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HomeMy WebLinkAbout20091969.tiffCOLORADO January 26, 2010 Conquest Disposal Service Attn: Jim Goddard 8207 W. 20th Street, Suite B Greeley, Colorado 80634 DEPARTMENT OF PUBLIC HEALTH & ENVIRONMENT 1555 N. 17th Avenue Greeley, CO 80631 WEBSITE: www.co.weld.co.us ADMINISTRATION: (970) 304-6410 FAX: (970) 304-6412 PUBLIC HEALTH EDUCATION & NURSING: (970) 304-6420 FAX: (970) 304-6416 ENVIRONMENTAL HEALTH SERVICES: (970) 304-6415 FAX: (970) 304-6411 Weld County Planning Department GREELEY OFFICE .IAN 27nun RECEIVED Subject: Conquest #2 (SWD 2-28) — I" Semi-annual Inspection 2010 Dear Mr. Goddard: On January 25, 2010, the Weld County Dept. of Public Health & Environment conducted a routine inspection of the Conquest Disposal Service disposal well, located at 1191 Weld County Road 19, Weld County, Colorado. The purpose of the inspection was to assess the facility's compliance with the Approved Site Specific Development Plan and the Use by Special Review Permit Number 1033 (USR- 1033) and applicable Weld County Code. The following needs to be addressed by Conquest Disposal: The Department previously requested that Conquest file an Air Pollutant Emission Notice and Construction Permit Application with the Colorado Department of Public Health and Environment's Air Pollution Control Division and copy the submittal to this Department. To date, this Department has not been provided with any copy of an APEN submittal or emissions estimates for this facility. This matter has already been referred to the Air Pollution Control Division. A copy of the inspection checklist and an e-mail regarding Benzene in Monitoring Wells MW -2 and MW - 7 was attached. If you have any questions regarding this inspection, please contact me at 304-6415, extension 2219. Sincerely, Troy E. Swain Environmental Health Specialist Environmental Health Services Attachments: (3) cc: Trevor Jiricek. Director. Weld County Environmental Health Services (e-mail with attachments USR-1033, Weld County Department of Planning Services (with attachments) Denise Onyskiw, COGCC, 1 120 Lincoln St., Ste. 801. Denver, CO 80203 (with attachments) Scott Patefield, Colorado Dept. of Public Health and Environment APCD (e-mail without attachment) 2c001- 'gag • Troy Swain From: Sent: To: Cc: Subject: Troy Swain Tuesday, January 26, 2010 10:35 AM 'Craig Mulica' 'jim goddard' RE: What is the status of any Corrective Actions at Conquest C-2 and C-3 for Benzene contamination? Thanks Craig. Please keep me updated on C2. Troy E. Swain Environmental Health Specialist Weld County Dept. of Public Health & Environment 1555 N. 17th Avenue Greeley, CO 80631 (970) 304-6415, ext. 2219 (970) 673-2218 (cell) (970) 304-6411 (fax) Original Message From: Craig Mulica [mailto:craig@cgrs.com] Sent: Tuesday, January 26, 2010 10:30 AM To: Troy Swain; jim goddard Cc: Trevor Jiricek Subject: RE: What is the status of any Corrective Actions at Conquest C-2 and C-3 for Benzene contamination? C3- remediation system active; quarterly GW sampling C2- bi-weekly product and impacted GW extraction from impacted monitoring wells and quarterly monitoring. Additional remedial options under review. Craig S. Mulica Project Manager -Geologist CGRS, Inc. P.O. Box 1489 Fort Collins, CO 80522 ph: (970) 493-7780 fax: (970) 493-7986 cell: (970) 420-6837 CraigOCGRS.com www.cgrs.com Original Message From: Troy Swain [mailto:tswain@co.weld.co.us] Sent: Tuesday, January 26, 2010 10:29 AM To: jim goddard Cc: Trevor Jiricek; Craig Mulica Subject: What is the status of any Corrective Actions at Conquest C-2 and C-3 for Benzene contamination? What is the status of any Corrective Actions at Conquest C-2 and C-3 for Benzene contamination? August 24, 2009 Weld County Planning Department Attn: Kim Ogle 918 10"' Street Greeley, CO 80631 Dear Kim: Re: SR #1604 a Weld County Planning Department GREELEY OFFICE AUG 25 ?nog RECEIVED As you are aware, Conqucst Oil Company (Conquest) on hehatt of the Marcum Midstream 1995-2 Business Trust has undertaken a pilot project to clean the Class II Oilfield Waste that is currently being injected into its disposal wells for reuse in the oil and natural gas industry. The pilot has successfully shown that the waste water can be cleaned to a quality that will allow its reuse. Several companies have studied the analyses of the recycled water and determined it can be effectively used in "cased -hole" operations. When the Weld County Commissioners approved this pilot project in June there was discussion about whether the existing USR allowed the recycled water to be sold by Conquest. At that time Conquest agreed to not sell the water unless the Planning Staff or County Commissioners specifically agreed to allow such. In addition, approval for re -use of the water by the Colorado Oil and Gas Conservation Commission (COGCC) is pending. A Form 4 and supplemental information have been submitted as requested by the COGCC. To allow Conquest to expedite the two parallel regulatory approval processes we are asking that the Planning Staff or County Commissioners approve the sale of the recycled water if, and when, reuse is approved b / the COGCC. At this time Conquest is asking for no other changes to its USR permit. Specifically, Conquest will not exceed the maximum number of truck visits stipulated in Development Standard 22. We may, at a later date, be submitting plans for expansion of the pump building and tank farm for review and approval. This is an exciting, necessary and unique technology. We trust you agree. Your approval of this minor change to the USR would be greatly appreciated. Sincere Dale S. Butcher Vice President Cc: William Garcia Douglas Rademacher Sean P. Conway Barbara Kirkmeyer David E. Long 8207 W. 20th Street • Suite B • Greeley, CO 80634 •970-356-5560 ia:rn Wi�Yc. COLORADO August 18, 2009 Conquest Disposal Company Attn: Jim Goddard 8207 W. 20th Street, Suite B Greeley, CO 80634 DEPARTMENT OF PUBLIC HEALTH & ENVIRONMENT 1555 N. 17th Avenue Greeley, CO 80631 WEBSITE: www.co.weld.co.us ADMINISTRATION: (970) 304-6410 FAX: (970) 304-6412 PUBLIC HEALTH EDUCATION & NURSING: (970) 304-6420 FAX: (970) 304-6416 ENVIRONMENTAL HEALTH SERVICES: (970) 304-6415 FAX: (970) 304-6411 Weld County Planning Department GREELEY OFFICE Al IG 19 ?nnq RECEIVED Subject: Conquest Disposal Service, Ltd., Conquest -6 — 3rd Quarter Inspection 2009 Dear Mr. Goddard: On August 12, 2009, the Weld County Dept. of Public Health & Environment conducted a routine inspection of the Conquest Disposal Service disposal well, located at 13159 WCR 39, Weld County, Colorado. The purpose of the inspection was to assess the facility's compliance with the approved Use by Special Review Permit Number 1604 (USR-1604) and applicable Weld County Code. Based on the inspection, the following needs to be addressed by Conquest Disposal: Though the facility is operating as a commercial oil & gas support facility without the plat having been recorded, the Department understands that you are working with the Weld County Department of Planning Services regarding this matter. The facility is in compliance with all Health Department related prior to recoding the plat conditions of USR-1604. Liquids have been observed in the receiving pad trench underdrain system and repairs were made to the receiving pad trench. Please keep the Department informed regarding your progress. The Department will follow-up with you regarding the above items during the next quarterly inspection. A copy of the inspection checklist is attached. If you have any questions regarding this inspection, please contact me at 304-6415, extension 2219. Sincerely, Troy E. Swain Environmental Health Specialist Environmental Health Services cc: Trevor Jiricek, Director, Weld County Environmental Health Services (e-mail without attachment) Kim Ogle, Weld County Department of Planning Services (with attachment) Denise Onyskiw, COGCC, 1120 Lincoln St., Ste. 801, Denver, CO 80203 (with attachment) • UNDERGROUND INJECTION CONTROL QUARTERLY REPORT DATE: e' I Z ' Uel QUARTER: ] \in? WELL CLASS: II CONTACT PERSON: PHONE: ADDRESS: LOCATION: TRUCK DELIVERIES (APPROX): x3 > BARRELS OF BRINE PER DAY (APPROX): ti 35 °i _ '1oao LIMIT: INJECTION PRESSURE: LINED CELLAR/COVERED: Y / N SOLIDS/SEDIMENT DISPOSAL NAME: `'SS PETROLEUM CONTAMINATED SOILS: CONDITION OF CONCRETE RECEIVING PAD: ) 4ee o C WEEKLY UNDERDRAIN INSPECTION/MAINTENANCE LOG: Y / N , CHEMICALS STORED: 0k- (MANUFACTURER RECOMMENDATIONS) PROPER SIGNAGE{Y)/ N EMERGENCY RELEASES: Y N ISDS(Y I N ENVIRONMENTAL SPECIALIST: / (Z�7 Sc,�„¢ (if PERSONS PRESENT AT TIME OF INSPECTION: COMMENTS: .1V')ecAn-2' afi ?os--6 oci 3yt 5/13-- IGfuc"-ea J3&LS a:\El'CWWASCEComOINSPLST DOC Kim Ogle From: Sent: To: Cc: Subject: Troy Swain Tuesday, July 28, 2009 3:44 PM Chris Gathman Trevor Jiricek; Craig Mulica; jim goddard; Kim Ogle Conquest C-6 Injection Well USR-1604 The Weld County Department of Public Health & Environment (Department) was able to confirm that the CDPHE Air Pollution Control Division received Conquest's APEN submittal for this facility. Also, their groundwater monitoring plan has been approved by this Department. All Health Department related "prior to recording the plat" conditions of USR-1604 have been satisfied to this Department's satisfaction, specifically conditions 1.K., L., and M. Troy E. Swain Environmental Health Specialist Weld County Dept. of Public Health & Environment 1555 N. 17th Avenue Greeley, CO 80631 (970) 304-6415, ext. 2219 (970) 304-6411 (fax) 1 Page 1 of 1 Kim Ogle From: jim goddard [jimgoddardl@yahoo.com] Sent: Monday, July 20, 2009 10:09 AM To: Trevor Jiricek Cc: Troy Swain; Kim Ogle Subject: USR 1604 Good Morning! Thanks for taking time out of your busy day to visit the C6 facility where we are cleaning the water that is brought into us by our customers. I hope you were as impressed as I was when I first saw this being done! As you well know, I dropped the ball on the completion of the USR 1604. I have since then completed all the tasks that were given to me by your office. 1. Complete the APEN. Sent to Health Department 2. Quarterly sampling of monitoring wells. Being e -mailed 3. Repair the receiving trench. ( we are scheduled to do this 7/31/2009. With everything being completed is there a chance that the mylar might get signed in the near future? With the water project going as planned, we, Conquest, would like the opportunity to sell the water back to our customers. It is my understanding that we can not do so until the USR 1604 is completed. If you can offer any guidance please feel free to do so! Thanks for your time! Jim Jim Goddard Conquest Water Services General Manager 970-381-5005 jimgoddard 8207 W. 20th Street Suite B Greeley, Colorado 80634 7/29/2009 Kim Ogle From: Sent: To: Cc: Subject: Attachments: Conquest -6 090413 insp.doc (60... Troy Swain Thursday, June 04, 2009 10:28 AM Kim Ogle jim goddard; Trevor Jiricek Conquest C-6 Conquest -6 090413 insp.doc Based on a file search, this Department has never received/approved a groundwater monitoring plan for Conquest C-6. Conquest has been sampling semi-annual. I asked Craig at CGRS to send me the plan and to sample quarterly. We will revisit the sample frequency later. I asked Craig to copy this Department on the APEN submittal, after that, we will confirm CDPHE Air Pollution Control Division has received it. We also discussed the leak below the receiving trench and asked him to report it to COGCC. We've already discussed the leak with COGCC. I attached a copy of the inspection letter for our Department's April 13, 2009 inspection. Troy E. Swain Environmental Health Specialist Weld County Dept. of Public Health & Environment 1555 N. 17th Avenue Greeley, CO 80631 (970) 304-6415, ext. 2219 (970) 304-6411 (fax) Kim Ogle From: jim goddard [jimgoddardl@yahoo.com] Sent: Tuesday, June 02, 2009 12:03 PM To: Troy Swain Cc: Kim Ogle Subject: APEN Attachments: c62009_0129_analytical.pdf Good Morning! I received a call this morning from Kim Ogle letting me know that we need to address the APEN portion of the USR 1604 before Weld County Health will sign off on the USR. I contacted Craig Mulica from CGRS Environmental, which is the company we contract all of our environmental work to regarding the APEN issue. After Craig explaining what was going on with the APEN and how new this is to the commercial disposal regulations we are ready to do the testing necessary. We are scheduled a couple of weeks from now to run the test. We will keep you in the loop regarding the testing and will