00 0675 1150 North Fork Cache La Poudre River 06/30 100 2.98 below Halligan Reservoir near V Dal 10:45 06752260 Cache La Poudre River at Fort Collins, 06/30 14.9 -- 409 3.51 48 -- 8.3 Co. 12:15 06752280 Cache La Poudre R ab Boxelder C, nr 06/30 273 5.16 Timnath, Co. 10:45 06/30 06754000 South Platte River near Kersey, Co. -- -- 509 3.65 -- -- __ 10:30 06/30 393109104464500 Cherry Creek near Parker, Co -- -- 1.9 2.66 -- -- __ 01:45 393647105425317 South Clear Creek abv Naylor Creek 06/30 7.6 3.3 7.41 68 nr Georgetown 02:00 394839104570300 Sand Creek at mouth nr Commerce 310 5.74 06/30 City,co -- -- 04.30 gill UPPER ARKANSAS RIVER BASIN http://nwis-colo.cr.usgs.gov/rt-cgi/gen_tblpg_ex 6/30/98 CGRS,Inc. APPENDIX B Methods and Procedures CGRS,Inc. METHODS AND PROCEDURES Soil Borings Soil sampling will be conducted in accordance with ASTM:D 1586-87. Using this procedure, a 2- inch O.D. split-spoon sampler will be driven into the soil by a 140 pound weight falling 30 inches. After an initial set of 6 inches, the number of blows required to drive the sample an additional 12 inches, known as the penetration resistance (N value), will be recorded. The N value is an index of the relative density of cohesionless soils and the consistency of cohesive soils. Soil Classification/Characterization As samples are obtained in the field, they will be visually inspected and classified in accordance with ASTM:D 1488-84. Representative portions of the samples will then be retained for further examination and for verification of the various strata, the N value, water level data, and pertinent information regarding the method of maintaining and advancing the boring will be provided. Charts illustrating the soil classification procedure, descriptive terminology and symbols used on the logs will be provided. Decontamination To avoid potential transport of contaminated materials to the project site, all drilling equipment and down-hole tools will be steam cleaned prior to mobilization. To prevent cross contamination between soil borings or monitoring wells all down-hole equipment will also be steam cleaned and rinsed with water between soil borings. Monitoring Well Construction Monitoring wells will be installed utilizing the following general construction criteria: • borehole diameter: minimum 6.25 inches • well diameter: 2 inches • estimated depth: 15 feet below ground surface • casing material: schedule 40, flush thread PVC CGRS, Inc. • well screen: 2 inch I.D., 10 feet in length, # 0.01 slot PVC • estimated screened interval: 5 feet above and 5 feet below the groundwater table • annular pack: 10-20 silica sand • protective casing: minimum 12 inch I.D., steel flush or above grade, locking cap • annular seal: cement grout and bentonite pellets. Groundwater Sampling All borings where groundwater is encountered will be sampled from the suspected cleanest to the most contaminated according to the protocols listed below. All pertinent information will be recorded on a sampling information form. Field Protocol — Step 1 -Measure water level. Step 2 -A dedicated polyethylene bailer will be used to develop each boring. Three bore volumes will be evacuated from each boring prior to sampling. Step 3 -Collect water samples. Water samples will be collected using a polyethylene bailer. A field blank will be collected during the sampling program to ensure quality control. Step 4 -Store samples in a cooler on ice for transport to the laboratory. Follow all documentation and chain-of-custody procedures. Step 5 -Clean equipment. Water level measurement equipment will be cleaned with ethanol followed by a deionized water rinse. Upon completion of soil or groundwater sampling, a chain of custody log will be initiated. A copy of the chain of custody will be returned to the project manager. CGRS,Inc. METHODS AND PROCEDURES Soil Borings Soil sampling will be conducted in accordance with ASTM:D 1586-87. Using this procedure, a 2- inch O.D. split-spoon sampler will be driven into the soil by a 140 pound weight falling 30 inches. After an initial set of 6 inches, the number of blows required to drive the sample an additional 12 inches, known as the penetration resistance (N value), will be recorded. The N value is an index of the relative density of cohesionless soils and the consistency of cohesive soils. Soil Classification/Characterization As samples are obtained in the field, they will be visually inspected and classified in accordance with ASTM:D 1488-84. Representative portions of the samples will then be retained for further examination and for verification of the various strata, the N value, water level data, and pertinent information regarding the method of maintaining and advancing the boring will be provided. Charts illustrating the soil classification procedure, descriptive terminology and symbols used on the logs will be provided. Decontamination To avoid potential transport of contaminated materials to the project site, all drilling equipment and down-hole tools will be steam cleaned prior to mobilization. To prevent cross contamination between soil borings or monitoring wells all down-hole equipment will also be steam cleaned and rinsed with water between soil borings. Monitoring Well Construction Monitoring wells will be installed utilizing the following general construction criteria: • borehole diameter: minimum 6.25 inches • well diameter: 2 inches • estimated depth: 15 feet below ground surface • casing material: schedule 40, flush thread PVC i CGRS, Inc. • well screen: 2 inch I.D., 10 feet in length, # 0.01 slot PVC • estimated screened interval: 5 feet above and 5 feet below the groundwater table • annular pack: 10-20 silica sand • protective casing: minimum 12 inch I.D., steel flush or above grade, locking cap • annular seal: cement grout and bentonite pellets. Groundwater Sampling All borings where groundwater