submit the forms necessary to comply with the County. Attached is the analytical you requested from our monitoring well. I apologize for the delay I thought Craig had already sent this to you. We are taking corrective actions regarding the cracks that need sealed in the trench. We just need a couple of days of nice hot weather. Please call with any concerns and I'll keep you in the loop regarding the APEN. Have a great day! Jim Jim Goddard Conquest Water Services General Manager 970-381-5005 jimgoddardl@yahoo.com 8207 W. 20th Street Suite B Greeley, Colorado 80634 1 • •sue «u 4 - June 1, 2009 Weld County Planning and Building Department Attn: Kim Ogle 918 10th Street Greeley, CO 80631 Dear Kim, We are currently in the beginning stages of a water recycling pilot project at the C6 (13159 WCR 39, Platteville). Pro Treat Technology Corporation is the company that will be testing their technology and thus the firm we will be working with. ProTreat has developed water treatment systems throughout the western United States for many years. We will set up a temporary facility to the North of our existing pump house. The temporary facility will be bermed, as well as lined with plastic to contain any spills. There will be five (5) 60 barrel poly tanks, one (1) 165 barrel poly tank and six (6) chemical totes. The pilot project will last 60-90 days and only run during the daylight hours, in addition, it will be manned by Protreat's staff. The ultimate goal of this project is to be able to recycle a portion of our water and ready it for re -use in the oilfield. Should you have any further questions, please don't hesitate to contact me at (970) 356-5560. Sincerely, Dale Butcher Conquest Water Services 6/Z 8207 W. 20th Street • Suite B • Greeley, CO 80634 •970-356-5560 ieft COLORADO April 14, 2009 Conquest Disposal Company Attn: Dave Gage 8207 W. 20th Street, Suite B Greeley, CO 80634 DEPARTMENT OF PUBLIC HEALTH & ENVIRONMENT 1555 N. 17th Avenue Greeley, CO 80631 WEBSITE: www.co.weld.co.us ADMINISTRATION: (970) 304-6410 FAX: (970) 304-6412 PUBLIC HEALTH EDUCATION & NURSING: (970) 304-6420 FAX: (970) 304-6416 ENVIRONMENTAL HEALTH SERVICES: (970) 304-6415 FAX: (970) 304-6411 Subject: Conquest Disposal Service, Ltd., Conquest -6 — 2"d Quarter Inspection, 2009 Dear Mr. Gage: On April 13, 2009, the Weld County Dept. of Public Health & Environment conducted a routine inspection of the Conquest Disposal Service disposal well, located at 13159 WCR 39, Weld County, Colorado. The purpose of the inspection was to assess the facility's compliance with the approved Use by Special Review Permit Number 1604 (USR-1604) and applicable Weld County Code. Based on the inspection, the following three items need to be addressed by Conquest Disposal: Based on a recent Air Pollutant Emission Notice (APEN) submittal from a like facility, this department has reason to believe your facility may need to report air emissions of Volatile Organic Compounds. Section 23-2-250 of the Weld County Code requires the operation of this use to comply with the air quality regulations promulgated by the Air Quality Control Commission. In addition, USR-1604 "prior to recording the plat" condition 1.K. requires all required air emissions permits to be obtained and Development Standards 12 & 15 of USR-1604 require compliance with Air Quality Control Commission regulations and permit requirements. An APEN and Construction Permit Application must be filed with the Colorado Dept. of Public Health & Environment's Air Pollution Control Division (APCD). Based on the inspection, the receiving pad trench underdrain has been observed to contain liquids, which may indicate a leak or water infiltration. This liquid must be sampled to determine the source. Sample and provide results to this Department and the Colorado Oil & Gas Conservation Commission. The facility has been operating as a commercial oil & gas support facility (Class II disposal well). The plat must be recorded prior to operation as a commercial disposal facility; therefore, this matter was referred to the Weld County Department of Planning Services. • 0 Conquest Disposal Company Dave Gage April 14, 2009 Page 2 The liquid in the pad trench underdrain must be tested and the test results forwarded to this Department. Submit an APEN/Construction Permit Application to the APCD (copy submittal to this Department). The Department will follow-up with you regarding the above items during the next quarterly inspection. A copy of the inspection checklist is attached. If you have any questions regarding this inspection, please contact me at 304-6415, extension 2219. Sincerely, Troy E. Swain Environmental Health Specialist Environmental Health Services cc: Trevor Jiricek, Director, Weld County Environmental Health Services (e-mail without attachment) Kim Ogle, Weld County Department of Planning Services (with attachment) Ed Hinkley, COGCC, 1120 Lincoln St., Ste. 801, Denver, CO 80203 (with attachment) Robert Jorgenson, Colorado Dept. of Public Health and Environment APCD Jim Goddard, Conquest Disposal Company USR 1604 Conditions: 1. Prior to Recording the Plat: A. Plat is being prepared by King Surveyors. B. King Surveyors C. King Surveyors 1. Plat will have attached the "Development Standards" 2. This has been addressed and approved by Weld County Health. (Please see exhibit #1-C-#2) 3. This has been addressed. 4. This has been addressed. 5. This has been addressed. 6. This has been addressed. 7. This has been addressed. 8. This has been addressed. 9. This has been addressed. D. This has been addressed. E. This has been addressed. F. This has been addressed. G. Platteville Fire Department has visited location and inspected the property and will send Kim Ogle a letter of approval. (Please see Exhibit #1-G) H. Sheriffs department has been out to location and discussed security. Conquest uses Dictoguard as its security service. I. Division of Wildlife has visited location and approved the fencing. This will be followed up with a letter from Chris Mettenbrink for the Division of Wildlife. 12/11/2007 at 9:00 a.m. J. This has been addressed. K. Not Applicable at time of application. L. All ground water monitoring is done with CGRS and is reported to Weld County Health Dept. quarterly. M. Not applicable. N. The agreement is attached. (please see exhibit #1-N) O. This has already been approved by Weld County Department of Public Health (please refer to exhibit C#2) P. Weld County Department of Public Health has been out to location and approved our operation. Q. This has been addressed. (please see exhibit #1-Q) R. This has been addressed. (please see Exhibit #1-R). 2. This has been done by King Surveyors. 3. This has been done by King Surveyors. 8207 W. 20th Street • Suite B • Greeley, CO 80634 •970-356-5560 4. Understood. 5. Prior to the Release of Building Permits a. This has been completed. b. This has been completed. c. The buildings were built to code. d. This was done and approved by the Platteville fire department. e. The building height was to code. f. Photos and physical inspection was made and approved by the Weld County Department of Public Health. g. This has been completed. h. This has been completed. (Please see Exhibit #5-H) i. This has been addressed. j. Once per year, Conquest cleans out the bottom of the system tanks. The sludge is removed by a vacuum truck and hauled to CSI in Bennett, Colorado. k. This has been addressed. (Please see Exhibit #5-K) I. This has been addressed. (Please see Exhibit #5-L) m. Septic was installed and approved by the Weld County Health Department. n. Letter was submitted to the Weld County Planning Department. (Please see Exhibit G) 6. a. Approved per Weld County Sheriff's Department. • • Page 1 of 1 Kim Ogle From: Bradley A. Curtis [Bradley.Curtis@lra-inc.com] Sent: Tuesday, July 22, 2008 4:14 PM To: Kim Ogle Subject: RE: Please clarify what was provided. It appears there are comments that can/should be addressed following the "official" USR application submittal. My understanding of the 4 copies of the presubmittal submittal was to verify what we are proposing to submit conforms with the USR application requirement/checklist. I would like to submit for the "official" submittal so that it is in the system. If you could please give me a call at your earliest convenience, it would be appreciated. Bradley A. Curtis, PE, LEEDTM AP Senior Project Manager LAMP, RYNEARSON & ASSOCIATES, INC. Civil Engineers, Surveyors, Land Planners 808 8th Street Greeley, CO 80631 Phone 970.356.6362 Fax 970.356.6486 Cell 970.590.0440 Email Bradley.Curtis@LRA-Inc.com Website www.LRA-Inc.com "Leaving a Legacy of Enduring Improvements Within the Community" ;)) Please consider the environment before printing this email «j From: Kim Ogle [mailto:kogle@co.weld.co.us] Sent: Tuesday, July 22, 2008 4:00 PM To: Bradley A. Curtis Cc: Don Dunker; Kim Ogle; Roger Vigil; Lauren Light Subject: 7 -day reviews for Apollo Operating, LLC Have not received comments from Health or Building. Comments if any will be short coming Kim Ogle I Planning Manager T: 970 356.4000 x 3549 F: 970 304 6498 Weld County Planning Services - Greeley Office 978 Tenth Street I Greeley ('O 80631 I ,og cia,a,co.weld co us 07/22/2008 Troy 6-4-2008 Ground Water Monitoring Plan - Need Pad leaks — samples from trench, concrete trench is leaking, secondary plastic liner COGCC, report of COGCC CRGS send GWMP, Quarterly review Found in January, spoke to Troy Water in sump Water is system in April Troy sample and provide results, results provided — produced water in trench APEN — 8 tons Apollo, all facilities need to stack test protocols, emission factors, tanks model, speak with state CRGS guy to get APEN going. Financial Assurance • • Kim Ogle From: Sent: To: Subject: Kim, Laurie Exby Thursday, January 24, 2008 10:00 AM Kim Ogle; Trevor Jiricek; jim goddard Conquest C6 I was out at the Conquest C6 injection well on December 28, 2007 and did observe the trash enclosure. It adequately screens the trash collection area. The enclosure appears to be cedar plank approximately 6 ft. high. The facility is in compliance with this development standard however we are still waiting on several items from Jim Godard in order to ascertain whether the facility is in compliance with all Development Standards for USR-1604. I will contact Jim as to when we will be receiving the necessary documentation. The facility is not operating, but has taken water (per Commissioner Approval) to test the various systems and tanks. At the time of the inspection the facility was neat and orderly with appropriate signage in place. Any questions please contact me at ext. 2223 or ext. 8723. Laurie 1 8 8 l08S-989 (OLO) xa3 I n0s-989 (0L6) atiogd 0SS08 ope1o,o3 `1osPunN a.u3Q U0p1EO 099 `SHIOAHAIIR5 DNI}I Iova S,pSN3b MOP 00V6010D A3133N0 V# 13381S H100 153M sag 110 1S3001,100 0/3 hoar SS]N1509 0-566RV3wiS0if WO]tlVW M31A3a 1VI03dS AG 390 W 6Fp avow FIN/I0.9 07311 .9# Lin 3•1S.L0.00S sE 0 VICINITY MAP g —C2•2242‘4)--"12 A 8 1 ;s e� ;s : II if ff ff i!}!1! UU i • @ 4 . >2"o 1 Y p dKa� /Foci _--47667--- (%c St��rLLE . �� `�* Platteville/Gilcrest Fire Protection District March 18, 2010 Conquest Disposal 13159 WCR 39 Platteville, CO 80651 Re: New Tent Structure To Whom It May Concern: On March 16th, I met with Jim Goddard at the facility on WCR 39 to go through their new structure. At the time, there were three items that needed to be corrected to be compliant with the fire code. Today we met again with Mr. Goddard and all items have been corrected. If anything further is needed please let me know. Sincerely, /2 W7 Russell Kissler Captain / Fire Prevention Tech. 303 Main Street, P.O. Box 407 • Platteville, CO 80651 • 970-785-2232 • Fax 970-785-0139 21 Main Street, P.O. Box 43 • Gilcrest, CO 80623 • 970-737-2966 • Fax 970-737-9006 &c'9-i9�i ,A1 /Roy co 1.0 FROM -EVERGREEN ANALYTICAL 29 -NAY -2009 02:55PM 29 -MAY -2009 02:55PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.002 F-156 Evergreen Analytical, Inc. 4036 Youngfield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Project ID C6 Composite Sample Date Received: 5/12/09 Lab Order: 09-3343 Date Prepared: 5/20/09 Units: rng/L Method: E1664A Lab IT) Client ID 09-3343-01C CG it n -Hexane Extractable Material (Oil & Grease) HEM - Oil & Grease Prep Method: ])ate Date Matrix Collected Anal ced -__ Results LQ - DF Water 5/12/09 5/20/09 223 5.00 1 nlyy-t ' Approved Qualifiers' B - Analyze detected in the associated Method Blank, value not subtracted from tisult E • Exuapolated valuc.Valuc exceeds calibration range H - Sample analysis exceeded analytical holding tim 1- indicates an estimated value when the compound is detected, but is below the LQL S - Spike Recovery outside accepted limis U - Compound urtalyzeU var but teat ecteCtca X - Sec case narrative • -Value exceeded the Maximum Conutminudon Level (MCL), TCLP limit, ur if compound is undetected, LQL exceeds MCL Definitions: DF - Dilution Factor PF Pep factor LQL - Lowey Quanntuion Limit Print Date: 5/2012009 29 -)MY -2009 02:55PM FROM -EVERGREEN ANALYTICAL 3034256854 Evergreen Analyytical, Inc - 4036 Youngfoid Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID: Client Project 1D: Date Collected: Date Received: Date Prepared: Date Analyzed: Percent Moisture: CO C6 Composite Sample 5/12/09 5112J09 5/15/09 5/22/09 NA Method: SW8270C Prep Method: SW3520C Analytes Accnaphthenc Acenuphthylene Anthracene Benzo(a)anthraccne B enzo(b& k) tl u Oran then e Benzoic acid B enzo(g,h,i)petyl cnc Benzo(a)pyrcnc Benzyl alcohol 4•Bromophcnyl phenyl ether Butyl benzyl phthalate 4-Chloroanilinc Bis(2-chloroethoxy)mcthune His(2-chloraethyl)ether 4-Chloro-3-mcthylphenol 2-Chloronaphthalcnc 2-Chlorophcnol 4-Chlorophenyl phenyl ether Chryscnc Dibenz(u,h)anthracene Dibenzofdran Di -n -butyl phthalate l,2-Diehlorobenzene l 3-Dichlorobenzenc l ,4-Dichlorobenzcne 3,3'-Dichlorobcnzidine Dichlorodiisopropyt ether 2,4-Dichlorophenol Diethyl phthalate 2,4-Dhncthylphcnol Diniethy1 phthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenel 2,4-Dinitroldluene 2,6-Dinitrotoluene Di-n-octyl phthalate B is(2-e thy l hrxy l)p h th al at e Fluoranlhene Fluorene Hexuchlorobenzene 7-757 P.003 F-156 Lab Work Order: 09-3343 Lab Sample ID: 09-3343-01 D Sample Matrix: Lab File ID: Method Blank: Prep Factor: 0.00 Dilution Factor: 2.00 Water El G34\1O00744 .D MB -19146 SEMIVOLATILE ORGANICS CAS Number 83-32-9 208-96-8 120-12-7 56-55-3 205-99-2 & 207-08.9 65-85.0 191.24-2 50.3;.-8 100-51-6 101-55-3 Rc suit U U U U U 430 85.68.7 106.47-8 111-91-I 111-44-4 59-50-7 U U U U U U U U U Units: µg/L MDL LQL 12 12 16 12 24 49 24 11 24 18 13 12 26 12 30 12 12 16 12 24 60 24 12 60 60 13 12 60 12 60 91-58.7 95-57-8 7005-72-3 218-01-9 53-70-3 132.64-9 84-74-2 95-50-1 541-73-1 106-46.7 U U U U U U U U U U 91-94-I 10840-t 120-83-2 84-66-2 105.67.9 U U U U 180 131.11.3 534.52-1 51-28-5 121-14-2 606-20-2 U U U U U 22 14 30 12 10 22 16 12 12 12 60 18 60 12 24 60 16 12 12 12 12 30 20 24 12 12 60 24 60 12 24 12 14 12 22 GO 24 60 12 60 117-84--0 117-81-7 206-44-0 86-73-7 118-74-i Analyst U U U U Qualifiers: See cuss narrative for a discussion B - Analytc detected in the Method Blank, value not subtracted from result E • Extrapolated value.Value exceeds calibration range Il - Prep or Analytical holding time exceeded S - Spike Recovery outride acceptance limi6 X - See case nanativc • -Value exceeded the Maximum Contamination Level (MCL), TCLP limit, or if compound is undetected, LQL exceeds MCI. 22 18 14 17 24 77 18 14 17 60 Approved Qualifiarx: U Analyse not detected at or above the reporting limit I • Estimated value below the LQL Dann hions:NA -Not Applicable LQL - Lower Qtmntitation Limit MDL - Method Detection Limit Surr - Surrogate Standard Print Dote; 5/25/00 29 -MAY -2009 02:56PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.004 F-156 Evergreen Analytical Inc. 4036 Yoansftcld Street, Wheat Ridge, Colorado 80033-3867. (303) 4154021 Client Sample ID: Client Project ID: Date Collected: Date Received: Date Prepared: Date Analyzed: Percent Moisture; CG C6 Composite Sample 5/12109 5/12/09 5/15/09 5/22/09 NA Lab Work Order: Lab Sample ID: Sample Matrix; Lab File ID: Method Blank: Prep Factor: Dilution Factor: 09-3343 09-3343-01 D Water El G34',l G00744 -D MB -19146 0.006 2.00 Method: SW8270C Prep Method: SW3520C Maly tes Hcxachlorobutadiene Hexachlarocyclopcntadicne FIexachloroethanc lndeno(1,2,3-cd)pyrene lsophoranc 2-Methylnaphdtalcnc 2-Metliylphcnol 4-Mcthylphcnol Naphthalene 2-Nltroaniline 3•Nitroanilinc 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodi •n-propylaminc N •Nitrosodiphenylamine Pentseldorophenol Phenanthrene Phenol SEMIYOLAT1LE ORGANICS CAS Number Result 87.68.3 77-474 67-72-1 193-39-5 78-59-1 U U U U U 91.57-6 95-48-7 106-44-5 91-20-3 88-74-4 Pyrene 1,2,4-Trichlorobenzenc 2,45-Trichloroplicool 2,4,6-Trichlorophenol Surr: 2,4,6-Tribromophenol Surr: 2-Iluorobiphenyl Sun: 2-Fluorophenol Surr: Nitrobenzene -d5 Suer: Phenol -d6 Suer: Terphenyl-d14 99-09-2 100-01-6 98.95.3 88-75.5 100-02-7 621-64-7 86.30.6 87-86-5 85-01-8 108-95-2 129-D0-0 120.82.1 95.95.4 88.06-2 120 900 570 43 U Units: µg/L MDL LQL 12 22 12 30 12 12 60 12 60 12 22 30 22 12 26 60 60 24 12 60 U U LI U U u U U 31.1 1700 118-79-6 321-60-8 367-12-4 4165-60-0 13127-88-3 1718-51-0 Annlyat U U U U 22 18 12 34 13 19 12 16 24 26 60 60 12 60 13 24 12 60 60 GO 12 :3 16 20 12 60 1 24 99 QC Limits: 32-138 %R2C 98 QC Limits: 45.130 VeREC 119 QC Limits: 43-130 %REC 146 S QC Limits: 45-130 %REC 113 QC Limits: 47-130 %REC 101 QC Limits: 47.136 %REC 2Y ---- Approved Qualifiers: Sec case narrative for a discussion B • Analyte detected in the Method Blank, value not subtracted from result E • Extrapolated value.Value exceeds calibration range 14 - Prep or Analytical holding time exceeded S • Spike Recovery outside acceptance limits X - See cue narrative -Value exceeded the Maximum Contamination Level (MCL), TCLP limit, or if compound is undetected, LQL exceeds MCL QuaIit crs: U • Anelyte not detected at or above the moaning limit ! - E.srimated value below the LQL Definitions: NA - Not Applicable LQL - Lower Quantiration Linric MDL - Method Detection Limit Star - Surrojatc Standard Print Date: 5/26/09 29 -MAY -2009 02:56PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.005/018 F -I56 Evergreen Analytical, 'Pc. 4036 Youngtield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID Client Project ID Date Collected: Date Received: C6 C6 Composite Sample 5/12/O9 1500 5/12/09 Lab Work Order 091343 Lab Sample ID: 09.3343-01 Sample Matrix: Water ALKALINITY Method: SM2320B Prep Method: Date Prepared: 5/15/O9 Date Analyzed: 5/15/O9 Analytes Total Alkalinity Lab File ID: 122 Method Blank: ?ABU( O3/15/O9 CAS Number Result 383 'Dilution Factor: 1 Lab Fraction ID: 09-3343-01F LQL Units 5,0 mg/L. CaCO3 Method: S?V14500-NH3 D Date Prepared: 5/18/09 Date Analyzed: 5/18/O9 Analytes Ammonia -N AMMONIA -N Prep Method: Lab File I): 13 Method Blank: MBLK O5/18/O9 CAS Number Result 15 Dilution Factor: 1 Lab Fraction ID: O9-3343-01P LQL Units 0.10 mg/L Method: SM5210B Comments: Seed blank subtracted, BIOCHEMICAL OXYGEN DEMAND Prep Method: Date Prepared: 5/13/09 1100 Date Analyzed: 5/18/09 Analytes CAS Number Result Dilution Factor: 1 Lab Fraction ID; O9-3343-01E LQL Units Biochemical Oxygen Demand 859 10.0 ntg/L Method: SMV14500-CN E Date Prepared: 5/15/O9 Date Analyzed; 5/15/O9 Analyzes Total Cyanide TOTAL CYANIDE Prep Method: Lab File ID: 58 Method Blank: MBLK 3/15/09 CAS Number Result 0,024 Dilution Factor: 1 Lab Fraction ID: 09-3343-01R LQL Units 0.010 mg/L. LApproved Qualitler:r l - Atutivte detected in the Lexoeiatetl 4lethud Blud:, value nut subtractod from result E - Extrapolated value. Value exceeds calibration range H • Sampla analysis exceeded analytical holding (info - indicates en estimutedvalue when the t:umpeuud ix detected, but is below the LQL S • Spike Recovery outside accepted limits L • Compound analysed for but not detected X • Stu caso narrative • -Value exceeded the Maximum Contamination Level (MCL), TCLP limit, or U' eompoUnd is undetected, LQL exceeds MCL. Dctuxitluna; NA • Net Applicable LQL - Lower Qua natation Limit Suer - Surrogate Print Date: 5/21/2009 29 -MAY -2009 02:56PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.006/018 F-156 Evergreen Analytical, Inc. 4036 Youngfield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID Client Project ID Date Collected: Date Received: C6 C6 Composite Sample 5/12/09 1500 5/12/09 Lab Work Order 09-3343 Lab Sample ID: 09-3343-0I Sample Matrix: Water Method: Hach 8000 CHEMICAL OXYGEN DEMAND Prep Method; Date Prepared: 5/20/09 Date Analyzed: 5/20/09 Analytes Lab File ID: 49 CAS Number Result Dilution Factor: 20 Lab Fraction ID: 09 3343-U 1G LQL Units Chemical Oxygen Demand 1600 200 ntg/L .---••••• Method: SM2510 B SPECLFIC CONDUCTANCE ® 25°C Prep Method: Date Prepared: 5/14/09 Date Analyzed: 5/14/09 Analytes Specific Conductance Lab File ID: 65 CAS Number Result Dilution Factor: 1 Lab Fraction ID: 09.3343.01F LQL Units 17300 1.00 µtnhos/cm FLUORIDE Method: SM 4500-F C Prep Method: Date Prepared: 5/13/09 Date Analyzed: 5/13/09 Analytes Fluoride Lab File ID: 124 Method Blank: Iv1AI'-K 051309 CAS Number 16984-48-8 Result 0.82 Dilution Factor: 1 Lab Fraction ID: 09-3343-015 LQL Units 0.20 mg/L LA_NGELLER INDEX Method: SM2330B Prep Method: Date Prepared: 5121/09 Date Analyzed: 5/21/09 Analytes Langelier Index CAS Number Result Dilution Factor: 1 Lab Fraction ID: 09-.3343-01F LQL Units + 0.12 Analyst Approved Ctu llilirrs: B - Aualyte dctooted in ih:TIatltod Blank, value not subtracted from resuh. 1i - EalrttpoluTed value. Value exceeds calibration range FI - Sample analysis exceeded analytical holding time I - Indicates an estimated value when the compound is detected, but is below tiro LQL 5 - Spike ft:cav-r'y vutaido uo:.eptcd limits U • Compound analyzed for but not detected X - See case narrative •V:dua exceeded the ivinximum Contamination Level (MCI.), TCLP limit, or ii compound is undetected, LQL elu::ds IvICL. Definitions: NA -Not ApplicAble LQL - Lower Quzniutlien Limit Sus' • surrogate Print Dale! 5/21/2009 29 -MAY -2009 02:56PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.007/018 F -I56 Evergreen Analytical, Inc. 4036 Youngfield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID Client Project ID Date Collected: Date Received: C6 C6 Composite Sample 5/12/09 1500 5/12/09 Method: E150.1 Lab Work Order 09-3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water E150,1 PH Prep Method: Date Prepared: Date Analyzed: Aualytes 5/13/09 5/13/09 0835 CAS Number Result Dilution Factor: 1 Lab Fraction ID: 09-3343-01F LQL Units pH 6.77 1.00 pH Units TOTAL SULFIDE Method: SM 4500-S C/F Prep Method: Date Prepared: 5/19/09 Date Analyzed: 5/19/09 Analytes Lab File ID: 100 Method Blank: MBLK 5/19/09 CAS Number Result Dilution Factor: 1 Lab Fraction 1D: 09-3343-01S LQL Unite Total Sulfide 2.2 0.50 nigh. Method: SM 2540C TOTAL DISSOLVED SOLIDS (TDS) Prep Method: Date Prepared: 5/14/09 Date Analyzed: 5/14/09 Analyses Total Dissolved Solids Lab File D): 71 Method Blank: MBLK 5/14/09 CAS Number Result 12200 Dilution Factor: 1 Lab Fraction ID: 09-3343-01F LQL Units 10,0 nig/L Method: SM 2540 D TOTAL SUSPENDED SOLIDS (TSS) Prep Method: Date Prepared: 5/15/09 Date Analyzed: 5/15/09 Analyzes Lab File YD: 6 Method Blank: MBLK 051509 CAS Number Result Dilution Factor: 1 Lab Fraction ID: 09-3343-01T LQL Units Total Suspended Solids 138 5.0 .mg/L PG, Approved QuaGliers: B - Analyse detecedin1hsiSwcialadMethod Blank, valuenotsubtriaudfromr=salt E - Extrapolated valuo.Vuluc exceeds calibration =me H • Sample analysis exceeded analytical holding time I • Indiotca An taimated value 1O,41111c compound ie detected, but it b,aow the LQL S - Spike Ftwovtry outside accepted Junin U • Compound analyzed for but not detected X • Sc t alst naaati.r: -Value excootl:.t1 iltr 1viaxiinum Conlancination Level (MCL), TCLP limp, or if compound 19 undetected, LQL escectla MCL. Definitions: NA - Not Applicable LQL • Lower Qunttitatinn Lilt Surr • Sttrrog;o Print Date: 5121/2009 FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.008/018 F-156 29 -MAY -2009 02:57PM Evergreen Analytical, Inc. 4036 Yuungfield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample TD Client Project ID Date Collected: Date Received: C6 C6 Composite Siurrple 5/12/09 1500 5/12/09 Method: L•It1Cfl 8146 Lab Work Order 09-3343 Lab Sample ID: 09-3343.01 Sample Matrix: Water DISSOLVED FERROUS IRON Prep Method: Date Prepared: 5/14/09 Date Analyzed: 5/14/09 1245 Antdytcs CAS Number Ferrous iron Result Dilution Factor: 10 Lab Fraction ID: 09-3343-01K LQL Units 11.9 1.0 mJL SULFITE Method: SM 4500-SO3 2- B Comments: This is a field parameter with a 15min holding time. Prep Method: Date Prepared: 5/13/09 Date Analyzed: 5/13/09 1200 Aualytes Sulfite Method Blank: MB -R47157 CAS Number Result Dilution Factor: 1 Lab Fraction TD: 09-3343-01Q LQL Units U 2.0 me/1. TURBIDITY Method: SM 2130 B Prep Method: Date Prepared: 5/14/09 Date Analyzed: 5/14/091015 Analytes Lab File ID: 74 Method Blank: MBLK 05/14/09 CAS Number Result Dilution