is encountered will be sampled from the suspected cleanest to the most contaminated according to the protocols listed below. All pertinent information will be recorded on a sampling information form. Field Protocol — Step 1 -Measure water level. Step 2 -A dedicated polyethylene bailer will be used to develop each boring. Three bore volumes will be evacuated from each boring prior to sampling. Step 3 -Collect water samples. Water samples will be collected using a polyethylene bailer. A field blank will be collected during the sampling program to ensure quality control. Step 4 -Store samples in a cooler on ice for transport to the laboratory. Follow all documentation and chain-of-custody procedures. Step 5 -Clean equipment. Water level measurement equipment will be cleaned with ethanol followed by a deionized water rinse. Upon completion of soil or groundwater sampling, a chain of custody log will be initiated. A copy of the chain of custody will be returned to the project manager. ii CGRS, Inc. Chemical Analysis All analytical parameters are described in the Laboratory Quality Assurance Project Plan (QAPP) presented as Appendix C. Groundwater Elevation Measurements The following outlines our standard groundwater quality sampling methodology. Before purging any of the soil test borings or monitoring wells,water level measurements must be taken. Measuring Point Establish the measuring point for the well. The measuring point is marked on the north side of the top of the temporary monitoring well riser. The top of the riser is normally a 2 inch casing inside a locked protective casing. The riser will be PVC pipe, galvanized pipe or stainless steel pipe. The measuring point should be described on the groundwater sample collection record. Access _ After unlocking or opening a monitoring well, the first task will be to obtain a water level measurement. Water level measurements will be made using an electronic water level indicator. Depth to water and total depth of the well will be measured for calculation of purge volume. Measurement To obtain a water level measurement, lower a decontaminated electronic water level probe into the monitoring well. Care must be taken to assure that the electronic probe hangs freely in the monitoring well and is not adhering to the well casing. The electronic probe will be lowered into the well until the audible sound of the unit is detected and the light on the electronic sounder illuminates. At this time,the precise measurement should be determined by repeatedly raising and lowering the probe to obtain an exact measurement. The water level measurement is then entered on the groundwater sampling collection record sheet or groundwater level data sheet to the nearest 0.01 feet. Decontamination The electronic probe shall be decontaminated immediately after use by wiping with isopropyl alcohol-soaked paper towels. Always proceed in order from the suspected cleanest well or soil test boring to the suspected most contaminated one. iii CGRS, Inc. Purge Volume Computation All soil test borings and temporary monitoring wells will be purged prior to sample collection. Depending upon the rate of recovery,three to five volumes of groundwater present in a well or bore hole shall be withdrawn prior to sample collection. If a well or bore hole bails dry,the well or bore hole should be allowed to recharge and a sample taken as soon as there is sufficient volume for the intended analysis. The volume of water present in each well or bore hole shall be computed using the two measurable variables, length of water column in soil boring or monitoring well and diameter. Purging and Sample Collection Procedures Bailing • Obtain a laboratory decontaminated disposable bailer and a spool of nylon rope or equivalent bailer cord. Tie a bowline knot or equivalent through the bailer loop. Test the knot for _ _ adequacy by creating tension between the line and the bailer. Tie again if needed. New rope will be used for every sample or purge. New clean latex gloves will be used when touching the rope or bailer. • Spread a clean plastic sheet near the base of the well. The plastic sheet should be of sufficient size to prevent bailer or bailer rope from contacting the ground surface. • Place the bailer inside the well to verify that an adequate annulus is present between the bailer and the well casing to allow free movement of the bailer. • Lower the bailer carefully into the well casing to remove the sample from the top of the water column,taking care not to agitate the water in the well. • Pour the bailed groundwater into a bucket. Once the bucket is full,transfer the water to a barrel and contain on-site. iv CGRS, Inc. • Raise the bailer by grasping a section of cord, using each hand alternately. This bailer lift method will assure that the bailer cord will not come into contact with the ground or other potentially contaminated surfaces. Sampling • Instructions for obtaining samples for parameters are reviewed with the laboratory coordinator to insure that proper preservation and filtering requirements are met. • Appropriate sample containers will be obtained from the contract laboratory. After samples are collected, they will be put on ice in coolers (4°C). Care will be taken to prevent breakage during transportation or shipment. • Samples collected by bailing will be poured directly into sample containers from bailers. The sample should be poured slowly to minimize air entrapment into the sample bottle. During collection, bailers will not be allowed to contact the sample containers. • Upon completion of sampling a chain-of-custody log will be initiated. Chain-of-custody records will include the following information: project name and number, shipped by, shipped sampling point, location, field ID number, date, time, sample type, number of containers, analysis required and sampler's signature. The