Factor: 10 Lab Fraction ID: 09-3343-01F LQL Units Turbidity 214 1.0 NTU Analyst Approved Qualifiers: B • Auslyto denoted in titc associated Method Blank, value not evbtn:cled [Run result L• - Extrapolated value,Valua arcade calibration range 11- Sample analysis exceeded :ulalytical holding time T • Jndic=sea art estimated value when the compound iv detected, but is below the LQL S - Spike Recovery outside wo:opted limits U- Compound analyzed fur but not detected X - See case annuli ve * -Value a canned /te Maximum Contamination Level (ItACL), TCLI limit, or if compound is undetected, LQL aaoeaAS MCL. Dtllnitintw: Ni -Not Applivable LQL - Lower Qua:uitution Lirai! Sure • Surrogate Print Date: 5/21/2009 28 -MAY -2009 02:57PM FROM -EVERGREEN ANALYTICAL Evergreen Analytical, Inc. 4036 Youngfield Street, Wbeat Ridge, Colorado 80033-3862 (303)425-6021 3034256854 T-757 P.009/018 F-156 Client Project ID C6 Composite Sample Collection Dale: 5/12/09 Lab Order: 09-3343 Date Received: 5/12/09 Units: mg/L Method: SM 5310 B Lail lb Client ID 09-3343-01O C6 Total Organic Carbon (TOC) Total Organic Carbon Prep Method: Date Date Matrix Prepared Analyzed Results _.LQL DP Water 3/18/09 5/18/09 480 30 50 Comments TOC as NPOC (Non Purgable Organic Carbon) y7it Analyse QuailGess: ! - lodicatcs an estimated value wizen the compound i dawned, but is below Mc LQL fI • Semitic analysis exceeded nnalytictl holding lima U • Compound atmlyccd for bul nob detected X - See cane narrative • - Value exceeds Maximum Cuuiumininioa Lsvc1(MCL), TCLP licit, or if compound is undetected, LQL exceeds MCL. Definitions; DE • Dilution Factor LQL - Lower Quentitation Limit Print Date: 5/19/09 29 -MAY -2009 02:5TPM FROM -EVERGREEN ANALYTICAL 3034256654 T-757 P.010/018 F-156 Evergreen Analytical, Inc. 4036 Youngf cld Street, Wheat Ridge, Colorado 80033.3862 (303) 425-G021 Client Sample ID: Client Project TD: Date Collected: Date Received: C6 C6 Composite Sample 5/12/09 1500 5/12/09 Lab Work Order 09-3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water ANIONS BY IC Method: E300.0 Prep Method: Date Prepared: 5/13/09 Date Analyzed: 5/13/09 1127 Analyzes Nitrate o -Phosphate Sulfate Method Blnnlc: MB 05/13/09 CAS Number 7778-77-0 7778-80-2 Result Dilution Factor: 25 Lab Fraction R): 09-3343-011 LQL Units 119 U U 5.0 mg/L 5.0 mg/L 13 mg/L Date Prepared: 5/13/09 Date Analyzed: 5/13/09 1631 Analytes Bromide Method Blank: MB 05/13/09 CAS Number 7647-15-6 Result 54.0 Dilution Factor: 50 Lab Fraction II): 09-3343-01I LQL Units Date Prepared: 5/13/09 Date Analyzed: 5/13/09 1644 Analyzes Method Blank: MB 05/13/09 CAS Number Result 10 mg(L Dilution Factor: 250 Lab Fraction ID: 09-3343-0.1I LQL Units Chloride Nitrite 7647-14-5 6880 U 130 mg/L 50 mg/1- Analyst Approved Qualifiers: B • Analyze detected in Mc areociated Method Bltutte value not subtracted front result E - Extrapolated value:Value exceeds calibration range H - Sample analysis exceeded tutalytical bolding time I - Indicates an estimated value when the compound in detected, but is below the LQL S - Spike Recovery outside accepted limns U - Compound analyzed for hut not detected X • Sec ease ntumive 4 -Value exceeded the lvkttimum Contltninalion Level (MCL), TCLP limit, or if compound i u undetected, LQL exceeds MCL. Ikibtitiotu: Nr\ • Not Applicable i-QL - Lwver Quaraitution Limit Suer - Surrogate Print Data: 5/14/09 29 -MAY -2009 02:57PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.011/018 F-156 Evergreen Analytical, Inc. 4036 Youngfield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID: C6 Client Project TD: C6 Composite Sample Date Collected: 5/12/09 Date Received: 5/12/09 Lab Work Order: 09.3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water DISSOLVED METALS Method: E200.7, Rev. 4.4 Prep Method: E200.7/S`V3010A Date Prepared: 5/20/09 Date Analyzed: 5/20/09 Lab File ID: 052009AM Method Blank: MB -19197 Analytes CAS Number Iron 7439-39-6 Dilution Factor: 1 Lab Fraction ID: 09-3343-01K Result LQL Units Analyst Approved 26.3 0.0700 me - Qualifiers: 13 • Artnlytc detected In the associated Method Blank, value not subtracted from result Definitions: NA -Nor Applicable - lixtrupolated value.Value exceeds calibration range LQL - (Amer Quuntitntion Limit H • Sample analysis exceeded analytical holding Lime Surr - Surrogate f - Indicates an estimated value when the compound is detected, but is below the LQL S - Spike Recovery outside accepted limits U - Compound analyzed for but not detected X - Net: cave nurrutive -value exceeded the Maximum Contamination Level (MCL), ICU) limit, or if compound is undetected, LQL exceeds MCL, Print Oate: 5/29/2009 29 -MAY -2009 02:58PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.012/016 F -I56 Evergreen Analytical, Inc. 4036 YoungBeld Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID: CO Client Project ID: C6 Composite Sample Date Collected: 5/12/09 Date Received: 5/12/09 Lab Work Order: 09-3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water Method: E200.7, Rev. 4.4 Date Prepared: 5/20/09 Date Analyzed: 5/20/09 Analytes Aluminum Antimony Arsenic Barium Cadmium Calcium Chromium Cobalt Copper Lend Magnesium Manganese Molybdenum Nickel Selenium Silver Thallium Tin Titanium Vanadium Zinc DISSOLVED METALS Prep Method: E200.7/SW3010A Lab File ID: 052009AM Method Blank: MB -19197 CAS Number 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440.5 0.8 7439-92-1 7439.95.4 7439-96-5 7439-98-7 7440-02-0 7782-49-2 7440.2 2.4 7440-28-0 7440.31-5 7440-32-6 7440-62-2 7440-66-6 Dilution Factor; 1 Lab Fraction 1D: 09-3343-01M Result LQL Units 0.133 0.100 mg/L U 0.0250 mg/L U 0.0500 mg/L 0.00200 mg/L U 0.0100 mg/L 197 0.387 mg/I, U 0.0100 mg/L. U 0.00500 mg/L 0.0827 0.00500 mg/L U 0.0730 mg/L 22.8 0.150 mg/L 0.642 0.00500 mg/L 0.0333 0.00500 mg/L U 0.0300 mg/L 0.133 0.100 mg/L U 0.0300 mg/L U 0.100 mg/L U 0.0400 mg/L U 0,0100 mg/I.. U 0,0100 mg/L lJ 0.0300 mg/L Silicon as SiO2(Silicz.) 7440.21-3 50.9 0.107 tng/L Analyst Approved tl,utliticrs: B - Analyze detected in the associated Method Blank. value not subtracted from result 12 - Extrapolated va lue.Value exceeds calibration range 1i - Sample analysis exceeded analytical holding time .1 - Indicates an estimated value when the compound is detected. but is below die LQL S • Spih. Recovery nutcidc =opted fimia.. U - Compound analyzed Cur but not dcteCted X - See case narrative * -Value exeudcd the Maximum Contamination Level (MCL),'I CLI' limit, or ii compound is undetected, LQL exceeds MCL. Definitions; NA - Not Applicable LQL - Lower Qaantitation Limit Surr - Surrogate Print Date: 5/29/2009 29 -MAY -2009 02:58PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.013/018 F-156 Evergreen Analytical, Inc. 4036 Youngtseld Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID: C6 Client Project ID: C6 Composite Sample Date Collected: 5/12/09 Date Received: 5/12/09 Lab Work Order: 09-3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water DISSOLVED METALS Method: E200.7, Rev. 4.4 Prep Method: E200.7/SW3010A Date Prepared: 5/20/09 Date Analyzed: 5/22/09 Ann lytes Beryllium Boron Potassium Sodium Date Prepared: 5/20/09 Dale Analyzed: 5/23/09 Analyzes Lithium Strontium Analyst Lab File YD: 052209AM Method Blank; MB -19197 CAS Number 7440-41-7 7440.42-8 7440-09-7 7440.23.5 Dilution Factor: 10 Lab Fraction ID: 09-3343-01M Result LQL Units U 0.00450 mg/I, 11.6 0.200 mg/L 998 3.40 mg/L 3590 4.00 nab/L Lab File ID: 052209AM Method Blank: MB -19197 CAS Number Result 7439-93-2 7440-24-6 3.02 23.4 Dilution Factor: 10 Lab Fraction ID: 09-3343-01M LQL Units 0.0200 mg/L 0.00500 mg/L Jee7/ Approved Qualincrs: Li -Analyze delectcd in the assoclated Method Ellen}:, value not subtracted from exult - Extrapolated value. Value excccd5 calibration range H - Sample analysis exceeded analytical holding time .1 - Indicates an estinuued value when the compound is detected, hut is below the 1.01. ti - Spike Recovery outside acceprad liaatF U - Compound nnulyied For hut not detected X - 5a case narrative -Value exceeded the Maximum Contamination Level (MCL), TCLI' limit, or iC ;Niemand is undetected. LQL exceeds MCI.. Definitions: NA - Not Applicable I.nwcr Qunntit Lion Limit Slur - Surrogate Print Date: 5/29/2009 29 -MAY -2009 02:58PM FROM -EVERGREEN ANALYTICAL 3034256854 1-757 P.014/019 F-156 Evergreen Analytical, Inc. 4036 Youngfield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID: C6 Client Preject ID: C6 Composite Sample Date Collected: 5/12/09 Date Received: 5/12/09 Lab Work Order: 09-3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water Method: E200.7, Rev. 4.4 Date Prepared: 5/14/09 Date Analyzed: 5/15/09 Ana lytes Aluminum Antimony Arsenic Barium Boron Cadmium Calcium Chromium Cobalt Copper Lead Magnesium Manganese Molybdenum Nickel Selenium Silver Thallium Tin titanium Vanadium Zinc TOTAL METALS Prep Method: E200.7, Rev. 4.4 Lab File ID: O515O9AM Method Blank: MB -19145 CAS Number Result 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440.42-8 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92.1 7439-954 7439-96-5 7439-98-7 7440-02-0 7782-49-2 7440-22-4 7440-28-0 7440-31-5 7440-32-6 7440-62-2 7440-66-6 Dilution Factor: 1 Lab Fraction ID: 09-3343-01L LQL Units 0.273 0.100 mg/L U 0.0250 mg/L U 0.0500 mg/L 3.42 0.00200 mg/L 9.79 0.0200 mg/L U 0.0100 mg/L 199 0.387 mg/L U 0.0100 mg/L 0.00509 0.00500 mg/L 0.776 0.00500 mg/L 1J 0.0730 rng/L 23.0 0.150 mg/L 0.671 0.00500 mg/L 0.0373 0.00500 mg/L U 0.0300 mg/L 0.208 0.100 rng/L U 0.0300 mg/L U 0.100 mg/L U 0.0400 mg/L U 0.0100 mg/L U 0.0100 mg/L 0.0828 0.0300 mg/L Analyst Qualifiers: 13 - Anulyte deteeied iu the assaciated Method Blank, vulue nut subtracted from result 1: - Extrapolated vnitte,Vnluc cscccds calibration range 11- Sample analysis exceeded analytical holding dine l - indicate: an etirnated value when the compound is detected, but is below the LQL ti - Spike Recovery outside accepted limits tl - Cnmpnumd analyzed for but not dcrecre(1 X • 54d case narrative -Value exceeded the Maximum Contamination Level (IvMCL), TCLP limit; or it' compound is undetected, LQL exceeds MCL. Approve Delinitiuns: NA -Not Applicable Lower Quuntitution Limit Surr - Surrogate Print Date: 5/29/2009 29 -MAY -2008 02:58PM FROM -EVERGREEN ANALYTICAL 3034256854 T-757 P.015/018 F -I56 Evergreen Analytical, Inc. 4036 Youngfield Street, Wheat Ridge, Colorado 80033-3862 (303)425-6021 Client Sample ID: C6 Client Project ID: C6 Composite Sample Date Collected: 5/12/09 Date Received: 5/12/09 Lab Work Order: 09-3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water TOTAL METALS Method: E200.7, Rev. 4.4 Prep Method: E200.7, Rev. 4.4 Date Prepared: 5/14/09 Date Analyzed: 5/18/09 Analytes Lithium Strontium Date Prepared: 5/14/09 Date Analyzed: 5/16/09 Analytes Potassium Sodium Date Prepared: 5/14/09 Date Analyzed: 5/22/09 Analytes Beryllium Lab File ID: 051709AM Method Blank: IvIB-19145 CAS Number 7439.93-2 7440-24-6 Lab File ID: 051609AM Method Blank: MB -19145 CAS Number 7440-09-7 7440-23-5 • Dilution Factor: I Lab Fraction ID: 09-3343-01L Result 3.79 U LQL Units 0.00200 me./L 0.000500 me/L. Dilution Factor; 10 Lab Fraction ID: 09-3343-01L Result LQL 917 3.40 3440 4.00 Lab File ID: 052209AM Method Blank: MB -19145 CAS Number 7440-41-7 Result Units mg/L mg/L Dilution Factor: 10 Lab Fraction ID: 09-3343-011. LQL Units U 0.00450 mg/L Method: E245.1 Date Prepared: 5/18/09 Date Analyzed: 5/19/09 Analytcs Mercury MERCURY, DISSOLVED Prep Method: E245.I Lab File ID: 51909 Method Blank: MB -19178 CAS Number 7439-97-6 Analyst Result 0.000112 Dilution Factor: 1 Lab Fraction ID: 09-3343-0IM LQL Units 0.000100 mg/L Qualifiers: R - Analytc detected In the associated Ivtcthod Blank, value not subtracted 110iii result - Extrapolated valuc.Valuc exceeds calibration range I.1 -Sample analysis exceeded analytical holding time - Indicates an estimated value when the compound is detected, hut Is below the LQI. S • spike Recovery outside accepted limits li - Compound analyzed for but not detected X - See ctl5e narrative • -Value exceeded the Maximum Contamination Level (MCL), TCLP limit, or if compound is undetected. LQL exceeds MCL. Approved Dcfinitiuns: NA - Nor Applicable L01_ - Lower Quantitncinn Lint tiurt - Surrogate Print Date: 5/29/2009 29 -MAY -2000 0Z:58PM FROM -EVERGREEN ANALYTICAL Client Sample ID: Client Project ID: Date Collected: Date Received: 3034256854 Evergreen Analytical, Inc. 4036 YoungfteId Street, Wheat Ridge, Colorado 80033-3862 (303)425-6021 C6 C6 Composite Sample 5/12/09 5/12/09 T-757 P.016/018 F-156 Lab Work Order: 09-3343 Lab Sample ID: 09-3343-01 Sample Matrix: Water Method: E245.1 Date Prepared: 5/18/09 Date Analyzed: 5/19/09 Analytes Mercury MERCURY, TOTAL Prep Method: E245.J Lab File ID: 51909 Method Blank: MB -19178 CAS Number 7439-97-6 Result Dilution Factor: 1 Lab Fraction ID: 09 -3343 -OIL LQL Units xeS" U _ _ Analyst_ Qualifiers; 3 - Annlyle detected in the mnciated Method f3lank, value not subtracted firm result C • Extrapolated valuc.Valuc exceeds calibration range II • Sample analysis exceeded analytical holding time - Indicates nn estimated value when the compound is detected, but is below the LQL S - Spike Recovery outside accepted limits U - Compound analyzed for but eat detected X - Sec case narrative • -Value exceeded the Maximum Comminution Level (MCL), TCL1' limit, or if compound is undetected, LQL exceeds MCL 0.000100 mg/L Approved Definiriony: NA - Nnt Appticnble LQL. - Lower Quantization Limit Surr - Surrogate Print Date: 512912009 29 -MAY -2009 02:59PM FROM -EVERGREEN ANALYTICAL 3034256854 7-757 P.017/018 F-156 Evergreen Analytical, Inc. 4036 Youngield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID; Client Project JD; Date Collected; Date Received: Date Prepared: Date Analyzed: Percent Moisture C6 C6 Composite Sample 5/12/2009 5/12/2009 5/20/2009 5/20/2009 NA Lab Work Order Lab Sample ID: Sample Matrix: Lab File ID: Method Blank: Prep Factor: Dilution Factor: 09-3343 09-3343-01O Water 5V00481.D 1v035052009 -W 1.000 50.00 Method: SW826013 Prep Method: SW5030B Analytes VOLATILE ORGANICS CAS Number Result Units: µg/L LQL Acetone Benzene Bromodichloromethane Bromoform Bromomethane 67-64-1 71-43-2 75.27-4 75-25-2 74.83-9 8800 2400 U U U 500 50 100 200 200 2-Butanone Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromelhanc l,2-Dichlorobenzene 78-93-3 75-15-0 56-23.5 108-90-7 75-00.3 110-75-8 67-66-3 74-87-3 124-48.1 95.50-1 1,3-Dichlorobenzene 541-73-1 1,4-Diclilorobenzene 10646-7 1,1-Dichloroethane 75-34.3 1,2-Dichloroethane 107-06-2 1 1 _Dichloroetltene 75-35-4 cis-1,2-Dichloroetheue 156-59-2 trans-1,2-Dichloraethene 156-60-5 1,2-Dichloropropane 78-87-5 cis-1,3-Dichloropropenc 10061-01-5 trans-1,3-Dichloropropene - 10061-02-6 Elhylbenzene 100-41-4 `tr Analyst U U U U U U U U U U U U U 71 J U U 0 U U U 150 250 100 100 100 200 200 100 200 100 100 100 100 100 100 100 100 100 100 100 100 100 Approved Qualifiers: Sec the ciuc narrative for n discussion B - Analyte detected in the Method Blank, value not subtracted front result E . Extrapolated value.\Jalua exceeds calibration range tI - Prep or Analytical holding time exceeded S - Spike Recovery outside nec:ptance limits X - See case narrative ' -Value exceeded the Maximum Contamination Level (MCL), TCLP limit, or if compound is undetected. LQL exceeds MCL. Qualifiers: U - Analyse not detected at or above the reponing limit I • Estimated value below the LQL Definitions: NA- Not Applicable LQL - Luwco Quantttot:on Limit MDL- Method Detection Limit Starr - Surrogate Standard Print Date: 5/2612009 29 -MAY -2009 02:59PM FROM -EVERGREEN ANALYTICAL 3034256854 7-757 P.018/018 F-156 Evergreen Analytical, Inc. 4036 Youngfield Street, Wheat Ridge, Colorado 80033-3862 (303) 425-6021 Client Sample ID: Client Project ID: Date Collected: Date Received: Date Prepared: Date Analyzed; Percent Moisture C6 C6 Composite Sample 5/12/2009 5/12/2009 5/20/2009 5/20/2009 NA Lab Work Order Lab Sample ID: Sample Matrix: Lab File JD: Method Blank: Prep Factor: Dilution Factor: 09-3343 09-3313.01O Water 51/00481.D MB5052009-W 1.000 50.00 Method: SW8260B Prep Method: SW5030B Analytes 2-1-Texanone Methylene chloride 4-Methyl-2-pentanonc Styrene 1,1-2.2 Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloraethane 1,1,2-Trichloroethane Trichloroethene Vinyl acetate Vinyl chloride Xylcne, Total VOLATILE ORGANICS CAS Number 591-78-6 75-09-2 108-10-1 100-42.5 79.34-5 127.18-4 108-88-3 71-55-6 79-00-5 79.01.6 108-05-4 75-0I-4 1330-20-7 Result U U U U U U 4100 U 130 U Units: }tg/L LQL U U 2800 100 250 100 200 100 100 100 100 100 100 200 100 200 Surr: 1,2-Diehloroelhane-d4 Surr: 4-Bromolluorobenzeae Surr: Toluene -d8 17060-07-0 460-00.4 2037-26-5 93 QC Limits. 70-130 °AtREC 96 QC Limits; 70-130 %REC 105 QC Limits; 70-I30 %REC Analyst Qualifiers: See the case narrative for a discussion B - Antdyte detected in the Method Blank, value not subtracted from result E - Extrapolated v:due,Value exceeds calibration tango H • Prep or Analytical holding time exceeded S • Spike Recovery outride acceptance limits X • Sec ease narrative * -Value exceeded the Maximum Contamination Level (MvfCL), TCLP limit, or if compound is undetected, LQL exceeds MCL. Qualifiers: U - Annlyte not detected at or above the reporting limit J • Estimated value below the LQL Definitions: NA.- Not Applie.tble LQL - Lower Quandtadoa Limit MDL • Method Detection Limit Sur-- Surrogate Standard Print Date: 5/202009 Si1B3N19N39NLLViSNOO O31VNOddOONI 9NIN33NION3 � 1J3NOId ate. 196L -R6-0091 area,00 A0 �tl31x30 x011YO11IiW 11lil 1•W PEYGO CV 3�WB6,�1 K3fICN401.o7z • coz NYId ONIOYNO V U 111OAY1 TV3A0 NSOd51Q 153lN7N07 • 9 0� DEPARTMENT OF PLANNING SERVICES Greeley Planning Office 918 Tenth Street Greeley, Colorado 80631 WEBSITE: www.co.weld.co.us E-MAIL: kogle@co.weld.co.us PHONE (970) 353-6100, EXT. 3549 FAX (970) 304-6498 February 24, 2010 Mr. Dale Butcher Conquest Oil Company 8207 W. 20th Street, Suite B Greeley, CO 80634 Subject: Conquest C-6, Platteville Facility, USR-1604 Dear Dale: The Department of Planning Services has reviewed your request, undated letter received shortly after the January 27, 2010 meeting with staff, to commence the commercial recycling component of the previously permitted Special Use Permit for a Class II Oilfield Waste Disposal Facility, specifically a Saltwater Injection Facility. Concerns were raised internally on the oversight of the two activities, specifically the oversight by the Colorado Oil and Gas Conservation Commission and for the recycling component, the Colorado Department of Public Health and Environment. While these concerns were aired and discussed at length, it is the determination of this office, for this specific facility, an amendment to the existing Special Use Permit No. USR-1604 will not be required. This determination is based on the following criteria: The Development Standards associated with USR-1604 must be adhered to at all times, including but not limited to: USR-1604 Development Standard #3. The facility shall be constructed and operated to ensure that contamination of soil and groundwater does not occur. (Department of Public Health and Environment) USR-1604 Development Standard #4. A manager, knowledgeable in operating an injection well, and water recycling facility shall be on site when the facility is receiving waste or processing water. (Department of Public Health and Environment) USR-1604 Development Standard #23. Access to the site shall be from County Road 39. The designated haul route shall be on County Road with the agreement 1 mile north on County Road 39 and extending 1 mile east on County Road 28. Transport trucks weighing up to 40 tons will visit the site approximately 60-70 times daily and less on weekends. (Department of Public Works) USR-1604 Development Standard #28. Hours of operation, acceptance of waste water, are limited to 7:00AM until 10:00PM daily as stated in the application materials. (Department of Planning Services) It is the understanding of this office that the one-year pilot project was installed in a temporary condition therefore appropriate building permits will be required. Please contact this office for the appropriate permits. Given the temporary condition of installation, this office requests additional information on the secondary containment proposed for the "Recycling Facility Tanks" and also for the slightly elevated tanks associated —O2D/e) /L /Jny with the "Cleaned Water" component. The undated Conquest Oil Letter, Butcher to Jiricek states "[a]ll appropriate areas will be bermed with liners." Building Condition 5.F from USR-1604 speaks to the stipulated construction method and form. "A concrete secondary containment structure (floor and walls) surrounding each tank or battery of tanks shall be constructed. The volume retained by the structure shall be 150% greater than the volume of the largest tank inside the structure. A registered professional engineer shall design the structure. The structure shall prevent any release from the tank system from reaching land or waters outside of the containment area. The operator shall provide evidence from the engineer to the Weld County Department of Public Health and Environment and Planning Services that the structure has been constructed to meet this criterion." (Department of Public Health and Environment) Staff understands that there are seven Polyethylene Mixing Tanks having the following capacity: (1) 10 Bbl tank, (5) 60 Bbl tank and (1) 160 Bbl tank, one filter system and associated piping. This configuration is set up to address the recycling component of the facility. The Storage Tank configuration is for six tanks of unknown size and dimension. The undated letter states the entire recycling facility will be housed in an eighty (80) by twenty-six (26) fabric enclosure. The Department of Building Inspection requests additional information concerning this structure, specific to the construction type, method of installation, utility components, and structural integrity for wind and snow loads. The Department of Planning Services is on record that should there be any modifications to the components associated with this facility including, but not limited to, site or structural modifications, i.e., new on -site activities or expansion of on -site structures, including the tank farm, to the existing approved operations be requested, an amendment to the original permit may be required. In an effort to bring this commercial recycling component on-line, the Department of Planning Services requests an updated drawing for USR-1604 with the new recycling facility and injection well facility delineated, including site circulation, location of all existing improvements and the Development Standards to be submitted to this office for recording prior to Monday March 15, 2010. Staff requests one additional Note be placed on the plat stating "The Water Recycling Component associated with the Class II Oilfield Waste Disposal Facility— Saltwater Injection Facility, was administratively approved by the Department of Planning Services in February 2010, as there is not any changes to the existing Development Standards." Finally, this office requests a letter of approval from the Platteville-Gilcrest Fire Protection District stipulating that all concerns have been reviewed, addressed and approved. (Department of Building Inspection/ Platteville-Gilcrest Fire Protection District) Should you have additional questions or require clarification on any of the points presented herein, please contact this office. Thank you for your inquiry. Sincerely, Kim Ogle Planning Services ec: T. Jiricek, Director K. Swanson, Building D. Bauer, Public 'Works Building Inspection File: USR-1604 Properly research 30-3-65 caNWT 8207 W. 20th Street Greeley, CO 80634 970.356.0023 Trevor Jiricek Director Planning and Building Department 918 10th Street Greeley, CO 80631 RE: Weld County USR Permit 1604, Conquest Water Services Dear Mr. Jiricek: As you and the Board of County Commissioners know, Conquest Water Services (Marcum Midstream 1995-2 Business Trust) has developed a water recycling process for the oil and gas industry in Weld County. The County Commissioners approved a one-year pilot project at the referenced location in June of 2009. In August of 2009 a three week field test of the process was successfully performed. For periods of up to eight hours, the pilot was operated at a rate of up to 7,000 barrels of recycled water per day. During and after the test period, Conquest worked closely with the Colorado Oil and Gas Conservation Commission (COGCC) , the Colorado Department of Public Health and Environment (CDPHE), and the Weld County Department of Public Health and Environment, to determine the proper regulatory agencies to oversee the recycling activity. It has been determined that the CDPHE, Solid Waste Division, will be the regulatory agency to adjudicate our recycling efforts. After a thorough regulatory review, in early January of 2010, the CDPHE notified us that we are now an approved recycling facility, falling under Section 8 of the Solid Waste and Facilities Act, Title 30, Article 20, Part 1, C.R.S 6 CCR 1007-2. Please find attached, a copy of the CDPHE approval letter (Attachment A). In addition, Kim Ogle has informed us that the Weld County Attorney has determined that we may sell the water under the existing USR. Within a few weeks Conquest will be ready to sell the recycled water and a long time disposal customer has agreed to buy it. The issue now is what County regulatory approval is necessary to allow the operation to continue after the pilot project time frame has passed. To bring our recycling effort to a commercial application Conquest will add six frac tanks, similar to those utilized in the stimulation of an oil and gas wellbore, and enclose the recycling operation to keep the water from freezing in the winter. We intend to use a fabric structure for the enclosure and slightly elevated tanks to hold the cleaned water for delivery to the purchasers. All appropriate areas will be bermed with liners. Please find attached, schematics (Attachment B), and a photograph (Attachment C) of the additions. -1- caltsr 8207 W. 20th Street Greeley, CO 80634 970.356.0023 We believe that these changes should be considered minor and not require an amendment to the existing USR for the following reasons: 1) Water received at the facility will not change as to source or quantity. We are recycling water that otherwise would have been pumped down the injection well. 2) The number of truck trips to and from the facility will remain within that allowed by the existing USR. 3) Traffic patterns within the facility will not change. 