samples and chain-of-custody will be delivered to the laboratory. Upon arrival at the laboratory the samples will be checked in by the appropriate laboratory personnel. Laboratory identification numbers will be noted on the chain- - of-custody record. Upon completion of the laboratory analysis, the completed chain-of-custody record will be returned to the project manager. Field Cleaning Procedures For all equipment to be reused in the field,the following cleaning procedures must be followed: • Disassemble the equipment to the extent practical. • Wash the equipment with distilled water and laboratory-grade detergent. • Rinse with distilled water until all detergent is removed. • Rinse the equipment with isopropyl or methanol, making sure all surfaces, inside and out,are rinsed. • Triple rinse the equipment with distilled water. v CGRS,Inc. Laboratory Selection The project manager should consider the following factors when selecting a laboratory: • Capabilities(facilities, personnel, instrumentation), including: • Participation in interlaboratory studies(e.g., EPA or other Federal or State agency sponsored analytical programs); • Certifications(e.g., Federal or State); • References(e.g. other clients); and • Experience(UST,RCRA and other environmentally related projects). • Service; • Turnaround time; and • Technical input(e.g., recommendations on analytical procedures). The project manager is encouraged to gather pertinent laboratory-selection information prior to extensively defining analytical requirements under the project. A request may be made to a laboratory to provide a qualifications package that should address the points listed above. Once the project manager has reviewed the various laboratory qualifications, further specific discussions with the laboratory or laboratories should take place. In addition, more than one laboratory should be considered. For large-scale investigations, selection of one laboratory as a primary candidate and one or two laboratories as fall-back candidates should be considered. The quality of the laboratory service provided is dependent on various factors. The project manager should be able to control the quality of the information(e.g., samples) provided to the laboratory. It is extremely important that the project manager communicate to the laboratory all the requirements relevant to the project. This includes the number of samples and their matrices, sampling schedule, parameters and constituents of interest, required analytical methodologies, detection limits, holding times, deliverables, level of QA/QC, and required turnaround of analytical results. Field and Laboratory Quality Control General Quality control checks are performed to ensure that the data collected is representative and valid data. Quality control checks are the mechanisms whereby the components of QA objectives ore monitored. Examples of items to be considered are as follows: vi CGRS, Inc. I. Field Activities: • Use of standardized checklists and field notebooks; • Verification of checklist information by an independent person; • Strict adherence to chain-of-custody procedures; • Calibration of field devices; • Collection of replicate samples; and • Submission of field blanks,where appropriate. 2. Analytical Activities: • Method blanks; • Laboratory control samples: • Calibration check samples; • replicate samples; • Matrix-spiked samples; • "Blind" quality control samplers; _ — • Control charts; • Surrogate samples; • Zero and span gases; and • Reagent quality control checks. Blind Duplicates Blind duplicate samples will be collected for 10% of the samples collected or once per site, whichever is greater. These blind duplicate samples will be forwarded to the laboratory as a check of laboratory reproducibility. Equipment(Rinseate)Blank The equipment (rinseate) blank is designed to identify potential cross-contamination in the field between sample sources due to deficient field cleaning procedures. This blank also addresses field preservation procedures, environmental site interference, integrity of the source blank water for field cleaning and those concerns singularly addressed by the travel blank. Equipment blanks are taken once per site, when equipment is cleaned in the field. This provides a quality control check on field cleaning procedures. vii CGRS, Inc. Field Blank Field blanks are used to evaluate the sample container filling procedure, the effects of environmental contaminants at the site, purity of preservatives or additives and those concerns uniquely addressed by the travel blank. Field blanks are taken downwind of the most contaminated area of the site by filling laboratory cleaned and prepared sample containers (appropriate for the parameters group) with deionized or - organic-free water supplied by the laboratory. The blank sample container is then sealed, grouped, transported and stored with the real samples collected for the same parameters group. Travel(Trip)Blanks The travel blank is designed to address interferences derived from improper sample container cleaning preparation, contaminated source blank water, sample cross-contamination during storage/transport and extraneous environmental conditions affecting the sampling event to and from the site, including delivery to the laboratory. Travel blanks are composed in the appropriate sample container using source blank water. Preservatives or additives are added if required for the parameters group. Travel blanks are then sealed and stored in the ice chest where real samples will be stored and transported. Travel blanks are to originate at the laboratory providing the blank water for the equipment and field blanks. Protocol for Analyzing Blank Samples If used, the equipment blank will be analyzed first. If contamination is found to be present, the field blank will then be analyzed. If the equipment blank is not used, the first blank analyzed will be the field blank. If any blank is found to be contaminant-free, the sequence of analyses will be terminated. VI.ii CGRS, Inc. APPENDIX C Quality Assurance Project Plan QUALITY ASSURANCE PROJECT PLAN FOR THE VARRA COAL ASH BURIAL PROJECT WELD COUNTY, COLORADO 1.0 Introduction This Quality Assurance Project Plan (QAPP) briefly describes the field data collection activities and laboratory analyses being conducted as part of the Varra Coal Ash Burial Project in Weld County, Colorado. The work described in this QAPP is being conducted to address possible concerns related to coal ash burial in saturated mediums. Described in the sections below are the project objectives, scope of work, sample handling and Chain-of-Custody procedures, data quality assurance, and laboratory deliverables. 