4) The intensity of the activity at the property will not exceed that currently allowed by the USR. 5) Tank volumes inside the recycling facility approximate a 5.6 percent volume increase to existing disposal tank volumes. 6) The general nature of the business has not changed. The facility's purpose has been, and will remain, that of handling water. In addition, the recycling process will be very beneficial to the County in general as it will reduce the amount of potable water used by the oil and gas industry within the County. Recycling will also reduce the number of miles driven by large water trucks within the County. We are excited about the project and want to work to avoid any delays or interruptions in providing the product to our customers. Please let me know what else we can provide to you and the Commissioners to assist in making this decision. Sincerely, tL Dale Butcher President Marcum Midstream 1995-2 Business Trust CC: Troy Swaim, Weld County Department of Public Health and Environment ATTACHMENTS: (A) CDPHE Approval Letter for Section 8 Recycling Facility (B) Schematic of Recycling Facility Additions (C) Photograph of Recycling Facility Additions -2- ATTACHMENT (A) CDPHE Approval Letter for Section 8 Recycling Facility STATE OF COLORADO Bill Ritter, Jr., Governor Martha E. Rudolph, Executive Director Dedicated to protecting and improving the health and environment of the people of Colorado 4300 Cherry Creek Dr. S. Denver. Colorado 80246-1530 Phone (303) 692-2000 T0D Line (303) 691-7700 Located in Glendale, Colorado http.//www.cdphestate.co.us January 6, 2010 Laboratory Services Division 8100 Lowry Blvd. Denver, Colorado 80230-6928 (303) 692-3090 Ted Pagano Senior Engineering Consultant Conquest Oil Company 8207 W. 20th Street Greeley, CO 80634 Dear Mr, Pagano, Colorado Department of Public Health and Environment The Colorado Department of Public Health and Environment, Hazardous Materials and Solid Waste Management Division (the "Division") appreciates the opportunity to review your summary of the proposed water treatment and recycling plan and the Spill Prevention Control and Countermeasure Plan for the Conquest Oil Company ("Conquest") exploration and production produced water ("produced water") recycling facility in Weld County. The proposed produced water recycling facility diverts water from the current oil and gas production water injection well at the Conquest facility at 13159 WCR 39 in Platteville, CO. Produced water is diverted from the injection process to a series of tanks that remove solids and other contaminants, creating a quality of water acceptable for reuse in oil and gas drilling operations. On October 5, 2009 Conquest Oil gave a presentation outlining the proposed produced water recycling services at the Division office. Following the presentation, the division requested the following items: • SPCC Plan • Engineered drawings showing underground piping, and leak detection systems • Drawings of secondary containment with volume calculations • Document how the facility will maintain a 75% recycling rate • Document the closure process for the facility, including; o Process for removing waste and equipment from the site o Process for notifying customers of facility closure On November 12, 2009 the Division received the Project Booklet that addressed each of the items above. After reviewing the submittals, on December 8, the Division notified Conquest of the following concerns: • The containment area for the recycling tanks differed on two diagrams, • The Division was not on the emergency Notification List of the SPCC plan, • The plan did not include a diagram of the bermed containment area The Division received an addendum to the project booklet correcting the containment area size discrepancy on December 9. On December 18, Conquest submitted the updated SPCC plan with the Division listed as a contact in the emergency Notification List, and the containment berm diagram with an engineer inspection letter. The berm diagram and description were consistent with the description in the SPCC plan. After a review of your plans, the Division has concluded that Conquest's proposed produced water recycling operations arc subject to Section 8 of the Solid Wastes Disposal Sites and Facilities Act, Title 30, Article 20, Part 1, C.R.S., as amended, Regulations Pertaining to Solid Waste Sites and Facilities, 6 CCR 1007-2. Conquest must meet any local requirements prior to commencing recycling operations. Conquest submitted the Division recycling registration with the initial project booklet. Conquest must also submit, by May 1 of each calendar year, the Recycling Facility Reporting Form which can be found at: http://www.cdphe.state.co.us/hm/forms/recycl ingformstandard.pdf. It has been a pleasure to work with Conquest Oil on this project, and I would encourage you to contact me at (303) 692-3425, or david.snapp@state.co.us if you have any questions. Sincerely, David Snapp Solid Waste and Materials Management Unit Solid and Hazardous Waste Program CC: Doug Ikenberry, HMWMD Jerry Henderson, HMWMD Wolfgang Kray, HMWMD Troy Swain, Weld County Trim: SW/WLD/CON 3.4 ATTACHMENT (B) Schematic(s) of Recycling Facility Additions C6 F.duly SOn PP Recycling Facility in Blue gre rY ra Web= Utica( Bullring SCHEMATIC 1. THE C6 FACILITY WITH RECYCLING FACILITY ADDITIONS. The entire recycling facility will be housed in a 80' by 26' fabric enclosure. The recycling facility secondary containment will measure 92' by 36', encircling the building. Traffic Flow will not change, utilizing the existing loading pad, existing USR Traffic Flow patterns, and will remain well within USR Traffic volume constraints. -5 Into Existing Handling Facility Unloading Bay SCHEMATIC 2. RECYCLING FACILITY ADDITIONS. Shown in Blue. Recycling Facility in Blue Solids to Landfill 92' Liner and Dyke Filter 6" Line Poly 160 6 60 Dual Containment Chemical totes 6Line 60 6" Line 10 6"one I 2" Drain Line doo Shower/Eye Week 2" Drain Line to Existing Process • To Deep Well Injection V To Re -Use To Treatment From Clean Tank Supply / N Existing Facility Recycling Addition Nos. denote Tank Capacity in Bbls SCHEMATIC 3. TANK CONFIGURATION OF RECYCLING FACILITY; SHOWING SECONDARY CONTAINMENT. The entire recycling facility will be housed in a 80' by 26' fabric enclosure. The recycling facility secondary containment will measure 92' by 36', encircling the building. -7 KR', KIIJ4 sc.,. I. • I0• — - „M SLL11:N.A • A' DAL[ I'•IA Ursa] 1'-t „A. ,1 _. Y _._.— E, q q IA A) SIC Tip. B -B' SEALE. IM S I. t. fA M tINIAINALNT *EA IS CO S1p,CILO n f1AVAf.,r6 q.t AAv iM1f914. 2 UMW AKA IS LIKE WI„1 COM,MaA eta MIL A .5•'C LIVEN. 1 LOEA IS A SNMrir SKL, 0, N AS,10 IN 0000 fOM71 TEEN. MI SCAMS A. A,A,AOM]WIL'., r -r 0, AOAOP.SL MAE AL.M PUKKA 5'.15 IML UKR. . Sr, 0, cc C 4 9 ap s e I A SCHEMATIC 4. DRAWING AND INSPECTION OF FACILITY SECONDARY CONTAINMENT. Verification that the existing containment has been built, measures, 92' x 32', and is in good condition. -8- ATTACHMENT (C) Photograph of Recycling Facility Additions -9- PHOTOGRAPH 1. RECYCLING FACILITY TANKS. Tanks are high -density poly -ethylene tag tanks;' the same as those used for agricultural purposes through -out Weld County. - 10 - Kim Ogle From: Sent: To: Subject: jim goddard [limgoddardl@yahoo.com] Tuesday, February 02, 2010 10:09 AM Kim Ogle FW: Water Recycling Operation Jim Goddard Conquest Water Services General Manager 970-381-5005 jimgoddardl@yahoo.com 8207 W. 20th Street Suite B Greeley, Colorado 80634 --- On Tue, 2/2/10, Theodore A. Pagano, P.E., P.G. <theodorepagano a�yahoo.com> wrote: From: Theodore A. Pagano, P.E., P.G. <theodorepagano@yahoo.com> Subject: FW: Water Recycling Operation To: "'jim goddard"' <jimgoddardl@yahoo.com>, bruce@conquestcompanies.com, "'Dale Butcher' <dalebutche@ Date: Tuesday, February 2, 2010, 8:59 AM From: Trevor Jiricek [mailto: tjiricek@co.weld.co.us Sent: Tuesday, September 15, 2009 2:45 PM To: Bruce White (bruce@conquestcompanies.com) Cc: Barbara Kirkmeyer; theodorepagano@yahoo.com; Troy Swain Subject: Water Recycling Operation Bruce, I finally spoke with Debbie Baldwin at the COGCC today. I also just rec'd a copy of an email that was sent to Ted Pagano that your water recycling operation doesn't fall under the COGCC's authority. It indicates that the operation falls under I Authority, more specifically the "Recycling" regulations of the CDPHE. For your info, the below statute (30-20-102) is the reference that exempts facilities from being solid waste facilities but s of the state Solid Waste regulations as this is the section that pertains to Recycling. Note the second to last sentence of need to demonstrate to the CDPHE that your operation won't contaminate groundwater or create odors. In the past thi: 1 through the submittal of a detailed Design and Operations plan. I suggest you contact Charles Johnson and discuss your operation with him. We would be glad to meet with you if you'd This is the link to the Recycling Regs — see Section 8. (http://www.cdphe.state.co.us/regulations/solidwaste/100702pa rt1S W Regs.pdf). 30-20-102. Unlawful to operate site and facility without certificate of designation - exceptions. (5) Any site and facility operated for the purpose of processing, reclaiming, or recycling recyclable materials shall not be considered a solid wastes disposal site and facility and shall not require a certificate of designation as a solid wastes disposal site and facility; except that, after an initial accumulation period specified by rule, such a site or facility shall maintain documentation that proves recyclable materials are being recycled at the site at a rate that approximately equals the rate at which recyclable materials are being collected. The solid and hazardous waste commission shall promulgate rules to specify what time periods and volumes of recyclable materials constitute operations that qualify for this exemption and to define what materials shall be deemed to be recyclable materials for the purposes of this subsection (5); except that such rules shall not define the term "recyclable materials" to include materials that are likely to contaminate ground water or create off -site odors as a result of processing, reclaiming, recycling, or storage prior to recycling. This subsection (5) does not apply to activities regulated under section 25-8-205 (1) (e), C.R.S. Trevor Jiricek Director Environmental Health Services Weld County Department of Public Health & Environment 1555 North 17th Avenue Greeley , Colorado 80631 Email: tjiricek@co.weld.co.us Office #: 970-304-6415 970-304-6415, Extension 2214 Fax #: 970-304-6411 2 al\ntiksr 8207 W. 20'h Street Greeley, CO 80634 Mr. David Dillon Engineering Manager State of Colorado Oil and Gas Conservation Commission 1120 Lincoln Street, Suite 801 Denver , Colorado 80203 August 10, 2009 RE: Conquest Oil Company, Industrial Re-Use/Recycle Water Project as defined by Colorado Oil and Gas Commission ("COGCC") Rule 907(a)(3) at COGCC Facility ID No. 159193 Dear Mr. Dillon: Please find attached, as per Colorado Oil and Gas Conservation Commission Rule 907(a), a Form 4 Sundry Notice requesting permission to treat and condition Class II UIC Exploration and Production Waste for the purpose of Exploration and Production water re -use and recycling. Also attached for your information and as an addendum to COGCC Facility ID No. 159193, please find an operating summary of the conditioning and treatment processes proposed at the COGCC Facility ID No. 159193 Facility. Please do not hesitate to contact me at (970) 590-3944 for additional information. I highly appreciate your time and effort. Sincerely, Ted Pagano, P.E., P.G. Senior Engineering Consultant Attachments: Form 4 Sundry Notice, Operating Summary Page 1 FORM State of Colorado aev iGo5 Oil and Gas Conservation Commission 1120 Lincoln Sleet, Suite Bat,Denm, ComadoWIDJ Phone. 1303)694-2100 Fax003)8n4-2 SUNDRY NOTICE Submit original plus one copy. This form Is to be used for general, technical and environmental sundry Information. For proposed or completed operations, describe in full on Technical Information Page (Page 2 of this form.) Identify well or other facility by API Number or by OGCC Facility ID. Operator shall send an informational copy of all sundry notices for wells located in High Density Areas to the Local Government Designee (Rule 603b.) 1.OGCC Operator Number 19170 2. Name of Operator: Conquest Oil Company 3. Address: 8207 W. 20th SL, Suite B City'. Greeley State'. CO ZIP'. 80634 API Number OS 123-26004 4. Contact Name Theodore Pagano Phone: 910-590-3944 Fax: 910-356-5563 Complete the Attachment Checklist OP OGCC OGCC Facility ID Number 159193 Survey PI Directional Survey Surface Eqpmt Diagr Technical Info Page Other 6. WeIVFacility Name: Conquest SWD 7. Well/Facility Number 1-30 (C-6) 8. Location (OtrOtr, Sec, Twp, Rng, Meridian)'. SE SE 30-T3N-R6SW 9, County: Weld 11, Federal, Indian or Slate Lease Number N/A 10. Field Name: attenberq 90150 General Notice CHANGE OF LOCATION: Attach New Survey Plat Change of Surface Footage from Exterior Section Lines: Change of Surface Footage to Exterior Section Lines: Change of Bottomhole Footage from Exterior Section Lines: Change of Bottomhole Footage to Exterior Section Lines: Bottomhole location Otr/Otr, Sac, Twp, Rng, Mer (a change of surface gtrlgtr is substantive FNUFSL ❑ and requires a new permit) FELIFWL anach direa:nnat survey bldg, public rd, utility or RR Latitude Distance to nearest property line Distance to nearest in a High consuhation Longitude Distance to nearest lease line Is location Density Area (Me 603b)? veswol Ground Elevation Distance to nearest well same formation Surface owner data: taP5 DAIA: Date of Measurement PROP Reading Instrument Oparatofs Name CHANGE SPACING UNIT Formation Formation Code Spacing order number Unit Acreage unit configuration ❑Remove from surface bond Signed surface use agreement attached OF OPERATOR (prior to drilling): Pave Date. Pave Date: CHANGE WELL NAME NUMBER mm Pon Plugging Bond: O Blanket ll Individual To: Effective Date: ABANDONED LOCATION: Was location ever built? Yes No Is site ready for Inspection? Yes No Date Ready for Inspector:MIT NOTICE OF CONTINUED SHUT ae well shut in or temporarily abandoned'. Has Production Equipment been removed required ifshut in longer than two IN STATUS from site? ri Yes .No years. Date of lastMIT SPUD DATE: REQUEST FOR CONFIDENTIAL STATUS lo axis from date casing set) . SUBSEQUENT REPORT OF STAGE, SQUEEZE OR REMEDIAL CEMENT WORK 'submitcbl and cement job summanes volume Cement top Cement bottom Date Method used Cementing tool setting/ped depth Cement I—IRECLAMATION: Attach technical page describing final reclamation Ina reclamation will commence on approximately procedures per Rule 1004. is completed and site is ready for inspection. ■ Final reclamation Technical Engineering/Environmental Notice f]Notice of Intent Approximate Start Date: r1Report of Work Done Date Work Completed'. its of work must be described in lull on Technical Information Page (Page 2 must be submitted.) 1.-i Intent to Recomplete (submit form 2) Charge Drilling Plans nGross Interval Changed? nCasing/Cementing Program Change r Request to Vent or Flare DEW' Waste Disposal Repair Well cBeneticial Reuse of E&P Waste Rule 502 variance requested nStalus Update/Change of Remediation Plans I7Other: Water Recycle Project Plan for Spills and Releases I hereby certify that the statements made in this form am, to the best of my knowledge, true, correct and complete. Signed: Date' 8/10/2009 Email. ted@conquesicompanies.com Print Name'. Theodore Pagano, P.E., P.G. Title. Consultant COGCC Approved'. CONDITIONS OF APPROVAL, IF ANY: Title'. Date: FORM 4 Page 2 State of Colorado Oil and Gas Conservation Commission Technical Information Page Respectfully submitted for your consideration, Conquest Oil proposes an industrial Re- Use/Recycle Water Project as defined by Colorado Oil and Gas Commission ("COGCC") Rule 907(a)(3) at COGCC Facility ID No. 159193. In accordance with COGCC Rule 907(a)(3), the following details are being submitted via a From 4 Sundry Notice, Page 2, Technical Information Page: 1. The type of waste to be treated and conditioned for recycling and reuse will be from water volumes that come from fluids already entering COGCC Disposal facility No. 159193 that may otherwise be disposed of via deep well injection. 2. Further defined, the type of E & P waste to be treated and conditioned for recycling and reuse are those fluids determined to fall under Class II UIC Oil Field E & P Waste, which include by type, as defined by the COGCC Rule 907(c) produced water, 907(d) drilling fluids, 907(e) oily waste, and 907(f) other E & P waste. 3. The intended use for the treated and conditioned water will be enhanced recovery; i.e. stimulation fluids, drilling, and other approved uses in a manner consistent with existing water rights, and when necessary, consideration of water quality standards and classifications as established by the WQCC for waters of the state, and in accordance with COGCC Rule 907(c)(3). 4. The method of waste treatment contains proprietary processes that break and remove those constituents that prohibit E & P water re -use. The principle means of waste treatment is both mechanical and chemical. 5. There are no pits. All treatment, conditioning, and holding capacity, occurs in closed loop, above ground storage tanks. 6. The waste stream is treated via a chemical softening process, where thereafter, the total suspended solids ("TSS") are removed via coagulation and flocculation processes. Page 1 of 2 7. The flocculated material is drained to a filter box, which through gravity feed processes, enables the flocculated material to be sent to a land fill for disposal after meeting the appropriate regulatory requirements. There is no waste fluid stream. 8. Treated and conditioned water volumes may be disposed of via deep well injection at the discretion of Conquest. 9. Continuous water quality assessments are monitored real time. Page 2 of 2 ccaWv OPERATING SUMMARY Water Treatment and Conditioning Operator Number: 19170 Facility Number: 159193 "Conquest SWD 1-30" Weld County Road 32 and 39, South 2 Miles, West Into 13159 WCR 39 Platteville, CO 80651 Weld County, Colorado August 2009 Prepared by T.A. Pagano, P.E., P.G. 'Dalt' 8207 W. 20th Street Greeley, CO 80634 Emergency Contacts Always Call 911. Weld County Sheriff - Fire Department 970-356-1212 Hospital Northern Colorado Medical Center - Ambulance and Flight for Life 970-352-4121 Hospital Platte Valley Medical Center and Ambulance 303-659-1531 Colorado State Patrol 303-239-4501 Hazardous Chemicals Poison Control Center 1-800-332-3073 CHEMTREC 1-800-424-9300 CONQUEST EMERGENCY CONTACTS General Manager — Jim Goddard. Cell No. 970-381-5005 Facility Area Manager — Dave Gage. Cell No. 970-381-6871 Page 2 of 12 osr 8207 W. 20th Street Greeley, CO 80634 Table of Contents Operating Summary, Water Treatment and Conditioning EMERGENCY CONTACTS (I) EXECUTIVE SUMMARY (II) PROJECT OBJECTIVES (A) Water Treatment for Potential Industrial Re -Use (III) OVERVIEW OF PROJECT COMPONENTS (A) Existing Facility (i) Tanks (ii) Fluids (iii) Chemicals (B) Facility Additions (i) Tanks (ii) Fluids (iii) Chemicals (IV) OVERVIEW OF PROJECT PROCESSES (A) Existing Facility (B) Facility Additions (V) REGULATORY AGENCIES AND CORRESPONDENCE (VI) FIGURES Figure 1 Showing Existing Process Stream and Facility Addition. 1 4 4 5 5 5 6 6 6 6 7 7 8 8 9 9 10 10 Figure 2 11 Showing Facility Addition Process Flow APPENDIX ONE, Detailed Tank Drawings of High Density Polyethene Tanks 12 Page 3 of 12 caWer 8207 W. 20th Street Greeley, CO 80634 (I) EXECUTIVE SUMMARY Conquest Oil Company (the "Conquest") is in the process of treating and conditioning Class II UIC Oil Field Exploration and Production ("E & P") Waste for the purpose of (1) re -utilization by Oil Field E & P operators. Said treatment and conditioning processes ("treatment") are to be implemented at the CONQUEST SWD 1-30 Disposal Facility, located at 13159 WCR 39 Platteville, Weld County, Colorado, for an indeterminate period, principally dependent on the market success and reception by those oil field E & P operators active in the Denver-Julesburg Basin. Said treatment equipment and process will be a minor addition to the exiting facilities and liquid holding capacity, constituting an approximate volume of 474 bbls, or 5.7% of the existing 8,321 of current fluid holding and processing capacity. Treated volumes will be withdrawn from the existing effluent delivered to the CONQUEST SWD 1-30 facility, from waste volumes that would otherwise be disposed of via deep well injection. Treated volumes can, and may be, injected via deep well disposal. Said treatment process will create a treated and conditioned brine, with an intended application to E & P industrial use only. (II) PROJECT OBJECTIVES (A) Water Treatment for Potential Industrial Re -Use Conquest currently receives and handles Class II UIC Oil Field E & P Waste volumes for the purpose of disposal via deep well injection. Conquest has successfully treated and conditioned Class II UIC waste volumes for the sole purpose of industrial E & P re -use in applications where treated volumes can be applied according to the prudent discretion of those E & P operators versed in the art of E & P procedures. In doing so, Conquest proactively seeks to reduce fresh water utilization of E & P operators within Weld County and the greater Wattenberg Field Area. Class II UIC Oil Field E & P Waste typically arrives as a `brine,' or salt water, with a range of various constituents, either naturally occurring or introduced by E & P activities. Conquest aims to treat and condition the said volumes by removing only those constituents that operationally inhibit immediate industrial re -use; thereby enabling brine recycling within the confines of the E & P industry. Page 4 of 12 csa\il sr 1L 8207 W. 20`h Street Greeley, CO 80634 (III) OVERVIEW OF PROJECT COMPONENTS Treatment and conditioning of Class II UIC Oil Field E & P Waste shall occur at an established E & P Waste disposal facility with existing tanks, equipment, and processes. More specifically, it shall be initially implemented at the CONQUEST SWD 1-30 Disposal Facility, located at 13159 WCR 39 Platteville, Weld County, Colorado. Therefore, the proposed treatment and conditioning project is a minor addition to already established and utilized equipment and processes. (A) Existing Facility (i) Tanks There are currently 14 Above Ground Storage Tanks ("ASTs") at the CONQUEST SWD 1-30 Facility. Combined volume and holding capacity approximates 8,321 bbls of fluid. Each tank is integral to the current Class II UIC Waste handling and treatment processes for the purpose of disposal via deep well injection. Each tank has been strategically placed and engineered for the purpose of Class II UIC Waste handling. All existing tanks are within countermeasure spill prevention containment. No of Capacity Capacity AST (Gallons) (Bbls) Contents Construction Single Wall steel shop fabricated System Production Fluid horizontal AST elevated on skids with 1 41,202 981 Unloading Tank unlaoding pad containment. Single Wall steel shop fabricated vertical ASTs within secondary 6 21,000 500 Pre -Filtered Fluids concrete containment. Single wall fiberglass shop fabricated vertical ASTs within main concrete 2 33,600 800 Various Disposal Fluids containment Single wall fiberglass shop fabricated vertical ASTs within main