2.0 Objectives The data being collected are intended to support the following objectives: • Identify potential adverse environmental impacts to groundwater resources and - surface waters from coal ash burial; • Determine variations in water quality from coal ash burial (if any); • Characterize hydrogeologic and surface water conditions in sufficient detail to describe hydrostratigraphy, direction and velocity of groundwater flow, and the relationship between groundwater and surface water; • Develop and implement monitoring programs for the various media; and, • Employ industry standard field and laboratory methods suitable to meet CLP or equivalent(such as EPA QC Level III) Data Quality Objectives. 3.0 Scope of Work The scope of work for this project involves, development of Health and Safety and site-specific Work Plans, field investigations, laboratory analysis of water samples, analysis of hydraulic and hydrogeologic properties, and the preparation of a report detailing the results of the investigation. Field investigative techniques include soil and groundwater sampling using direct push and hollow stem auger techniques. 3.1 Sample Identification A sample identification scheme will be used that maintains consistency for the names of boreholes and monitoring wells, as well labels affixed to each sample container, and entered on to the Chain-of-Custody(COC)forms. The following scheme will be followed: 1. Samples from soil borings that are not converted to monitoring wells are named SB; 2. Samples from soils collected during drilling of monitoring wells are named MW; and 3. Depth of soil sampled indicated by @ (depth interval). For example a soil sample might be identified as MW-4 @ 10-11.5. Groundwater, surface water, and sediment samples will be named with no depth interval (i.e. MW-4, SW-4, SED-4, respectively). 3.2 Analytical Suites Analytical procedures for water and soil samples will conform to the USEPA guidelines described in SW 846 (Test Methods for Evaluating Solid Waste/Physical/Chemical Methods, 3rd ed.). Table 1 presents the analyses that are anticipated on the project. 3.3 Sample Custody Strict chain of custody(COC) protocol will be maintained throughout the life of the field program and will be controlled through the use of a COC Record supplied by the laboratory. The following procedures will be used to document, establish, and maintain custody of field samples: • Sample labels will be completed for each sample using waterproof ink; making sure that the labels are legible and affixed firmly on the sample container; • All sample-related information will be recorded in the project log book; • The field sampling technician will retain custody of the samples until they are transferred or properly dispatched to a laboratory; and, • As fieldwork is conducted the on-site CGRS technical lead will determine whether these procedures are being followed, if corrections need to be made, and if additional samples are required. 3.3.1 Chain of Custody Records A Chain-of-Custody Record will be maintained in the field for all samples to be shipped to the laboratory for analysis. The three lines of information to be entered into the COC box titled "Project or P.O.#"are: Line 1. Client Name, i.e. "Varra Companies" Line 2. Site Name, i.e. "Pit 112" Line 3. Site Number, i.e. "2755" The three lines of information will be provided on the laboratory paper (hard copy) reports as a page header, and on the electronic deliverables as three individual fields in each analytical record. The "Sample Identification" entries to the COC will be completed as described in Section 3.1 of this QAPP. Varra Companies Quality Assurance Project Plan Page I 33.2 Transfer of Custody and Shipment Due to the evidentiary nature of field sample collection, the possession of samples must be traceable from the time the samples are collected until they are introduced as evidence in legal proceedings. A sample is defined as being under a person's custody if any of the following conditions exist: (1) it is in their possession, (2) it is in their view after being in their possession, (3) it is in a secure locked location after having been in their possession, and (4) it is in a designated secure area. The following procedures will be used in transferring and shipping samples: • Field personnel will maintain detailed notes in field logbooks, documenting the collection and identification of the required samples. The logbooks will be checked against the COC records for completeness and traceability. • A COC record will accompany all sample shipments. When transferring samples,the individuals relinquishing and receiving will sign, date, and note time on the record. The COC documents transfer of sample custody from the field sampling technician to another person or to the laboratory. • Each cooler is to contain samples from one site. No mixing of samples from multiple sites will be allowed in a given cooler. • Samples will be properly packaged for shipment and shipped to the laboratory for analysis with a separate signed COC record enclosed in each sample box or cooler. Two copies of this record will accompany the samples to the laboratory. The — - laboratory maintains one file copy, and the completed original will be returned to the project manager as part of the final analytical report. This record will be used to document sample custody transfer from the field sampling technician to the laboratory or to the CGRS offices. Just prior to shipment to the laboratory, coolers will be secured with custody seals. • Whenever samples are split with a facility operator or government agency, a separate COC record will be prepared for those samples and so marked to indicate with whom the samples are being split. • The COC record showing identification of the contents will accompany all packages. The original record will accompany the shipment and the field team leader will retain a copy. • A bill of lading will be used for all samples sent by common carrier. Receipt of bills of lading will be retained as part of the COC permanent documentation. 3.3.3 Laboratory Custody Procedures The laboratory, at a minimum, will check all incoming samples for integrity and note any observations of the original COC record. Each sample will be logged into the laboratory system by assigning it a unique laboratory identification number. This number and the field sample identification number will be recorded on the laboratory report. Samples will be stored and analyzed according to the methods described in Section 3.1. The original COC record will be returned to the CGRS project manager for filing. The laboratory sample custodian will use the following procedures to maintain the COC records once the samples arrive at the laboratory: Varra Companies Quality Assurance Project Plan Page 2 • The samples received by the laboratory will be cross-checked to verify that the information on the sample labels matches that on the COC record included with the sample shipment; • The "Received by Laboratory" box on the COC record will be signed on receipt. Any discrepancies between the COC record and the shipment contents will be resolved as soon as possible through communication with CGRS personnel; • The status of the sample receipt and analysis will be tracked within the analytical laboratory by a laboratory information management system (LIMS) or equivalent computerized management system. For data that are input by an analyst and processed using a computer, a copy of the input data will be kept and identified with the project number and any other needed information. The samples analyzed will be clearly noted and the input data signed and dated by the analyst. 3.4 Laboratory Deliverables The laboratory is required to submit EPA QC Level III data packages (CLP-equivalent)to CGRS, Inc. within 21 days from the date of acceptance on the Sample Receipt Form. Details of the deliverables are presented below. _ • Sample Receipt - The laboratory will complete and submit a "Sample Receipt" form for all sample shipments received. The purpose of the form is to note problems with sample packaging, COCs, and sample preservation. Problems noted on the form will be communicated to CGRS, Inc. as soon as possible. • Reporting of Analytical Results — For each analytical method performed, the laboratory will report all analytes as detected concentrations or as less than the specific limits or quantification. All samples with out-of-control spike recoveries being attributed to matrix interferences should be designated as such. All soil/sediment and solid waste samples should be reported on a dry-weight basis with percent moisture also reported. Also, report dates of extraction/preparation, dates of analysis, and dilution factors when applicable. An electronic deliverable (LIMS) will be provided that conforms to the CGRS project data requirements. An example of the data deliverable is presented in Table 2. • Internal Quality Control Reporting—Internal QC samples should be analyzed at rates _ specified in the method (SW-846). At a minimum, QC deliverables will consist of laboratory blank results, surrogate spike percent recoveries, results of MS/MSD analyses, laboratory control sample data, laboratory duplicate results, and if requested, calibration and tuning data. The internal.QC data will not be delivered unless requested by Varra or CGRS personnel. 3.5 Field and Laboratory QA/QC Procedures • Quality control checks are performed to ensure that the data collected are representative and valid. Quality control checks are the mechanisms whereby the data quality objectives are monitored. The quality control samples to be collected on the project are described below. • Duplicate Samples — As a check for laboratory reproducibility, blind duplicate samples (unknown by the laboratory to be duplicates) will be collected and submitted Varra Companies _. Quality Assurance Project Plan Page 3 to the laboratory at a rate of one every 10 water samples collected, or once per site, whichever is greater. No duplicate soil samples will be collected. • Field Blank Samples—To evaluate sample bottle filling procedures and the effects of environmental contaminants at the site, one VOA water sample per site is collected in laboratory-cleaned and prepared containers of deionized or organic-free water supplied by the laboratory. Field blanks are collected downwind of the most contaminated area within a site. The sample is sealed, labeled and shipped with the real samples collected for the same parameter group. • Travel (Trip) Blanks—Trip blanks are intended to address interferences derived from improper sample container cleaning, preparation, contaminated source blank water, sample cross-contamination during storage and shipment, and environmental conditions affecting the sampling event to and from the site, including delivery to the laboratory. Trip blanks will originate at the