concrete 2 30,240 720 Filtered and Treated Brine containment Single Wall steel shop fabricated vertical ASTs within secondary 1 21,000 500 Various Disposal Fluid_ s concrete containment. Single Wall steel shop fabricated vertical ASTs within secondary 2 16,800 400 Various Disposal Fluids concrete containment. Total 14 349,482 8,321 Page 5 of 12 cc9k5r 8207 W. 20th Street Greeley, CO 80634 (ii) Fluids Fluids currently handled at the CONQUEST SWD 1-30 Disposal facility are those fluids determined to fall under Class II UIC Oil Field E & P Waste, which include by type as defined by the Colorado Oil and Gas Commission ("COGCC") 907(c) produced water, 907(e) oily waste, 907(f) other E & P waste, and to a limited extent, 907(d) drilling fluids. Fluid handling, stop -loss control procedures, emergency response, and Spill Prevention Control and Countermeasure Plans are all in place and can be referenced at the CONQUEST SWD 1-30 Facility and/or Conquest Main Office at 8207 W. 20th Street, Greeley, CO 80634. All required Material Data Saftey Sheets ("MSDS") for known substances entering the CONQUEST SWD 1-30 Disposal facility are in place at the CONQUEST SWD 1-30 Facility and can be accessed or requested at the Conquest main Office at 8207 W. 20`h Street, Greeley, CO 80634. (ii) Chemicals There are no Extremely Hazardous Substances ("EHS") as defined by the Environmental Protection Agency ("EPA") Subject to the Emergency Planning and Community Right to Know Act ("EPCRA"), Section 302, or Section 313, Toxic Chemicals utilized above the Threshold Planning Quantity Requirements. All required Material Data Safety Sheets ("MSDS") for known substances entering the CONQUEST SWD 1-30 Disposal facility are in place at the CONQUEST SWD 1-30 Facility and can be accessed or requested at the Conquest main Office at 8207 W. 20`h Street, Greeley, CO 80634. (B) Facility Additions (i) Tanks Treatment and conditioning equipment will be placed on the North side of the facility (See Figure 1). A total of 7 treatment tanks constructed from high density poly-ethelyne with a total capacity of 474 bbls will be raised. Each tank is integral to the treatment and conditioning process for the purpose of waste re -use and recycling. Page 6 of 12 caWsr 8207 W. 20th Street Greeley, CO 80634 (i) Tanks (continued) Spill and countermeasure containment via the required liner thickness and material has been constructed on a forty (40') by eighty (80') foot rectangle flat grade. All 7 treatment tanks will be placed within the said containment area/volume. Total No of Capacity Capacity AST (Gallons) (Bbls) Contents Construction high density polyethylene within System Production Fluid secondary gravel bermed containment 5 2,500 60 Unloading Tank and Plastic Liner. high density polyethylene within secondary gravel berrm containment 1 6,900 164 Pre -Filtered Fluids and Plastic Liner. high density polyethylene within secondary gravel berrm containment 1 500 12 Various Disposal Fluids and Plastic Liner. 7 19,900 474 (ii) Fluids Treated and conditioned water volumes will come from fluids already entering the CONQUEST SWD 1-30 Disposal facility that would otherwise be disposed of via deep well injection. Therefore, fluid intake into the CONQUEST SWD 1-30 facility will not change. Please reference Section (A) (ii) Fluids, concerning fluids to be handled in the treatment and conditioning process. Adjustments to the SPCC will be made as nccessary. Additional required Material Data Safety Sheets ("MSDS") for known substances entering or being utilized at the CONQUEST SWD 1-30 Disposal facility for the purpose of water treatment and conditioning are in place at the CONQUEST SWD 1-30 Facility and can be accessed or requested at the Conquest main Office at 8207 W. 20`h Street, Greeley, CO 80634. (iii) Chemicals There will be five (5) additional chemicals employed during the water treatment and conditioning process contained in individual chemical totes made from high density poly -ethylene with fiberglass containment. Page 7 of 12 cc9PT 8207 W. 20th Street Greeley, CO 80634 (iii) Chemicals (continued) No of Capacity Capacity Totes (Gallons) (Bbls) Contents Construction high density polyethylene within fiberglass tote containment, within Light Acids, Caustic, Water secondary gravel berm containment 5 275 7 Soluble Flocculation Aids and Plastic Liner. Total 5 1,375 33 All chemical totes and fiberglass containment will be placed within the 40' x 80' gravel berm secondary containment. There are no Extremely Hazardous Substances ("EHS") as defined by the Environmental Protection Agency ("EPA") Subject to the Emergency Planning and Community Right to Know Act ("EPCRA"), Section 302, or Section 313, Toxic Chemicals utilized above the Threshold Planning Quantity Requirements. All required Material Data Safety Sheets ("MSDS") for known substances entering the CONQUEST SWD 1-30 Disposal facility are in place at the CONQUEST SWD 1-30 Facility and can be accessed or requested at the Conquest main Office at 8207 W. 20`h Street, Greeley, CO 80634. A shower and eye wash station has been installed. (IV) OVERVIEW OF PROJECT PROCESSES (C) Existing Facility Oilfield Class II UIC Oil Field E & P Waste is transported to the site by unaffiliated tanker trucks with varying fluid quantity, fluid quality, and fluid constituents, within the realm of Class II UIC E & P Waste as defined by the COGCC. Said waste delivered to the site is offloaded from the tanker trucks from an unloading bay, or concrete pad, that slopes to the center for the purpose of spill containment and surface runoff. Fluid is pumped into the existing facility whereby the Class II UIC Oil Field waste is handled, treated, and filtered to accommodate disposal via deep well injection. This process includes moving the waste through most of the available 8,321 bbls of holding capacity, some of which is designed for the purpose of separating solids from the fluids stream, and other portions that are designed to separate varying fluid types, gravities, and grades of fluid. Combined with a filtration system, the tanks enable a treated fluid stream capable of disposal via deep well injection. This fluid stream is held in a clean fluid Page 8 of 12 8207 W. 20th Street Greeley, CO 80634 tank before disposal via deep well injection. Solids separated as a result of the above described processes are sent to the landfill after passing the required regulatory considerations. (D) Facility Additions The waste treatment and conditioning process will occur after all fluids have passed through the existing facility processes including filtration. A portion of those fluids in the `clean' fluid tank will be diverted into the facility additions, rather than sent to disposal via deep well injection. Each new facility tank, as described in Section (B)(ii) contains a proprietary process that breaks and removes those constituents that prohibit industrial re -use. Each step and chemical addition must strategically occur one before the other. The chemicals utilized in the water treatment and conditioning process are inert after they have been spent in the treatment and conditioning process. Some dissolved metals/solids are precipitated via a chemical softening process, where thereafter, the total suspended solids ("TSS") are removed via coagulation and flocculation processes. The flocculated sediment is drained to a filter box, which through gravity feed processes, enables the sediment to be sent to a land fill for disposal. There is no waste fluid stream. All fluids sent through the facility addition for treatment and conditioning can be utilized for industrial E & P application. However, the treated and conditioned water volumes may be disposed of via deep well injection. (V) REGULATORY AGENCIES AND CORRESPONDENCE The appropriate regulatory agencies, process and procedures, and legal conditions have been and are being addressed by Conquest according to the direction of expert council. Regulative agencies with water quality control considerations, whether partially involved or thoroughly involved include the COGCC, Colorado Division of Water Resources (State Engineers Office), Colorado Department of Public Health and Environment -Water Quality Control Division, Weld County Commissioners Office, and the Weld County Department of Public Health and Environment. The treated waste volumes are to be utilized for the exclusive purpose of oil and gas E & P applications where oil and gas E & P brine can be prudently applied according to the pre -established conditions in the confines of the rules and regulations of the above mentioned regulatory agencies. As a result of direct industrial E & P use only, regulatory oversight by some agencies is greater than others. Page 9 of 12 0 a 0 v O .14 O a z I0 ro 00 00 • 0 To Treatment C O a) C a) a • • > co co 9 Existing Facility Facility Addition Capacity in Bbls 0 Into Existing Handling Facility Unloading Bay Temporary Frac Tank O O Ln O O To Re -Use c tip ti CV, N O O bq con Oq C 0 cb d T L 7 a cua ca'aiSe 8207 W. 20th Street Greeley, CO 80634 APPENDIX ONE Detailed Tank Drawings of High Density Polyethene Tanks Page 12 of 12 CB0500-52 PROPRIETARY D m n n it V V V V a s 2' FITTING ST N U7 z 0 0 w z 0 U z 0 J a a0 bi O ti ri S 4I 0 0 0 0 U riF a s a 0 6 PROPRIETARY DATA 81 =m Wi Pei kilks 13 id 001 WI QO lg '41 D Q z N V 04.50 CENTER OPENING 2500 GALLON 090" 15° CONE BOTTOM TANK CLIENT / DESCRIPTION N 0 cc cc J V N tir 0 Z 1 SHOT WEIGHT 435 L DRAWN / DATE S O v W = W CC 0 6. a z 1,1 z HEIGHT WAS 108 75 ISOLATED TANK FROM STAND CB6900-122 IE D❑WN LUGS X 4 PROPRIETARY } S § FLAT F❑R FITTING 2 INCH FITTING STANDARD /q h CLIENT / DESCRIPTION CB6900-122 2 a vi Z < U, MATERIAL / SHOT WEIGHT 1700 LBS. ) 2 DRAWN / DATE \ \ \ ow 0 K 0 / / 0 a. CHANGE PART ) § m TOLERANCES UNLESS OTHERWISE SPECIFIED % O ■ +I Kim Ogle From: jim goddard [jimgoddardl@yahoo.com] Sent: Tuesday, February 02, 2010 10:10 AM To: Kim Ogle Subject: FW: Conquest Recycled Water Effort Attachments: COGCC, Conquest 907a3 Form4.pdf Is this what you are looking for from us? Jim Jim Goddard Conquest Water Services General Manager 970-381-5005 j imgoddardl@yahoo.com 8207 W. 20th Street Suite B Greeley, Colorado 80634 --- On Tue, 2/2/10, Theodore A. Pagano, P.E., P.G. <theodorepagano@yahoo.com> wrote: From: Theodore A. Pagano, P.E., P.G. <theodorepagano@yahoo.com> Subject: FW: Conquest Recycled Water Effort To: "'jim goddardr" <jimgoddardl@yahoo.com>, "'Dale Butcher' <dalebutche@aol.com>, bruce@conquestcompanies.com, "'Rae Chrisman " <raeconques@aol.com> Date: Tuesday, February 2, 2010, 8:58 AM Will we need more than this? From: Chesson, Robert [mailto:Robert.Chesson@state.co.us] Sent: Tuesday, September 15, 2009 2:37 PM To: theodorepagano@yahoo.com Cc: Baldwin, Debbie; Dillon,David; Neslin, David; charles.johnson@state.co.us; tjiricek@co.weld.co.us Subject: FW: Conquest Recycled Water Effort Mr. Pagano: After detailed discussions with COGCC staff and with CDPHE the COGCC has determined that, because of the non-UIC nature of the proposed treatment and recycling facility and because Conquest intends to operate the facility as a commercial concern, the proposed treatment facility does not fall under the jurisdiction of the COGCC. The COGCC has no jurisdiction to permit any non-UIC commercial facility and the regulatory jurisdiction for permitting this proposed commercial facility falls to the CDPHE Hazardous Materials and Waste Management Division. Please contact Charles Johnson at the CDPHE (303-692-3348) to discuss the permitting requirements. Bob Chesson COGCC From: Dillon,David Sent: Tuesday, September 15, 2009 2:23 PM To: Chesson, Robert Subject: FW: Conquest Recycled Water Effort FYI Sincerely, David Dillon Engineering Manager Colorado Oil and Gas Conservation Commission 303-894-2100 x 5104 From: Theodore A. Pagano, P.E., P.G. [mailto:theodorepagano@yahoo.com] Sent: Monday, August 10, 2009 2:58 PM To: Dillon,David Cc: 'Steven Bushong' Subject: Conquest Recycled Water Effort Dear Mr. Dillon, As per our conversation and as per your voice -mail message received 8-6-09, please find attached, a revised Form 4 directed to your attention. 2 In addition, you will find an operating summary as an addendum to our existing permit for E&P waste handling. Is it possible that this operating summary might suffice in placement of the requested Form 28 since Conquest's handling of E&P waste has been pre -established, and pre -bonded via Form 33 and Form 31? This possibility may remove some redundancy. 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