laboratory and will consist of VOA vials filled with source blank water, and will be sealed and stored in the cooler where real samples will be stored and shipped. • Equipment(Rinseate) Blanks — Rinseate blanks, intended to provide quality control on field cleaning procedures,will be collected once per site. Varra Companies Quality Assurance Project Plan Page 4 Table 1 Summary of Parameters, Sample Containers, Holding Times, and Analytical Methods No.and Type of Analytical Holding Time(1) Parameter• MatrixMethod(2) Containers Free Cyanide . _...._.. Water 1-200 ml P,G 14 days,4C,NaOH to ph>12 EPA 300.0 Chloride Water 1-200 ml,P,G 28 days no preservative required EPA 300.0 Fluoride Water 1-500 ml,P 28 days no preservative required EPA 300.0 Sulfate Water I -200 ml,P 28 days cool to 4C EPA 300.0 Nitrate Water 1 - 100 mL P,G 48 hours cool to 4C EPA 300.0 Mercury Water 1-500 ml P,G 28 days,HNO3 to pH--t2 245.1/7170 Total Metals(RCRA) Water 125-500 ml nalgene(Red dot) 6 months except Mercury at 28 days. For (010/7000 water,preserved with HNO3,not filtered. • Dissolved Metals(RCRA) 125-500 ml nalgene 6 months except Mercury at 28 days. Filtered 6010/7000 Water (Green dot) and preserved in Lab. Anions/General Chemistry Water 250 ml nalgene(White 28 days 200 Series dot) Notes: (1)All collected samples to be kept cool(4 degrees C) (2)USEPA Method,SW-846(Revised), 1986 Table 2 Content of Digital Analytical Deliverables - (LIMS Download) Origin of Data Laboratory Name of Data Example of Delivered Generated by CGRS Generated in Lab Field Digital Data and Entered on by Quanterra COC COMPANY_NA Varra Energy X SITE_NAME Coal Ash Project X SITE_NO 2755aa X SAMPLE_ID1 MW-1 X SAMPLE_DAT 08/27/97 X LAB_ID L15316-01 X MATRIX Water X X __ METHOD M6010ICP X DATE ANALY 09/04/97 X ANALYTE Silver, total(3051) X TEXT RESUL (blank if ND) X NUMBER_RES (blank if ND) X QUALIFIER U X DILUTION 106 X MDL 0.50000 X PQL 3.00000 X UNITS mg/Kg X DATE_RECEI 09/03/97 X DATE_EXTRA 09/04/97 X CAS 007440-22-4 X BATCH ID WG47359 X VARRA COMPANIES - COAL ASH PROJECT ANALYTICAL SUITES FIELD PILOT TESTS Analyte Standard Units Aluminum 5.000 mg/L Arsenic 0.050 mg/L Barium 2.000 mg/L Boron 0.750 mg/L Cadmium 0.005 mg/L Chromium 0.100 mg/L Colbalt 0.050 mg/L Iron 0.300 mg/L Lead 0.050 mg/L Manganese 0.050 mg/L Mercury 0.002 mg/L Nickel 0.100 mg/L Selenium 0.050 mg/L Chloride 250.000 mg/L Free Cyanide 0.200 mg/L pH 6.5-8.5 s.u. Sulfate 250.000 mg/L CG'S April 9, 1999 Mr. Roger Doak Colorado Department of Public Health and Environment(CDPHE) Hazardous Materials and Waste Management Division 4300 Cherry Creek Drive South Denver, CO 80246-1530 weld County Planning Dept. RE: Varra Coal Ash Project R 2 Iggq Weld County, Colorado O CGRS No. 1-135-2755 ED Dear Mr. Doak: Enclosed please find the application checklist to aid you in your review of our coal ash proposal. Information requested on your checklist, which may not be adequately addressed in our work plan or USR application, is addressed below. > In regard to operational data the normal business hours for Varra quarry operations is 7 AM to 5 PM, Monday through Friday. ➢ In regard to qualifications of the person responsible for correcting noncompliance, we offer CGRS, Inc.'s Statement-of-Qualifications, which details our company's experience. The resumes attached within provide qualifications of individuals involved in this project. S. We have provided precipitation data as Attachment A to this letter. ➢ Groundwater travel calculations and hydrologic properties of the surficial aquifer will be made prior to deposition of any materials as stated in our Work Plan. We anticipate that the hydraulic conductivity will be about of 100 feet per day. • Available background water quality data from unconsolidated alluvial aquifers is provided in Attachment A. The spatial distribution of these data is over the Boulder - Fort Collins - Greeley area. ➢ A financial assurance plan will be provided by Varra Companies upon approval of the Certificate of Designation. P.O. Box 1489 f,xt Collins, CO 80522 P5o nn (970) 493-7/80 Fax. (9/0) 493 /988 Mr. Roger Doak Varra Coal Ash Project April 9. 1999 Page 2 If you have any questions regarding this letter or require further information, please contact me at (800) 288-2657. Sincerely, CGRS, INC. b . Adams, P.G. Principal/Hydrogeologist Attachments cc: Mr. Chris Varra - Varra Companies Mr. Trevor Jiricek -Weld County Health Department Mr. Ben Patton- Weld County Planning 04/06/99 16:07 FAX 3037595355 CDP V1002 SOLID WASTE DISPOSAL SITES AND FACILITIES APPLICATION CHECKLIST LANDFILL (THIS DOCUMENT IS NOT AN APPLICATION FORM) (This document is meant to be used as a checklist, application format and annotated table of contents for applications) FACILITY NAME Varra Companies, Inc. COUNTY Weld Unincorporated X Incorporated City Longmont GENERAL DATA (3 .3 .1) Mailing Address Name : Varra Companies Attention : Chris Varra Address : 12910 Weld County Rd. 13 Zip 8nsnd City : Longmont State r0 Phone : (303 ) -666 -8269 Location : Twn 3 0 Rng (new Section 3/ Area Total site 35 acres ac. Disposal area 0.25 ac. Type of Facility Gravel Quarry Discussion of facility service area, including transportation corridors and surrounding access. Page 8 in application LOCATION RESTRICTIONS AND SITE STANDARDS (3 . 1) Page f in application OPERATIONAL DATA (3 .3 . 2) OPERATOR Name Varra Companies, Inca Attention: Chris Varra Address. . : 12910 Weld County Rd. 13 City Longmont State rn Zip flfsna Phone : ( 303 ) 666 - 8269 Qualifications of person responsible for correcting non-compliance. Page / in application sae Cove/ le fe Hours of operation (3 .3 .2 . (B) ) Page f in application._ y •Describe Gravel quarry operations 7am-5pm m-f JANUARY 1994 Page 1 of 6 04/06/99 16:08 FAX 3037595355 CDP 10003 Description of Waste Stream and volumes (3 . 3 . 2 . (C) ) Page / in application M/A •Describe Not applirahle - Deposits on estimated 400 tons within a trench measuring 100 ft in length 1O ft. in width and 10 ft. in depth. Commercial Yes/No Community Yes/No Industrial Yes/No Asbestos Yes/No Inert Material Yes/No Construction Demolition Yes/No Special Yes/No Sludge Yes/No Other Expected life of facility ( 1 years Personnel Descriptions (3 . 3 .2 . (D) ) Page / in applicatTc.s\ pg 11 in workplan Equipment (3 . 3 .2. (E) ) Page f in application Appendi*B in wnrrplan Size and types of disposal cells (3.3 .2. (F) ) Page # urn application •Describe Page 10 in Work Plan. A single trenrh measuring 100 ft in length 10 ft in width and 10 ft in depth wi ll be used for the rnnal ash nlarement. Composition and frequency of cover material (3 .3 .2 . (G) ) Page / in application page 10 in work plan Fencing (3 .3.2 . (H) ) Page / in application N/A Provisions to minimize nuisance conditions (3 .3 .2 . (I) ) Page # in application Page i USE Section 3, Part E Fire Protection (3 .3 .2 . (J) ) Page / in application Page 2nf DSR. Section K Windblown debris (3 .3 . 2 . (K) ) Page / in application N/A Conceptual plans for impacts to surface or ground waters (3 . 3 . 2 . (L) ) Page / in application Page 11 in Work Plan Section 4.5 Sources of water for on site use (3 . 3 . 2 . (M) ) Page # in application_W1L Hazardous waste exclusion plan (2 . 1. 2 . ) Page # in application _Nat___ Surface water control systems (2. 1. 6) Page # in application N/A JANUARY 1994 Page 2 of 6 04/06/99 16:08 FAX 3037595355 CDP VI 004 GEOLOGICAL DATA (3 . 2 .1) Unconsolidated materials (3.2 . 1. (A) ) Page t in application page 1 in work plan Name(s) Allvvinm- Holnrene in age Type(s) candy to C;ravnlly al1uvinm Thickness(es) ,n-snp Consolidated materials (3 .2.1. (B) ) Page 1 in application N/A Name(s) Type(s) Thickness(es) Regional and local geological structure (3 .2. 1. (C) ) Page 1 in application N/A Regional strike Dip Local strike Dip Geological structures Geological hazards (3.2.1. (D) Page / in application N/A Precipitation See Attachment A Floodplain (3.1.7) Page 1 in application page 4 of USR Aquifer recharge area (2. 1.5) Page 1 in application N/A Groundwater travel calculation (3.2 .5 (11) ) Page f in applicationpq.9 of Airport restriction (3 .3. 1) Page / in application N/A work plan Notification of FAA if airport within 5 miles (3 .3 .1) Page 1 in application N/A HYDROLOGIC DATA (3 . 2 .2) Surface water features within 2 miles (3 .2 .2 (A) ) Page 1 in application see attachment *Summarize The Saint Vrain Creek lies approximately 270 feet immediately south of the proposed study area (see Figure 3 in work plan) Depth to and thickness of perched zones and uppermost aquifer (3 .2 .2 . (B) ) Page 1 in application *Summarize Allu ial depos s a e st'ma d o Va y tween 90 and 50 feet. in t.hir•kness and overlies the Laramie-Fnx Hills fnrmatinn JANUARY 1994 Page 3 of 6 04/06/99 16:08 FAX 3037595355 _ CDP (j005 Ground water wells within one mile of site boundary (3 . 2 . 2. (C) ) Page / in application Appendix A work plan, pg. 2 Work plan Hydrologic properties of perched zones and uppermost aquifer (3 . 2 .2. (D) ) Page / in application -,E£ (avrf Ce7TE2 Perched Zone Upper Aquifer Name Unconfined/confined unconfined Hydraulic conductivity (cm. /sec) estimated at 0 n9n Hydraulic gradient (ft. /ft. ) tn he determined Porosity, (Percent %) tn be determined Flow direction estimated N 40 degrees W Potentiometric surface (ft,bgs) 4- 10' Transmissivity (cm2/sec) tn }le determined Storativity, S to he estimated Site location in relation to the base floodplain of nearby drainages (3 .2 .2. (E) ) Page / in application page 4 of USR Potential for impacts to existing surface and ground water quality (3 .2 .2 . (F) ) Page f in application purpose of the proposal -See tables of leaching studies Existing quality of ground water beneath the. proposed facility (3 .2 .2 . (G) ) Page t in application Appendix A of Wnrk Plan and Attachment to this checklist ENGINEERING DATA (3 . 2 .3 . ) Daily and intermediate cover material; type, quantity, and location (3 .2 . 3 . (1) ) Page / in application < 1 feet gnil Liner and final cover material; type, quantity, and location (3 .2 . 3 . (2) Page / in application N/A Maps and plans drawn to a conveniently readable scale showing the following information (3 . 2 . 3 . (3) ) : (a) Location and depth of cut for liners Page # in application Fig 3 (b) Daily, intermediate, and final cover Page / in application pig -4 (c) Location and depths of proposed fill and processing Page / in application page 10 Work plan (d) Location, dimensions, and grades of all surface water diversion structures Page / in application N/A (e) Locations and dimensions of all surface water containment structures Page / in applicationFig. 3 Aerial photo in USR application JANUARY 1994 Page 4 of 6 04/06/99 16:09 FAX 3037595355 GDP V]006 (f) Spatial distribution of engineering, geologic, and hydrologic data; relation to proposed facility Page / in applicationSCE (bvfizz,crTZZ (g) Location of all proposed facility structures and access roads Page f in application page 2 TJSR (h) Location of all proposed monitoring points for surface water, ground water, explosive gases Page i in application Fig 3 work plan (i) Final contours and grades of the fill surface after closure Page 1 in application Page / in application NA (j) Location of fencing Page # in application ,JR (k) Location of each discrete phase of development Page # in application NIA (1) Design details of the final cap, liner, and leachate collection system Page / in application 0 Construction details for all proposed monitoring points for (3 . 2. 4) : •Surface water quality Page f in application Appendix B page 1 Work Plan •Ground water quality Page f in application Appendix A •Explosive gases Page / in application N/A Liner design components (3 .2 . 5 .A) (1) Barrier layer hydraulic conductivity N/A cm/sec Page / in application (2) Barrier layer thickness N/A feet Page / in application N/A (3) Barrier layer porosity % (If available, for HELP model) Page f in application (4) Barrier layer slope N/A feet/foot Page / in application (5) Maximum design hydraulic head on barrier layer N/A inches Page / in application (6) Distance to relevant point of compliance (<=150 m) feet Page 1 in application to he established (7) Distance and characteristics, including quality, of the uppermost aquifer or monitored unit Page f in application sEE gnncwme, r '1 (8) Climatic factors Page / in application N A (9) Estimated volume, physical characteristics, and chemical characteristics of the leachate Page f in application Tables 2-6 work (10) Chemical compatibility of the barrier layer to estimated leachate plan chemical characteristics Page # in application IJ/R (11) The distance ground water beneath the site would flow during the facility's operating life and post-closure care period Wp feet (12) The distance to domestic wells or springs shown to tap the uppermost aquifer downgradient of the site feet Barrier layer type (Section 3 . 2 .5. (C) ) Page i# in application • Summarize N/A JANUARY 1994 Page 5 of 6 04/06/09 16: U0 PAX JOS/00b3bb UUt' 4007 Leachate collection and removal systems (3 .2.5. (D) ) Page # in application N/A • Summarize Surface water control systems (3.2 . 6) Page / in application N/A Provision for as-built construction documentation (3 . 2.7) Page # in application N/A Quality assurance and quality control plan (3 . 3 .3) Page / in application Section 4.5 Work Plan Cover material requirements (3 .3.4) Page / in application N/A Soil balance calculations (3.3 .5) Page # in application N/A Water availability (3 .3 . 6) Page / in application N/A Leachate and landfill gas condensate management (3 . 3 . 7) Page # in application N/A Recordkeeping (2.4, 3.4) Page # in application N/A Waste volumes ( ) Water monitoring ( ) Gas monitoring ( ) Approved operational plan ( ) Construction as-built ( ) Operation variances ( ) Training program ( - ) Special waste program ( ) Ground water monitoring plan (2 . 2) Page # in application Appendix B,C page 10 of workplan Explosive gas monitoring (2 . 3) Page ,/ in application N/A Closure plan (3 .5, 2.5) Page # in application to be determined Post-closure care and maintenance (3 . 6, 2 . 6) Page # in application N/A Financial assurance plan (1. 8) Page / in application See attached letter JANAURY 1994 Page 6 of 6 ATTACHMENT A PRECIPITAION AND WATER QUALITY DATA http://ccc.atmos.colostate.edo!- bin/mlydb.pl Monthly Climatic Data for GREELEY UNC for years 1995 - 1997 Station - 53553 Latitude - 4025 Longitude - 10442 Elevation - 4650 Jan Feb Mar Apr May Jun Jul Aug Sep Oct Nov Dec Annual Monthly mean temperature. Ave 27. 6 34. 0 41. 4 46. 5 57. 0 67.7 73. 5 72. 9 63. 5 51. 0 38. 6 32 . 4 50. 5 Max 30 .3 35 .9 44.3 50.4 59 .7 69 .7 74.5 75.4 66.0 51.7 42 . 1 33 .0 50 . 6 Year 1995 1995 1997 1996 1997 1996 1997 1995 1997 1996 1995 1995 1996 Min 25 .3 32.7 38.4 44. 5 51 . 6 64.0 72 .9 71.2 62 .0 50 .2 36.4 31 .2 50.3 Year 1997 1997 1996 1997+ 1995 1995 1995 1997 1996 1995 1997 1997 1995 Count 3 3 3 3 3 3 3 3 3 3 3 3 3 Monthly mean maximum temperature. Ave 39 .9 46.7 56 .2 59 . 5 69 .3 81 . 8 88. 6 88.0 77 .5 65.7 51.1 44.1 64. 0 Max 42 . 5 49 .2 61.2 64.8 74.1 84.7 90.2 91.6 80.2 66 .2 55 .8 46 .3 64.7 Year 1995 1995 1997 1996 1997 1996 1997 1995 1997 1996 1995 1996 1996 Min 36.2 42 .8 52 .4 56 .5 60 . 9 77 .1 87 .0 84. 6 76.1 65 .2 48 .1 41.0 63 .7 Year 1997 1997 1996 1995 1995 1995 1996 1997 1995 1995 1997 1997 1995 Count 3 3 3 3 3 3 3 3 3 3 3 3 3 Monthly mean minimum temperature. Ave 15 . 3 21 .3 26 . 6 33 . 5 44.6 53 . 6 58 .4 57 .8 49 .5 36.3 26. 1 20.6 37 .0 Max 18.2 22 . 6 28 .0 36 . 0 46 .4 55 .3 59 .3 59 .2 51.7 37 .2 28 .4 21 .4 37 .3 Year 1995 1997 1995 1996 1996 1997 1996 1995 1997 1996 1995 1997 1997 Min 13 .3 18 .9 24.4 31 . 9 42 .2 50 .9 57 . 1 56.4 47 .7 35.3 24. 8 19. 5 36.6 Year 1996 1996 1996 1997 1995 1995 1995 1996 1996 1995 1997 1996 1996 Count 3 3 3 3 3 3 3 3 3 3 3 3 3 Total monthly precipitation. Ave 0. 55 0. 48 0. 61 1. 67 2.73 2. 66 1. 80 1.28 1. 81 1.00 0.44 0.14 15 .18 Max 0 . 82 0.88 0.94 2 . 85 4.13 3 .99 2 . 54 2 .97 2 .86 2 .07 0 .46 0 .32 17 .05 Year 1997 1995 1996 1995 1995 1995 1996 1997 1995 1997 1995 1997 1995 Min 0 . 06 0 .08 0 .44 0.67 1.61 1 . 65 0 . 57 0.23 0 .83 0.44 0.41 0.00 12 .35 Year 1995 1996 1995 1996 1997 1996 1995 1995 1997 1996 1996 1996 1996 Count 3 3 3 3 3 3 3 3 3 3 3 3 3 Total monthly snowfall. Ave 8 .0 5 . 8 5 .5 6 . 9 0 .0 0.0 0.0 0 .0 1.7 9 .7 4 . 8 1 .7 44.1 Max 13 .0 9 .7 5 . 6 10.2 0.0 0.0 0.0 0.0 4 .0 20.2 5.8 3 .5 59 .2 Year 1997 1995 1995 1995 1997+ 1997+ 1997+ 1997+ 1995 1997 1995 1997 1997 Min 0.5 0 .7 5. 5 4 .0 0 . 0 0.0 0.0 0 .0 0.0 3 . 0 3 . 5 0 .0 29 .9 Year 1995 1996 1997+ 1996 1997+ 1997+ 1997+ 1997+ 1997 1996 1997 1996 1996 4/8/99 10:47 AM Water Quality of Unconsolidated Alluvial Deposits Boulder - Fort Collins - Greeley Area Varra Coal Ash Burial Project Weld County, Colorado CGRS Project No. 1-135-2755 Number of Number of Samples where Constituent Units Standard -Range Samples standard was exceeded Dissolved Solids mg/L 500 53-6,570 178 161 Dissolved Arsenic ug/L 50 < 1-5 89 0 Dissolved Chloride mg/L 250 .4-1,100 295 2 Dissolved Fluoride mg/L 1.8 .2-5 145 12 Dissolved Iron ug/L 300 <1-16,000 164 15 Dissolved Manganese ug/L 50 < 1-920 92 14 Dissolved Magnesium mg/L 125 1.9-510 170 30 Dissolved Nitrite (plus nitrate as nitrogen) mg/L 10 .00-73 289 43 Dissolved Selenium ug/L 10 < 1-100 94 15 Dissolved Sulfate mg/L 250 5.9-3,640 180 136 Hardness, as calcium carbonate mg/L None 31-3,540 177 N/A Hillier and Schnider, 1972. Well Yields and Chemical Quality of Water, Boulder-Fort Collins-Greeley Area, Colorado. US Geological Survey Miscellaneous Series, Map 1855-J. Hello